#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/35/2203570.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203570_Fobs loop_ _publ_author_name 'Zhang, Zhu-Yan' 'Gao, Shan' 'Huo, Li-Hua' 'Zhao, Hui' 'Zhao, Jing-Gui' 'Ng, Seik Weng' _publ_section_title ; Hexaaquacobalt(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m676 _journal_page_last m678 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.425 _cell_angle_gamma 90.000 _cell_length_a 12.3872 _cell_length_b 12.8165 _cell_length_c 6.7661 _exptl_crystal_F_000 530.00 _reflns_d_resolution_high 0.7667 _[local]_cod_data_source_file ci6368Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' z in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 124.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2312.68 2228.31 24.62 o 3 0 0 1917.95 1962.55 12.34 o 4 0 0 12308.57 10670.89 43.86 o 5 0 0 11820.30 10899.04 82.12 o 6 0 0 25.41 49.15 0.49 o 7 0 0 4848.32 5183.90 5.58 o 8 0 0 1460.84 1462.94 2.91 o 9 0 0 826.96 822.05 6.45 o 10 0 0 636.83 654.50 2.65 o 11 0 0 1986.54 1811.18 20.84 o 12 0 0 56.00 70.02 1.08 o 13 0 0 185.02 180.28 3.18 o 14 0 0 11.35 9.87 1.09 o 15 0 0 37.38 28.06 1.38 o 2 1 0 349.45 364.36 1.70 o 3 1 0 5.89 8.14 0.73 o 4 1 0 18.22 12.74 0.51 o 5 1 0 58.65 65.23 0.33 o 6 1 0 173.12 155.81 1.49 o 7 1 0 1631.33 1820.08 8.93 o 8 1 0 126.76 142.86 0.77 o 9 1 0 26.80 20.43 0.36 o 10 1 0 64.77 59.12 1.19 o 11 1 0 164.83 160.03 1.29 o 12 1 0 83.85 75.50 1.26 o 13 1 0 27.94 25.00 0.51 o 14 1 0 44.82 43.87 0.71 o 15 1 0 50.91 38.03 1.55 o 0 2 0 967.69 845.21 21.85 o 1 2 0 1628.13 1598.67 16.87 o 2 2 0 6405.92 4755.96 70.06 o 3 2 0 2486.54 2428.71 44.76 o 4 2 0 508.50 500.25 1.93 o 5 2 0 2917.47 2993.71 44.40 o 6 2 0 4810.07 4925.69 44.47 o 7 2 0 2448.21 2514.45 35.04 o 8 2 0 157.23 151.49 2.20 o 9 2 0 7.77 6.92 0.38 o 10 2 0 72.19 75.44 0.68 o 11 2 0 272.21 274.43 3.30 o 12 2 0 333.57 330.42 4.53 o 13 2 0 342.22 315.30 4.50 o 14 2 0 109.19 98.71 2.22 o 15 2 0 18.52 15.59 0.54 o 1 3 0 751.21 803.81 5.85 o 2 3 0 568.39 520.12 2.80 o 3 3 0 11.98 12.23 0.57 o 4 3 0 1232.43 1290.51 9.33 o 5 3 0 993.54 1091.99 5.63 o 6 3 0 4.57 9.57 1.03 o 7 3 0 61.24 69.64 0.86 o 8 3 0 12.11 10.84 0.38 o 9 3 0 15.80 15.10 0.48 o 10 3 0 61.74 65.22 1.25 o 11 3 0 336.16 328.71 4.18 o 12 3 0 52.65 47.20 1.20 o 13 3 0 9.41 6.55 0.62 o 14 3 0 1.32 1.70 0.57 o 15 3 0 13.74 10.97 1.08 o 0 4 0 7881.49 7391.71 75.25 o 1 4 0 14652.94 12501.15 139.21 o 2 4 0 367.15 334.70 2.51 o 3 4 0 169.75 189.86 0.52 o 4 4 0 148.96 127.85 0.83 o 5 4 0 93.58 74.96 1.09 o 6 4 0 3354.22 