#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/33/2203384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203384_Fobs loop_ _publ_author_name 'Rafizadeh, Masoud' 'Ranjbar, Maryam' 'Amani, Vahid' _publ_section_title ; Dihydronium 2,6-diaminopyridinium tris(2,6-pyridinedicarboxylato)ytterbate(III) dihydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m479 _journal_page_last m481 _journal_volume 60 _journal_year 2004 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.953 _cell_angle_gamma 90.000 _cell_length_a 9.6357 _cell_length_b 10.5295 _cell_length_c 17.7932 _exptl_crystal_F_000 962.00 _reflns_d_resolution_high 0.7099 _[local]_cod_data_source_file cf6321Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ybamm in P2/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 310.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7260.00 7519.53 253.67 o 4 0 0 3105.88 3102.45 110.97 o 6 0 0 3963.12 3781.17 113.05 o 8 0 0 6725.79 7129.95 149.46 o 10 0 0 2797.01 2835.54 168.21 o 12 0 0 1685.77 1993.41 172.33 o 1 1 0 799.33 976.45 51.76 o 2 1 0 15751.25 16995.61 112.99 o 3 1 0 10.88 -1.85 42.73 o 4 1 0 15198.75 15297.13 205.37 o 5 1 0 78.49 22.38 46.76 o 6 1 0 4895.91 4960.02 86.30 o 7 1 0 1325.96 1146.76 67.13 o 8 1 0 3666.01 3744.34 88.06 o 9 1 0 159.45 132.96 73.71 o 10 1 0 2384.48 2451.41 114.52 o 11 1 0 105.93 119.09 82.00 o 12 1 0 2083.39 2203.13 124.32 o 13 1 0 149.80 114.52 146.23 o 0 2 0 12097.35 12736.28 225.41 o 1 2 0 12417.19 13765.09 116.44 o 2 2 0 96615.11 107860.63 406.14 o 3 2 0 6953.73 7659.05 140.09 o 4 2 0 7378.89 7967.45 134.08 o 5 2 0 186.71 71.54 47.88 o 6 2 0 2475.85 2316.89 72.60 o 7 2 0 5221.97 5153.71 93.12 o 8 2 0 1531.74 1455.57 72.77 o 9 2 0 243.04 193.51 75.67 o 10 2 0 2910.83 3056.64 121.11 o 11 2 0 303.82 240.80 85.98 o 12 2 0 1200.41 1375.38 114.24 o 13 2 0 179.42 198.76 148.43 o 0 3 0 14261.63 15754.51 268.12 o 1 3 0 2804.24 2642.60 103.01 o 2 3 0 16071.60 16263.13 198.45 o 3 3 0 7833.64 8311.22 112.15 o 4 3 0 7638.94 7475.22 100.65 o 5 3 0 161.29 77.85 53.31 o 6 3 0 2806.43 2793.81 77.34 o 7 3 0 2042.28 1782.80 73.82 o 8 3 0 1988.02 2006.12 78.20 o 9 3 0 1574.79 1563.98 99.81 o 10 3 0 3010.83 3038.49 121.74 o 11 3 0 997.93 972.18 102.13 o 12 3 0 727.55 823.41 104.98 o 13 3 0 242.67 276.93 151.63 o 0 4 0 15998.35 17700.84 306.02 o 1 4 0 46.55 70.72 54.49 o 2 4 0 8569.47 8292.50 107.39 o 3 4 0 12053.82 13140.77 