#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203544.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203544_Fobs loop_ _publ_author_name 'Zeller, Matthias' 'Hunter, Allen D.' 'Sampson, Paul' 'Chumachenko, Nataliya' _publ_section_title ; (4aSR,7RS,9aSR)-7,9a-Dimethyl-5,5-dioxo-1,2,4a,6,7,9a-hexahydro-8-oxa-5\l^6^-thia-1,4-benzocyclohepten-9-one ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o729 _journal_page_last o730 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.062 _cell_angle_gamma 90.000 _cell_length_a 10.0232 _cell_length_b 10.6255 _cell_length_c 11.6726 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file bt6435Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 04mz08am in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22808.26 22078.31 883.54 o 4 0 0 395.54 328.73 5.85 o 6 0 0 231.94 230.74 4.65 o 8 0 0 1416.89 1439.96 29.66 o 10 0 0 0.13 1.41 0.72 o 12 0 0 53.77 54.04 3.12 o 1 1 0 18.41 19.91 0.52 o 2 1 0 8838.91 9296.60 102.71 o 3 1 0 193.22 221.77 2.85 o 4 1 0 530.80 616.33 7.29 o 5 1 0 148.85 147.91 2.24 o 6 1 0 716.56 647.26 7.89 o 7 1 0 102.95 94.29 2.04 o 8 1 0 211.64 190.21 3.46 o 9 1 0 114.96 109.55 2.96 o 10 1 0 15.93 16.83 1.14 o 11 1 0 135.62 135.01 3.69 o 12 1 0 39.00 47.18 2.42 o 0 2 0 1288.92 1445.27 22.71 o 1 2 0 366.89 386.98 4.52 o 2 2 0 1347.49 1502.83 16.75 o 3 2 0 99.37 112.42 1.66 o 4 2 0 807.91 740.17 8.68 o 5 2 0 888.24 932.44 12.81 o 6 2 0 785.54 796.62 11.52 o 7 2 0 251.35 255.24 4.20 o 8 2 0 376.65 348.87 5.53 o 9 2 0 17.57 19.61 1.20 o 10 2 0 143.10 138.82 3.60 o 11 2 0 54.56 51.81 2.10 o 12 2 0 41.85 46.04 2.42 o 1 3 0 6739.14 6798.04 85.48 o 2 3 0 2686.16 2891.51 31.91 o 3 3 0 1296.37 1303.12 14.74 o 4 3 0 1687.04 1838.29 20.68 o 5 3 0 393.66 385.47 4.97 o 6 3 0 5.80 7.90 0.63 o 7 3 0 1862.13 1872.22 23.65 o 8 3 0 184.60 177.51 3.39 o 9 3 0 16.00 17.35 1.13 o 10 3 0 32.63 32.53 1.64 o 11 3 0 9.95 12.33 1.33 o 0 4 0 32.97 30.12 1.04 o 1 4 0 39.35 20.57 0.78 o 2 4 0 196.61 222.25 2.95 o 3 4 0 3105.90 3589.72 43.56 o 4 4 0 147.04 147.43 2.27 o 5 4 0 1698.16 1792.50 20.38 o 6 4 0 140.95 138.99 2.69 o 7 4 0 10.24 12.30 0.79 o 8 4 0 30.86 31.63 1.26 o 9 4 0 151.27 144.85 3.58 o 10 4 0 219.62 220.06 4.92 o 11 4 0 10.64 14.63 1.31 o 1 5 0 5689.93 6021.14 66.12 o 2 5 0 556.30 570.49 6.88 o 3 5 0 2693.38 2716.24 30.28 o 4 5 0 51.54 47.01 1.10 o 5 5 0 460.90 441.33 5.72 o 6 5 0 8.24 6.15 0.64 o 7 5 0 244.82 220.15 4.65 o 8 5 0 