3505.85 30.05 o 7 4 0 9.35 15.68 0.84 o 8 4 0 392.44 410.62 5.76 o 9 4 0 281.58 288.26 3.40 o 10 4 0 270.02 266.32 5.27 o 11 4 0 60.46 65.35 1.48 o 12 4 0 919.83 865.05 14.15 o 13 4 0 36.69 36.28 0.95 o 14 4 0 60.41 48.52 2.43 o 15 4 0 48.29 41.04 3.65 o 1 5 0 2036.88 2122.58 13.78 o 2 5 0 103.07 106.32 0.88 o 3 5 0 966.77 922.86 5.43 o 4 5 0 331.93 325.85 1.46 o 5 5 0 67.19 62.91 0.65 o 6 5 0 16.93 22.33 0.76 o 7 5 0 12.62 13.95 1.12 o 8 5 0 13.54 12.07 0.41 o 9 5 0 6.43 7.20 0.68 o 10 5 0 40.86 39.81 1.33 o 11 5 0 14.93 13.82 1.16 o 12 5 0 6.18 5.11 0.56 o 13 5 0 0.16 0.66 0.45 o 14 5 0 7.41 7.02 0.67 o 15 5 0 2.95 2.63 0.93 o 0 6 0 1604.89 1651.15 24.90 o 1 6 0 3744.50 3754.43 39.74 o 2 6 0 506.47 456.70 2.30 o 3 6 0 57.47 37.69 0.48 o 4 6 0 809.83 783.16 3.26 o 5 6 0 1474.46 1430.59 11.88 o 6 6 0 1778.31 1738.34 5.64 o 7 6 0 293.14 291.41 1.50 o 8 6 0 366.70 394.82 1.68 o 9 6 0 686.25 731.97 5.20 o 10 6 0 594.12 601.51 11.29 o 11 6 0 245.31 249.40 2.62 o 12 6 0 388.77 402.98 5.81 o 13 6 0 230.73 245.72 7.82 o 14 6 0 120.61 115.11 5.40 o 1 7 0 42.51 41.94 0.51 o 2 7 0 232.64 239.47 2.16 o 3 7 0 50.84 53.04 0.98 o 4 7 0 58.06 47.57 1.00 o 5 7 0 121.17 125.07 1.33 o 6 7 0 338.09 332.62 2.21 o 7 7 0 21.34 21.47 0.58 o 8 7 0 20.52 22.27 0.58 o 9 7 0 63.42 56.18 1.02 o 10 7 0 50.14 47.70 1.95 o 11 7 0 2.87 3.64 0.60 o 12 7 0 0.20 1.44 0.82 o 13 7 0 8.63 7.24 1.26 o 14 7 0 4.99 4.17 0.76 o 0 8 0 3822.20 3873.71 70.41 o 1 8 0 232.61 274.82 2.48 o 2 8 0 1585.56 1533.36 13.71 o 3 8 0 1154.19 1132.33 9.35 o 4 8 0 361.46 331.70 1.56 o 5 8 0 1305.38 1239.60 9.45 o 6 8 0 519.96 466.09 2.67 o 7 8 0 1898.18 1899.73 15.38 o 8 8 0 234.17 234.72 1.28 o 9 8 0 18.30 22.26 0.71 o 10 8 0 146.05 148.25 2.41 o 11 8 0 481.04 487.56 10.25 o 12 8 0 81.26 81.78 2.52 o 13 8 0 372.39 384.40 3.00 o 1 9 0 342.98 322.14 2.35 o 2 9 0 0.02 1.20 0.51 o 3 9 0 38.62 34.75 0.59 o 4 9 0 96.23 91.90 0.86 o 5 9 0 300.17 276.98 1.52 o 6 9 0 42.89 41.95 0.85 o 7 9 0 160.88 152.90 0.99 o 8 9 0 98.95 95.50 1.56 o 9 9 0 23.12 21.71 0.62 o 10 9 0 3.69 5.56 0.59 o 11 9 0 105.97 109.88 3.39 o 12 9 0 33.99 34.83 1.54 o 13 9 0 4.40 3.31 0.92 o 0 10 0 2612.18 2522.41 38.27 o 1 10 0 185.89 174.27 1.74 o 2 10 0 7.61 8.57 0.54 o 3 10 0 124.21 119.82 1.03 o 4 10 0 142.26 127.92 1.16 o 5 10 0 117.98 110.58 1.08 o 6 10 0 2.26 4.99 0.90 o 7 10 0 290.43 314.74 2.67 o 8 10 0 265.81 262.27 1.47 o 9 10 0 64.85 62.69 2.05 o 10 10 0 163.17 164.40 3.78 o 11 10 0 424.05 419.22 12.07 o 12 10 0 85.95 90.86 4.23 o 1 11 0 721.99 704.02 3.97 o 2 11 0 268.08 266.40 3.72 o 3 11 0 4.64 4.91 