133.51 o 4 4 0 20773.90 21550.32 298.49 o 5 4 0 4493.68 4371.25 93.52 o 6 4 0 2038.62 1992.19 80.87 o 7 4 0 4456.30 4303.04 92.02 o 8 4 0 1771.75 1720.80 77.43 o 9 4 0 2303.66 2275.81 109.70 o 10 4 0 1207.83 1221.86 101.34 o 11 4 0 756.53 753.87 98.94 o 12 4 0 1011.61 1054.52 110.45 o 13 4 0 662.76 679.90 170.25 o 0 5 0 15359.10 16147.84 314.24 o 1 5 0 1288.86 1306.77 114.28 o 2 5 0 4703.69 4528.33 92.66 o 3 5 0 2862.56 2730.39 87.98 o 4 5 0 2879.81 2741.87 92.47 o 5 5 0 8291.84 8451.15 130.30 o 6 5 0 3188.96 3146.02 92.51 o 7 5 0 3244.44 3258.85 96.63 o 8 5 0 1797.92 1641.75 78.83 o 9 5 0 1638.03 1666.19 104.45 o 10 5 0 867.23 839.23 97.62 o 11 5 0 1217.94 1235.90 109.09 o 12 5 0 637.77 695.57 104.44 o 0 6 0 842.56 596.91 153.95 o 1 6 0 824.40 685.55 111.30 o 2 6 0 5921.56 6281.71 151.01 o 3 6 0 6395.99 6520.79 111.92 o 4 6 0 1410.34 1290.12 97.31 o 5 6 0 7208.79 7181.91 127.10 o 6 6 0 2047.11 1863.24 95.47 o 7 6 0 6662.33 6738.90 135.51 o 8 6 0 400.51 398.18 72.52 o 9 6 0 1193.32 1157.56 116.67 o 10 6 0 642.60 638.11 110.77 o 11 6 0 1306.61 1279.83 131.93 o 12 6 0 728.13 673.50 163.00 o 0 7 0 184.11 178.36 141.16 o 1 7 0 1435.83 1551.02 132.33 o 2 7 0 3397.61 3504.29 157.33 o 3 7 0 6075.61 6259.10 112.49 o 4 7 0 10.25 -8.56 64.03 o 5 7 0 3768.67 3774.69 109.32 o 6 7 0 131.70 72.93 71.22 o 7 7 0 6895.80 6916.36 140.58 o 8 7 0 922.94 839.41 92.38 o 9 7 0 2391.68 2408.20 136.57 o 10 7 0 37.74 21.81 97.89 o 11 7 0 1567.37 1605.39 168.93 o 0 8 0 644.94 618.97 168.62 o 1 8 0 3514.75 3520.06 187.92 o 2 8 0 330.88 231.45 108.53 o 3 8 0 6747.00 6549.41 198.51 o 4 8 0 115.54 65.70 104.54 o 5 8 0 8733.23 9196.89 229.17 o 6 8 0 8.28 8.00 104.90 o 7 8 0 3378.79 3402.89 171.86 o 8 8 0 254.50 179.65 164.39 o 9 8 0 2546.24 2407.48 238.08 o 10 8 0 283.68 253.46 176.25 o 11 8 0 1369.73 1407.74 229.64 o 0 9 0 0.01 -44.59 143.39 o 1 9 0 3962.94 4034.60 178.45 o 2 9 0 8.37 20.90 102.74 o 3 9 0 2152.54 2201.96 155.52 o 4 9 0 4.76 27.52 105.40 o 5 9 0 5195.51 5142.57 196.09 o 6 9 0 251.99 134.48 113.88 o 7 9 0 3485.49 3457.60 179.51 o 10 9 0 3.50 86.83 175.19 o 0 10 0 266.06 157.82 156.65 o 1 10 0 4188.19 4329.68 189.91 o 2 10 0 44.99 49.94 106.61 o 3 10 0 3823.46 3871.88 185.60 o 4 10 0 289.44 291.52 120.06 o 5 10 0 4247.60 4234.85 194.98 o 6 10 0 40.32 42.52 116.05 o 7 10 0 1688.84 1713.19 163.98 o 0 11 0 639.70 545.75 183.64 o 1 11 0 2337.38 2100.46 252.40 o 2 11 0 615.13 409.52 