16.71 12.68 0.86 o 9 5 0 105.10 101.79 2.53 o 10 5 0 9.24 11.25 1.13 o 11 5 0 31.11 34.97 2.99 o 0 6 0 916.44 883.33 14.64 o 1 6 0 2157.73 2171.78 24.35 o 2 6 0 0.12 1.78 0.30 o 3 6 0 837.32 867.26 10.38 o 4 6 0 14.90 16.55 1.07 o 5 6 0 2472.53 2498.63 38.86 o 6 6 0 0.85 0.86 0.41 o 7 6 0 168.91 166.56 3.30 o 8 6 0 244.26 237.16 4.36 o 9 6 0 83.27 77.06 2.17 o 10 6 0 2.97 5.87 1.23 o 11 6 0 11.31 10.02 1.77 o 1 7 0 110.64 114.25 1.95 o 2 7 0 88.68 78.73 1.81 o 3 7 0 37.13 39.78 1.06 o 4 7 0 113.47 97.53 2.00 o 5 7 0 183.37 165.87 3.12 o 6 7 0 16.37 13.82 0.84 o 7 7 0 446.72 455.36 7.97 o 8 7 0 29.86 29.95 1.51 o 9 7 0 163.53 168.31 4.89 o 10 7 0 107.31 111.55 4.95 o 0 8 0 1937.08 1933.21 32.04 o 1 8 0 0.02 1.04 0.79 o 2 8 0 180.59 157.49 2.57 o 3 8 0 21.85 17.97 0.88 o 4 8 0 89.93 84.53 2.11 o 5 8 0 106.53 119.35 3.98 o 6 8 0 2.67 2.66 0.66 o 7 8 0 135.10 139.01 3.53 o 8 8 0 385.02 397.07 12.38 o 9 8 0 54.27 53.24 2.73 o 10 8 0 83.45 82.92 3.30 o 1 9 0 28.18 26.20 1.32 o 2 9 0 998.13 985.14 13.15 o 3 9 0 2.74 2.19 0.45 o 4 9 0 55.42 43.26 1.43 o 5 9 0 5.26 8.71 0.86 o 6 9 0 545.45 575.41 9.77 o 7 9 0 99.78 96.88 2.91 o 8 9 0 124.19 125.94 6.45 o 9 9 0 42.77 41.61 4.54 o 0 10 0 1058.81 989.28 21.38 o 1 10 0 28.79 29.84 1.44 o 2 10 0 102.59 80.84 2.46 o 3 10 0 87.52 93.01 2.65 o 4 10 0 16.54 13.32 1.22 o 5 10 0 56.90 60.85 3.12 o 6 10 0 83.51 81.16 3.13 o 7 10 0 29.31 35.80 2.79 o 8 10 0 52.44 62.41 2.84 o 1 11 0 10.65 12.06 0.98 o 2 11 0 106.83 109.36 3.06 o 3 11 0 2.87 6.88 1.15 o 4 11 0 36.70 33.45 1.96 o 5 11 0 49.22 54.81 2.56 o 6 11 0 57.44 60.31 5.76 o 7 11 0 48.80 42.23 3.08 o 0 12 0 207.36 204.31 6.67 o 1 12 0 68.37 67.42 2.41 o 2 12 0 6.67 8.88 1.07 o 3 12 0 7.32 9.12 0.82 o 4 12 0 58.48 64.01 2.87 o 5 12 0 151.61 155.86 6.44 o 6 12 0 231.71 241.09 11.83 o 1 13 0 2.16 2.82 0.81 o 2 13 0 2.05 3.34 0.69 o 3 13 0 17.45 19.32 1.64 o 4 13 0 83.08 86.80 3.49 o 0 14 0 90.89 92.02 4.33 o 1 14 0 0.90 3.14 0.65 o -11 0 1 1157.04 1201.33 40.08 o -9 0 1 836.38 830.84 18.33 o -7 0 1 2202.07 2345.88 37.46 o -5 0 1 12.33 24.10 0.97 o -3 0 1 3873.68 4108.38 86.24 o -1 0 1 2144.81 2282.38 32.07 o 1 0 1 8172.62 8611.68 169.11 o 3 0 1 59.80 73.61 1.70 o 5 0 1 668.63 804.12 13.44 o 7 0 1 147.22 127.00 4.21 o 9 0 1 24.39 30.36 2.44 o 11 0 1 18.96 18.77 1.80 o -12 1 1 53.32 59.20 3.54 o -11 1 1 62.91 63.64 2.30 o -10 1 1 86.84 86.14 2.91 o -9 1 1 1456.30 1495.59 21.85 o -8 1 1 45.16 46.16 1.42 o -7 1 1 1575.77 