#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203380.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203380_Fobs loop_ _publ_author_name 'Kang, Qing-Qing' 'Long, La-Sheng' 'Huang, Rong-Bin' 'Zheng, Lan-Sun' _publ_section_title ; Polymeric bis(glycolato)nickel(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m406 _journal_page_last m407 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.443 _cell_angle_gamma 90.000 _cell_length_a 5.1304 _cell_length_b 7.6367 _cell_length_c 8.6076 _exptl_crystal_F_000 212.00 _reflns_d_resolution_high 0.7551 _[local]_cod_data_source_file bt6422Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 81.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 488.02 459.45 8.21 o 4 0 0 952.69 1018.04 17.87 o 1 1 0 3543.20 3355.12 43.63 o 2 1 0 1.09 2.46 0.18 o 3 1 0 2427.38 2560.36 23.96 o 4 1 0 64.15 63.56 1.37 o 5 1 0 333.03 353.20 5.48 o 1 2 0 321.21 360.35 6.32 o 2 2 0 2954.34 3055.69 34.51 o 3 2 0 105.28 102.66 1.87 o 4 2 0 632.18 634.71 9.41 o 5 2 0 27.60 26.30 1.32 o 6 2 0 106.39 128.60 6.79 o 1 3 0 929.37 902.22 12.18 o 2 3 0 1.05 3.06 0.37 o 3 3 0 82.36 69.23 1.94 o 4 3 0 10.23 10.62 0.62 o 5 3 0 436.33 439.72 7.55 o 6 3 0 0.84 2.23 1.39 o 0 4 0 615.64 569.98 13.98 o 1 4 0 0.47 2.31 0.32 o 2 4 0 660.88 563.02 33.25 o 3 4 0 102.16 101.86 2.95 o 4 4 0 179.17 174.11 4.24 o 5 4 0 40.92 39.36 1.73 o 1 5 0 995.00 986.07 16.63 o 2 5 0 3.48 2.46 0.75 o 3 5 0 514.43 515.21 9.98 o 4 5 0 19.83 19.25 1.38 o 5 5 0 156.38 149.20 3.82 o 0 6 0 1624.74 1691.33 39.65 o 1 6 0 41.95 36.82 1.26 o 2 6 0 479.62 523.68 10.20 o 3 6 0 28.32 23.69 1.51 o 4 6 0 607.56 593.55 11.83 o 5 6 0 33.71 34.09 2.04 o 1 7 0 587.31 626.59 11.89 o 2 7 0 53.27 51.11 2.24 o 3 7 0 643.91 634.94 13.78 o 4 7 0 12.28 16.11 1.55 o 0 8 0 333.45 353.27 10.30 o 1 8 0 1.22 1.68 0.60 o 2 8 0 418.98 446.81 9.57 o 3 8 0 1.71 2.65 0.75 o 1 9 0 141.74 148.23 4.48 o 2 9 0 39.14 40.38 2.24 o -5 0 1 4.06 2.78 0.89 o -3 0 1 3108.65 3061.84 40.25 o -1 0 1 6661.56 5569.45 125.37 o 1 0 1 4.70 6.55 0.78 o 3 0 1 3380.30 3443.29 45.25 o 5 0 1 788.53 832.02 23.11 o -6 1 1 168.65 181.52 4.96 o -5 1 1 33.61 35.14 1.49 o -4 1 1 1062.32 1099.39 13.30 o -3 1 1 47.07 49.70 0.87 o -2 1 1 783.54 774.01 9.10 o -1 1 1 3.80 10.61 0.39 o 0 1 1 5667.67 5232.50 117.46 o 1 1 1 2460.34 2496.24 25.14 o 2 1 1 1826.51 1925.57 18.01 o 3 1 1 134.78 157.22 2.15 o 4 1 1 775.53 785.28 8.93 o 5 1 1 61.11 61.66 2.85 o 6 1 1 288.33 314.28 11.81 o -6 2 1 0.22 1.04 0.56 o -5 2 1 1023.39 1081.92 15.86 o -4 2 1 236.64 221.62 5.26 o -3 2 1 511.60 513.83 