#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203582.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203582_Fobs loop_ _publ_author_name 'Zeller, Matthias' 'Hunter, Allen D.' 'Perrine, Cynthia L.' 'Payton, John' _publ_section_title ; Tricarbonyl(\h^6^-trifluoromethylbenzene)chromium(0) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m668 _journal_page_last m669 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.908 _cell_angle_gamma 90.000 _cell_length_a 6.4008 _cell_length_b 11.5000 _cell_length_c 13.9317 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file cv6300Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PhCF3 (i.e., (C6H5CF3)Cr(CO)3)in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2510.98 2434.80 74.89 o 4 0 0 5039.00 5114.66 174.62 o 6 0 0 117.45 127.70 7.25 o 8 0 0 363.58 397.41 55.60 o 1 1 0 76.42 80.21 1.95 o 2 1 0 7076.25 7714.29 166.99 o 3 1 0 2168.88 2106.88 45.99 o 4 1 0 7981.21 8089.78 174.87 o 5 1 0 26.31 28.48 3.82 o 6 1 0 118.64 125.68 7.17 o 7 1 0 193.49 196.19 15.41 o 8 1 0 655.01 625.76 40.70 o 0 2 0 19975.07 20220.71 666.46 o 1 2 0 6415.14 7090.95 167.91 o 2 2 0 303.50 315.31 7.20 o 3 2 0 1013.44 1090.56 24.09 o 4 2 0 1427.52 1415.45 31.23 o 5 2 0 811.26 733.22 18.40 o 6 2 0 173.17 166.66 6.19 o 7 2 0 467.69 467.74 16.53 o 8 2 0 45.77 48.87 12.27 o 1 3 0 2029.80 2210.22 48.07 o 2 3 0 774.78 731.31 19.95 o 3 3 0 4079.17 4050.65 81.40 o 4 3 0 597.62 651.78 21.91 o 5 3 0 585.82 563.02 14.47 o 6 3 0 18.05 10.49 2.05 o 7 3 0 280.65 292.14 10.15 o 8 3 0 211.60 237.89 13.85 o 0 4 0 5774.25 6175.67 188.89 o 1 4 0 6399.48 6508.48 154.48 o 2 4 0 27.00 27.44 1.72 o 3 4 0 101.72 109.09 3.13 o 4 4 0 55.51 59.33 2.22 o 5 4 0 845.34 861.79 21.60 o 6 4 0 95.07 104.96 4.67 o 7 4 0 188.69 200.56 7.48 o 8 4 0 2.17 -1.16 2.47 o 1 5 0 427.06 304.25 7.78 o 2 5 0 1074.25 1140.30 25.14 o 3 5 0 2381.73 2389.16 52.21 o 4 5 0 180.65 161.69 5.09 o 5 5 0 1195.71 1253.42 34.54 o 6 5 0 21.22 20.56 2.42 o 7 5 0 490.10 475.17 14.73 o 8 5 0 10.98 14.22 3.71 o 0 6 0 1377.82 1087.43 41.87 o 1 6 0 988.07 984.97 23.93 o 2 6 0 1771.96 1790.06 39.29 o 3 6 0 1190.50 1379.07 37.42 o 4 6 0 253.65 245.88 6.33 o 6 6 0 429.97 467.64 15.19 o 7 6 0 76.18 84.52 4.66 o 1 7 0 223.35 174.88 5.53 o 2 7 0 2298.07 2458.86 65.94 