126.43 o 3 11 0 1772.42 1875.67 162.66 o 4 11 0 20.71 36.57 116.65 o 5 11 0 1615.90 1568.59 161.99 o 6 11 0 436.70 346.26 132.75 o 7 11 0 1678.40 1744.11 172.82 o 0 12 0 764.69 556.78 192.32 o 1 12 0 1767.49 1718.46 164.28 o 2 12 0 1393.12 1191.19 156.15 o 3 12 0 2640.15 2528.94 182.50 o 4 12 0 776.69 902.68 150.74 o 5 12 0 2518.57 2580.63 189.50 o 6 12 0 186.54 217.04 136.64 o 7 12 0 1542.62 1489.80 177.44 o 0 13 0 1508.80 1417.12 237.61 o 1 13 0 1301.42 1115.24 160.70 o 2 13 0 788.92 682.38 149.46 o 3 13 0 1013.53 891.90 157.74 o 4 13 0 728.90 559.20 150.64 o 5 13 0 1816.72 1847.29 186.31 o 6 13 0 346.65 390.55 152.00 o 0 14 0 1376.87 1279.95 247.35 o 1 14 0 1505.42 1402.61 177.34 o 2 14 0 1336.19 1146.36 170.67 o 3 14 0 356.17 334.33 150.58 o 4 14 0 357.56 294.71 149.14 o -13 0 1 1837.29 2087.85 185.91 o -11 0 1 3349.44 3636.00 207.99 o -9 0 1 10039.60 10738.58 242.21 o -7 0 1 2644.09 2516.80 106.77 o -5 0 1 9875.65 10392.83 239.20 o -3 0 1 569.48 470.60 68.91 o 3 0 1 63490.88 71107.49 1215.84 o 5 0 1 10716.12 10775.84 173.68 o 7 0 1 4976.01 5244.53 131.52 o 9 0 1 8220.40 8806.36 225.42 o 11 0 1 2898.15 3115.26 180.84 o 13 0 1 1728.03 1965.46 276.34 o -13 1 1 1918.00 2135.86 131.19 o -12 1 1 3.15 26.58 85.05 o -11 1 1 3186.03 3402.18 130.82 o -10 1 1 43.90 41.06 74.46 o -9 1 1 5643.76 5910.34 139.44 o -8 1 1 175.19 128.06 70.13 o -7 1 1 2818.26 2714.21 77.01 o -6 1 1 229.51 139.35 56.70 o -5 1 1 8673.37 8886.54 95.89 o -4 1 1 994.40 965.92 55.80 o -3 1 1 10020.34 10279.93 89.54 o -2 1 1 674.35 633.43 52.80 o 0 1 1 1421.20 1577.57 58.92 o 1 1 1 18372.21 20552.57 184.22 o 2 1 1 10873.44 11656.16 98.61 o 3 1 1 1272.92 1223.60 55.85 o 4 1 1 3369.78 3102.83 69.95 o 5 1 1 8717.20 9271.76 114.12 o 6 1 1 1228.57 1025.47 63.34 o 7 1 1 2269.82 2258.36 75.57 o 8 1 1 112.54 64.36 54.41 o 9 1 1 3947.79 4087.23 124.34 o 10 1 1 315.53 260.41 81.56 o 11 1 1 3179.24 3408.43 131.52 o 12 1 1 20.51 23.57 129.19 o 13 1 1 2122.26 2268.84 204.86 o -13 2 1 1482.39 1650.93 126.00 o -12 2 1 322.35 327.27 93.04 o -11 2 1 3019.57 3213.44 134.80 o -10 2 1 385.51 384.70 83.87 o -9 2 1 2548.73 2686.26 112.26 o -8 2 1 36.73 61.19 78.37 o -7 2 1 5777.35 5823.95 136.93 o -6 2 1 693.17 497.04 57.25 o -5 2 1 4731.25 4283.93 79.24 o -4 2 1 936.64 899.16 61.64 o -3 2 1 3253.87 2950.90 71.84 o -1 2 1 225.50 372.93 57.14 o 0 2 1 2217.64 2274.89 60.36 o 2 2 1 9530.54 9840.20 185.80 o 3 2 1 