#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203466.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203466_Fobs loop_ _publ_author_name 'Song, Qing Bao' 'Hu, You Hua' 'Shen, Tian Hua' 'Jin, Zhi Min' _publ_section_title ; 1-Aminocyclopentanecarboxamide ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o539 _journal_page_last o541 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 125.509 _cell_angle_gamma 90.000 _cell_length_a 15.3005 _cell_length_b 18.5860 _cell_length_c 12.2311 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file na6295Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 31115am C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 383.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11327.51 11495.78 19.23 o 4 0 0 1213.57 1210.55 35.57 o 6 0 0 3040.23 2989.32 30.96 o 8 0 0 12.97 32.88 14.18 o 10 0 0 307.60 314.95 22.08 o 12 0 0 292.22 308.00 37.42 o 14 0 0 91.66 174.23 125.42 o 1 1 0 2026.80 2111.64 55.54 o 3 1 0 578.82 619.29 28.14 o 5 1 0 1508.61 1538.93 12.71 o 7 1 0 1879.95 1851.73 10.32 o 9 1 0 898.99 876.47 27.60 o 11 1 0 57.57 53.78 24.68 o 13 1 0 291.87 300.36 46.33 o 2 2 0 33119.76 33319.80 33.14 o 4 2 0 306.27 336.71 17.74 o 6 2 0 971.10 949.53 16.27 o 8 2 0 11.41 36.61 11.77 o 10 2 0 299.33 313.32 18.61 o 12 2 0 32.03 33.94 6.28 o 14 2 0 39.30 91.72 49.94 o 1 3 0 1596.37 1701.23 56.37 o 3 3 0 3193.84 3197.20 21.78 o 5 3 0 7896.95 7837.16 17.85 o 7 3 0 1413.12 1370.47 20.15 o 9 3 0 701.14 692.91 30.16 o 11 3 0 105.54 113.48 12.86 o 13 3 0 121.72 134.69 26.68 o 0 4 0 147415.14 148919.22 118.09 o 2 4 0 84.03 102.85 31.74 o 4 4 0 6230.86 6250.09 23.39 o 6 4 0 1903.85 1888.20 19.07 o 8 4 0 105.90 162.37 33.41 o 10 4 0 13.20 14.05 24.13 o 12 4 0 371.80 369.14 19.40 o 14 4 0 4.78 71.56 84.46 o 1 5 0 134.84 134.16 23.93 o 3 5 0 3865.27 3840.67 14.29 o 5 5 0 2333.76 2266.01 17.82 o 7 5 0 98.34 126.63 24.08 o 9 5 0 1957.45 1847.18 22.16 o 11 5 0 197.63 184.03 30.82 o 13 5 0 136.62 140.24 20.65 o 0 6 0 5230.99 5202.03 93.31 o 2 6 0 507.39 524.13 21.11 o 4 6 0 6.50 83.44 67.41 o 6 6 0 715.14 716.69 23.16 o 8 6 0 88.49 116.15 18.85 o 10 6 0 267.31 253.74 16.39 o 12 6 0 135.10 148.34 16.34 o 14 6 0 28.80 58.15 28.63 o 1 7 0 24.94 67.42 27.53 o 3 7 0 5822.42 5730.17 15.88 o 5 7 0 2189.06 2250.32 69.99 o 7 7 0 1.21 38.61 22.85 o 9 7 0 852.53 871.88 44.63 o 11 7 0 0.04 13.89 28.66 o 13 7 0 0.10 