0.60 o 4 11 0 33.26 31.93 0.65 o 5 11 0 65.68 56.96 0.83 o 6 11 0 85.33 76.80 1.00 o 7 11 0 4.54 4.55 0.73 o 8 11 0 0.03 0.38 0.71 o 9 11 0 51.58 47.61 1.98 o 10 11 0 0.02 0.34 0.77 o 11 11 0 0.01 0.00 0.70 o 0 12 0 84.74 87.21 1.44 o 1 12 0 848.64 852.46 4.90 o 2 12 0 404.12 405.15 5.27 o 3 12 0 223.24 224.92 2.83 o 4 12 0 337.15 353.33 2.27 o 5 12 0 261.74 265.28 1.54 o 6 12 0 702.30 708.56 6.08 o 7 12 0 63.21 58.73 0.89 o 8 12 0 53.81 61.70 1.20 o 9 12 0 193.63 198.43 6.26 o 10 12 0 30.54 28.20 1.23 o 11 12 0 9.93 7.91 0.85 o 1 13 0 10.94 10.79 0.71 o 2 13 0 6.38 8.21 0.70 o 3 13 0 43.97 41.19 1.19 o 4 13 0 4.49 5.38 0.73 o 5 13 0 20.17 19.50 0.93 o 6 13 0 5.98 6.95 0.75 o 7 13 0 70.96 65.64 1.43 o 8 13 0 68.41 66.42 1.59 o 9 13 0 46.98 44.18 1.70 o 0 14 0 294.30 299.31 6.96 o 1 14 0 665.77 672.93 8.45 o 2 14 0 307.54 319.40 2.27 o 3 14 0 204.33 215.96 2.42 o 4 14 0 492.21 494.65 3.53 o 5 14 0 232.46 241.54 2.00 o 6 14 0 256.38 264.09 2.46 o 7 14 0 106.11 101.94 1.86 o 8 14 0 115.42 118.05 4.00 o 1 15 0 58.68 58.37 1.23 o 2 15 0 6.31 6.50 0.88 o 3 15 0 42.30 42.22 1.60 o 4 15 0 29.67 32.13 1.25 o 5 15 0 5.33 6.33 0.84 o 6 15 0 3.01 3.69 1.07 o 0 16 0 149.28 142.85 1.80 o 1 16 0 37.06 40.03 1.50 o 2 16 0 255.19 274.00 2.79 o 3 16 0 174.39 182.10 2.35 o 4 16 0 8.85 9.03 0.99 o -16 1 1 45.12 43.43 1.84 o -15 1 1 81.66 80.58 2.05 o -14 1 1 165.14 161.66 4.39 o -13 1 1 226.12 220.60 6.20 o -12 1 1 635.43 625.68 4.41 o -11 1 1 241.18 251.13 3.53 o -10 1 1 18.59 20.19 1.15 o -9 1 1 126.84 117.25 0.73 o -8 1 1 974.63 973.99 8.06 o -7 1 1 1812.63 1902.40 19.19 o -6 1 1 2042.36 2049.91 17.90 o -5 1 1 940.82 904.57 8.18 o -4 1 1 1407.66 1478.41 32.30 o -3 1 1 323.01 314.60 4.17 o -2 1 1 1895.49 2040.81 14.03 o -1 1 1 7677.78 7626.99 94.45 o 0 1 1 382.89 368.37 2.28 o 1 1 1 7571.63 6712.05 70.34 o 2 1 1 3724.63 3690.81 45.26 o 3 1 1 1071.20 1158.84 16.59 o 4 1 1 2073.41 2035.68 7.55 o 5 1 1 4903.81 4953.89 25.51 o 6 1 1 7031.78 7062.58 81.87 o 7 1 1 1276.22 1203.74 11.97 o 8 1 1 53.06 53.16 0.39 o 9 1 1 1022.00 1017.65 7.65 o 10 1 1 417.99 436.83 3.87 o 11 1 1 474.77 468.47 2.18 o 12 1 1 703.08 640.83 6.01 o 13 1 1 250.05 228.01 2.27 o 14 1 1 95.80 90.23 2.12 o 15 1 1 15.41 10.40 0.54 o -15 2 1 3.74 2.05 0.74 o -14 2 1 0.28 1.39 0.83 o -13 2 1 7.86 6.11 0.64 o -12 2 1 314.65 285.59 1.90 o -11 2 1 267.04 233.03 3.12 o -10 2 1 3.86 2.84 0.32 o -9 2 1 8.91 12.66 0.53 o -8 2 1 17.20 19.07 0.55 o -7 2 1 2031.64 2224.59 11.13 o -6 2 1 553.95 700.28 2.39 o -5 2 1 3.05 1.36 0.25 o -4 2 1 309.61 318.97 2.25 o -3 2 1 4.76 10.58 0.64 