o 3 7 0 84.81 83.91 3.38 o 4 7 0 826.65 803.43 20.18 o 5 7 0 4.88 5.37 1.89 o 6 7 0 12.74 12.77 2.46 o 7 7 0 45.66 50.35 8.40 o 0 8 0 65.36 83.11 7.15 o 1 8 0 499.18 490.22 16.40 o 2 8 0 2031.08 2015.67 54.26 o 3 8 0 100.04 89.09 3.33 o 4 8 0 719.02 727.75 29.66 o 5 8 0 79.92 93.77 4.38 o 6 8 0 1293.52 1354.04 53.88 o 7 8 0 80.17 96.74 14.95 o 1 9 0 66.36 62.91 3.19 o 2 9 0 1405.54 1215.46 33.58 o 3 9 0 254.85 241.02 8.67 o 4 9 0 4.21 6.61 2.98 o 5 9 0 26.46 24.85 5.53 o 6 9 0 7.64 11.47 3.17 o 0 10 0 506.35 521.29 32.36 o 1 10 0 803.75 729.37 25.02 o 2 10 0 8.45 6.55 1.77 o 3 10 0 40.74 31.19 2.94 o 4 10 0 69.88 70.43 4.64 o 5 10 0 289.41 296.94 14.03 o 6 10 0 439.72 464.21 21.24 o 1 11 0 17.87 19.54 3.75 o 2 11 0 76.06 61.87 4.99 o 3 11 0 739.81 689.35 20.16 o 4 11 0 75.36 75.87 5.61 o 5 11 0 127.66 133.03 7.07 o 0 12 0 0.12 3.96 2.97 o 1 12 0 590.44 538.70 16.21 o 2 12 0 93.43 77.48 4.85 o 3 12 0 204.67 180.55 9.59 o 4 12 0 35.57 30.95 3.71 o 5 12 0 257.66 273.67 11.58 o 1 13 0 12.89 20.62 3.98 o 2 13 0 67.19 66.28 4.17 o 3 13 0 721.41 685.26 21.38 o 4 13 0 76.29 72.36 5.52 o 0 14 0 461.85 456.56 52.69 o 1 14 0 18.82 19.91 2.97 o 2 14 0 5.41 4.56 2.51 o 3 14 0 0.01 -2.73 2.73 o 1 15 0 91.56 107.21 10.62 o -7 0 1 636.64 612.69 28.80 o -5 0 1 17.39 9.61 1.82 o -3 0 1 13.09 5.88 0.99 o -1 0 1 572.96 496.30 17.72 o 1 0 1 26358.91 26687.56 1554.66 o 3 0 1 1738.18 1783.72 62.89 o 5 0 1 2144.51 1979.76 119.65 o 7 0 1 2902.51 2887.05 265.99 o -8 1 1 95.74 109.68 6.71 o -7 1 1 1178.59 1241.81 54.96 o -6 1 1 0.48 0.21 1.54 o -5 1 1 928.26 905.13 22.41 o -4 1 1 443.19 450.09 10.42 o -3 1 1 4476.80 4555.52 98.78 o -2 1 1 110.93 102.03 2.59 o -1 1 1 2133.47 2283.16 49.60 o 0 1 1 756.74 829.85 18.17 o 1 1 1 436.34 440.17 9.08 o 2 1 1 723.93 775.93 18.77 o 3 1 1 1594.69 1374.76 33.10 o 4 1 1 1870.94 1818.82 43.84 o 5 1 1 318.26 285.36 11.89 o 6 1 1 321.62 339.02 14.25 o 7 1 1 1151.48 1130.19 35.78 o 8 1 1 65.98 64.93 5.93 o -8 2 1 106.03 103.72 8.95 o -7 2 1 119.11 125.64 10.23 o -6 2 1 96.97 96.64 4.34 o -5 2 1 515.21 464.84 12.10 o -4 2 1 1825.73 1673.34 36.82 o -3 2 1 12.90 3.23 0.76 o -2 2 1 3954.60 4453.35 96.56 o -1 2 1 665.85 701.70 15.47 o 0 2 1 5628.37 6151.77 163.13 o 1 2 1 7447.09 8210.80 177.49 o 2 2 1 468.46 407.42 8.53 o 3 2 1 