22.10 17.92 o 0 8 0 9451.01 9069.67 113.54 o 2 8 0 1251.50 1194.29 16.51 o 4 8 0 1029.41 1067.91 50.43 o 6 8 0 179.16 254.34 70.80 o 8 8 0 155.82 148.16 11.03 o 10 8 0 241.81 242.83 17.86 o 12 8 0 86.40 105.36 19.98 o 14 8 0 27.44 77.38 70.30 o 1 9 0 2360.67 2372.20 35.91 o 3 9 0 2505.97 2551.45 37.40 o 5 9 0 1628.38 1555.12 24.53 o 7 9 0 119.19 141.97 38.29 o 9 9 0 4.46 88.26 59.19 o 11 9 0 25.63 47.24 14.81 o 13 9 0 1.44 44.57 36.57 o 0 10 0 2654.77 2605.32 69.03 o 2 10 0 512.06 564.19 48.73 o 4 10 0 3189.95 3115.29 17.81 o 6 10 0 87.06 129.59 44.71 o 8 10 0 130.72 135.37 9.52 o 10 10 0 49.52 75.63 23.44 o 12 10 0 109.30 153.72 45.48 o 1 11 0 124.37 130.82 17.50 o 3 11 0 701.82 704.35 30.48 o 5 11 0 837.31 850.66 22.69 o 7 11 0 105.59 126.19 31.61 o 9 11 0 466.75 480.22 31.25 o 11 11 0 158.14 162.77 32.62 o 13 11 0 16.91 34.05 31.61 o 0 12 0 906.53 921.20 113.54 o 2 12 0 44.42 51.63 22.76 o 4 12 0 548.26 570.22 51.09 o 6 12 0 1901.40 1843.05 45.60 o 8 12 0 17.37 88.74 63.18 o 10 12 0 4.69 30.81 18.41 o 12 12 0 17.88 41.91 22.62 o 1 13 0 27.05 73.49 31.27 o 3 13 0 903.46 869.37 23.52 o 5 13 0 34.15 118.44 74.69 o 7 13 0 220.59 257.10 50.28 o 9 13 0 291.18 283.06 21.46 o 11 13 0 12.40 17.05 28.70 o 0 14 0 651.57 629.08 25.29 o 2 14 0 425.81 404.84 23.14 o 4 14 0 3975.63 3779.38 49.57 o 6 14 0 193.49 188.04 3.80 o 8 14 0 296.54 289.33 37.68 o 10 14 0 182.00 179.43 17.39 o 12 14 0 17.00 42.08 24.28 o 1 15 0 138.91 145.45 18.97 o 3 15 0 82.68 81.53 8.22 o 5 15 0 25.40 103.35 68.62 o 7 15 0 3.42 9.68 5.31 o 9 15 0 195.36 181.83 33.00 o 11 15 0 24.75 50.71 24.91 o 0 16 0 48.60 150.96 121.88 o 2 16 0 172.05 172.29 13.92 o 4 16 0 41.81 64.52 21.83 o 6 16 0 718.90 716.95 59.32 o 8 16 0 1.03 5.56 5.01 o 10 16 0 50.73 63.81 14.99 o 1 17 0 719.87 688.09 17.59 o 3 17 0 206.63 213.50 29.59 o 5 17 0 0.04 61.94 54.70 o 7 17 0 45.64 50.99 39.45 o 9 17 0 8.87 62.85 45.76 o 0 18 0 68.83 76.87 24.02 o 2 18 0 185.85 199.91 27.79 o 4 18 0 370.67 348.25 24.28 o 6 18 0 1.45 33.04 38.44 o 8 18 0 15.94 61.50 42.09 o 1 19 0 228.88 207.45 23.14 o 3 19 0 79.23 160.68 84.73 o 5 19 0 25.89 64.76 34.50 o 7 19 0 32.44 76.76 41.27 o 0 20 0 110.94 139.33 42.73 o 2 20 0 1.02 37.11 28.07 o 4 20 0 37.79 78.83 39.93 o 6 20 0 38.25 39.27 24.53 o 1 21 0 338.01 339.41 40.99 o 3 21 0 51.51 109.98 58.71 o 5 21 0 0.23 71.04 61.19 o 0 22 0 38.79 54.37 24.78 o 2 22 0 56.62 81.20 27.96 