24067.13 24884.90 186.02 o 4 2 1 778.23 769.67 61.72 o 5 2 1 17096.10 18140.40 173.93 o 6 2 1 12.62 3.33 48.23 o 7 2 1 3679.25 3640.80 85.46 o 8 2 1 2141.30 1945.17 77.45 o 9 2 1 2894.89 2888.24 113.71 o 10 2 1 1052.47 967.94 96.20 o 11 2 1 1843.90 1850.38 114.11 o 12 2 1 120.11 79.40 103.37 o 13 2 1 1766.15 1795.96 195.59 o -13 3 1 617.93 735.62 129.81 o -12 3 1 598.00 657.12 101.57 o -11 3 1 1804.39 1841.76 113.71 o -10 3 1 41.10 81.79 77.00 o -9 3 1 3241.38 3161.43 117.46 o -8 3 1 770.58 772.58 85.66 o -7 3 1 5587.69 5545.12 95.88 o -6 3 1 2916.90 2771.19 76.75 o -5 3 1 3880.85 3633.96 85.20 o -4 3 1 4088.68 3773.08 82.72 o -3 3 1 2927.95 3037.68 124.00 o -2 3 1 11186.25 12083.73 116.89 o -1 3 1 1481.63 1423.60 66.56 o 0 3 1 83.96 131.29 64.22 o 1 3 1 8970.27 9852.49 135.92 o 2 3 1 12140.94 12687.62 289.52 o 3 3 1 26842.79 30443.30 367.75 o 4 3 1 224.87 131.13 53.50 o 5 3 1 1302.75 1089.95 68.47 o 6 3 1 6157.96 6092.52 96.11 o 7 3 1 2203.80 2069.61 76.54 o 8 3 1 2071.65 1833.79 77.91 o 9 3 1 2700.88 2732.87 113.20 o 10 3 1 627.88 594.03 90.47 o 11 3 1 1151.68 1242.23 105.98 o 12 3 1 775.12 884.12 124.99 o 13 3 1 1366.58 1315.38 184.28 o -13 4 1 671.79 815.77 133.50 o -12 4 1 1021.01 1133.00 112.48 o -11 4 1 1141.15 1243.76 107.67 o -10 4 1 261.72 263.13 82.58 o -9 4 1 4611.27 4461.37 130.31 o -8 4 1 1900.35 1844.77 99.71 o -7 4 1 2354.55 2223.97 78.51 o -6 4 1 1585.97 1459.18 76.47 o -5 4 1 3603.86 3573.59 88.14 o -4 4 1 17197.47 18085.26 142.72 o -3 4 1 237.73 159.53 60.35 o -1 4 1 15793.32 17252.83 384.63 o 0 4 1 6551.50 7014.40 156.29 o 1 4 1 8179.04 8845.47 100.62 o 2 4 1 9768.77 9734.91 161.54 o 3 4 1 12924.20 14192.14 139.28 o 4 4 1 2771.50 2553.17 89.41 o 5 4 1 12956.39 13336.31 142.07 o 6 4 1 3382.69 3219.15 90.66 o 7 4 1 2870.31 2682.46 82.30 o 8 4 1 3004.90 2813.41 86.67 o 9 4 1 1317.62 1251.06 97.85 o 10 4 1 2143.20 1963.21 110.62 o 11 4 1 1183.42 1229.77 107.19 o 12 4 1 577.26 661.24 120.46 o -12 5 1 315.63 450.67 100.65 o -11 5 1 693.76 580.77 97.36 o -10 5 1 249.91 284.03 85.25 o -9 5 1 1744.20 1551.01 102.68 o -8 5 1 2356.56 2334.67 106.76 o -7 5 1 3776.52 3667.92 99.32 o -6 5 1 4235.12 4238.15 99.26 o -5 5 1 1430.98 1289.68 84.16 o -4 5 1 9623.70 10432.58 145.66 o -3 5 1 1635.97 1519.40 78.38 o -2 5 1 5184.28 5007.52 94.72 o -1 5 1 2261.25 2165.74 133.59 o 0 5 1 723.51 559.21 103.59 o 1 5 1 8997.66 9947.35 132.21 o 2 5 1 9393.15 9891.96 114.37 