o -2 2 1 183.24 175.17 1.23 o -1 2 1 3582.81 3709.18 25.33 o 0 2 1 5339.22 5195.26 61.01 o 1 2 1 2884.89 3027.46 19.46 o 2 2 1 349.49 378.07 4.52 o 3 2 1 3900.18 3924.71 30.91 o 4 2 1 8.60 7.25 0.28 o 5 2 1 29.73 33.97 0.40 o 6 2 1 0.61 0.38 0.20 o 7 2 1 167.59 162.35 1.71 o 8 2 1 44.80 40.98 0.33 o 9 2 1 178.14 164.68 2.23 o 10 2 1 362.12 369.44 4.10 o 11 2 1 256.32 231.33 3.60 o 12 2 1 9.40 9.21 0.45 o 13 2 1 48.44 38.47 1.57 o 14 2 1 5.66 3.60 0.59 o 15 2 1 13.69 15.53 0.78 o -15 3 1 17.65 14.51 1.18 o -14 3 1 66.73 70.65 2.15 o -13 3 1 148.02 138.93 3.50 o -12 3 1 27.73 23.68 1.22 o -11 3 1 469.64 459.69 2.94 o -10 3 1 790.80 774.83 11.58 o -9 3 1 173.65 176.26 2.30 o -8 3 1 148.48 139.51 1.92 o -7 3 1 459.88 489.04 4.02 o -6 3 1 1466.46 1450.08 16.96 o -5 3 1 670.23 574.54 3.80 o -4 3 1 1221.76 1404.19 4.96 o -3 3 1 410.61 417.29 2.21 o -2 3 1 3094.25 3394.96 36.54 o -1 3 1 2512.55 2533.64 25.61 o 0 3 1 15596.45 13236.00 180.42 o 1 3 1 81.35 83.90 0.59 o 2 3 1 13.09 13.99 0.32 o 3 3 1 6.60 4.17 0.17 o 4 3 1 1515.31 1486.70 22.03 o 5 3 1 2576.12 2609.51 25.54 o 6 3 1 238.96 217.33 0.67 o 7 3 1 546.81 564.95 4.41 o 8 3 1 1053.27 1053.59 5.31 o 9 3 1 736.81 737.95 5.74 o 10 3 1 883.62 842.55 9.53 o 11 3 1 679.69 647.63 6.11 o 12 3 1 223.61 220.40 5.60 o 13 3 1 229.60 213.21 3.98 o 14 3 1 73.73 56.81 2.88 o 15 3 1 55.81 48.27 1.87 o -15 4 1 35.57 31.56 2.12 o -14 4 1 29.72 25.97 1.16 o -13 4 1 22.34 17.89 0.64 o -12 4 1 27.18 24.53 1.19 o -11 4 1 117.83 110.99 2.61 o -10 4 1 8.25 7.79 0.73 o -9 4 1 182.87 175.59 4.78 o -8 4 1 16.64 15.62 0.65 o -7 4 1 12.68 11.45 0.58 o -6 4 1 931.96 964.62 8.43 o -5 4 1 672.62 707.06 6.61 o -4 4 1 35.40 43.56 0.53 o -3 4 1 162.61 191.37 3.05 o -2 4 1 212.26 208.82 1.84 o -1 4 1 3111.23 3315.68 23.12 o 0 4 1 76.28 80.36 0.96 o 1 4 1 3040.88 3077.34 14.59 o 2 4 1 6391.67 6180.28 63.24 o 3 4 1 2937.12 3106.87 38.31 o 4 4 1 20.46 16.18 0.48 o 5 4 1 187.87 200.98 0.66 o 6 4 1 670.48 680.83 3.53 o 7 4 1 119.96 127.45 1.35 o 8 4 1 46.49 40.82 0.77 o 9 4 1 202.46 200.37 2.63 o 10 4 1 120.53 116.77 0.83 o 11 4 1 37.21 41.67 0.59 o 12 4 1 16.89 14.94 0.92 o 13 4 1 1.78 2.54 0.44 o 14 4 1 1.55 1.53 0.45 o 15 4 1 0.00 1.27 0.75 o -15 5 1 35.22 32.06 1.57 o -14 5 1 53.84 50.49 1.13 o -13 5 1 510.61 537.77 8.41 o -12 5 1 539.16 565.36 6.67 o -11 5 1 83.00 77.34 0.96 o -10 5 1 4.01 3.63 0.49 o -9 5 1 102.06 110.81 0.91 o -8 5 1 1964.91 1960.34 20.26 o -7 5 1 1835.23 1813.48 11.21 o -6 5 1 1016.04 961.65 2.47 o -5 5 1 1949.05 1902.27 16.76 o -4 5 1 2745.10 2814.62 12.87 o -3 5 1 3199.32 3249.02 