o 4 22 0 32.85 55.63 41.72 o -13 1 1 82.44 119.52 25.21 o -11 1 1 51.92 113.38 32.62 o -9 1 1 128.68 119.20 30.03 o -7 1 1 1934.67 1977.36 24.88 o -5 1 1 1154.17 1122.39 19.29 o -3 1 1 29908.21 30006.87 14.31 o -1 1 1 4218.25 4345.30 68.25 o 1 1 1 9696.15 9788.89 18.22 o 3 1 1 1064.76 1089.11 14.06 o 5 1 1 2809.69 2780.10 18.82 o 7 1 1 52.47 74.71 14.06 o 9 1 1 252.29 255.41 15.15 o 11 1 1 63.94 81.67 18.50 o 13 1 1 33.71 71.33 35.08 o -14 2 1 9.67 25.40 27.69 o -12 2 1 67.80 74.05 18.04 o -10 2 1 352.64 375.75 28.06 o -8 2 1 277.31 287.44 16.07 o -6 2 1 343.53 352.98 15.90 o -4 2 1 8297.12 8339.98 24.21 o -2 2 1 5107.86 5184.85 20.62 o 0 2 1 61.57 61.36 20.05 o 2 2 1 2017.12 2036.98 7.70 o 4 2 1 934.58 919.99 16.30 o 6 2 1 2302.42 2240.05 30.33 o 8 2 1 0.16 57.39 27.77 o 10 2 1 320.03 323.01 21.46 o 12 2 1 145.07 188.35 52.76 o 14 2 1 60.78 70.26 33.00 o -13 3 1 2.88 72.56 43.40 o -11 3 1 55.59 74.26 12.28 o -9 3 1 581.20 578.30 24.60 o -7 3 1 1525.41 1513.37 26.12 o -5 3 1 5600.27 5610.94 29.57 o -3 3 1 67394.98 67471.59 15.70 o -1 3 1 5537.42 5626.22 44.41 o 1 3 1 21388.73 21415.85 40.71 o 3 3 1 695.84 714.49 24.89 o 5 3 1 358.74 353.77 15.85 o 7 3 1 0.04 20.08 9.07 o 9 3 1 535.31 541.98 22.83 o 11 3 1 109.77 149.18 36.80 o 13 3 1 187.37 201.22 39.87 o -14 4 1 4.09 42.18 28.68 o -12 4 1 324.14 301.90 11.34 o -10 4 1 425.62 414.35 18.69 o -8 4 1 9.45 38.20 14.38 o -6 4 1 3242.16 3259.55 16.96 o -4 4 1 917.76 905.02 17.70 o -2 4 1 1384.59 1428.08 22.86 o 0 4 1 20825.57 20822.92 26.43 o 2 4 1 5277.63 5293.27 15.45 o 4 4 1 291.80 353.24 34.20 o 6 4 1 888.85 887.50 23.01 o 8 4 1 178.66 190.99 20.28 o 10 4 1 193.31 198.61 22.46 o 12 4 1 33.59 33.22 13.39 o 14 4 1 3.03 52.06 40.97 o -13 5 1 82.81 89.34 12.03 o -11 5 1 61.88 64.12 20.07 o -9 5 1 17.10 77.45 36.81 o -7 5 1 7767.60 7591.50 20.18 o -5 5 1 621.10 618.72 26.73 o -3 5 1 462.63 448.91 12.69 o -1 5 1 4545.18 4553.71 45.72 o 1 5 1 4306.55 4363.68 18.82 o 3 5 1 761.18 794.69 26.08 o 5 5 1 494.99 501.20 19.16 o 7 5 1 4.88 57.39 28.97 o 9 5 1 110.57 163.16 37.30 o 11 5 1 3.88 18.30 16.31 o 13 5 1 0.52 40.98 28.91 o -14 6 1 8.07 33.65 23.38 o -12 6 1 138.99 136.31 10.87 o -10 6 1 442.13 449.86 33.04 o -8 6 1 2418.14 2290.70 27.01 o -6 6 1 784.47 799.43 17.58 o -4 6 1 4255.65 4281.17 33.36 o -2 6 1 255.54 288.70 28.80 o 0 6 1 128.33 142.00 25.89 o 2 6 1 25.23 62.72 33.77 o 4 6 1 2556.24 2534.58 