#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203596.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203596_Fobs loop_ _publ_author_name 'Boyle, Robert C.' 'Mague, Joel T.' 'Fink, Mark J.' _publ_section_title ; \m-1,2-Bis(dicyclohexylphosphino)ethane-\k^2^P:P'-bis{[1,2-bis(dicyclohexylphosphino)ethane-\k^2^P,P']palladium(0)} ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m625 _journal_page_last m627 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 106.244 _cell_angle_beta 73.645 _cell_angle_gamma 102.621 _cell_length_a 10.7317 _cell_length_b 12.4425 _cell_length_c 15.5226 _exptl_crystal_F_000 794.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file fl6100Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mjf246 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5321.59 6075.59 39.15 o 1 0 0 4503.10 5095.39 43.82 o 2 0 0 1.58 1.71 11.05 o 2 0 0 1.34 2.80 10.32 o 3 0 0 10296.31 10934.10 77.32 o 4 0 0 1351.59 1261.00 31.17 o 4 0 0 1597.25 1533.56 36.35 o 5 0 0 285.61 279.77 22.61 o 5 0 0 337.52 289.88 24.42 o 6 0 0 2575.25 2670.42 56.89 o 7 0 0 1252.09 1210.44 43.87 o 7 0 0 1059.52 1023.65 56.99 o 8 0 0 1295.00 1310.84 49.32 o 8 0 0 1095.83 1100.40 64.15 o 9 0 0 1111.99 1186.28 71.72 o 10 0 0 1066.55 1059.64 74.05 o 10 0 0 1260.40 1141.52 106.31 o 11 0 0 829.27 791.07 105.89 o 11 0 0 701.72 765.56 71.82 o 12 0 0 122.72 124.56 81.31 o 13 0 0 4.27 -6.90 53.46 o 13 0 0 5.05 25.10 71.93 o -13 1 0 169.93 143.28 84.68 o -13 1 0 143.79 145.30 58.03 o -12 1 0 138.46 142.92 52.17 o -12 1 0 163.62 192.13 78.77 o -11 1 0 337.35 307.10 84.16 o -10 1 0 1369.41 1319.44 78.04 o -10 1 0 1619.76 1555.13 129.49 o -10 1 0 1618.31 1666.31 126.27 o -9 1 0 3781.75 3804.00 110.77 o -9 1 0 3200.10 3125.04 104.44 o -8 1 0 237.82 256.48 35.99 o -7 1 0 559.78 487.76 43.20 o -7 1 0 713.16 606.67 74.78 o -7 1 0 661.53 612.53 42.83 o -6 1 0 1944.09 1816.54 43.87 o -6 1 0 2297.44 2142.25 50.35 o -5 1 0 1105.56 1146.19 38.53 o -4 1 0 12.56 7.78 14.52 o -4 1 0 14.84 18.51 13.12 o -3 1 0 1958.77 2141.84 36.04 o -3 1 0 1657.50 1748.77 31.68 o -2 1 0 3313.22 3582.58 44.75 o -2 1 0 3915.43 4200.76 41.59 o -1 1 0 2661.08 2779.06 26.08 o -1 1 0 2251.79 2400.97 24.37 o 0 1 0 838.41 988.49 17.68 o 0 1 0 709.46 793.20 15.92 o 1 1 0 9875.04 10825.00 58.44 o 1 1 0 8356.21 9251.66 53.00 o 2 1 0 3971.03 