6.56 o -2 2 1 471.49 518.37 7.01 o -1 2 1 1038.88 1003.09 11.53 o 0 2 1 103.63 96.11 1.97 o 1 2 1 4635.12 4590.45 59.21 o 2 2 1 911.77 988.12 10.34 o 3 2 1 524.38 504.13 5.91 o 4 2 1 11.87 11.32 0.62 o 5 2 1 147.44 153.76 4.79 o 6 2 1 17.79 19.10 2.95 o -6 3 1 390.78 400.07 7.40 o -5 3 1 1.53 2.68 1.15 o -4 3 1 209.07 202.64 3.88 o -2 3 1 3326.34 3364.82 43.71 o -1 3 1 509.22 542.59 7.62 o 0 3 1 107.88 86.62 2.03 o 1 3 1 103.68 103.89 2.42 o 2 3 1 1228.04 1235.90 20.49 o 3 3 1 44.03 42.97 1.14 o 4 3 1 202.18 207.50 3.15 o 5 3 1 4.33 4.51 1.62 o 6 3 1 96.11 106.77 6.46 o -6 4 1 0.89 1.41 0.57 o -5 4 1 338.85 330.37 5.33 o -4 4 1 49.32 47.51 1.94 o -3 4 1 686.74 692.84 10.17 o -2 4 1 150.00 157.26 3.76 o -1 4 1 1197.77 1249.81 16.87 o 0 4 1 52.56 52.46 1.57 o 1 4 1 1032.08 1016.18 17.09 o 2 4 1 157.13 175.50 4.02 o 3 4 1 142.13 152.56 4.73 o 4 4 1 14.18 13.80 0.99 o 5 4 1 307.71 301.80 7.47 o -5 5 1 9.91 8.08 1.12 o -4 5 1 612.83 613.20 11.91 o -3 5 1 66.00 61.81 2.32 o -2 5 1 506.82 509.03 17.79 o -1 5 1 273.75 261.30 9.65 o 0 5 1 1414.00 1393.23 23.12 o 1 5 1 56.48 49.46 1.37 o 2 5 1 319.52 330.22 11.72 o 3 5 1 6.71 7.27 0.89 o 4 5 1 661.39 649.83 12.42 o 5 5 1 35.88 30.78 3.01 o -5 6 1 100.27 98.51 5.68 o -4 6 1 11.75 15.49 1.35 o -3 6 1 502.08 513.09 10.34 o -2 6 1 9.89 6.83 0.89 o -1 6 1 574.26 563.56 8.48 o 0 6 1 54.78 54.08 2.56 o 1 6 1 699.43 703.64 10.27 o 2 6 1 26.60 21.75 1.34 o 3 6 1 930.49 927.93 16.83 o 4 6 1 5.30 6.34 1.01 o -4 7 1 146.52 141.25 4.49 o -3 7 1 89.24 85.07 3.51 o -2 7 1 282.05 296.09 6.83 o -1 7 1 36.42 34.09 2.92 o 0 7 1 762.36 768.28 13.74 o 1 7 1 24.72 22.20 1.81 o 2 7 1 637.96 655.58 12.58 o 3 7 1 0.94 0.77 0.55 o 4 7 1 111.44 110.52 8.74 o -3 8 1 171.51 188.83 11.78 o -2 8 1 25.32 24.46 1.67 o -1 8 1 499.74 514.15 17.04 o 0 8 1 41.18 39.49 1.52 o 1 8 1 219.95 221.77 5.56 o 2 8 1 15.72 16.42 1.42 o 3 8 1 139.04 158.67 6.85 o -2 9 1 186.86 204.86 5.77 o -1 9 1 161.53 171.26 6.74 o 0 9 1 110.13 114.12 4.02 o 1 9 1 0.28 0.35 0.49 o 2 9 1 177.42 185.98 5.37 o -6 0 2 8.42 7.52 1.56 o -4 0 2 1875.66 1941.01 32.30 o -2 0 2 182.38 243.29 4.50 o 0 0 2 1143.92 1132.91 16.90 o 2 0 2 1470.91 1496.03 19.98 o 4 0 2 551.57 560.57 16.32 o 6 0 2 67.10 76.58 5.18 o -6 1 2 4.63 6.84 1.06 o -5 1 2 224.10 226.29 5.43 o -4 1 2 206.24 210.01 3.38 o -3 1 2 559.68 553.99 6.89 o -2 1 2 1365.05 1388.05 14.25 o -1 1 2 1774.75 1783.45 20.08 o 0 1 2 194.57 188.53 2.80 o 1 1 2 1007.07 968.96 10.14 o 2 1 2 4.81 6.46 0.29 o 3 1 2 793.44 812.78 8.11 o 4 1 2 94.87 102.58 3.56 o 5 1 2 317.80 325.95 8.17 o 6 1 