o 3 5 1 4800.73 5189.46 103.61 o 4 5 1 11608.04 11916.88 153.31 o 5 5 1 7104.04 7164.65 125.27 o 6 5 1 2112.92 1969.26 93.79 o 7 5 1 2451.62 2369.47 90.49 o 8 5 1 2966.74 3022.70 90.64 o 9 5 1 495.57 453.61 85.11 o 10 5 1 1189.06 1201.39 102.57 o 11 5 1 999.42 935.02 103.78 o 12 5 1 804.60 850.43 163.46 o -12 6 1 571.21 700.53 126.34 o -11 6 1 436.24 352.36 94.18 o -10 6 1 1448.43 1434.77 108.41 o -9 6 1 247.51 192.12 79.91 o -8 6 1 755.62 761.34 103.18 o -7 6 1 3419.11 3203.91 109.89 o -6 6 1 8338.70 8487.36 147.49 o -5 6 1 33.13 6.39 63.95 o -4 6 1 4485.53 4691.30 126.63 o -3 6 1 1855.03 1910.11 84.16 o -2 6 1 9738.05 10098.80 118.69 o -1 6 1 1568.08 1362.44 120.84 o 0 6 1 8006.44 8024.73 186.44 o 1 6 1 6704.32 6848.04 300.80 o 2 6 1 4195.03 4330.76 122.32 o 3 6 1 2881.21 2885.86 92.17 o 4 6 1 6016.88 6100.01 116.97 o 5 6 1 2112.73 1958.80 92.79 o 6 6 1 7336.21 7144.42 134.45 o 7 6 1 3178.90 3131.32 111.10 o 8 6 1 2995.15 2819.31 100.25 o 9 6 1 15.02 24.85 88.95 o 10 6 1 1328.31 1225.64 122.36 o 11 6 1 341.90 359.61 110.89 o 12 6 1 595.28 717.81 164.23 o -11 7 1 371.04 286.75 135.95 o -10 7 1 866.89 1034.38 122.76 o -9 7 1 270.77 258.70 97.53 o -8 7 1 3044.43 3156.14 170.26 o -7 7 1 21.13 49.95 72.73 o -6 7 1 5975.52 6140.77 129.88 o -5 7 1 9.11 -16.48 65.71 o -4 7 1 2125.28 1892.60 89.73 o -3 7 1 312.64 264.15 67.34 o -2 7 1 9065.13 9171.80 206.89 o -1 7 1 2306.97 2270.30 140.80 o 0 7 1 9390.01 8958.78 205.13 o 1 7 1 853.23 848.73 121.39 o 2 7 1 5296.36 5284.95 167.01 o 3 7 1 675.34 634.98 73.68 o 4 7 1 1182.27 1186.70 84.11 o 5 7 1 261.34 248.72 72.37 o 6 7 1 9167.31 9289.90 149.57 o 7 7 1 1407.49 1232.06 95.30 o 8 7 1 2763.90 2700.64 114.02 o 9 7 1 481.27 358.37 101.55 o 10 7 1 1305.96 1246.53 153.03 o 11 7 1 145.65 92.23 199.71 o -11 8 1 12.82 49.28 177.77 o -10 8 1 657.79 814.23 200.77 o -9 8 1 107.77 35.20 158.41 o -7 8 1 24.17 -36.00 105.54 o -6 8 1 2684.04 2846.02 161.25 o -5 8 1 38.53 3.41 102.97 o -4 8 1 7175.85 7338.26 206.34 o -3 8 1 756.82 652.89 120.43 o -2 8 1 8588.77 8697.08 284.14 o -1 8 1 483.44 480.29 114.99 o 0 8 1 6082.61 6072.60 190.50 o 1 8 1 2.43 -14.16 97.24 o 2 8 1 5994.74 6094.11 192.65 o 3 8 1 1341.82 1276.13 136.89 o 4 8 1 6035.06 6165.69 196.61 o 5 8 1 35.81 49.94 103.20 o 6 8 1 8419.95 8867.22 414.45 o 7 8 1 15.30 15.68 107.13 o 8 8 1 3673.62 3672.44 179.41 o 9 8 1 122.86 125.79 162.52 o 10 8 1 1205.82 1178.10 211.68 o -10 9 