#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:04:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180954 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203427.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203427_Fobs loop_ _publ_author_name 'Ni, Chun-Lin' 'Li, Yi-Zhi' 'Ni, Zhao-Ping' 'Dang, Dong-Bin' 'Meng, Qing-Jin' _publ_section_title ; [1,2-Bis(diphenylphosphino)ethane](2,3-quinoxalinedithiolato)nickel(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m410 _journal_page_last m412 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.4270 _cell_length_b 12.9470 _cell_length_c 20.7520 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file fl6084Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FL6084' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3697.68 3787.52 69.78 o 4 0 0 2561.26 3346.52 70.01 o 6 0 0 4315.25 4603.62 79.13 o 8 0 0 9.47 37.65 14.71 o 10 0 0 698.01 581.83 27.30 o 12 0 0 682.05 696.18 48.86 o 14 0 0 1.67 0.00 49.09 o 1 1 0 16535.92 17736.45 266.02 o 2 1 0 10514.90 11849.86 170.37 o 3 1 0 2562.61 2645.18 29.96 o 4 1 0 0.82 15.61 3.31 o 5 1 0 306.21 335.42 6.94 o 6 1 0 4529.56 5057.11 61.57 o 7 1 0 6315.89 6784.36 74.05 o 8 1 0 1.12 46.73 10.39 o 9 1 0 354.36 329.96 12.39 o 10 1 0 975.13 971.05 27.47 o 11 1 0 35.47 45.77 12.18 o 12 1 0 58.16 34.32 20.51 o 13 1 0 54.47 61.11 29.79 o 14 1 0 3.13 9.66 37.85 o 0 2 0 3596.17 3813.37 100.83 o 1 2 0 3261.44 3562.12 70.42 o 2 2 0 1883.49 2065.00 37.17 o 3 2 0 12980.61 12260.75 143.61 o 4 2 0 12927.42 12442.19 155.43 o 5 2 0 8561.29 8658.51 98.16 o 6 2 0 9329.67 9383.98 106.97 o 7 2 0 3228.27 3452.76 47.49 o 8 2 0 1853.71 1693.23 23.06 o 9 2 0 10.40 3.09 8.90 o 10 2 0 56.78 69.31 12.96 o 11 2 0 152.84 100.65 14.09 o 12 2 0 124.17 116.14 16.75 o 13 2 0 191.17 234.48 33.15 o 1 3 0 1190.73 1049.04 16.55 o 2 3 0 2363.46 1996.64 26.19 o 3 3 0 2.38 17.07 13.07 o 4 3 0 1591.78 1445.91 18.66 o 5 3 0 9409.38 9187.43 101.63 o 6 3 0 1411.64 1486.93 21.25 o 7 3 0 251.35 320.50 12.55 o 8 3 0 198.14 238.99 11.95 o 9 3 0 196.44 265.82 15.91 o 10 3 0 4.46 18.70 15.04 o 11 3 0 1.18 27.30 14.73 o 12 3 0 365.52 528.33 27.30 o 13 3 0 3.01 32.15 20.65 o 0 4 0 19645.55 21387.69 581.74 o 1 4 0 3785.51 3960.25 59.73 o 2 4 0 17654.55 16948.55 356.00 o 3 4 0 3639.55 3314.05 51.26 o 4 4 0 32.07 40.94 18.35 o 5 4 0 1394.09 1526.86 28.97 o 6 4 0 130.76 172.39 8.12 o 7 4 0 2.25 9.86 8.82 o 8 4 0 155.84 194.82 12.68 o 9 4 0 646.43 651.65 