4351.92 43.35 o 2 1 0 4692.80 5082.79 47.86 o 3 1 0 196.35 202.09 16.80 o 3 1 0 232.04 246.73 19.60 o 4 1 0 148.75 158.11 36.87 o 4 1 0 3355.34 3379.14 63.89 o 4 1 0 175.78 136.44 34.43 o 5 1 0 375.66 341.58 51.18 o 5 1 0 317.88 292.42 26.14 o 5 1 0 2570.43 2621.72 66.12 o 6 1 0 364.98 369.22 29.40 o 6 1 0 308.84 309.64 23.96 o 7 1 0 2903.88 2931.83 67.67 o 8 1 0 212.55 154.17 52.17 o 8 1 0 772.35 738.54 84.68 o 8 1 0 179.86 173.67 54.24 o 9 1 0 835.94 871.45 65.50 o 9 1 0 987.88 945.04 64.56 o 10 1 0 858.76 862.43 114.50 o 11 1 0 268.81 232.21 101.69 o 11 1 0 69.64 62.28 63.11 o 12 1 0 698.09 677.98 77.47 o 12 1 0 824.98 789.62 113.62 o 13 1 0 412.74 371.76 96.04 o -13 2 0 316.97 438.50 120.15 o -12 2 0 261.32 295.58 112.32 o -12 2 0 1.29 38.79 65.34 o -11 2 0 826.69 724.44 70.42 o -11 2 0 976.95 1006.38 112.11 o -10 2 0 22.65 27.38 46.62 o -10 2 0 61.74 50.30 52.27 o -9 2 0 649.28 584.22 79.86 o -9 2 0 767.81 768.78 95.05 o -9 2 0 767.29 866.47 91.48 o -8 2 0 1747.00 1773.19 55.38 o -8 2 0 1478.30 1520.28 71.61 o -7 2 0 471.96 376.17 35.99 o -7 2 0 399.37 390.17 57.87 o -7 2 0 472.23 510.94 70.78 o -6 2 0 338.34 330.38 30.91 o -6 2 0 286.30 305.23 49.26 o -6 2 0 1202.78 1290.09 83.13 o -5 2 0 2542.04 2402.73 47.14 o -5 2 0 3004.08 2948.73 47.40 o -4 2 0 1424.36 1411.28 40.40 o -4 2 0 1683.25 1677.31 38.32 o -3 2 0 649.90 738.28 28.83 o -3 2 0 768.02 850.71 26.76 o -2 2 0 599.37 585.67 22.14 o -2 2 0 708.31 697.21 23.28 o -1 2 0 5110.13 5742.00 44.65 o -1 2 0 6038.95 6885.49 49.11 o 0 2 0 1848.46 1980.41 25.46 o 0 2 0 1564.16 1615.08 22.56 o 1 2 0 31.15 43.66 13.43 o 1 2 0 36.81 47.60 13.28 o 2 2 0 2770.96 2796.84 40.29 o 2 2 0 2344.77 2387.28 37.08 o 3 2 0 10775.80 11937.38 109.42 o 3 2 0 9118.43 9736.57 93.03 o 3 2 0 13189.76 14299.97 169.36 o 4 2 0 1256.57 1312.08 37.39 o 4 2 0 1063.30 1071.72 32.77 o 5 2 0 133.06 117.40 35.68 o 5 2 0 112.59 99.62 18.72 o 5 2 0 2666.53 2775.79 99.88 o 6 2 0 926.48 916.67 42.94 o 6 2 0 595.50 617.93 36.97 o 7 2 0 1.77 2.70 19.96 o 7 2 0 1.50 -18.20 27.80 o 8 2 0 429.46 433.99 84.42 o 8 2 0 118.62 111.54 34.38 o 8 2 0 100.37 90.23 50.98 o 9 2 0 77.73 7.73 71.77 o 10 2 0 37.76 59.53 38.22 o 10 2 0 44.63 47.45 50.82 o 11 2 0 369.23 394.47 82.30 o 11 2 0 312.44 376.74 59.17 o 12 2 0 110.01 173.25 101.07 o -13 3 0 4.75 -5.03 50.40 o -13 3 0 5.61 -24.58 