25.12 o -2 5 1 87.94 67.24 0.53 o -1 5 1 266.69 211.74 2.04 o 0 5 1 4250.52 4239.69 42.60 o 1 5 1 244.73 185.34 0.64 o 2 5 1 82.47 66.40 0.68 o 3 5 1 2399.76 2426.02 24.02 o 4 5 1 1990.78 1889.52 20.91 o 5 5 1 1027.95 962.78 4.32 o 6 5 1 611.18 565.99 3.49 o 7 5 1 1769.00 1745.33 6.72 o 8 5 1 622.57 634.80 3.28 o 9 5 1 693.90 663.75 5.42 o 10 5 1 89.44 93.34 1.59 o 11 5 1 749.23 764.88 4.24 o 12 5 1 319.74 303.49 2.68 o 13 5 1 52.81 42.74 3.05 o 14 5 1 31.84 24.36 1.61 o -15 6 1 2.63 2.51 0.88 o -14 6 1 14.12 11.83 1.64 o -13 6 1 0.51 1.48 0.87 o -12 6 1 29.56 21.31 2.44 o -11 6 1 708.77 685.47 5.74 o -10 6 1 8.50 8.75 0.94 o -9 6 1 640.52 627.88 11.64 o -8 6 1 202.30 206.44 1.81 o -7 6 1 642.61 674.87 7.24 o -6 6 1 187.68 214.10 1.20 o -5 6 1 48.27 53.35 0.65 o -4 6 1 506.58 511.87 3.22 o -3 6 1 1482.11 1514.20 7.53 o -2 6 1 286.40 265.33 2.01 o -1 6 1 366.33 421.11 3.21 o 0 6 1 4657.70 5001.19 41.14 o 1 6 1 23.67 20.44 0.32 o 2 6 1 173.02 179.51 0.91 o 3 6 1 305.03 289.22 2.87 o 4 6 1 99.01 92.86 0.77 o 5 6 1 266.44 277.37 3.14 o 6 6 1 11.41 8.74 0.38 o 7 6 1 401.98 407.63 1.72 o 8 6 1 1097.73 1088.26 11.04 o 9 6 1 9.36 11.80 0.85 o 10 6 1 8.30 7.51 0.55 o 11 6 1 77.65 75.56 2.04 o 12 6 1 0.18 0.53 0.46 o 13 6 1 54.78 53.21 2.65 o 14 6 1 4.84 2.84 0.85 o -14 7 1 172.98 184.17 9.61 o -13 7 1 113.16 116.06 4.10 o -12 7 1 471.56 483.28 14.96 o -11 7 1 659.16 685.92 5.29 o -10 7 1 1111.95 1148.53 5.74 o -9 7 1 549.86 564.11 3.93 o -8 7 1 1098.60 1144.67 7.59 o -7 7 1 922.86 935.26 3.83 o -6 7 1 2883.46 2916.04 27.60 o -5 7 1 1145.80 1107.88 8.23 o -4 7 1 753.93 704.33 4.89 o -3 7 1 1787.83 1706.58 2.32 o -2 7 1 1800.59 1799.33 22.53 o -1 7 1 7227.28 7261.75 69.11 o 0 7 1 937.25 872.29 3.84 o 1 7 1 4442.01 4494.00 32.38 o 2 7 1 694.10 671.57 2.53 o 3 7 1 64.63 53.61 0.63 o 4 7 1 88.80 77.75 0.61 o 5 7 1 758.50 752.29 7.50 o 6 7 1 1205.02 1229.56 8.54 o 7 7 1 3.00 4.23 0.42 o 8 7 1 31.16 31.08 0.74 o 9 7 1 440.78 462.31 6.69 o 10 7 1 528.62 571.80 7.61 o 11 7 1 31.44 31.87 0.90 o 12 7 1 48.35 39.53 2.16 o 13 7 1 49.81 45.35 4.50 o 14 7 1 32.00 29.23 3.74 o -14 8 1 1.44 2.56 1.14 o -13 8 1 14.06 13.32 1.41 o -12 8 1 23.73 22.20 1.01 o -11 8 1 0.02 0.38 0.55 o -10 8 1 20.56 18.61 0.68 o -9 8 1 38.18 34.69 1.28 o -8 8 1 0.46 1.50 0.58 o -7 8 1 31.32 30.11 1.04 o -6 8 1 118.51 105.22 0.74 o -5 8 1 184.79 182.51 2.01 o -4 8 1 15.58 12.57 0.53 o -3 8 1 659.96 675.28 3.87 o -2 8 1 777.69 753.93 2.26 o -1 8 1 1297.08 1269.02 7.19 o 0 8 1 433.64 413.20 2.19 o 1 8 1 71.54 68.87 0.62 o 2 8 1 2.47 1.24 0.38 o 3 8 1 209.80 205.46 