20.98 o 10 4 0 602.37 595.43 23.25 o 11 4 0 602.60 613.50 26.27 o 12 4 0 55.09 53.31 17.76 o 13 4 0 626.71 737.22 35.36 o 1 5 0 2160.43 2276.00 38.31 o 2 5 0 1210.94 1299.33 25.41 o 3 5 0 3925.52 3981.00 78.23 o 4 5 0 628.39 847.77 30.81 o 5 5 0 468.06 388.11 11.88 o 6 5 0 2362.59 2765.00 78.61 o 7 5 0 979.80 777.33 13.79 o 8 5 0 21.44 25.62 9.72 o 9 5 0 515.40 526.67 15.52 o 10 5 0 33.33 68.77 13.58 o 11 5 0 36.19 19.32 12.82 o 12 5 0 107.24 174.63 25.87 o 13 5 0 4.96 12.06 22.34 o 0 6 0 273.96 263.95 16.24 o 1 6 0 18.62 94.47 9.57 o 2 6 0 967.62 1098.26 23.75 o 3 6 0 8809.78 8824.09 154.16 o 4 6 0 5481.19 4757.71 66.38 o 5 6 0 3558.70 4269.60 114.46 o 6 6 0 156.01 109.16 11.57 o 7 6 0 1050.93 1051.43 35.45 o 8 6 0 0.34 3.13 10.31 o 9 6 0 26.06 21.06 11.30 o 10 6 0 11.05 0.00 11.28 o 11 6 0 276.41 241.94 17.00 o 12 6 0 20.11 59.61 17.80 o 13 6 0 7.36 4.27 17.93 o 1 7 0 225.87 253.34 10.47 o 2 7 0 2321.62 2373.78 41.00 o 3 7 0 23.44 60.26 16.98 o 4 7 0 5002.23 5028.77 92.22 o 5 7 0 3871.56 3843.42 74.95 o 6 7 0 171.52 319.99 22.68 o 7 7 0 73.41 75.67 14.07 o 8 7 0 50.01 65.28 10.97 o 9 7 0 1203.72 963.04 20.61 o 10 7 0 44.30 50.12 17.72 o 11 7 0 235.11 194.48 21.60 o 12 7 0 7.11 14.60 21.10 o 0 8 0 7.65 44.86 10.93 o 1 8 0 66.22 102.74 9.33 o 2 8 0 81.63 86.04 20.51 o 3 8 0 936.92 1099.63 36.66 o 4 8 0 2922.98 3262.40 80.35 o 5 8 0 423.51 344.31 16.81 o 6 8 0 1075.45 943.15 25.30 o 7 8 0 1070.98 1031.07 34.99 o 8 8 0 1070.95 1068.22 28.89 o 9 8 0 12.21 64.90 16.34 o 10 8 0 108.31 167.83 18.90 o 11 8 0 439.41 469.01 31.52 o 12 8 0 41.56 17.20 21.98 o 1 9 0 287.59 293.87 12.99 o 2 9 0 42.70 115.17 37.15 o 3 9 0 421.30 362.41 16.92 o 4 9 0 14.67 0.00 10.37 o 5 9 0 1971.09 1908.12 68.72 o 6 9 0 586.93 653.80 27.06 o 7 9 0 177.35 292.87 25.25 o 8 9 0 11.45 38.60 13.91 o 9 9 0 810.70 753.27 24.80 o 10 9 0 543.73 554.94 24.11 o 11 9 0 164.04 115.40 22.62 o 0 10 0 61.63 63.56 14.46 o 1 10 0 960.74 959.87 29.81 o 2 10 0 82.40 73.22 13.94 o 3 10 0 105.88 153.95 17.87 o 4 10 0 20.12 33.81 14.92 o 5 10 0 582.93 583.16 43.17 o 6 10 0 753.79 703.30 25.61 o 7 10 0 217.64 290.97 62.58 o 8 10 0 524.23 636.90 32.37 o 9 10 0 62.05 106.04 27.49 o 10 10 0 138.99 188.54 20.53 o 1 11 0 205.24 279.65 17.22 o 2 11 0 656.82 623.37 24.44 o 3 11 0 482.00 431.78 24.98 o 4 11 0 281.37 432.25 28.65 o 5 11 0 880.93 880.99 30.31 o 6 11 0 303.00 335.67 23.37 o 7 11 0 255.98 304.50 24.08 o 8 11 0 705.42 709.68 72.49 o 9 11 0 370.92 398.57 24.15 