1512.42 1569.81 37.81 o 4 2 1 80.41 80.75 2.92 o 5 2 1 1583.45 1574.95 43.02 o 6 2 1 687.45 675.96 19.61 o 7 2 1 180.72 189.57 7.61 o 8 2 1 136.20 155.20 8.58 o -8 3 1 540.59 554.82 21.96 o -7 3 1 2.37 0.52 1.96 o -6 3 1 178.96 194.56 7.75 o -5 3 1 289.22 271.81 10.75 o -4 3 1 276.56 294.76 7.16 o -3 3 1 2009.82 2056.41 45.00 o -2 3 1 9503.44 9875.04 213.48 o -1 3 1 638.54 674.89 15.02 o 0 3 1 543.03 596.83 16.35 o 1 3 1 780.54 835.73 20.15 o 2 3 1 3555.47 3609.84 85.88 o 3 3 1 1449.76 1629.19 35.74 o 4 3 1 1249.36 1219.23 29.75 o 5 3 1 1587.76 1505.81 36.73 o 6 3 1 1233.76 1267.74 35.21 o 7 3 1 0.82 -0.06 3.30 o 8 3 1 115.69 118.13 5.90 o -8 4 1 75.13 60.28 5.25 o -7 4 1 21.59 17.57 2.55 o -6 4 1 131.65 129.56 5.25 o -5 4 1 17.82 17.43 1.87 o -4 4 1 502.97 468.36 9.48 o -3 4 1 1377.40 1502.65 33.09 o -2 4 1 353.06 322.70 7.53 o -1 4 1 764.18 828.62 20.42 o 0 4 1 20.34 30.37 1.36 o 1 4 1 1030.89 1151.01 27.76 o 2 4 1 8633.21 8954.03 193.34 o 3 4 1 189.98 191.65 5.28 o 4 4 1 130.05 128.88 4.16 o 5 4 1 36.92 33.48 2.22 o 6 4 1 1206.56 1234.44 34.39 o 7 4 1 302.26 288.01 13.27 o 8 4 1 258.20 270.73 11.52 o -8 5 1 397.28 480.26 33.66 o -7 5 1 51.35 60.39 3.94 o -6 5 1 1355.39 1447.76 54.03 o -5 5 1 2.12 0.51 1.29 o -4 5 1 2625.85 2771.32 75.99 o -3 5 1 202.13 230.72 5.76 o -2 5 1 2830.07 2854.69 57.56 o -1 5 1 2710.69 2872.92 70.33 o 0 5 1 1071.63 935.43 22.70 o 1 5 1 19.69 18.23 1.24 o 2 5 1 2547.64 2760.12 73.73 o 3 5 1 2443.11 2633.30 70.49 o 4 5 1 706.49 665.06 15.38 o 5 5 1 63.24 56.60 2.85 o 6 5 1 82.58 81.96 4.43 o 7 5 1 105.93 111.47 5.56 o 8 5 1 9.37 8.00 2.92 o -7 6 1 0.77 0.17 2.97 o -6 6 1 131.90 148.69 6.89 o -5 6 1 418.25 438.71 10.77 o -4 6 1 289.79 285.25 7.63 o -3 6 1 363.19 378.80 10.82 o -2 6 1 2947.63 3383.36 80.66 o -1 6 1 2117.26 2257.81 62.78 o 0 6 1 276.85 195.70 5.36 o 1 6 1 312.67 222.35 7.95 o 2 6 1 3240.65 3470.98 92.53 o 3 6 1 180.24 145.90 4.44 o 4 6 1 191.22 185.38 7.26 o 6 6 1 285.43 288.55 9.60 o 7 6 1 168.91 173.41 7.54 o -7 7 1 226.88 263.84 23.53 o -6 7 1 65.88 77.03 3.77 o -5 7 1 154.56 165.34 5.71 o -4 7 1 7.28 11.08 1.44 o -3 7 1 699.09 659.81 16.66 o -2 7 1 826.41 819.67 20.26 o -1 7 1 2619.42 2606.65 62.36 o 0 7 1 141.25 99.46 3.79 o 1 7 1 93.20 104.74 4.54 o 2 7 1 58.66 49.09 2.20 o 3 7 1 243.97 