2 4.75 4.40 1.84 o -6 2 2 491.34 522.70 10.71 o -5 2 2 19.97 21.94 2.09 o -4 2 2 238.37 227.82 6.90 o -3 2 2 23.92 21.26 1.64 o -2 2 2 3637.06 3628.12 49.68 o -1 2 2 32.35 34.84 0.83 o 0 2 2 2495.79 2449.14 31.81 o 1 2 2 2176.30 2297.89 26.14 o 2 2 2 1476.88 1423.70 13.55 o 3 2 2 98.94 85.58 1.55 o 4 2 2 268.12 270.70 5.15 o 5 2 2 101.30 94.39 3.76 o -6 3 2 11.39 14.71 1.44 o -5 3 2 739.73 739.04 9.92 o -4 3 2 91.14 90.69 2.38 o -3 3 2 1844.02 1814.12 29.56 o -2 3 2 5.17 3.61 0.58 o -1 3 2 2492.65 2450.66 39.05 o 0 3 2 127.61 126.59 2.70 o 1 3 2 2545.62 2527.26 33.01 o 2 3 2 145.39 157.15 2.72 o 3 3 2 711.92 702.22 9.14 o 4 3 2 8.64 7.47 0.86 o 5 3 2 279.47 282.91 7.47 o -6 4 2 271.12 266.68 6.67 o -5 4 2 0.45 1.26 0.46 o -4 4 2 654.04 654.07 9.99 o -3 4 2 1.33 1.77 0.42 o -2 4 2 2203.63 2151.99 85.43 o -1 4 2 37.02 35.75 1.43 o 0 4 2 1422.64 1412.53 23.35 o 1 4 2 842.93 894.02 12.33 o 2 4 2 678.98 714.95 12.62 o 3 4 2 74.26 76.42 2.46 o 4 4 2 802.28 764.76 17.18 o 5 4 2 47.12 45.58 2.67 o -5 5 2 279.27 278.15 5.50 o -4 5 2 13.05 14.24 0.99 o -3 5 2 588.95 582.58 11.18 o -2 5 2 71.94 73.27 3.15 o -1 5 2 403.47 399.75 7.65 o 0 5 2 35.57 37.33 2.95 o 1 5 2 1257.85 1294.49 17.71 o 2 5 2 208.21 206.46 4.74 o 3 5 2 504.91 490.56 9.58 o 4 5 2 56.55 52.08 6.07 o 5 5 2 80.87 80.03 4.40 o -5 6 2 11.90 11.54 1.70 o -4 6 2 282.54 275.16 6.71 o -3 6 2 11.09 9.92 1.12 o -2 6 2 67.22 64.29 2.46 o -1 6 2 103.50 109.84 2.47 o 0 6 2 918.21 926.42 22.61 o 1 6 2 10.22 8.78 0.89 o 2 6 2 330.56 323.59 9.86 o 3 6 2 25.89 29.41 1.67 o 4 6 2 100.16 95.48 11.97 o -4 7 2 0.83 1.26 0.68 o -3 7 2 156.64 166.10 4.78 o -2 7 2 0.32 0.84 0.55 o -1 7 2 598.43 593.10 14.68 o 0 7 2 0.16 0.46 0.32 o 1 7 2 50.21 45.77 2.01 o 2 7 2 13.79 11.89 1.18 o 3 7 2 220.92 219.03 5.67 o -3 8 2 0.29 0.78 0.59 o -2 8 2 419.47 440.41 15.01 o -1 8 2 29.85 33.03 1.85 o 0 8 2 47.68 49.52 1.73 o 1 8 2 3.26 3.32 0.75 o 2 8 2 362.23 387.87 8.56 o 3 8 2 2.72 2.45 1.00 o -2 9 2 26.43 25.70 1.89 o -1 9 2 226.32 241.15 6.26 o 0 9 2 2.67 2.12 1.06 o 1 9 2 340.44 355.69 8.10 o 2 9 2 5.80 8.19 1.73 o -5 0 3 327.79 347.87 10.58 o -3 0 3 275.40 258.57 5.05 o -1 0 3 1302.71 1350.34 21.70 o 1 0 3 918.09 931.17 15.78 o 3 0 3 137.85 138.30 3.49 o 5 0 3 158.22 157.67 7.41 o -6 1 3 140.27 143.06 4.35 o -5 1 3 114.05 111.72 3.47 o -4 1 3 743.79 755.84 11.01 o -3 1 3 222.18 242.83 3.42 o -2 1 3 1057.96 1035.06 12.06 o -1 1 3 1508.10 1600.09 16.30 o 0 1 3 1011.50 986.42 10.28 o 1 1 3 98.66 105.05 1.48 o 2 1 3 598.95 627.13 7.71 o 3 1 3 19.13 16.14 0.92 o 4 1 3 356.80 346.78 14.59 