43.93 o 6 6 1 3242.13 3149.17 29.66 o 8 6 1 0.03 33.70 18.57 o 10 6 1 282.89 254.73 33.26 o 12 6 1 278.63 258.97 18.71 o 14 6 1 26.70 24.28 6.07 o -15 7 1 11.88 44.42 30.36 o -13 7 1 44.72 86.24 35.85 o -11 7 1 330.07 327.63 22.01 o -9 7 1 146.61 162.01 31.79 o -7 7 1 28.53 32.90 29.50 o -5 7 1 1448.89 1460.01 19.65 o -3 7 1 4548.12 4628.73 50.65 o -1 7 1 6887.72 6893.58 42.09 o 1 7 1 9732.86 9686.37 24.64 o 3 7 1 8.51 87.46 67.97 o 5 7 1 1867.88 1868.81 53.47 o 7 7 1 38.30 95.82 39.48 o 9 7 1 393.72 395.68 22.10 o 11 7 1 1.54 48.63 26.91 o 13 7 1 127.30 167.82 37.91 o -14 8 1 34.38 101.69 59.17 o -12 8 1 317.55 367.81 59.73 o -10 8 1 43.25 124.04 56.60 o -8 8 1 4.67 52.60 32.68 o -6 8 1 115.96 166.82 52.24 o -4 8 1 487.08 475.08 34.88 o -2 8 1 13.50 47.94 29.78 o 0 8 1 44.60 81.08 25.12 o 2 8 1 2362.41 2358.81 39.11 o 4 8 1 1062.00 1047.32 38.44 o 6 8 1 2.29 37.12 28.63 o 8 8 1 55.19 83.07 23.69 o 10 8 1 140.26 160.52 26.93 o 12 8 1 19.13 41.32 15.20 o -13 9 1 12.38 39.71 27.82 o -11 9 1 13.27 15.93 17.46 o -9 9 1 655.05 639.96 18.92 o -7 9 1 81.98 141.25 56.82 o -5 9 1 4.66 76.19 51.80 o -3 9 1 154.07 164.81 17.71 o -1 9 1 583.20 578.95 31.61 o 1 9 1 649.87 658.71 12.88 o 3 9 1 91.72 155.10 61.22 o 5 9 1 338.45 378.34 46.16 o 7 9 1 117.18 174.09 57.44 o 9 9 1 88.65 152.37 54.37 o 11 9 1 1.12 5.81 40.11 o 13 9 1 17.25 59.60 38.18 o -14 10 1 5.68 47.48 37.18 o -12 10 1 2.35 66.61 55.57 o -10 10 1 8.72 27.06 15.61 o -8 10 1 738.65 733.74 22.04 o -6 10 1 160.26 200.29 36.27 o -4 10 1 123.02 177.44 46.83 o -2 10 1 4078.79 3979.52 2.78 o 0 10 1 235.73 267.92 37.00 o 2 10 1 23.68 35.24 15.53 o 4 10 1 322.21 364.76 49.88 o 6 10 1 22.91 97.32 66.82 o 8 10 1 23.11 26.09 23.71 o 10 10 1 4.70 26.02 22.42 o 12 10 1 25.64 41.11 12.25 o -13 11 1 46.20 101.22 52.07 o -11 11 1 88.26 101.15 19.06 o -9 11 1 95.19 94.46 40.02 o -7 11 1 437.70 491.44 75.14 o -5 11 1 63.99 88.63 29.22 o -3 11 1 14.37 61.71 37.65 o -1 11 1 3328.74 3206.24 31.98 o 1 11 1 2328.10 2350.46 53.53 o 3 11 1 486.84 517.86 49.16 o 5 11 1 456.30 492.25 63.24 o 7 11 1 154.01 225.18 78.98 o 9 11 1 169.75 152.95 30.23 o 11 11 1 1.06 65.83 45.20 o -12 12 1 1.97 15.50 11.38 o -10 12 1 268.25 258.47 15.31 o -8 12 1 4.85 20.85 12.52 o -6 12 1 384.70 440.29 82.70 o -4 12 1 20.55 75.57 45.81 o -2 12 1 0.77 36.92 30.04 o 0 12 1 157.03 183.53 33.42 o 2 12 1 211.41 207.66 11.27 o 4 12 1 200.02 