239.20 7.11 o 4 7 1 113.69 125.73 5.03 o 5 7 1 2526.52 2610.48 81.58 o 6 7 1 10.30 10.81 2.43 o 7 7 1 6.56 7.59 2.98 o -7 8 1 78.96 100.96 8.18 o -6 8 1 137.32 147.95 7.17 o -5 8 1 1411.62 1464.27 40.42 o -4 8 1 113.72 115.05 3.74 o -3 8 1 782.18 848.24 23.65 o -2 8 1 81.25 73.73 3.14 o -1 8 1 309.67 291.25 8.60 o 0 8 1 598.81 570.73 16.31 o 1 8 1 2546.61 2428.48 75.58 o 2 8 1 193.18 188.31 8.03 o 3 8 1 529.02 511.16 17.20 o 4 8 1 110.35 103.63 6.73 o 5 8 1 397.04 396.59 14.64 o 6 8 1 46.78 64.97 4.71 o 7 8 1 125.45 156.92 8.21 o -6 9 1 297.31 312.28 31.60 o -5 9 1 132.80 134.35 15.42 o -4 9 1 517.48 524.78 18.50 o -3 9 1 237.08 245.88 10.11 o -2 9 1 10.97 14.28 2.09 o -1 9 1 1667.67 1558.88 46.67 o 0 9 1 137.89 128.01 4.84 o 1 9 1 140.54 100.94 6.52 o 2 9 1 0.09 0.26 1.42 o 3 9 1 1.78 4.26 2.33 o 4 9 1 369.30 341.78 12.59 o 5 9 1 717.65 770.56 26.33 o 6 9 1 50.44 52.64 4.62 o -6 10 1 180.07 239.39 13.77 o -5 10 1 685.13 666.49 30.97 o -4 10 1 107.28 105.06 5.65 o -3 10 1 691.68 691.67 20.04 o -2 10 1 525.68 485.34 14.46 o -1 10 1 65.00 52.54 3.94 o 0 10 1 752.21 724.06 20.65 o 1 10 1 1399.47 1310.17 36.16 o 2 10 1 1379.02 1272.88 35.28 o 3 10 1 38.12 40.92 3.10 o 4 10 1 48.84 45.24 3.93 o 5 10 1 11.74 9.05 2.77 o 6 10 1 255.67 276.39 14.25 o -5 11 1 124.25 140.12 7.24 o -4 11 1 168.87 161.68 14.81 o -3 11 1 2.11 -0.94 1.85 o -2 11 1 1322.67 1234.00 34.41 o -1 11 1 20.46 17.45 2.35 o 0 11 1 13.81 19.51 2.33 o 1 11 1 691.07 608.54 17.84 o 2 11 1 18.29 15.94 2.34 o 3 11 1 273.69 256.38 8.79 o 4 11 1 233.54 249.91 16.86 o 5 11 1 26.76 24.97 3.64 o -5 12 1 4.57 3.13 4.38 o -4 12 1 356.47 398.90 15.03 o -3 12 1 105.74 105.57 5.01 o -2 12 1 858.31 834.61 34.42 o -1 12 1 24.83 22.36 2.54 o 1 12 1 27.96 31.45 3.94 o 2 12 1 1377.49 1236.56 37.88 o 3 12 1 12.02 8.32 2.80 o 4 12 1 88.06 94.63 7.60 o 5 12 1 77.48 87.12 10.63 o -4 13 1 115.49 125.64 13.35 o -3 13 1 109.99 114.17 5.55 o -2 13 1 1160.91 1113.90 37.85 o -1 13 1 56.80 45.59 5.12 o 0 13 1 4.20 0.24 1.99 o 1 13 1 48.04 54.76 3.84 o 2 13 1 62.69 65.82 5.72 o 3 13 1 2.34 0.81 2.53 o 4 13 1 247.08 282.25 21.98 o -3 14 1 277.86 291.06 10.48 o -2 14 1 117.35 115.97 5.93 o -1 14 1 0.51 -0.27 2.25 o 0 14 1 13.17 15.59 2.85 o 1 14 1 628.14 621.36 31.62 o 2 14 1 310.43 283.81 17.60 o 3 14 1 