o 5 1 3 55.03 53.14 2.87 o -6 2 3 4.17 4.49 0.90 o -5 2 3 464.64 483.24 9.73 o -4 2 3 376.69 369.01 6.33 o -3 2 3 1128.92 1095.60 15.16 o -2 2 3 241.58 245.47 3.33 o -1 2 3 2535.23 2558.45 25.87 o 0 2 3 506.37 556.43 6.74 o 1 2 3 1228.77 1217.81 17.94 o 2 2 3 73.13 79.23 2.76 o 3 2 3 813.10 806.52 12.16 o 4 2 3 96.82 84.36 4.65 o 5 2 3 357.38 354.47 8.91 o -6 3 3 424.94 414.61 18.05 o -5 3 3 40.35 38.46 1.56 o -4 3 3 576.61 568.03 8.82 o -3 3 3 290.96 286.81 4.87 o -2 3 3 2219.72 2288.33 26.01 o -1 3 3 1.47 6.27 0.81 o 0 3 3 1914.77 1910.80 25.16 o 1 3 3 78.41 89.41 1.91 o 2 3 3 2154.61 2186.71 22.77 o 3 3 3 12.36 14.64 1.00 o 4 3 3 409.17 384.84 7.02 o 5 3 3 25.09 26.28 2.15 o -6 4 3 0.38 0.60 0.52 o -5 4 3 369.42 349.78 6.34 o -4 4 3 152.34 145.68 3.28 o -3 4 3 1584.09 1535.68 21.06 o -2 4 3 102.03 96.93 4.82 o -1 4 3 839.01 795.31 11.13 o 0 4 3 107.49 115.50 3.21 o 1 4 3 1965.86 1939.49 25.75 o 2 4 3 9.55 9.90 0.84 o 3 4 3 1049.86 999.88 18.36 o 4 4 3 38.11 39.24 2.17 o 5 4 3 109.47 103.48 6.40 o -5 5 3 0.18 0.95 0.44 o -4 5 3 302.61 287.89 5.43 o -3 5 3 127.36 120.13 4.79 o -2 5 3 492.06 469.24 9.25 o -1 5 3 177.73 181.79 3.39 o 0 5 3 1965.11 1797.80 66.67 o 1 5 3 234.81 236.05 5.50 o 2 5 3 88.30 75.86 3.62 o 3 5 3 50.62 43.69 2.22 o 4 5 3 366.34 356.35 8.52 o -5 6 3 93.94 101.53 4.20 o -4 6 3 4.19 3.55 0.82 o -3 6 3 187.29 188.05 5.03 o -2 6 3 5.91 4.97 0.82 o -1 6 3 605.50 621.40 9.35 o 0 6 3 2.48 2.15 0.42 o 1 6 3 152.19 150.70 3.90 o 2 6 3 2.38 2.33 0.58 o 3 6 3 99.73 105.82 4.96 o 4 6 3 4.23 5.32 1.08 o -4 7 3 292.89 297.14 7.99 o -3 7 3 0.59 0.95 0.59 o -2 7 3 225.49 228.23 5.79 o -1 7 3 24.70 23.98 1.54 o 0 7 3 9.71 11.67 0.96 o 1 7 3 48.08 44.99 1.99 o 2 7 3 528.21 534.67 10.63 o 3 7 3 21.49 21.83 2.28 o -3 8 3 105.35 106.04 5.46 o -2 8 3 0.03 0.47 0.55 o -1 8 3 201.23 211.12 5.93 o 0 8 3 19.40 18.57 1.28 o 1 8 3 292.72 298.60 8.08 o 2 8 3 0.27 1.64 0.59 o -2 9 3 300.59 313.59 7.76 o -1 9 3 2.34 2.70 0.82 o 0 9 3 312.05 309.33 10.58 o 1 9 3 2.49 2.90 0.65 o -6 0 4 261.06 282.32 9.75 o -4 0 4 1451.79 1424.78 33.92 o -2 0 4 1651.53 1650.62 26.76 o 0 0 4 1550.61 1558.25 29.88 o 2 0 4 442.68 438.65 8.45 o 4 0 4 499.45 476.91 15.09 o -6 1 4 47.69 47.26 2.34 o -5 1 4 610.76 640.90 12.27 o -4 1 4 105.68 106.77 2.53 o -3 1 4 1263.75 1175.38 25.10 o -2 1 4 250.80 264.00 3.60 o -1 1 4 1146.76 1164.38 12.03 o 0 1 4 472.47 526.84 7.51 o 1 1 4 1651.71 1650.21 19.44 o 2 1 4 18.66 17.95 0.74 o 3 1 4 395.17 378.92 6.59 o 4 1 4 2.93 3.42 0.94 o 5 1 4 166.79 169.63 5.69 o -6 2 4 220.06 226.45 5.95 o -5 2 4 19.15 