0.99 o 4 8 1 509.55 524.22 4.18 o 5 8 1 55.45 59.41 0.62 o 6 8 1 59.43 61.67 1.04 o 7 8 1 0.01 0.05 0.42 o 8 8 1 254.16 253.40 3.66 o 9 8 1 17.12 15.34 0.71 o 10 8 1 46.85 46.58 2.88 o 11 8 1 29.23 25.48 1.21 o 12 8 1 27.95 22.62 1.43 o 13 8 1 0.64 -0.75 0.79 o -13 9 1 98.47 112.14 2.91 o -12 9 1 232.79 238.34 3.40 o -11 9 1 157.62 159.74 1.60 o -10 9 1 55.97 54.82 1.66 o -9 9 1 306.96 344.33 3.29 o -8 9 1 290.96 314.28 1.80 o -7 9 1 488.81 481.64 5.20 o -6 9 1 587.52 589.81 4.01 o -5 9 1 851.28 847.90 5.76 o -4 9 1 923.18 945.78 3.24 o -3 9 1 28.81 27.11 0.51 o -2 9 1 648.26 611.57 4.74 o -1 9 1 1724.61 1701.39 10.04 o 0 9 1 386.67 377.84 3.12 o 1 9 1 249.43 241.08 1.75 o 2 9 1 435.98 408.38 2.01 o 3 9 1 440.69 421.88 1.26 o 4 9 1 786.43 811.35 6.93 o 5 9 1 180.29 169.28 0.81 o 6 9 1 468.04 435.30 3.37 o 7 9 1 306.89 315.45 1.62 o 8 9 1 29.12 33.78 0.59 o 9 9 1 404.33 404.32 5.81 o 10 9 1 1.64 2.14 0.97 o 11 9 1 133.77 137.04 4.84 o 12 9 1 263.26 294.16 2.34 o 13 9 1 87.76 99.13 2.89 o -12 10 1 137.69 138.95 4.12 o -11 10 1 5.37 6.25 0.93 o -10 10 1 6.63 6.71 0.84 o -9 10 1 11.12 12.48 0.71 o -8 10 1 30.12 25.96 1.16 o -7 10 1 12.23 10.65 0.66 o -6 10 1 131.35 138.30 1.08 o -5 10 1 61.97 65.46 0.72 o -4 10 1 55.52 50.96 0.65 o -3 10 1 79.66 80.36 0.78 o -2 10 1 68.61 61.48 1.17 o -1 10 1 13.58 11.22 0.53 o 0 10 1 693.77 678.74 5.88 o 1 10 1 29.62 32.68 0.63 o 2 10 1 0.63 1.29 0.49 o 3 10 1 316.28 312.65 3.27 o 4 10 1 17.61 15.10 0.52 o 5 10 1 193.69 192.08 0.99 o 6 10 1 37.79 39.25 0.80 o 7 10 1 1.38 1.00 0.52 o 8 10 1 1.89 1.86 0.81 o 9 10 1 36.98 39.33 1.11 o 10 10 1 296.37 312.32 5.13 o 11 10 1 7.74 6.77 0.77 o 12 10 1 32.14 35.41 1.48 o -12 11 1 4.74 4.43 1.33 o -11 11 1 61.02 61.36 3.06 o -10 11 1 57.47 58.71 1.60 o -9 11 1 106.84 109.81 1.44 o -8 11 1 1.24 1.37 0.95 o -7 11 1 394.29 390.37 3.83 o -6 11 1 179.46 184.71 2.15 o -5 11 1 221.62 220.95 1.36 o -4 11 1 141.12 139.52 1.35 o -3 11 1 125.08 126.24 1.31 o -2 11 1 743.50 742.99 6.16 o -1 11 1 20.15 19.32 0.97 o 0 11 1 635.93 609.00 5.27 o 1 11 1 189.15 194.85 2.43 o 2 11 1 514.78 502.00 3.20 o 3 11 1 86.51 84.34 0.97 o 4 11 1 268.11 275.13 3.15 o 5 11 1 691.04 686.33 5.52 o 6 11 1 272.63 266.80 1.12 o 7 11 1 208.67 210.95 2.85 o 8 11 1 60.17 64.68 2.59 o 9 11 1 235.41 257.71 1.75 o 10 11 1 72.17 69.25 3.16 o 11 11 1 133.35 143.42 3.56 o -11 12 1 0.36 1.48 0.83 o -10 12 1 2.29 2.05 0.92 o -9 12 1 12.34 11.01 0.90 o -8 12 1 34.27 31.04 0.79 o -7 12 1 93.42 88.85 1.24 o -6 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1941.12 1966.99 26.52 o -6 2 2 