1647.56 18.90 o -6 1 1 376.57 355.28 4.67 o -5 1 1 115.02 96.42 1.62 o -4 1 1 11.60 11.14 0.47 o -3 1 1 442.30 424.35 5.04 o -2 1 1 2.37 4.39 0.62 o -1 1 1 10667.19 10523.95 142.98 o 0 1 1 479.40 524.85 7.58 o 1 1 1 10933.62 11203.68 192.31 o 2 1 1 1238.95 1256.95 19.99 o 3 1 1 1106.00 1317.22 14.91 o 4 1 1 622.46 700.43 8.24 o 5 1 1 92.93 76.92 1.40 o 6 1 1 178.14 164.59 2.72 o 7 1 1 52.09 56.73 1.74 o 8 1 1 74.69 78.19 2.36 o 9 1 1 92.59 87.76 2.66 o 10 1 1 0.15 0.54 0.49 o 11 1 1 149.14 146.81 3.96 o -12 2 1 35.03 36.67 2.60 o -11 2 1 12.71 13.76 1.29 o -10 2 1 181.82 173.09 4.04 o -9 2 1 32.67 36.37 1.32 o -8 2 1 34.15 32.50 1.20 o -7 2 1 1244.41 1194.97 14.02 o -6 2 1 488.29 468.13 5.93 o -5 2 1 1056.00 1102.02 12.70 o -4 2 1 0.91 0.84 0.23 o -3 2 1 1610.63 1822.37 21.76 o -2 2 1 3083.53 3202.92 35.25 o -1 2 1 1461.04 1638.92 19.00 o 0 2 1 12.95 7.45 0.31 o 1 2 1 93.12 96.24 1.74 o 2 2 1 4322.70 4447.01 48.93 o 3 2 1 300.65 296.39 4.31 o 4 2 1 1586.61 1729.27 21.42 o 5 2 1 894.26 1015.75 13.10 o 6 2 1 54.73 32.78 1.37 o 7 2 1 607.89 576.87 8.20 o 8 2 1 484.49 449.56 7.79 o 9 2 1 346.87 338.63 6.49 o 10 2 1 26.56 28.81 1.66 o 11 2 1 51.83 49.87 2.19 o -12 3 1 103.83 107.53 5.85 o -11 3 1 123.82 130.21 4.82 o -10 3 1 1.61 2.51 0.56 o -9 3 1 287.03 280.14 4.80 o -8 3 1 102.20 90.15 2.98 o -7 3 1 11.02 13.73 0.71 o -6 3 1 2593.97 2754.89 30.86 o -5 3 1 106.81 93.50 1.65 o -4 3 1 1750.94 1943.74 21.79 o -3 3 1 1024.54 1110.98 12.64 o -2 3 1 150.32 168.98 2.27 o -1 3 1 0.37 3.53 0.27 o 0 3 1 1633.41 1652.74 18.48 o 1 3 1 1199.45 1248.46 25.87 o 2 3 1 992.16 1178.99 15.95 o 3 3 1 12.50 10.73 0.42 o 4 3 1 292.02 337.22 4.87 o 5 3 1 1828.27 1900.82 23.72 o 6 3 1 1763.35 1851.41 23.32 o 7 3 1 643.94 663.22 9.31 o 8 3 1 172.86 181.24 3.49 o 9 3 1 20.09 18.87 1.20 o 10 3 1 1.77 3.17 0.68 o 11 3 1 50.15 55.37 2.24 o -12 4 1 42.37 42.45 2.30 o -11 4 1 0.03 1.16 0.77 o -10 4 1 704.27 693.35 19.57 o -9 4 1 19.41 21.54 1.06 o -8 4 1 8.74 10.71 0.78 o -7 4 1 30.70 30.97 1.15 o -6 4 1 862.10 856.69 10.92 o -5 4 1 57.74 62.07 1.30 o -4 4 1 37.52 38.36 0.95 o -3 4 1 818.82 900.60 10.44 o -2 4 1 3110.84 3255.92 35.94 o -1 4 1 6861.80 7194.84 85.94 o 0 4 1 213.58 237.26 3.04 o 1 4 1 120.90 121.19 2.10 o 2 4 1 396.23 362.48 4.53 o 3 4 1 4040.47 4392.16 52.28 o 4 4 1 407.13 333.79 4.37 o 5 4 1 1217.27 1271.80 22.63 o 6 4 1 24.57 22.80 0.99 o 7 4 1 15.33 14.27 0.87 o 8 4 1 385.61 363.07 5.90 o 9 4 1 31.48 33.42 