59.70 64.32 5.25 o -1 15 1 237.06 241.34 10.68 o 0 15 1 28.12 30.21 3.56 o 1 15 1 1.32 2.03 2.60 o -8 0 2 176.69 202.70 32.33 o -6 0 2 40.04 34.26 3.94 o -4 0 2 1726.34 1550.19 48.27 o -2 0 2 205.21 138.32 8.22 o 0 0 2 505.07 566.70 17.79 o 2 0 2 755.62 955.94 38.26 o 4 0 2 1083.83 1023.12 39.81 o 6 0 2 1.71 -3.24 3.81 o 8 0 2 603.11 592.61 77.22 o -8 1 2 22.88 21.97 5.02 o -7 1 2 261.26 235.18 11.43 o -6 1 2 2222.08 2287.31 62.07 o -5 1 2 271.54 261.49 6.57 o -4 1 2 1963.04 1916.80 42.03 o -3 1 2 53.88 43.93 1.77 o -2 1 2 1292.07 1312.87 28.70 o -1 1 2 562.25 586.46 11.97 o 0 1 2 10102.17 11332.71 245.30 o 1 1 2 408.72 415.42 9.21 o 2 1 2 1542.20 1544.71 36.94 o 3 1 2 448.81 465.82 11.70 o 4 1 2 2993.57 3040.10 81.47 o 5 1 2 95.85 87.10 3.81 o 6 1 2 488.40 489.72 14.74 o 7 1 2 196.35 192.23 7.94 o 8 1 2 31.65 31.51 4.45 o -8 2 2 305.94 306.91 16.03 o -7 2 2 268.54 274.04 12.78 o -6 2 2 14.40 12.75 2.10 o -5 2 2 23.68 23.14 2.96 o -4 2 2 85.06 68.99 2.56 o -3 2 2 514.82 431.28 9.16 o -2 2 2 2432.21 2281.69 49.66 o -1 2 2 13197.13 14649.96 316.84 o 0 2 2 1891.16 2166.72 47.05 o 1 2 2 2239.62 2458.62 53.35 o 2 2 2 2906.54 2710.67 64.56 o 3 2 2 856.50 758.54 20.86 o 4 2 2 541.31 529.31 13.43 o 5 2 2 19.52 18.81 1.97 o 6 2 2 3.43 0.92 1.72 o 7 2 2 411.99 385.12 17.60 o 8 2 2 235.77 237.92 12.99 o -8 3 2 46.57 43.28 4.73 o -7 3 2 217.35 224.94 10.31 o -6 3 2 21.06 21.66 2.34 o -5 3 2 1606.50 1615.03 50.70 o -4 3 2 62.84 54.07 2.08 o -3 3 2 256.07 248.77 6.01 o -2 3 2 2076.77 2171.07 47.36 o -1 3 2 9017.04 9993.93 264.89 o 0 3 2 0.90 1.03 0.71 o 1 3 2 633.38 698.99 15.45 o 2 3 2 1.50 0.13 0.60 o 3 3 2 1.35 1.89 0.77 o 4 3 2 16.50 21.84 1.65 o 5 3 2 378.26 367.29 11.18 o 6 3 2 193.75 189.28 7.92 o 7 3 2 555.82 560.56 20.87 o 8 3 2 12.64 16.73 3.09 o -8 4 2 7.39 9.83 3.29 o -7 4 2 796.03 810.09 27.16 o -6 4 2 47.64 44.81 3.07 o -5 4 2 351.96 349.67 9.49 o -4 4 2 146.72 148.60 3.85 o -3 4 2 3166.44 3076.84 67.09 o -2 4 2 1291.20 1349.34 25.73 o -1 4 2 2238.49 2269.44 49.38 o 0 4 2 2998.25 3086.38 73.61 o 1 4 2 417.34 498.96 11.24 o 2 4 2 413.91 451.39 11.56 o 3 4 2 5477.74 5361.80 127.44 o 4 4 2 2.87 1.75 1.88 o 5 4 2 502.29 521.92 15.30 o 6 4 2 156.65 148.98 5.88 o 7 4 2 356.18 373.15 12.11 o 8 4 2 122.03 135.14 6.42 o -8 5 2 77.52 78.76 