20.97 1.44 o -4 2 4 337.51 329.66 5.67 o -3 2 4 2.44 4.39 0.71 o -2 2 4 1824.99 1860.18 21.30 o -1 2 4 1927.35 2155.29 21.93 o 0 2 4 808.15 834.92 9.97 o 1 2 4 64.06 62.77 1.00 o 2 2 4 1176.98 1161.28 15.07 o 3 2 4 98.86 95.84 2.58 o 4 2 4 296.30 281.57 5.63 o 5 2 4 19.81 19.56 3.17 o -6 3 4 6.54 9.02 1.22 o -5 3 4 239.69 227.35 4.61 o -4 3 4 91.41 86.72 2.35 o -3 3 4 332.50 321.97 7.02 o -2 3 4 16.82 13.61 0.76 o -1 3 4 1824.55 1826.27 21.09 o 0 3 4 63.45 72.87 1.54 o 1 3 4 721.40 743.55 9.18 o 2 3 4 256.82 272.41 4.16 o 3 3 4 652.11 642.06 10.33 o 4 3 4 0.94 0.71 0.51 o 5 3 4 237.90 255.86 10.08 o -5 4 4 9.33 6.85 0.82 o -4 4 4 400.55 386.70 6.65 o -3 4 4 8.87 7.32 0.73 o -2 4 4 169.73 168.79 4.30 o -1 4 4 580.00 599.57 10.57 o 0 4 4 1760.24 1771.99 23.67 o 1 4 4 103.38 105.61 2.00 o 2 4 4 591.06 580.44 16.96 o 3 4 4 81.47 72.42 2.89 o 4 4 4 170.31 172.97 5.22 o -5 5 4 89.75 88.22 2.70 o -4 5 4 237.37 229.85 4.70 o -3 5 4 1143.10 1100.87 19.80 o -2 5 4 1.04 0.88 0.45 o -1 5 4 387.52 386.00 6.13 o 0 5 4 2.64 2.86 0.44 o 1 5 4 345.33 322.85 9.23 o 2 5 4 320.34 298.96 6.95 o 3 5 4 483.53 483.08 11.28 o 4 5 4 1.08 2.77 0.88 o -5 6 4 0.34 1.89 1.17 o -4 6 4 437.77 419.16 9.27 o -3 6 4 3.93 4.56 0.92 o -2 6 4 725.29 704.79 13.36 o -1 6 4 9.74 11.27 0.81 o 0 6 4 309.50 292.08 8.94 o 1 6 4 55.63 58.40 2.17 o 2 6 4 219.50 226.23 7.74 o 3 6 4 7.46 10.73 1.39 o -4 7 4 33.68 35.75 2.21 o -3 7 4 75.46 72.20 3.01 o -2 7 4 4.96 5.78 0.98 o -1 7 4 509.65 520.42 8.34 o 0 7 4 2.69 3.44 0.58 o 1 7 4 562.38 539.89 8.57 o 2 7 4 16.66 16.43 1.89 o 3 7 4 31.60 31.44 2.15 o -3 8 4 0.97 1.47 1.34 o -2 8 4 333.10 345.66 8.13 o -1 8 4 66.84 63.61 2.74 o 0 8 4 199.74 193.47 4.97 o 1 8 4 5.61 6.72 0.79 o 2 8 4 245.27 236.09 8.52 o -1 9 4 145.17 159.79 4.90 o 0 9 4 3.32 3.06 1.17 o 1 9 4 94.78 105.43 5.29 o -5 0 5 626.31 612.86 16.82 o -3 0 5 1662.88 1677.32 27.59 o -1 0 5 1326.69 1293.88 21.10 o 1 0 5 3617.96 3587.80 58.49 o 3 0 5 293.60 300.36 6.71 o -6 1 5 377.97 407.15 18.91 o -5 1 5 16.44 18.10 1.46 o -4 1 5 727.91 704.50 10.45 o -3 1 5 44.71 43.67 1.14 o -2 1 5 1770.78 1778.80 20.45 o -1 1 5 148.31 171.48 2.28 o 0 1 5 2240.99 2290.54 23.59 o 1 1 5 98.02 107.53 2.05 o 2 1 5 558.98 557.97 7.52 o 3 1 5 141.48 141.81 3.38 o 4 1 5 473.19 476.84 10.95 o -6 2 5 100.72 101.48 6.29 o -5 2 5 441.61 435.90 9.12 o -4 2 5 72.73 64.07 2.38 o -3 2 5 705.26 686.64 8.58 o -2 2 5 1.95 2.04 0.31 o -1 2 5 1023.48 1066.74 11.22 o 0 2 5 23.11 31.16 0.83 o 1 2 5 378.39 356.17 12.49 o 2 2 5 191.79 177.64 5.29 o 3 2 5 639.08 623.77 10.16 o 4 2 5 4.91 