1.59 o 10 4 1 146.11 143.52 3.79 o 11 4 1 92.68 100.19 5.05 o -11 5 1 13.34 16.00 1.69 o -10 5 1 9.98 10.51 0.87 o -9 5 1 56.93 54.25 2.08 o -8 5 1 1693.23 1682.07 21.65 o -7 5 1 28.64 23.83 1.03 o -6 5 1 6.14 3.12 0.43 o -5 5 1 103.10 96.11 1.79 o -4 5 1 698.28 711.85 8.59 o -3 5 1 10.86 10.94 0.53 o -2 5 1 1009.51 1099.41 12.62 o -1 5 1 482.83 465.71 6.03 o 0 5 1 1264.53 1175.05 13.40 o 1 5 1 413.54 452.95 5.55 o 2 5 1 292.30 347.40 5.76 o 3 5 1 866.12 880.52 10.36 o 4 5 1 207.72 213.20 3.63 o 5 5 1 114.28 116.99 2.39 o 6 5 1 1142.27 1150.95 15.12 o 7 5 1 0.01 0.41 0.39 o 8 5 1 20.35 22.18 1.16 o 9 5 1 1.19 1.24 0.64 o 10 5 1 76.26 78.10 6.01 o 11 5 1 13.50 13.50 1.06 o -11 6 1 18.26 20.46 2.27 o -10 6 1 295.71 299.51 7.18 o -9 6 1 27.58 25.46 1.35 o -8 6 1 27.28 22.05 1.09 o -7 6 1 9.08 9.85 0.73 o -6 6 1 111.76 88.38 1.89 o -5 6 1 411.61 399.33 5.33 o -4 6 1 130.27 118.51 3.88 o -3 6 1 229.72 229.76 3.29 o -2 6 1 2096.71 2136.26 24.00 o -1 6 1 5.40 5.52 0.38 o 0 6 1 157.06 142.62 2.72 o 1 6 1 1046.15 1094.42 12.66 o 2 6 1 670.68 684.69 8.25 o 3 6 1 272.48 262.07 3.90 o 4 6 1 746.11 763.27 9.28 o 5 6 1 484.38 422.27 6.30 o 6 6 1 3.12 3.27 0.55 o 7 6 1 59.36 50.80 1.63 o 8 6 1 24.44 27.66 1.24 o 9 6 1 42.78 43.97 1.78 o 10 6 1 9.58 8.82 1.63 o -10 7 1 79.89 82.15 3.18 o -9 7 1 234.95 230.16 5.02 o -8 7 1 29.93 31.68 1.50 o -7 7 1 308.91 312.23 5.19 o -6 7 1 78.54 69.21 2.87 o -5 7 1 241.25 244.03 3.68 o -4 7 1 896.68 887.91 10.71 o -3 7 1 82.60 81.42 1.62 o -2 7 1 2819.99 2803.23 31.37 o -1 7 1 284.40 269.41 5.18 o 0 7 1 234.65 248.28 3.75 o 1 7 1 304.45 297.71 4.04 o 2 7 1 372.63 365.85 7.37 o 3 7 1 42.55 34.01 0.95 o 4 7 1 221.93 218.40 3.96 o 5 7 1 159.66 145.27 3.22 o 6 7 1 1166.63 1180.31 17.69 o 7 7 1 42.56 33.14 1.59 o 8 7 1 35.56 36.75 2.45 o 9 7 1 112.77 108.73 3.19 o 10 7 1 51.97 52.65 4.00 o -10 8 1 7.26 11.06 1.16 o -9 8 1 80.23 81.94 3.22 o -8 8 1 46.74 49.22 2.38 o -7 8 1 186.74 189.25 4.22 o -6 8 1 132.79 137.24 3.20 o -5 8 1 7.56 5.12 0.54 o -4 8 1 1153.53 1182.24 15.40 o -3 8 1 249.35 211.15 3.26 o -2 8 1 174.54 161.42 2.68 o -1 8 1 1077.83 1025.84 12.39 o 0 8 1 312.28 293.68 5.86 o 1 8 1 380.58 373.16 5.63 o 2 8 1 3.45 4.47 0.53 o 3 8 1 515.53 492.31 7.18 o 4 8 1 337.77 330.92 6.05 o 5 8 1 94.18 78.48 2.39 o 6 8 1 47.55 50.90 1.96 o 7 8 1 576.56 589.42 10.06 o 8 8 1 423.68 421.54 7.92 o 9 8 1 58.60 65.32 2.91 o -9 9 1 274.58 282.95 7.82 o -8 9 1 0.01 1.15 0.69 o -7 9 1 