67.00 o -12 3 0 193.40 232.73 55.59 o -12 3 0 228.56 309.07 85.77 o -11 3 0 723.26 691.82 74.05 o -10 3 0 1462.53 1444.42 81.99 o -10 3 0 1728.36 1650.81 82.61 o -9 3 0 403.54 284.02 85.72 o -9 3 0 260.17 320.32 67.78 o -9 3 0 307.45 277.85 66.84 o -8 3 0 132.89 136.64 34.69 o -7 3 0 1255.27 1179.33 44.60 o -7 3 0 1062.20 1031.85 40.81 o -6 3 0 1606.76 1571.67 44.39 o -6 3 0 1898.80 1983.37 50.46 o -5 3 0 5793.98 6588.09 80.79 o -4 3 0 4125.51 4221.50 59.58 o -4 3 0 3490.99 3671.87 56.11 o -3 3 0 2655.28 2685.14 43.82 o -3 3 0 3137.91 3110.84 46.36 o -2 3 0 5512.11 6051.53 78.10 o -2 3 0 2993.01 3532.17 61.09 o -2 3 0 3537.02 4526.94 73.07 o -1 3 0 32.90 62.59 11.72 o -1 3 0 38.88 53.67 12.65 o 0 3 0 940.96 917.24 23.91 o 0 3 0 796.23 747.88 21.16 o 1 3 0 4383.43 4666.85 78.67 o 1 3 0 3709.24 3926.59 70.99 o 1 3 0 5052.99 5265.90 70.94 o 2 3 0 2188.35 2217.19 39.46 o 2 3 0 1851.77 1886.03 37.08 o 3 3 0 5986.85 7159.29 74.83 o 3 3 0 7075.03 8381.25 80.22 o 4 3 0 1515.20 1420.15 41.38 o 5 3 0 860.78 845.63 34.54 o 5 3 0 1017.24 1024.17 38.84 o 6 3 0 113.95 122.28 22.09 o 6 3 0 134.66 147.17 24.74 o 7 3 0 764.76 796.73 44.29 o 8 3 0 253.82 225.94 32.67 o 8 3 0 214.78 227.91 43.51 o 9 3 0 84.50 69.02 36.40 o 9 3 0 99.86 92.15 57.72 o 10 3 0 182.25 198.40 75.61 o 11 3 0 9.07 13.38 41.12 o 11 3 0 10.72 8.61 61.24 o 12 3 0 448.79 402.05 99.93 o 12 3 0 379.76 399.09 67.36 o -13 4 0 530.54 616.78 112.22 o -12 4 0 600.98 565.50 70.53 o -12 4 0 710.22 722.78 106.46 o -11 4 0 6.38 -22.82 35.16 o -11 4 0 5.40 9.39 37.60 o -10 4 0 842.61 873.79 68.71 o -9 4 0 1113.80 1058.92 67.98 o -9 4 0 1316.24 1238.50 69.85 o -8 4 0 581.16 569.59 52.84 o -8 4 0 686.79 684.77 40.71 o -7 4 0 1630.05 1713.04 62.23 o -6 4 0 778.07 803.52 36.61 o -6 4 0 919.49 898.06 37.80 o -5 4 0 544.77 482.27 30.03 o -5 4 0 643.78 580.33 30.49 o -4 4 0 2551.08 2627.17 51.80 o -3 4 0 1704.48 1790.30 38.69 o -3 4 0 2014.29 2115.65 41.95 o -2 4 0 6046.99 6473.75 62.12 o -2 4 0 5116.93 5427.33 54.55 o -1 4 0 3653.22 3660.57 45.06 o 0 4 0 223.52 220.18 17.37 o 0 4 0 189.14 182.95 16.70 o 1 4 0 37.83 33.03 13.38 o 1 4 0 32.01 30.18 12.91 o 2 4 0 7768.92 8738.64 83.02 o 3 4 0 3008.45 3178.66 55.43 o 3 4 0 3555.27 3759.56 59.38 o 4 4 0 124.55 86.81 19.24 o 4 4 0 105.40 59.79 18.56 o 5 4 0 1195.13 1188.30 45.22 o 6 4 0 365.07 333.54 31.79 