9.33 o -7 5 2 529.89 543.17 32.88 o -6 5 2 233.43 226.46 7.36 o -5 5 2 141.98 176.21 12.94 o -4 5 2 157.78 162.97 4.52 o -3 5 2 91.61 74.48 3.13 o -2 5 2 40.69 32.63 1.50 o -1 5 2 449.64 407.53 9.34 o 0 5 2 445.61 436.07 12.28 o 1 5 2 7536.07 7794.98 206.72 o 2 5 2 306.52 283.89 7.47 o 3 5 2 2683.78 2933.23 78.41 o 4 5 2 23.38 30.84 2.04 o 5 5 2 327.21 330.52 11.97 o 6 5 2 243.04 248.57 8.51 o 7 5 2 3.43 6.92 2.30 o -7 6 2 150.22 148.26 9.91 o -6 6 2 227.77 242.76 9.18 o -5 6 2 10.65 13.50 2.39 o -4 6 2 441.66 471.76 12.09 o -3 6 2 4584.16 4892.62 106.39 o -2 6 2 3021.70 3236.42 70.52 o -1 6 2 1272.67 1478.46 36.65 o 0 6 2 21.68 19.85 1.49 o 1 6 2 1.82 12.50 1.20 o 2 6 2 174.52 159.22 6.07 o 3 6 2 1926.39 1922.41 51.72 o 4 6 2 525.88 533.85 13.89 o 5 6 2 1044.63 1050.76 33.97 o 6 6 2 0.13 -1.78 1.78 o 7 6 2 426.04 444.58 21.54 o -7 7 2 159.95 189.59 12.08 o -6 7 2 345.21 335.12 15.65 o -5 7 2 10.54 6.02 1.69 o -4 7 2 150.40 154.82 4.14 o -3 7 2 14.17 21.45 1.83 o -2 7 2 91.90 79.63 2.81 o -1 7 2 223.98 207.29 5.83 o 0 7 2 3475.73 3304.69 78.83 o 1 7 2 1646.98 1572.94 42.67 o 2 7 2 209.38 191.90 7.13 o 3 7 2 47.16 53.59 3.51 o 4 7 2 393.52 400.00 13.93 o 5 7 2 2.92 2.46 1.64 o 6 7 2 804.75 854.62 27.28 o 7 7 2 26.41 56.45 10.82 o -7 8 2 13.39 21.76 4.94 o -6 8 2 31.06 33.06 3.28 o -5 8 2 60.78 65.07 3.33 o -4 8 2 859.54 892.00 22.37 o -3 8 2 3.40 4.78 1.61 o -2 8 2 921.46 911.35 26.71 o -1 8 2 216.44 205.45 5.89 o 0 8 2 280.08 273.10 8.51 o 1 8 2 343.65 314.21 9.60 o 2 8 2 1543.78 1457.18 56.50 o 3 8 2 5.31 6.63 1.80 o 4 8 2 427.55 443.77 19.19 o 5 8 2 2.88 5.39 2.10 o 6 8 2 5.35 4.52 2.49 o 7 8 2 7.73 9.06 3.32 o -6 9 2 291.32 326.93 16.46 o -5 9 2 272.84 272.84 10.74 o -4 9 2 812.06 838.75 23.92 o -3 9 2 155.43 143.31 5.52 o -2 9 2 434.83 401.94 16.61 o -1 9 2 54.78 43.88 3.23 o 0 9 2 2826.92 2834.88 76.16 o 1 9 2 230.86 247.49 16.39 o 2 9 2 543.42 495.11 16.85 o 3 9 2 129.23 115.77 4.78 o 4 9 2 46.65 55.69 3.53 o 5 9 2 24.03 28.02 2.70 o 6 9 2 817.49 874.88 36.39 o -6 10 2 15.21 22.53 4.75 o -5 10 2 56.73 65.18 9.43 o -4 10 2 443.80 448.43 21.93 o -3 10 2 308.57 304.25 9.85 o -2 10 2 17.30 18.11 2.59 o -1 10 2 140.37 127.96 5.05 o 0 10 2 47.53 40.25 3.79 o 1 10 2 39.81 44.05 2.97 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