5.66 1.18 o -6 3 5 73.79 71.64 3.03 o -5 3 5 1.10 1.54 0.52 o -4 3 5 248.32 245.88 4.72 o -3 3 5 69.99 64.11 1.80 o -2 3 5 533.91 536.42 7.95 o -1 3 5 7.76 6.03 0.60 o 0 3 5 118.70 99.51 5.60 o 1 3 5 189.43 174.23 5.06 o 2 3 5 710.15 684.89 10.72 o 3 3 5 73.59 66.95 2.26 o 4 3 5 61.37 62.41 2.35 o -5 4 5 52.46 48.84 2.34 o -4 4 5 77.05 72.29 2.22 o -3 4 5 171.48 161.48 4.07 o -2 4 5 49.47 46.40 1.77 o -1 4 5 929.00 962.69 14.61 o 0 4 5 0.51 0.86 0.56 o 1 4 5 164.37 157.84 5.80 o 2 4 5 66.79 66.12 2.62 o 3 4 5 157.47 151.22 4.61 o 4 4 5 0.24 1.05 0.65 o -5 5 5 10.64 8.34 0.98 o -4 5 5 580.90 545.69 9.01 o -3 5 5 158.27 160.28 4.50 o -2 5 5 128.62 129.11 3.62 o -1 5 5 79.64 71.94 2.05 o 0 5 5 918.13 902.55 11.26 o 1 5 5 64.21 58.59 1.83 o 2 5 5 321.19 315.31 18.77 o 3 5 5 5.95 8.28 1.24 o -4 6 5 27.59 27.42 1.85 o -3 6 5 707.19 676.85 20.52 o -2 6 5 79.47 77.06 3.15 o -1 6 5 293.01 278.77 7.02 o 0 6 5 26.70 25.82 1.17 o 1 6 5 784.53 766.62 14.64 o 2 6 5 1.99 1.84 0.67 o 3 6 5 253.34 231.56 6.52 o -4 7 5 121.40 116.51 5.74 o -3 7 5 24.76 23.85 1.73 o -2 7 5 994.23 993.33 18.33 o -1 7 5 17.59 16.67 1.03 o 0 7 5 348.21 348.70 7.40 o 1 7 5 0.87 1.23 0.78 o 2 7 5 167.57 181.23 5.37 o -3 8 5 148.81 133.11 6.24 o -2 8 5 25.49 23.08 1.73 o -1 8 5 341.08 347.46 8.03 o 0 8 5 3.01 4.12 1.11 o 1 8 5 175.05 173.82 6.79 o 2 8 5 16.81 12.48 2.39 o -1 9 5 1.84 2.34 0.80 o -6 0 6 151.43 151.38 6.74 o -4 0 6 376.55 399.81 12.00 o -2 0 6 1876.33 1904.64 31.01 o 0 0 6 2560.03 2603.78 42.82 o 2 0 6 80.38 75.25 2.62 o 4 0 6 914.40 916.01 26.18 o -6 1 6 57.91 50.72 2.90 o -5 1 6 233.48 231.27 5.81 o -4 1 6 2.13 3.67 0.58 o -3 1 6 1341.01 1360.14 16.12 o -2 1 6 153.03 154.12 2.50 o -1 1 6 729.62 754.10 8.15 o 0 1 6 38.84 41.43 1.15 o 1 1 6 1080.54 1080.55 13.39 o 2 1 6 0.03 0.35 0.30 o 3 1 6 531.77 541.42 9.14 o 4 1 6 0.11 0.36 0.68 o -6 2 6 389.91 401.89 9.12 o -5 2 6 2.69 2.50 0.77 o -4 2 6 501.24 459.01 10.09 o -3 2 6 424.77 409.85 8.64 o -2 2 6 406.51 417.61 5.55 o -1 2 6 3.18 3.55 0.34 o 0 2 6 470.65 456.19 8.97 o 1 2 6 3.20 2.79 0.44 o 2 2 6 976.31 976.78 12.48 o 3 2 6 21.35 19.79 1.29 o 4 2 6 26.15 29.96 2.20 o -5 3 6 591.89 585.07 9.57 o -4 3 6 74.86 70.41 2.12 o -3 3 6 101.26 89.17 2.57 o -2 3 6 84.82 82.54 1.72 o -1 3 6 998.00 988.08 13.80 o 0 3 6 26.72 25.00 1.22 o 1 3 6 185.22 178.55 3.61 o 2 3 6 27.17 26.10 1.59 o 3 3 6 132.76 121.74 4.53 o 4 3 6 4.69 7.96 1.62 o -5 4 6 1.02 1.24 0.55 o -4 4 6 482.76 453.28 7.71 o -3 4 6 254.07 236.83 4.49 o -2 4 6 696.37 672.39 9.96 o -1 4 6 35.85 36.81 2.01 o 0 4 6 153.79 147.99 3.12 