o 10 11 0 11.50 39.56 31.16 o 0 12 0 1192.85 1097.47 54.14 o 1 12 0 135.72 114.80 25.49 o 2 12 0 1668.13 1726.99 73.84 o 3 12 0 55.20 68.10 19.06 o 4 12 0 11.63 30.68 17.00 o 5 12 0 42.10 82.32 22.09 o 6 12 0 60.35 98.92 28.10 o 7 12 0 267.95 266.00 40.04 o 8 12 0 42.34 126.85 28.46 o 9 12 0 130.27 142.27 25.34 o 1 13 0 2304.96 2165.13 43.58 o 2 13 0 77.23 103.81 20.70 o 3 13 0 469.56 471.17 39.89 o 4 13 0 4.19 35.62 20.99 o 5 13 0 175.08 224.44 24.87 o 6 13 0 0.29 55.46 24.70 o 7 13 0 4.61 61.88 24.63 o 8 13 0 38.02 53.36 23.30 o 0 14 0 50.30 81.06 36.16 o 1 14 0 163.45 149.59 25.78 o 2 14 0 149.19 191.28 37.81 o 3 14 0 395.11 436.15 42.09 o 4 14 0 227.16 193.84 43.12 o 5 14 0 222.10 264.45 34.89 o 6 14 0 75.99 96.18 28.70 o 1 15 0 101.84 114.96 35.79 o 2 15 0 147.05 136.67 30.89 o 3 15 0 199.08 204.44 30.12 o 4 15 0 96.06 123.19 46.42 o 1 0 1 6251.43 6644.50 77.23 o 2 0 1 1491.02 1364.83 13.15 o 3 0 1 5349.11 5936.20 68.03 o 4 0 1 2502.47 3023.31 42.10 o 5 0 1 11178.11 11615.18 128.12 o 6 0 1 1355.19 1745.25 29.10 o 7 0 1 217.07 227.94 9.34 o 8 0 1 302.82 330.79 11.74 o 9 0 1 206.62 141.30 9.69 o 10 0 1 587.28 462.04 12.98 o 11 0 1 2.13 52.40 19.97 o 12 0 1 416.40 445.56 31.10 o 13 0 1 205.99 244.72 31.19 o 14 0 1 4.79 12.37 32.11 o -14 1 1 3.67 0.00 34.97 o -13 1 1 38.79 68.42 32.72 o -12 1 1 280.35 334.18 30.17 o -11 1 1 219.20 285.61 28.69 o -10 1 1 1104.60 1025.26 28.03 o -9 1 1 274.35 314.13 13.06 o -8 1 1 912.96 780.78 22.97 o -7 1 1 1336.24 1300.74 17.27 o -6 1 1 6471.26 6736.00 73.55 o -5 1 1 1962.34 2187.39 30.28 o -4 1 1 5462.93 5668.06 61.25 o -3 1 1 287.26 273.25 7.63 o -2 1 1 18144.10 18375.98 210.41 o -1 1 1 2300.58 2422.23 72.13 o 1 1 1 2449.37 2653.55 32.35 o 2 1 1 17388.10 17607.76 188.05 o 3 1 1 298.51 271.59 5.66 o 4 1 1 5540.75 5708.30 61.55 o 5 1 1 2041.39 2207.07 25.70 o 6 1 1 6377.74 6690.82 73.45 o 7 1 1 1434.29 1406.09 20.09 o 8 1 1 959.54 818.44 17.95 o 9 1 1 283.41 313.82 12.48 o 10 1 1 1024.69 982.23 28.08 o 11 1 1 258.86 319.17 18.93 o 12 1 1 282.03 276.18 26.32 o 13 1 1 44.94 61.59 27.49 o 14 1 1 2.95 47.86 36.35 o -13 2 1 241.57 383.44 40.20 o -12 2 1 274.54 309.31 22.14 o -11 2 1 273.39 372.89 20.60 o -10 2 1 755.68 814.33 28.69 o -9 2 1 517.39 574.07 18.54 o -8 2 1 764.39 755.86 16.07 o -7 2 1 871.86 953.77 18.27 o -6 2 1 3258.12 3106.33 35.44 o -5 2 1 421.20 442.77 11.43 o -4 2 1 6142.36 6280.55 93.49 o -3 2 1 11304.76 11514.20 133.32 o -2 2 1 4789.99 5087.03 140.38 o -1 2 