2028.18 2051.10 25.97 o -5 2 2 491.79 459.54 2.38 o -4 2 2 650.05 642.91 1.48 o -3 2 2 1852.84 2140.23 25.96 o -2 2 2 268.51 258.95 2.29 o -1 2 2 58.18 40.40 1.15 o 0 2 2 187.10 146.22 0.72 o 1 2 2 2332.73 2554.69 16.56 o 2 2 2 360.17 355.92 1.15 o 3 2 2 64.58 61.54 0.65 o 4 2 2 1315.89 1288.93 18.57 o 5 2 2 4381.61 4553.46 97.90 o 6 2 2 1911.91 1935.01 13.24 o 7 2 2 112.29 107.18 1.03 o 8 2 2 44.66 44.82 0.82 o 9 2 2 115.21 121.96 1.42 o 10 2 2 438.85 463.14 6.45 o 11 2 2 378.73 374.94 5.57 o 12 2 2 477.89 464.18 7.14 o 13 2 2 244.11 238.57 4.94 o 14 2 2 77.89 70.74 3.82 o -15 3 2 5.81 4.30 1.32 o -14 3 2 11.38 11.29 0.77 o -13 3 2 19.14 15.04 1.16 o -12 3 2 19.09 17.34 1.41 o -11 3 2 2.92 5.44 0.62 o -10 3 2 1.39 0.67 0.58 o -9 3 2 1033.57 1045.82 4.36 o -8 3 2 181.14 206.28 0.97 o -7 3 2 261.58 263.32 2.19 o -6 3 2 53.76 64.54 1.06 o -5 3 2 144.31 145.83 0.76 o -4 3 2 1335.29 1469.30 3.47 o -3 3 2 205.94 219.98 2.33 o -2 3 2 932.22 971.73 8.53 o -1 3 2 161.96 167.86 1.07 o 0 3 2 199.56 194.24 1.77 o 1 3 2 94.60 80.74 0.88 o 2 3 2 1732.97 1902.05 22.96 o 3 3 2 543.89 546.28 2.07 o 4 3 2 136.91 163.34 1.43 o 5 3 2 0.16 1.64 0.46 o 6 3 2 175.78 178.89 1.29 o 7 3 2 68.10 74.78 0.86 o 8 3 2 1050.07 1007.11 10.33 o 9 3 2 693.77 696.55 7.04 o 10 3 2 156.32 146.71 2.46 o 11 3 2 2.09 2.09 0.33 o 12 3 2 0.78 0.53 0.43 o 13 3 2 16.10 16.28 0.98 o 14 3 2 0.34 1.00 1.11 o -15 4 2 52.17 52.00 3.48 o -14 4 2 64.03 62.58 1.29 o -13 4 2 155.68 151.79 2.29 o -12 4 2 106.07 111.63 3.12 o -11 4 2 298.63 312.83 8.46 o -10 4 2 291.05 308.59 4.23 o -9 4 2 6.88 8.18 0.64 o -8 4 2 1255.76 1260.65 5.17 o -7 4 2 999.36 1056.08 5.77 o -6 4 2 322.58 306.98 3.29 o -5 4 2 865.33 844.60 3.80 o -4 4 2 1043.70 1036.98 15.78 o -3 4 2 994.58 1053.14 13.15 o -2 4 2 727.32 704.52 4.67 o -1 4 2 6890.73 7171.85 70.72 o 0 4 2 6650.96 6845.44 65.94 o 1 4 2 1424.96 1386.18 16.88 o 2 4 2 58.20 40.57 0.65 o 3 4 2 2913.32 3005.65 11.88 o 4 4 2 1734.44 1695.29 7.16 o 5 4 2 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178.50 1.49 o -8 7 2 33.37 31.00 0.86 o -7 7 2 31.18 29.47 0.39 o -6 7 2 11.79 14.13 0.74 o -5 7 2 19.97 18.45 0.39 o -4 7 2 9.34 14.52 0.38 o -3 7 2 727.97 760.49 4.09 o -2 7 2 21.16 20.62 0.40 o -1 7 2 37.92 32.76 0.87 o 0 7 2 84.14 78.34 0.81 o 1 7 2 175.90 174.01 1.80 o 2 7 2 1292.71 1295.43 11.63 o 3 7 2 572.17 623.99 3.80 o 4 7 2 103.14 93.56 0.61 o 5 7 2 27.33 30.33 0.68 o 6 7 2 74.31 69.81 1.19 o 7 7 2 47.25 50.18 0.60 o 8 7 2 604.37 626.77 3.48 o 9 7 2 283.55 296.16 5.18 o 10 7 2 109.25 111.39 0.85 o 11 7 2 9.80 11.34 1.16 o 12 7 