o 1 4 6 20.66 18.59 1.81 o 2 4 6 262.10 247.69 7.10 o 3 4 6 3.44 5.35 1.03 o -5 5 6 73.86 66.70 3.77 o -4 5 6 97.55 89.84 2.69 o -3 5 6 474.86 443.16 26.43 o -2 5 6 2.27 2.22 0.50 o -1 5 6 486.90 471.04 12.18 o 0 5 6 40.99 34.71 1.67 o 1 5 6 470.12 460.91 7.68 o 2 5 6 39.97 42.57 3.59 o 3 5 6 122.15 121.46 4.37 o -4 6 6 189.28 181.73 5.35 o -3 6 6 3.67 3.67 0.86 o -2 6 6 251.14 236.94 9.47 o -1 6 6 144.80 138.04 3.12 o 0 6 6 796.93 787.85 14.45 o 1 6 6 9.25 6.74 0.99 o 2 6 6 190.99 194.62 5.59 o -3 7 6 352.27 351.21 11.36 o -2 7 6 4.57 5.74 1.00 o -1 7 6 194.32 196.46 5.12 o 0 7 6 14.70 14.15 1.62 o 1 7 6 290.38 272.62 9.19 o 2 7 6 6.63 9.13 2.06 o -2 8 6 283.09 276.34 7.06 o -1 8 6 36.46 36.31 3.06 o 0 8 6 123.61 118.96 5.24 o -5 0 7 43.88 52.63 3.45 o -3 0 7 1564.08 1557.62 26.05 o -1 0 7 3.87 7.30 1.11 o 1 0 7 507.00 479.02 9.50 o 3 0 7 705.46 746.36 21.67 o -5 1 7 7.60 8.08 1.16 o -4 1 7 373.81 383.94 6.49 o -3 1 7 46.40 45.19 1.29 o -2 1 7 240.21 239.69 3.58 o -1 1 7 47.93 43.59 1.77 o 0 1 7 965.49 955.99 11.97 o 1 1 7 25.84 23.59 0.99 o 2 1 7 250.77 238.87 4.11 o 3 1 7 0.99 0.89 0.49 o -5 2 7 377.81 356.14 8.01 o -4 2 7 28.18 23.86 1.21 o -3 2 7 150.25 155.58 3.61 o -2 2 7 0.56 1.27 0.29 o -1 2 7 1764.62 1797.13 30.03 o 0 2 7 36.63 35.83 1.34 o 1 2 7 385.78 382.10 5.67 o 2 2 7 123.18 115.85 2.59 o 3 2 7 86.90 87.58 2.81 o -5 3 7 3.00 3.53 0.72 o -4 3 7 393.42 376.05 8.22 o -3 3 7 10.56 12.05 0.89 o -2 3 7 1474.84 1530.38 18.09 o -1 3 7 56.98 52.84 2.04 o 0 3 7 199.74 208.10 4.92 o 1 3 7 0.01 0.41 0.40 o 2 3 7 581.38 558.32 11.46 o 3 3 7 0.78 0.91 0.57 o -5 4 7 589.06 597.57 9.98 o -4 4 7 0.21 0.28 0.42 o -3 4 7 525.08 515.21 8.26 o -2 4 7 0.32 3.16 1.98 o -1 4 7 383.45 398.34 8.15 o 0 4 7 19.40 18.30 1.28 o 1 4 7 524.92 526.27 8.60 o 2 4 7 53.23 59.93 5.29 o 3 4 7 191.80 187.34 5.63 o -4 5 7 370.17 345.53 8.14 o -3 5 7 0.71 0.78 0.55 o -2 5 7 255.76 251.99 5.83 o -1 5 7 81.19 71.92 2.58 o 0 5 7 445.97 435.46 8.92 o 1 5 7 34.00 33.86 2.56 o 2 5 7 142.12 145.36 4.65 o -4 6 7 55.25 57.03 3.84 o -3 6 7 253.57 242.09 8.13 o -2 6 7 4.83 7.13 1.62 o -1 6 7 201.65 195.05 4.99 o 0 6 7 1.49 2.49 0.71 o 1 6 7 232.61 251.74 8.74 o 2 6 7 2.65 3.23 1.28 o -3 7 7 0.00 -0.45 0.84 o -1 7 7 4.57 5.74 1.23 o 0 7 7 230.76 227.46 8.02 o -4 0 8 332.12 325.60 7.09 o -2 0 8 23.11 22.89 1.89 o 0 0 8 964.12 967.14 19.38 o 2 0 8 124.89 127.24 3.96 o -5 1 8 77.06 76.79 3.37 o -4 1 8 13.99 11.29 0.94 o -3 1 8 402.53 402.60 5.71 o -2 1 8 59.94 59.35 2.24 o -1 1 8 419.40 411.37 8.33 o 0 1 8 152.13 143.79 3.17 o 1 1 8 180.55 176.18 