o 6 4 0 308.92 273.80 28.78 o 7 4 0 61.69 98.01 26.29 o 7 4 0 52.20 65.44 35.00 o 8 4 0 691.98 733.51 64.46 o 9 4 0 1.40 15.51 36.56 o 9 4 0 1.65 0.05 44.96 o 10 4 0 204.47 137.16 69.23 o 10 4 0 173.02 169.73 47.86 o 12 4 0 12.72 38.43 81.93 o 12 4 0 10.77 19.14 49.26 o -13 5 0 91.60 52.01 52.79 o -13 5 0 108.25 83.70 76.49 o -12 5 0 1161.79 1276.04 94.69 o -11 5 0 1016.89 988.03 128.03 o -11 5 0 752.44 815.14 102.37 o -11 5 0 636.71 644.06 94.12 o -10 5 0 86.28 154.17 43.82 o -10 5 0 73.01 77.79 39.72 o -9 5 0 236.61 187.15 51.39 o -8 5 0 929.79 810.47 77.11 o -8 5 0 1098.79 1126.95 88.57 o -7 5 0 255.22 280.55 30.91 o -7 5 0 301.61 289.88 31.58 o -6 5 0 1.41 -0.67 20.38 o -6 5 0 170.50 138.46 64.98 o -6 5 0 1.19 -3.99 28.88 o -5 5 0 42.12 25.82 20.12 o -5 5 0 49.78 55.28 18.88 o -4 5 0 1264.86 1248.40 38.89 o -4 5 0 1494.76 1522.26 42.00 o -3 5 0 233.80 156.30 19.60 o -3 5 0 197.84 172.16 23.13 o -2 5 0 64.42 74.21 15.56 o -2 5 0 54.51 62.64 23.80 o -1 5 0 1989.94 2010.69 32.51 o -1 5 0 2351.63 2402.16 40.34 o 0 5 0 2372.21 2421.45 42.37 o 0 5 0 2007.35 2045.54 41.74 o 1 5 0 522.07 448.51 26.45 o 1 5 0 441.77 403.96 25.15 o 2 5 0 102.58 146.34 20.48 o 2 5 0 86.81 100.60 19.14 o 3 5 0 2223.12 2304.57 106.15 o 3 5 0 125.01 126.84 24.22 o 3 5 0 105.78 124.66 24.48 o 4 5 0 2358.02 2336.61 65.39 o 4 5 0 1995.34 2039.89 61.92 o 4 5 0 4353.36 4373.08 137.52 o 5 5 0 1120.69 1075.92 42.68 o 5 5 0 948.32 910.19 40.55 o 6 5 0 441.48 429.27 43.51 o 6 5 0 373.58 363.67 40.81 o 6 5 0 995.31 948.05 90.23 o 7 5 0 60.01 88.36 51.03 o 7 5 0 855.09 922.74 93.50 o 7 5 0 50.78 66.12 48.90 o 8 5 0 444.84 502.18 56.94 o 8 5 0 525.70 614.19 56.47 o 9 5 0 0.63 8.04 54.50 o 9 5 0 0.53 17.22 51.13 o 11 5 0 34.83 -7.62 45.06 o 11 5 0 41.16 15.25 64.25 o -12 6 0 21.75 14.93 45.17 o -12 6 0 18.41 21.83 62.95 o -11 6 0 610.75 651.89 123.16 o -11 6 0 436.27 438.35 86.29 o -10 6 0 816.03 913.82 77.84 o -10 6 0 502.97 554.82 79.76 o -9 6 0 540.30 480.30 54.45 o -9 6 0 457.20 486.36 52.32 o -8 6 0 71.15 55.75 47.81 o -8 6 0 60.21 100.60 45.37 o -8 6 0 344.38 391.26 92.31 o -7 6 0 4041.75 4153.99 167.96 o -7 6 0 2689.55 2852.28 80.27 o -7 6 0 2275.89 2368.87 103.40 o -6 6 0 145.45 127.78 23.80 o -6 6 0 171.89 167.24 25.46 o -5 6 0 1499.63 1527.13 46.36 o -5 6 0 1268.98 1269.51 50.25 o -4 6 0 1991.68 1947.38 71.51 o -3 