2 39.96 36.78 1.24 o 13 7 2 3.11 2.21 0.78 o -14 8 2 124.40 126.79 5.59 o -13 8 2 135.84 133.46 6.44 o -12 8 2 137.36 139.87 3.46 o -11 8 2 11.00 11.32 0.81 o -10 8 2 13.64 14.29 0.80 o -9 8 2 573.59 601.69 4.11 o -8 8 2 179.98 187.42 2.51 o -7 8 2 698.40 697.81 6.65 o -6 8 2 1120.53 1081.69 10.71 o -5 8 2 774.02 758.66 4.04 o -4 8 2 792.90 821.57 8.36 o -3 8 2 706.17 705.25 3.14 o -2 8 2 1248.82 1259.69 4.72 o -1 8 2 227.53 217.48 1.16 o 0 8 2 613.42 576.12 3.38 o 1 8 2 1338.80 1324.30 8.49 o 2 8 2 1377.12 1388.25 7.00 o 3 8 2 153.33 161.13 1.06 o 4 8 2 1261.62 1238.83 7.01 o 5 8 2 1522.26 1498.67 9.63 o 6 8 2 651.88 652.58 5.18 o 7 8 2 202.03 211.61 1.89 o 8 8 2 38.35 43.52 1.27 o 9 8 2 98.58 106.45 2.18 o 10 8 2 40.17 39.28 1.52 o 11 8 2 155.91 156.55 3.53 o 12 8 2 154.46 157.78 7.66 o -13 9 2 58.07 64.70 3.83 o -12 9 2 0.66 1.32 1.47 o -11 9 2 26.63 23.24 0.92 o -10 9 2 2.84 3.41 0.41 o -9 9 2 32.30 27.37 0.77 o -8 9 2 286.52 285.43 3.14 o -7 9 2 0.21 0.13 0.41 o -6 9 2 23.39 21.34 0.56 o -5 9 2 39.44 38.30 0.66 o -4 9 2 61.93 58.78 0.65 o -3 9 2 1.42 1.97 0.47 o -2 9 2 56.33 54.82 1.39 o -1 9 2 89.69 88.32 0.85 o 0 9 2 141.00 121.62 1.18 o 1 9 2 153.43 145.77 0.78 o 2 9 2 145.97 148.11 0.88 o 3 9 2 128.60 121.86 1.39 o 4 9 2 511.63 507.25 3.18 o 5 9 2 45.57 42.45 0.51 o 6 9 2 23.66 21.58 1.01 o 7 9 2 0.64 0.99 0.59 o 8 9 2 4.72 4.84 0.45 o 9 9 2 216.57 225.33 4.54 o 10 9 2 10.18 9.90 1.03 o 11 9 2 105.59 107.54 2.12 o 12 9 2 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5.41 0.59 o 0 11 2 1080.70 1075.95 7.14 o 1 11 2 286.35 294.54 3.57 o 2 11 2 250.12 247.87 1.80 o 3 11 2 26.74 27.63 1.04 o 4 11 2 0.09 0.47 0.61 o 5 11 2 6.98 6.80 0.50 o 6 11 2 114.56 103.86 1.38 o 7 11 2 50.02 45.96 1.98 o 8 11 2 114.74 114.27 3.22 o 9 11 2 344.58 371.50 3.33 o 10 11 2 1.28 1.34 1.23 o -11 12 2 91.98 91.31 2.54 o -10 12 2 110.50 114.74 3.20 o -9 12 2 0.95 2.30 0.86 o -8 12 2 245.81 253.64 4.09 o -7 12 2 312.94 314.45 3.40 o -6 12 2 309.22 313.97 3.05 o -5 12 2 101.90 106.88 2.09 o -4 12 2 115.47 121.58 0.90 o -3 12 2 544.08 556.12 6.08 o -2 12 2 125.70 124.24 1.04 o -1 12 2 83.26 82.00 0.80 o 0 12 2 33.09 35.09 0.83 o 1 12 2 294.58 293.64 3.16 o 2 12 2 297.25 298.58 2.85 o 3 12 2 367.78 378.49 3.70 o 4 12 2 88.75 92.16 1.78 o 5 12 2 271.38 260.25 2.34 o 6 12 2 307.93 300.73 3.63 o 7 12 2 112.92 117.55 2.76 o 8 12 2 86.30 98.64 1.45 o 9 12 2 23.43 25.28 1.35 o -9 13 2 23.09 21.06 1.90 o -8 13 2 20.63 23.98 0.94 o -7 13 2 2.37 3.93 0.66 o -6 13 2 103.14 101.63 2.15 o 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