200.58 7.00 o 6 12 1 99.89 161.00 60.42 o 8 12 1 307.41 313.64 36.42 o 10 12 1 16.15 71.14 41.25 o 12 12 1 5.38 63.77 42.39 o -13 13 1 19.61 75.09 53.94 o -11 13 1 20.83 19.09 17.07 o -9 13 1 28.66 69.74 30.48 o -7 13 1 2.80 4.05 1.79 o -5 13 1 960.44 939.76 12.28 o -3 13 1 47.54 107.04 59.59 o -1 13 1 345.30 341.89 35.64 o 1 13 1 319.86 333.76 30.19 o 3 13 1 47.03 104.00 57.29 o 5 13 1 68.35 84.17 19.60 o 7 13 1 13.28 59.13 37.94 o 9 13 1 136.89 131.71 13.12 o 11 13 1 11.11 30.97 13.68 o -12 14 1 14.51 15.17 38.06 o -10 14 1 21.80 29.58 21.87 o -8 14 1 115.87 113.36 32.49 o -6 14 1 96.32 104.35 18.24 o -4 14 1 24.62 92.88 60.25 o -2 14 1 967.28 932.52 19.54 o 0 14 1 451.16 454.72 30.87 o 2 14 1 973.99 961.72 18.30 o 4 14 1 1.26 35.85 30.62 o 6 14 1 8.25 80.15 65.07 o 8 14 1 21.45 69.04 39.27 o 10 14 1 0.04 92.47 66.69 o -11 15 1 100.25 126.82 31.43 o -9 15 1 34.64 97.00 58.93 o -7 15 1 27.71 79.39 42.54 o -5 15 1 28.69 34.77 14.67 o -3 15 1 92.01 118.59 25.54 o -1 15 1 3.57 34.63 18.29 o 1 15 1 0.00 31.82 28.95 o 3 15 1 68.83 97.10 27.14 o 5 15 1 31.83 115.57 78.88 o 7 15 1 0.58 68.56 60.36 o 9 15 1 0.10 8.13 39.83 o -10 16 1 12.35 105.06 82.91 o -8 16 1 27.96 81.40 50.96 o -6 16 1 1.19 42.87 35.15 o -4 16 1 14.90 26.84 9.32 o -2 16 1 223.82 236.87 30.41 o 0 16 1 664.07 687.03 46.45 o 2 16 1 112.97 155.29 50.79 o 4 16 1 83.69 127.49 48.37 o 6 16 1 39.82 55.34 42.73 o 8 16 1 54.00 50.87 41.72 o 10 16 1 0.63 80.20 57.84 o -9 17 1 12.75 55.56 39.85 o -7 17 1 194.49 185.75 12.81 o -5 17 1 502.51 487.80 38.02 o -3 17 1 6.83 46.66 37.35 o -1 17 1 59.59 88.18 35.15 o 1 17 1 196.92 176.08 33.51 o 3 17 1 48.02 111.11 56.20 o 5 17 1 55.07 72.44 22.79 o 7 17 1 22.69 45.30 40.96 o 9 17 1 114.77 102.48 24.15 o -10 18 1 0.06 10.44 34.90 o -8 18 1 100.25 126.50 37.48 o -6 18 1 104.51 125.25 33.72 o -4 18 1 376.46 376.89 41.92 o -2 18 1 41.24 83.57 37.94 o 0 18 1 227.42 214.05 30.85 o 2 18 1 340.32 326.54 15.30 o 4 18 1 4.61 87.92 73.76 o 6 18 1 11.41 47.69 30.98 o 8 18 1 3.60 40.74 31.74 o -9 19 1 98.18 145.15 85.47 o -7 19 1 3.62 26.23 16.94 o -5 19 1 35.14 85.63 46.58 o -3 19 1 31.29 57.05 23.46 o -1 19 1 80.68 124.58 49.94 o 1 19 1 300.39 289.28 23.01 o 3 19 1 19.47 81.29 58.20 o 5 19 1 16.19 96.02 73.76 o 7 19 1 27.15 59.51 32.76 o -8 20 1 52.38 60.46 13.44 o -6 20 1 7.62 29.73 19.17 o -4 20 1 103.89 172.71 105.70 o -2 20 1 64.46 141.61 107.47 o 0 20 