3.32 o 2 1 8 55.68 54.03 1.73 o 3 1 8 165.26 159.58 4.92 o -5 2 8 24.32 23.70 1.69 o -4 2 8 363.90 369.87 6.93 o -3 2 8 40.41 34.92 1.19 o -2 2 8 1308.83 1368.72 23.59 o -1 2 8 15.20 16.13 1.22 o 0 2 8 155.19 153.22 4.11 o 1 2 8 3.00 2.91 0.59 o 2 2 8 334.68 331.00 5.44 o 3 2 8 16.14 18.82 2.23 o -5 3 8 723.08 726.48 14.12 o -4 3 8 0.17 -0.15 0.41 o -3 3 8 400.85 407.63 8.70 o -2 3 8 17.09 16.60 1.25 o -1 3 8 659.62 666.75 12.60 o 0 3 8 3.45 3.83 0.78 o 1 3 8 616.10 610.33 9.79 o 2 3 8 0.84 1.56 0.71 o -5 4 8 30.44 28.18 2.90 o -4 4 8 245.65 239.83 4.93 o -3 4 8 0.74 1.34 0.89 o -2 4 8 507.14 519.64 12.56 o -1 4 8 9.67 9.48 1.07 o 0 4 8 541.50 539.81 10.75 o 1 4 8 4.09 5.59 0.94 o 2 4 8 340.71 340.27 9.38 o -4 5 8 12.74 14.12 1.48 o -3 5 8 324.98 335.11 11.08 o -2 5 8 0.47 1.11 1.06 o -1 5 8 201.86 207.52 5.28 o 0 5 8 2.46 3.56 0.80 o 1 5 8 313.85 327.87 10.64 o -2 6 8 102.41 109.22 5.46 o -1 6 8 0.01 0.51 0.53 o 0 6 8 198.25 198.28 7.80 o -1 7 8 131.07 128.53 4.10 o -5 0 9 32.78 36.26 3.01 o -3 0 9 474.55 483.76 13.81 o -1 0 9 614.27 635.64 17.21 o 1 0 9 133.02 130.69 4.04 o -5 1 9 22.16 26.79 2.78 o -4 1 9 483.54 511.22 14.65 o -3 1 9 44.38 49.17 2.16 o -2 1 9 291.83 305.74 6.83 o -1 1 9 185.30 180.34 4.73 o 0 1 9 266.54 261.40 6.20 o 1 1 9 50.32 45.94 1.57 o 2 1 9 196.42 200.94 3.96 o -5 2 9 461.50 486.45 23.70 o -4 2 9 56.73 53.13 3.40 o -3 2 9 230.20 228.40 5.61 o -2 2 9 4.95 5.43 0.91 o -1 2 9 268.00 276.94 6.42 o 0 2 9 176.90 179.35 4.82 o 1 2 9 307.60 310.67 7.21 o 2 2 9 0.03 0.38 0.63 o -4 3 9 60.71 65.94 3.90 o -3 3 9 12.83 12.87 1.25 o -2 3 9 466.39 466.23 9.62 o -1 3 9 9.94 10.88 1.18 o 0 3 9 374.72 367.36 8.09 o 1 3 9 18.31 17.59 1.49 o 2 3 9 232.84 246.95 9.69 o -4 4 9 19.29 19.10 2.17 o -3 4 9 265.31 272.51 9.58 o -2 4 9 12.46 8.48 1.56 o -1 4 9 283.55 286.09 6.77 o 0 4 9 93.82 95.68 3.38 o 1 4 9 323.46 351.99 11.42 o -2 5 9 218.56 223.53 8.97 o -1 5 9 6.70 8.24 1.12 o 0 5 9 206.08 206.23 5.57 o -1 6 9 93.25 83.82 4.34 o -4 0 10 603.75 636.81 17.82 o -2 0 10 482.23 496.80 14.54 o 0 0 10 266.20 274.24 9.41 o -4 1 10 217.60 229.02 8.41 o -3 1 10 301.37 306.35 7.13 o -2 1 10 17.04 19.95 1.46 o -1 1 10 351.32 368.23 8.19 o 0 1 10 0.83 0.87 0.86 o 1 1 10 312.08 310.11 10.47 o -4 2 10 118.20 127.15 5.85 o -3 2 10 3.69 4.85 0.94 o -2 2 10 225.49 234.53 5.94 o -1 2 10 60.21 59.13 2.60 o 0 2 10 223.12 227.81 11.08 o 1 2 10 9.26 9.25 1.89 o -3 3 10 139.54 145.98 4.38 o -2 3 10 0.47 0.98 0.60 o -1 3 10 213.07 219.52 6.85 o 0 3 10 18.87 19.94 2.45 o -2 4 10 157.64 173.71 6.79 o -1 4 10 20.02 20.93 1.66 o