1 14346.78 15112.47 402.46 o 0 2 1 2256.03 2452.99 49.63 o 1 2 1 14878.92 15780.06 233.54 o 2 2 1 4919.20 5235.48 70.54 o 3 2 1 10438.79 10569.89 119.88 o 4 2 1 6639.31 6707.27 66.55 o 5 2 1 395.49 412.53 8.20 o 6 2 1 3334.11 3199.65 35.67 o 7 2 1 827.39 904.33 18.76 o 8 2 1 791.98 796.17 23.04 o 9 2 1 525.76 595.65 19.57 o 10 2 1 764.70 801.45 28.00 o 11 2 1 264.60 377.72 20.36 o 12 2 1 297.33 361.67 23.82 o 13 2 1 250.65 331.63 48.54 o -13 3 1 388.45 400.73 29.11 o -12 3 1 532.36 562.50 35.87 o -11 3 1 342.10 479.85 23.99 o -10 3 1 1051.85 992.97 31.17 o -9 3 1 20.46 72.06 13.65 o -8 3 1 647.70 576.05 14.20 o -7 3 1 3201.54 3479.58 47.30 o -6 3 1 2198.87 2328.16 37.33 o -5 3 1 4366.91 4267.07 62.17 o -4 3 1 237.78 317.70 10.87 o -3 3 1 401.26 405.39 20.11 o -2 3 1 1566.52 1429.32 36.08 o -1 3 1 235.25 225.58 5.01 o 0 3 1 9897.54 10450.96 191.12 o 1 3 1 164.39 171.72 6.44 o 2 3 1 1795.04 1645.48 21.65 o 3 3 1 432.24 457.92 11.11 o 4 3 1 245.30 275.53 7.34 o 5 3 1 4743.25 4642.61 44.93 o 6 3 1 2111.37 2216.26 32.79 o 7 3 1 3186.26 3413.96 46.84 o 8 3 1 672.14 590.54 13.72 o 9 3 1 23.96 75.78 13.63 o 10 3 1 1061.89 969.86 34.50 o 11 3 1 324.94 379.99 20.13 o 12 3 1 550.37 625.79 28.64 o 13 3 1 372.78 439.82 36.38 o -13 4 1 84.50 106.72 39.22 o -12 4 1 334.27 305.49 33.52 o -11 4 1 363.92 438.39 38.64 o -10 4 1 326.63 293.34 16.23 o -9 4 1 160.83 161.78 16.82 o -8 4 1 1905.13 2032.37 39.65 o -7 4 1 2364.83 2562.08 62.82 o -6 4 1 2257.96 2337.31 38.23 o -5 4 1 893.43 949.75 19.82 o -4 4 1 464.52 493.56 24.60 o -3 4 1 1376.57 1275.45 37.41 o -2 4 1 8021.38 7592.42 116.16 o -1 4 1 5120.01 5002.73 65.57 o 0 4 1 5887.55 6278.74 122.75 o 1 4 1 4964.19 4901.61 67.15 o 2 4 1 8480.57 8081.85 97.79 o 3 4 1 1495.99 1393.51 41.49 o 4 4 1 400.03 450.16 18.53 o 5 4 1 963.45 1013.76 15.89 o 6 4 1 2443.11 2545.27 39.96 o 7 4 1 2309.24 2432.07 40.71 o 8 4 1 1994.47 2143.97 51.34 o 9 4 1 117.90 156.52 12.44 o 10 4 1 286.16 261.77 16.49 o 11 4 1 396.57 431.46 37.20 o 12 4 1 350.98 329.92 21.18 o 13 4 1 90.39 124.63 19.80 o -13 5 1 8.91 14.11 20.47 o -12 5 1 26.95 26.23 25.47 o -11 5 1 119.86 151.53 17.38 o -10 5 1 138.13 121.34 13.31 o -9 5 1 108.92 88.56 10.02 o -8 5 1 1129.62 1209.53 26.81 o -7 5 1 2681.27 2778.65 54.19 o -6 5 1 2454.70 2597.14 64.08 o -5 5 1 1306.40 1413.20 38.65 o -4 5 1 4779.70 4353.06 94.14 o -3 5 1 1257.41 1064.69 28.55 o -2 5 1 4995.24 5031.83 68.18 o -1 5 1 12856.55 13733.53 203.70 o 0 5 1 2584.42 2873.45 