1 247.98 265.99 37.53 o 2 20 1 50.56 112.53 88.76 o 4 20 1 4.76 39.41 33.51 o 6 20 1 44.27 66.31 23.52 o -5 21 1 18.93 109.20 81.00 o -3 21 1 3.43 66.31 54.18 o -1 21 1 9.96 96.13 75.46 o 1 21 1 8.96 62.77 45.41 o 3 21 1 5.05 17.09 37.42 o 5 21 1 7.34 80.52 65.79 o -4 22 1 37.76 96.96 57.49 o -2 22 1 22.57 63.78 38.74 o 0 22 1 33.29 60.44 27.06 o 2 22 1 2.37 44.18 38.09 o -14 0 2 112.00 146.66 63.22 o -12 0 2 1803.35 1708.42 40.82 o -10 0 2 160.70 178.35 22.52 o -8 0 2 1361.44 1407.20 37.83 o -6 0 2 11395.75 11303.91 15.64 o -4 0 2 32917.63 33030.21 16.84 o -2 0 2 32.11 85.09 46.29 o 0 0 2 5118.72 5259.99 35.28 o 2 0 2 9145.81 9215.53 55.52 o 4 0 2 4417.42 4405.68 45.44 o 6 0 2 2803.32 2785.91 23.35 o 8 0 2 353.36 351.25 32.30 o 10 0 2 178.72 246.04 105.19 o 12 0 2 17.82 77.63 75.36 o -15 1 2 0.01 28.34 22.24 o -13 1 2 543.04 495.51 22.99 o -11 1 2 401.41 386.18 22.58 o -9 1 2 651.85 661.64 16.70 o -7 1 2 84.46 96.53 10.49 o -5 1 2 849.79 880.70 24.45 o -3 1 2 33330.86 33687.78 14.76 o -1 1 2 8751.54 8858.35 37.03 o 1 1 2 2150.45 2157.40 28.28 o 3 1 2 2620.86 2643.41 26.58 o 5 1 2 2508.99 2464.43 15.63 o 7 1 2 739.05 742.78 22.55 o 9 1 2 18.90 18.22 29.14 o 11 1 2 34.73 59.52 22.19 o 13 1 2 59.55 55.68 41.34 o -14 2 2 164.61 168.96 23.24 o -12 2 2 480.20 471.00 14.73 o -10 2 2 2843.28 2755.73 16.49 o -8 2 2 96.42 112.53 15.61 o -6 2 2 1414.32 1391.40 12.86 o -4 2 2 8077.31 8083.53 17.87 o -2 2 2 22974.54 23137.82 44.70 o 0 2 2 71.40 86.41 16.95 o 2 2 2 2102.13 2095.49 23.68 o 4 2 2 594.57 598.75 14.26 o 6 2 2 329.99 315.11 20.80 o 8 2 2 417.92 409.66 9.30 o 10 2 2 82.64 82.77 25.31 o 12 2 2 0.02 17.46 18.84 o -15 3 2 76.37 113.03 57.91 o -13 3 2 25.36 45.53 23.87 o -11 3 2 17.89 54.61 19.88 o -9 3 2 603.14 605.52 19.43 o -7 3 2 17.76 25.34 8.13 o -5 3 2 1344.83 1365.12 25.78 o -3 3 2 24545.60 24623.86 20.06 o -1 3 2 3340.44 3369.10 26.43 o 1 3 2 1713.10 1718.82 17.65 o 3 3 2 760.75 752.75 27.97 o 5 3 2 904.50 929.47 24.35 o 7 3 2 1141.40 1102.02 13.21 o 9 3 2 101.67 122.59 19.16 o 11 3 2 2.96 50.65 31.35 o 13 3 2 29.21 75.61 41.39 o -16 4 2 0.24 88.25 110.50 o -14 4 2 7.64 66.62 43.02 o -12 4 2 630.41 608.31 22.53 o -10 4 2 21.64 70.11 24.05 o -8 4 2 425.70 446.93 14.48 o -6 4 2 5.73 31.04 20.00 o -4 4 2 1280.45 1289.67 14.77 o -2 4 2 11.47 40.96 17.69 o 0 4 2 3121.71 3160.57 21.29 o 2 4 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