1 2316.71 2351.98 253.22 o -7 9 1 36.75 65.03 114.13 o -6 9 1 1879.24 1868.18 156.44 o -5 9 1 0.76 21.71 105.65 o -4 9 1 9156.44 9346.53 233.03 o -3 9 1 786.66 581.05 122.99 o -2 9 1 5828.13 5953.58 200.88 o -1 9 1 333.57 223.29 111.47 o 0 9 1 6276.11 6362.96 203.78 o 1 9 1 81.04 63.04 104.44 o 2 9 1 1748.55 1681.24 148.01 o 3 9 1 523.03 459.81 120.48 o 4 9 1 5941.40 5981.57 203.75 o 5 9 1 3.61 -4.65 106.53 o 6 9 1 1814.19 2085.92 188.27 o 7 9 1 5.01 -26.42 112.98 o 8 9 1 3441.52 3789.72 189.97 o 10 9 1 2246.26 2142.29 244.19 o -10 10 1 1785.93 1735.47 248.41 o -7 10 1 31.96 95.99 120.80 o -6 10 1 1646.12 1512.51 245.07 o -5 10 1 83.21 54.41 113.68 o -4 10 1 2505.18 2416.43 165.70 o -3 10 1 27.15 -7.22 107.89 o -2 10 1 6215.07 6315.12 212.56 o -1 10 1 539.18 462.61 121.94 o 0 10 1 6152.44 5628.38 205.80 o 1 10 1 104.99 80.15 109.55 o 2 10 1 1514.97 1490.63 149.34 o 3 10 1 111.74 99.15 112.51 o 4 10 1 4428.36 4533.98 198.00 o 5 10 1 90.21 98.29 116.07 o 6 10 1 2261.50 2073.66 166.68 o 7 10 1 15.94 26.46 120.20 o 8 10 1 3656.79 3948.15 200.70 o -7 11 1 45.53 101.72 128.66 o -6 11 1 3348.85 3714.12 258.56 o -5 11 1 154.28 124.28 123.50 o -4 11 1 3856.68 3842.20 195.68 o -3 11 1 695.09 614.16 134.21 o -2 11 1 1800.00 1512.09 155.78 o -1 11 1 116.21 99.50 114.17 o 0 11 1 1865.86 1876.51 159.97 o 1 11 1 175.24 209.43 119.19 o 2 11 1 2422.96 2395.99 170.67 o 3 11 1 198.29 189.35 120.12 o 4 11 1 1581.49 1568.84 159.55 o 5 11 1 168.70 121.52 121.64 o 6 11 1 1155.80 1152.78 156.95 o 7 11 1 27.79 43.76 128.00 o -7 12 1 1193.94 1298.03 176.19 o -6 12 1 1306.12 1334.23 169.24 o -5 12 1 323.73 413.11 139.17 o -4 12 1 2891.12 2672.67 187.79 o -3 12 1 725.18 702.03 144.00 o -2 12 1 1072.36 917.75 149.68 o -1 12 1 649.71 432.51 132.32 o 0 12 1 3085.91 2692.44 182.91 o 1 12 1 1149.78 855.46 146.84 o 2 12 1 1806.63 1680.85 165.41 o 3 12 1 460.02 369.26 134.82 o 4 12 1 806.25 790.91 148.73 o 5 12 1 422.43 311.25 137.81 o 6 12 1 1778.83 1573.77 174.82 o 7 12 1 553.56 560.99 151.80 o -6 13 1 1459.25 1535.39 183.99 o -5 13 1 399.85 330.22 145.21 o -4 13 1 1415.23 1380.41 174.66 o -3 13 1 586.39 547.63 146.74 o -2 13 1 1261.67 1146.91 162.25 o -1 13 1 668.74 656.40 147.25 o 0 13 1 754.91 645.12 146.62 o 1 13 1 1444.70 1403.94 167.04 o 2 13 1 789.60 692.48 150.73 o 3 13 1 595.58 553.14 147.71 o 4 13 1 1431.90 1322.75 172.74 o 5 13 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