62.44 o 1 5 1 12771.65 13557.96 205.29 o 2 5 1 4668.35 4641.73 71.25 o 3 5 1 1377.70 1158.25 16.51 o 4 5 1 4647.80 4266.48 55.16 o 5 5 1 1272.14 1359.80 37.68 o 6 5 1 2389.65 2602.10 44.92 o 7 5 1 2880.45 3131.23 48.18 o 8 5 1 1022.38 1088.56 26.21 o 9 5 1 161.76 145.03 11.72 o 10 5 1 154.63 167.49 18.09 o 11 5 1 101.76 126.31 16.58 o 12 5 1 22.98 34.15 26.61 o 13 5 1 12.22 27.25 19.78 o -13 6 1 16.52 38.55 23.77 o -12 6 1 65.48 57.70 20.64 o -11 6 1 102.27 142.91 23.15 o -10 6 1 88.79 121.04 19.96 o -9 6 1 96.29 105.73 17.99 o -8 6 1 284.97 270.65 15.33 o -7 6 1 513.50 443.81 32.85 o -6 6 1 713.11 883.37 34.59 o -5 6 1 613.55 644.03 25.71 o -4 6 1 244.83 254.44 22.43 o -3 6 1 464.11 526.26 30.04 o -2 6 1 3167.99 3278.42 53.31 o -1 6 1 16748.01 17350.96 246.07 o 0 6 1 26674.38 28209.29 424.66 o 1 6 1 16342.20 16879.57 247.58 o 2 6 1 3375.59 3477.98 57.37 o 3 6 1 529.63 576.40 17.11 o 4 6 1 252.99 253.12 26.79 o 5 6 1 655.14 736.97 26.51 o 6 6 1 740.04 871.82 33.70 o 7 6 1 562.97 514.96 15.82 o 8 6 1 361.35 334.92 15.91 o 9 6 1 70.54 72.40 10.48 o 10 6 1 85.64 78.69 16.61 o 11 6 1 113.96 145.05 33.55 o 12 6 1 68.10 99.25 27.40 o 13 6 1 16.28 26.01 21.44 o -12 7 1 5.08 0.00 23.42 o -11 7 1 165.72 131.24 21.65 o -10 7 1 389.16 447.45 27.88 o -9 7 1 169.39 231.01 16.65 o -8 7 1 330.14 284.03 18.04 o -7 7 1 321.51 462.02 26.00 o -6 7 1 1994.52 1824.28 68.06 o -5 7 1 1090.59 1079.79 31.48 o -4 7 1 429.25 451.28 19.68 o -3 7 1 482.72 526.24 25.28 o -2 7 1 783.26 872.24 23.04 o -1 7 1 5469.49 5503.86 99.79 o 0 7 1 1729.98 1717.25 24.94 o 1 7 1 6055.55 5993.21 83.07 o 2 7 1 716.16 782.75 17.04 o 3 7 1 544.35 573.14 20.79 o 4 7 1 406.45 414.65 19.10 o 5 7 1 1083.84 1058.54 30.02 o 6 7 1 2072.89 1984.74 41.63 o 7 7 1 352.03 437.27 19.81 o 8 7 1 285.74 233.43 13.48 o 9 7 1 143.94 174.66 23.00 o 10 7 1 437.52 466.47 20.80 o 11 7 1 139.19 131.39 22.77 o 12 7 1 3.67 0.00 22.68 o -12 8 1 4.99 8.67 27.34 o -11 8 1 38.44 18.32 26.43 o -10 8 1 267.35 247.31 21.47 o -9 8 1 123.26 148.59 21.83 o -8 8 1 381.93 372.77 23.81 o -7 8 1 711.59 646.31 24.18 o -6 8 1 786.06 779.83 68.29 o -5 8 1 1717.80 1746.05 47.59 o -4 8 1 1774.77 1775.05 41.79 o -3 8 1 77.64 85.93 19.98 o -2 8 1 3190.02 3083.46 58.44 o -1 8 1 298.57 369.36 21.68 o 0 8 1 109.30 90.45 7.31 o 1 8 1 248.09 303.62 13.73 o 2 8 1 3182.05 3019.73 57.74 o 3 8 1 61.64 79.64 13.09 o 4 8 1 1877.74 1800.63 39.84 o 5 8 1 1720.00 1891.28 49.97 o 6 8 1 722.56 684.96 25.63 o 7 8 