34.71 35.61 1.99 o -6 9 1 7.00 5.79 0.77 o -5 9 1 48.45 47.21 1.76 o -4 9 1 1.14 0.25 0.38 o -3 9 1 58.65 41.94 1.75 o -2 9 1 4.24 7.48 0.82 o -1 9 1 1840.88 1730.04 22.02 o 0 9 1 599.51 584.94 8.32 o 1 9 1 1676.01 1627.77 20.82 o 2 9 1 1095.03 1094.19 14.52 o 3 9 1 89.96 74.16 1.95 o 4 9 1 16.10 14.58 1.03 o 5 9 1 107.70 116.21 3.12 o 6 9 1 94.33 93.90 2.84 o 7 9 1 15.27 18.03 1.24 o 8 9 1 2.68 4.86 1.05 o 9 9 1 3.34 4.33 0.98 o -8 10 1 8.57 12.95 1.95 o -7 10 1 287.43 272.56 8.63 o -6 10 1 1.78 0.67 0.89 o -5 10 1 519.85 534.81 13.00 o -4 10 1 83.25 81.16 2.46 o -3 10 1 140.69 127.17 3.25 o -2 10 1 246.24 232.90 4.82 o -1 10 1 272.09 282.18 5.51 o 0 10 1 173.70 177.06 3.99 o 1 10 1 267.53 238.93 4.90 o 2 10 1 10.62 9.55 0.85 o 3 10 1 372.27 352.62 6.53 o 4 10 1 45.44 47.85 1.86 o 5 10 1 35.75 36.64 1.68 o 6 10 1 17.95 20.84 1.36 o 7 10 1 411.51 412.77 7.92 o 8 10 1 10.68 10.62 1.24 o -7 11 1 62.02 64.85 5.20 o -6 11 1 31.71 30.26 2.58 o -5 11 1 0.04 0.94 0.53 o -4 11 1 14.97 16.54 1.28 o -3 11 1 190.59 199.41 4.53 o -2 11 1 7.66 8.30 0.92 o -1 11 1 7.47 8.75 0.91 o 0 11 1 292.13 281.19 5.67 o 1 11 1 139.26 136.75 3.68 o 2 11 1 15.36 13.66 1.10 o 3 11 1 13.23 16.50 1.32 o 4 11 1 155.67 166.70 4.86 o 5 11 1 131.61 123.94 5.14 o 6 11 1 238.58 245.83 6.51 o 7 11 1 21.09 20.48 2.16 o -6 12 1 1.58 2.14 1.00 o -5 12 1 1.85 2.78 1.36 o -4 12 1 1.39 1.27 0.60 o -3 12 1 37.40 39.85 1.81 o -2 12 1 26.70 29.54 1.55 o -1 12 1 369.52 382.08 7.32 o 0 12 1 3.50 6.53 0.93 o 1 12 1 7.91 10.00 1.00 o 2 12 1 63.74 65.55 2.36 o 3 12 1 65.96 65.79 2.88 o 4 12 1 54.62 55.57 2.65 o 5 12 1 22.40 23.67 1.75 o 6 12 1 103.39 122.38 5.57 o -5 13 1 1.87 3.47 1.09 o -4 13 1 85.22 86.73 4.49 o -3 13 1 91.27 93.76 3.82 o -2 13 1 237.63 249.77 5.60 o -1 13 1 18.44 21.68 1.39 o 0 13 1 68.73 69.43 2.55 o 1 13 1 75.90 70.77 2.76 o 2 13 1 8.01 9.87 1.20 o 3 13 1 10.16 9.13 1.14 o 4 13 1 110.88 119.44 4.92 o -2 14 1 295.46 312.71 6.74 o -1 14 1 3.07 4.74 0.78 o 0 14 1 25.74 30.88 1.71 o 1 14 1 96.57 111.86 3.44 o -12 0 2 26.69 28.36 3.35 o -10 0 2 18.34 21.24 2.08 o -8 0 2 813.45 815.17 14.11 o -6 0 2 5.77 6.01 1.15 o -4 0 2 1402.45 1796.47 28.35 o -2 0 2 538.37 560.88 9.08 o 0 0 2 13735.94 13672.45 213.16 o 2 0 2 9660.72 10365.43 162.13 o 4 0 2 5234.18 6266.42 97.32 o 6 0 2 979.57 937.78 15.76 o 8 0 2 56.30 60.29 2.97 o 10 0 2 76.25 73.81 3.68 o -12 1 2 150.95 161.26 6.27 o -11 1 2 110.65 108.35 3.65 o -10 1 2 609.15 614.14 10.16 