#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203403.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203403_Fobs loop_ _publ_author_name 'Crane, Jonathan D.' 'Young, Nigel' _publ_section_title ; Hydridotetrakis(triphenylphosphito)cobalt(I) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m487 _journal_page_last m488 _journal_volume 60 _journal_year 2004 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.117 _cell_angle_gamma 90.000 _cell_length_a 20.2331 _cell_length_b 17.2635 _cell_length_c 18.3682 _exptl_crystal_F_000 2704.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file ci6351Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' COBALT HYDRIDE P(OPH)3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 780.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -24 259.97 416.08 658.84 o 4 0 -24 469.41 240.43 592.32 o 6 0 -24 666.55 678.20 429.95 o 8 0 -24 444.66 439.19 448.16 o 1 1 -24 76.20 106.79 511.79 o 3 1 -24 55.68 116.11 372.37 o 5 1 -24 18.91 40.04 314.72 o 7 1 -24 633.77 449.92 322.41 o 2 2 -24 640.94 545.50 411.80 o 4 2 -24 233.55 223.54 336.75 o 6 2 -24 124.95 92.09 328.88 o 3 3 -24 226.88 321.89 400.32 o 5 3 -24 721.89 641.86 340.88 o 1 1 -23 166.72 242.84 403.56 o 3 1 -23 713.46 681.19 318.92 o 5 1 -23 622.41 566.28 302.99 o 7 1 -23 733.59 536.99 277.37 o 9 1 -23 2819.35 3064.58 271.64 o 11 1 -23 2878.46 2838.40 266.37 o 0 2 -23 1405.85 1251.59 427.94 o 2 2 -23 1.69 153.95 385.01 o 4 2 -23 148.56 264.34 307.87 o 6 2 -23 77.55 104.34 293.64 o 8 2 -23 76.08 3.50 257.16 o 10 2 -23 679.34 748.22 251.16 o 12 2 -23 39.03 82.68 263.52 o -1 3 -23 1107.20 1007.23 610.99 o 1 3 -23 1468.50 1271.22 391.17 o 3 3 -23 225.79 138.77 354.80 o 5 3 -23 203.65 235.92 286.48 o 7 3 -23 1017.70 835.15 283.29 o 9 3 -23 1011.09 1030.19 304.64 o 11 3 -23 402.67 430.84 255.69 o -2 4 -23 574.90 345.47 540.38 o 0 4 -23 992.17 878.05 368.44 o 2 4 -23 1083.07 922.18 328.83 o 4 4 -23 686.54 760.93 342.39 o 6 4 -23 191.84 156.58 322.58 o 8 4 -23 251.19 230.32 303.64 o 10 4 -23 803.89 763.16 285.14 o -1 5 -23 1555.28 1287.39 370.08 o 1 5 -23 2033.30 2026.39 321.69 o 3 5 -23 365.03 399.94 316.26 o 5 5 -23 301.44 234.26 321.50 o 7 5 -23 995.82 969.16 293.58 o 9 5 -23 289.03 265.43 308.56 o 0 6 -23 1133.44 1016.43 333.48 o 2 6 -23 251.33 268.91 320.98 o 4 6 -23 54.01 252.40 358.77 o 6 6 -23 94.51 65.72 224.40 o 8 6 -23 190.84 288.43 296.73 o 3 7 -23 66.71 -55.89 328.20 o 5 7 -23 246.56 288.04 327.48 o 2 0 -22 485.31 620.80 438.01 o 4 0 -22 1551.17 1329.73 378.55 o 6 0 -22 1982.85 2109.77 388.23 o 8 0 -22 4586.46 4514.46 371.59 o 10 0 -22 6135.96 6712.06 381.37 o 12 0 -22 2937.63 3138.41 413.75 o 14 0 -22 1239.78 1672.49 511.20 o 1 1 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284.86 o 10 4 -22 174.89 139.28 244.61 o 12 4 -22 448.58 462.51 227.25 o 14 4 -22 1900.77 2203.38 297.18 o -5 5 -22 782.86 1008.98 620.33 o -3 5 -22 224.37 235.76 526.37 o -1 5 -22 689.91 333.07 347.86 o 1 5 -22 901.74 820.25 302.42 o 3 5 -22 701.28 692.08 336.13 o 5 5 -22 516.75 372.64 308.45 o 7 5 -22 516.46 435.68 271.97 o 9 5 -22 711.97 856.66 267.44 o 11 5 -22 700.25 688.34 232.73 o 13 5 -22 486.31 469.63 254.73 o -4 6 -22 259.10 133.05 531.63 o -2 6 -22 339.50 480.97 318.32 o 0 6 -22 2293.14 1973.01 322.49 o 2 6 -22 1645.09 1745.16 312.91 o 4 6 -22 89.63 -64.73 334.68 o 6 6 -22 1103.95 1238.93 288.54 o 8 6 -22 274.22 265.67 291.70 o 10 6 -22 511.97 530.34 300.75 o 12 6 -22 1668.44 1849.24 245.51 o -3 7 -22 514.18 512.37 538.63 o -1 7 -22 648.24 517.62 316.72 o 1 7 -22 706.50 521.39 303.14 o 3 7 -22 1446.71 1336.73 305.95 o 5 7 -22 24.78 120.38 305.07 o 7 7 -22 73.92 24.10 285.26 o 9 7 -22 18.25 148.75 263.77 o 11 7 -22 64.23 -52.42 307.07 o 0 8 -22 881.93 1041.71 360.01 o 2 8 -22 2482.85 2343.91 323.21 o 4 8 -22 1225.27 869.90 354.20 o 6 8 -22 150.75 -5.75 314.36 o 8 8 -22 246.85 327.65 294.83 o 10 8 -22 1001.18 927.47 276.59 o 1 9 -22 961.12 1059.31 361.44 o 3 9 -22 1632.58 1356.12 321.92 o 5 9 -22 518.19 335.38 321.88 o 7 9 -22 424.93 530.03 330.04 o -1 1 -21 289.38 297.03 602.24 o 1 1 -21 1048.18 1062.09 292.87 o 3 1 -21 2532.45 2709.90 280.41 o 5 1 -21 2665.40 2604.79 253.71 o 7 1 -21 2318.40 2258.87 247.23 o 9 1 -21 4203.72 4210.78 247.70 o 11 1 -21 3318.48 3497.84 297.33 o 13 1 -21 2808.91 3070.57 284.40 o 15 1 -21 725.00 481.02 285.05 o 17 1 -21 1187.17 1099.94 334.25 o -2 2 -21 63.30 74.70 549.72 o 0 2 -21 56.22 178.33 339.67 o 2 2 -21 144.73 114.99 279.65 o 4 2 -21 306.36 226.72 271.91 o 6 2 -21 1161.88 1110.81 227.55 o 8 2 -21 171.80 41.58 233.54 o 10 2 -21 308.77 358.23 222.57 o 12 2 -21 340.89 316.39 301.28 o 14 2 -21 931.68 844.38 346.71 o 16 2 -21 240.64 382.00 322.06 o -3 3 -21 207.55 251.52 483.19 o -1 3 -21 1114.95 1048.54 325.99 o 1 3 -21 1302.55 1243.11 320.39 o 3 3 -21 1461.57 1386.04 281.10 o 5 3 -21 61.29 91.36 265.26 o 7 3 -21 406.95 482.47 249.39 o 9 3 -21 1371.02 1471.09 216.49 o 11 3 -21 1444.86 1710.32 251.17 o 13 3 -21 630.19 728.99 273.76 o 15 3 -21 2340.77 2285.93 328.74 o -4 4 -21 326.50 433.59 499.53 o -2 4 -21 115.99 184.75 334.84 o 0 4 -21 379.64 437.46 301.64 o 2 4 -21 288.12 295.55 284.10 o 4 4 -21 273.67 182.77 287.05 o 6 4 -21 405.89 437.24 266.60 o 8 4 -21 744.67 631.06 227.67 o 10 4 -21 721.32 449.10 221.23 o 12 4 -21 142.17 82.04 292.38 o 14 4 -21 97.15 260.75 276.15 o 16 4 -21 118.92 280.41 298.63 o -5 5 -21 122.99 240.43 513.54 o -3 5 -21 655.16 232.26 491.94 o -1 5 -21 1872.78 1828.79 332.81 o 1 5 -21 3880.60 3725.92 331.18 o 3 5 -21 235.91 287.15 318.89 o 5 5 -21 51.05 159.40 289.06 o 7 5 -21 86.17 137.12 251.34 o 9 5 -21 533.83 604.59 276.27 o 11 5 -21 1331.82 1363.10 238.63 o 13 5 -21 2598.57 2519.72 287.48 o 15 5 -21 2418.43 2330.95 271.52 o -6 6 -21 823.81 653.59 517.04 o -4 6 -21 1257.96 793.06 501.87 o -2 6 -21 282.48 305.31 298.40 o 0 6 -21 496.98 418.06 290.82 o 2 6 -21 51.96 250.13 269.24 o 4 6 -21 97.38 217.09 287.47 o 6 6 -21 639.49 596.36 266.74 o 8 6 -21 429.35 420.70 250.05 o 10 6 -21 593.26 617.52 261.51 o 12 6 -21 836.22 888.30 230.02 o 14 6 -21 104.50 145.12 294.33 o -5 7 -21 437.96 505.95 508.28 o -3 7 -21 186.16 62.93 283.45 o -1 7 -21 1254.15 1201.42 298.93 o 1 7 -21 2395.95 2450.56 342.28 o 3 7 -21 1523.77 1339.72 295.87 o 5 7 -21 59.51 31.08 286.99 o 7 7 -21 15.14 42.76 243.39 o 9 7 -21 144.10 150.65 243.97 o 11 7 -21 2467.33 2496.38 275.05 o 13 7 -21 1898.46 1957.57 242.71 o -4 8 -21 284.23 220.00 506.53 o -2 8 -21 430.87 344.38 284.99 o 0 8 -21 368.36 332.85 341.69 o 2 8 -21 869.44 767.92 334.82 o 4 8 -21 2287.91 1931.12 346.93 o 6 8 -21 54.81 -4.32 296.79 o 8 8 -21 48.05 105.07 299.41 o 10 8 -21 218.89 337.46 255.44 o 12 8 -21 96.70 68.30 250.08 o -3 9 -21 65.31 113.93 287.45 o -1 9 -21 1126.70 1095.13 314.19 o 1 9 -21 1127.85 1252.41 307.60 o 3 9 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