1 716.51 665.13 19.15 o 8 8 1 421.97 403.95 18.64 o 9 8 1 150.90 128.93 15.95 o 10 8 1 246.25 247.12 19.04 o 11 8 1 47.89 27.16 29.09 o 12 8 1 4.18 41.70 25.76 o -11 9 1 7.07 0.00 31.73 o -10 9 1 146.48 142.53 31.25 o -9 9 1 398.26 467.65 22.24 o -8 9 1 104.20 150.85 20.31 o -7 9 1 35.62 52.04 17.06 o -6 9 1 120.85 173.71 19.50 o -5 9 1 1436.36 1431.73 38.83 o -4 9 1 238.24 228.18 26.03 o -3 9 1 554.24 617.21 26.40 o -2 9 1 1254.20 1312.61 36.95 o -1 9 1 126.57 135.14 31.44 o 0 9 1 1176.45 1124.16 18.35 o 1 9 1 206.76 226.36 12.63 o 2 9 1 1293.84 1357.57 41.03 o 3 9 1 559.33 625.32 26.14 o 4 9 1 182.89 211.12 24.81 o 5 9 1 1539.46 1457.51 36.88 o 6 9 1 76.11 116.57 17.91 o 7 9 1 62.34 148.08 32.87 o 8 9 1 94.27 107.46 15.40 o 9 9 1 382.13 487.57 22.90 o 10 9 1 131.80 115.51 16.38 o 11 9 1 11.21 38.92 23.71 o -10 10 1 354.06 381.34 23.44 o -9 10 1 147.42 187.73 41.82 o -8 10 1 98.77 139.20 21.07 o -7 10 1 247.15 227.43 26.67 o -6 10 1 163.09 197.61 19.56 o -5 10 1 182.25 263.18 55.06 o -4 10 1 1428.23 1279.78 31.23 o -3 10 1 1429.82 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39.15 o 3 1 24 27.25 68.04 25.45 o 4 1 24 104.80 137.59 33.88 o -4 2 24 41.81 82.97 29.03 o -3 2 24 23.15 46.33 38.57 o -2 2 24 53.34 95.10 68.06 o -1 2 24 110.46 183.41 40.02 o 0 2 24 231.06 312.86 78.80 o 1 2 24 72.31 104.73 29.62 o 2 2 24 42.43 51.29 34.20 o 3 2 24 29.02 3.55 29.12 o 4 2 24 38.14 58.32 46.86 o -4 3 24 198.05 213.63 30.23 o -3 3 24 9.78 87.40 28.59 o -2 3 24 16.56 46.94 32.36 o -1 3 24 375.60 331.21 24.90 o 0 3 24 20.02 42.93 24.69 o 1 3 24 339.53 291.04 50.36 o 2 3 24 16.39 27.25 29.88 o 3 3 24 18.34 45.74 33.97 o 4 3 24 181.90 184.46 29.08 o -3 4 24 54.85 131.36 31.56 o -2 4 24 11.82 34.99 26.40 o -1 4 24 199.67 191.04 26.61 o 0 4 24 0.11 50.12 25.73 o 1 4 24 173.02 243.23 55.55 o 2 4 24 3.80 23.35 22.80 o 3 4 24 63.36 93.87 35.26 o -2 5 24 123.13 156.62 28.85 o -1 5 24 18.66 21.14 28.27 o 0 5 24 381.74 382.37 26.72 o 1 5 24 12.91 21.32 20.88 o 2 5 24 135.26 136.14 23.80 o 1 0 25 92.35 83.25 31.61 o 2 0 25 98.55 147.19 28.52 o 3 0 25 323.16 310.56 37.66 o -2 1 25 104.98 77.51 28.32 o -1 1 25 26.98 35.37 23.20 o 0 1 25 26.24 26.59 54.71 o 1 1 25 19.40 51.53 38.09 o 2 1 25 111.84 118.64 49.98 o -2 2 25 125.15 169.26 37.53 o -1 2 25 2.50 26.69 25.06 o 0 2 25 49.98 44.41 25.65 o 1 2 25 0.28 17.53 33.91 o 2 2 25 91.84 138.95 38.83 o -1 3 25 60.66 136.52 28.29 o 0 3 25 14.62 57.81 33.76 o 1 3 25 69.02 73.48 26.35 o