o -9 1 2 589.76 595.11 8.55 o -8 1 2 45.93 40.25 1.14 o -7 1 2 10.41 9.40 0.55 o -6 1 2 333.34 296.20 3.99 o -5 1 2 1422.54 1570.42 19.31 o -4 1 2 1088.23 1125.08 17.44 o -3 1 2 8353.05 8729.38 129.59 o -2 1 2 158.82 218.86 3.58 o -1 1 2 140.13 127.42 2.16 o 0 1 2 57.53 55.69 0.86 o 1 1 2 132.24 138.37 2.39 o 2 1 2 875.59 1070.12 13.32 o 3 1 2 526.67 514.16 6.83 o 4 1 2 1460.51 1577.50 19.66 o 5 1 2 304.80 337.85 5.01 o 6 1 2 110.23 120.04 2.82 o 7 1 2 252.17 240.22 4.76 o 8 1 2 638.09 611.83 10.14 o 9 1 2 21.36 19.08 1.23 o 10 1 2 524.14 519.89 9.37 o 11 1 2 85.18 86.89 2.97 o -12 2 2 2.65 4.53 1.20 o -11 2 2 149.45 143.95 4.39 o -10 2 2 18.90 20.00 1.46 o -9 2 2 8.72 7.44 0.68 o -8 2 2 1886.36 1959.70 22.45 o -7 2 2 203.21 205.70 3.12 o -6 2 2 1199.83 1272.72 14.67 o -5 2 2 243.55 264.02 3.53 o -4 2 2 173.35 218.20 3.53 o -3 2 2 841.46 896.70 10.21 o -2 2 2 9321.35 9703.05 107.32 o -1 2 2 902.70 967.30 12.23 o 0 2 2 414.46 460.53 5.54 o 1 2 2 35.91 49.34 0.86 o 2 2 2 30.73 24.91 0.71 o 3 2 2 744.31 763.96 9.86 o 4 2 2 0.95 6.02 0.48 o 5 2 2 9.07 13.50 0.70 o 6 2 2 2019.21 2061.81 26.05 o 7 2 2 7.48 10.54 0.88 o 8 2 2 62.23 65.03 2.20 o 9 2 2 51.44 42.80 1.82 o 10 2 2 84.71 83.82 3.41 o 11 2 2 42.47 43.93 2.10 o -12 3 2 46.46 47.74 2.43 o -11 3 2 85.42 85.90 4.15 o -10 3 2 20.68 20.22 1.16 o -9 3 2 338.56 295.15 4.93 o -8 3 2 23.68 26.36 1.06 o -7 3 2 146.91 158.94 2.60 o -6 3 2 380.20 393.43 5.40 o -5 3 2 58.82 49.10 1.08 o -4 3 2 2381.75 2714.18 30.16 o -3 3 2 2514.31 2703.95 29.97 o -2 3 2 49.76 35.56 1.00 o -1 3 2 1116.87 1199.57 14.02 o 0 3 2 760.24 786.82 10.04 o 1 3 2 260.29 278.26 3.49 o 2 3 2 176.76 183.02 3.05 o 3 3 2 0.47 5.03 0.42 o 4 3 2 1041.38 1146.84 14.66 o 5 3 2 464.75 476.16 12.12 o 6 3 2 53.77 56.29 1.59 o 7 3 2 1047.99 987.85 13.27 o 8 3 2 5.21 7.31 0.88 o 9 3 2 443.79 448.98 8.26 o 10 3 2 28.98 29.96 1.60 o 11 3 2 16.35 23.01 1.79 o -12 4 2 4.52 5.17 0.96 o -11 4 2 49.91 49.43 2.39 o -10 4 2 6.70 13.09 1.00 o -9 4 2 667.47 647.79 10.72 o -8 4 2 357.27 346.06 6.11 o -7 4 2 522.94 531.15 9.99 o -6 4 2 354.61 337.37 4.58 o -5 4 2 56.52 62.41 1.30 o -4 4 2 86.87 100.44 1.70 o -3 4 2 1404.82 1508.12 17.04 o -2 4 2 11.72 7.93 0.38 o -1 4 2 2492.73 2704.12 30.02 o 0 4 2 335.07 373.34 5.10 o 1 4 2 777.30 923.97 12.98 o 2 4 2 60.99 65.24 1.51 o 3 4 2 42.38 32.55 0.79 o 4 4 2 1.61 3.39 0.46 o 5 4 2 1143.60 1127.05 16.47 o 6 4 2 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