6 0 3203.65 3752.46 58.91 o -3 6 0 2710.91 3140.45 51.03 o -2 6 0 790.25 709.92 28.73 o -2 6 0 668.70 524.06 22.87 o -1 6 0 1410.84 1312.65 36.66 o -1 6 0 208.36 157.33 19.29 o 0 6 0 810.97 811.92 28.42 o 0 6 0 958.37 985.54 32.88 o 1 6 0 1260.83 1236.99 38.27 o 1 6 0 1066.91 1037.19 34.64 o 2 6 0 4370.32 4794.99 108.74 o 2 6 0 5165.53 5673.60 104.44 o 2 6 0 5164.67 5642.17 119.69 o 3 6 0 183.73 186.22 24.99 o 3 6 0 155.47 139.18 22.25 o 4 6 0 19.89 25.36 23.49 o 4 6 0 23.51 37.54 23.80 o 4 6 0 885.58 877.78 94.85 o 5 6 0 55.12 57.30 31.68 o 6 6 0 886.35 913.92 46.36 o 6 6 0 1047.46 1032.36 42.47 o 7 6 0 490.02 530.03 53.78 o 7 6 0 414.65 427.82 51.65 o 8 6 0 414.97 399.40 79.08 o 9 6 0 165.61 283.35 55.12 o 9 6 0 140.14 246.68 51.23 o 10 6 0 121.82 120.88 49.52 o 10 6 0 143.96 213.86 77.47 o 11 6 0 273.94 403.03 106.20 o -12 7 0 455.36 588.16 108.85 o -11 7 0 312.69 297.55 82.09 o -11 7 0 264.59 327.73 86.60 o -10 7 0 6.62 21.57 57.09 o -10 7 0 7.82 21.31 53.98 o -9 7 0 3199.38 3121.41 163.19 o -8 7 0 1516.16 1565.87 76.64 o -8 7 0 1282.97 1282.88 107.60 o -7 7 0 812.65 875.71 62.38 o -7 7 0 960.36 974.23 48.33 o -6 7 0 1463.62 1458.37 52.84 o -5 7 0 4.87 10.37 21.16 o -5 7 0 5.76 4.93 18.67 o -4 7 0 1.00 6.95 25.88 o -4 7 0 1.18 13.79 16.65 o -3 7 0 1178.04 1154.64 37.23 o -2 7 0 42.76 37.23 26.40 o -2 7 0 50.53 40.81 16.13 o -1 7 0 1575.57 1521.43 38.58 o -1 7 0 1333.24 1263.08 29.71 o 0 7 0 1212.01 1118.14 36.40 o 1 7 0 468.56 449.70 27.90 o 1 7 0 553.72 539.15 30.60 o 2 7 0 270.58 261.25 27.17 o 2 7 0 319.76 310.10 28.42 o 3 7 0 643.93 613.88 36.66 o 4 7 0 584.76 553.57 37.29 o 4 7 0 691.04 698.41 40.45 o 5 7 0 406.34 439.80 37.08 o 5 7 0 343.84 366.47 36.66 o 6 7 0 17.95 48.64 40.29 o 7 7 0 235.04 276.50 46.67 o 7 7 0 277.77 274.74 47.24 o 8 7 0 1419.39 1392.09 80.07 o 8 7 0 1201.08 1094.90 73.90 o 9 7 0 317.28 322.55 84.47 o 10 7 0 319.18 347.54 64.25 o 10 7 0 377.20 375.34 93.76 o -12 8 0 184.94 217.85 86.81 o -12 8 0 156.50 127.52 75.56 o -11 8 0 312.53 351.28 96.56 o -10 8 0 456.83 525.52 95.57 o -10 8 0 386.57 468.63 92.56 o -9 8 0 505.51 523.23 85.87 o -9 8 0 597.39 573.43 93.86 o -8 8 0 160.32 193.43 83.07 o -7 8 0 483.06 486.62 54.14 o -7 8 0 408.76 395.36 51.70 o -6 8 0 214.38 201.62 42.26 o -6 8 0 253.34 248.71 42.26 o -5 8 0 124.21 106.88 47.50 o -4 8 0 49.39 55.23 30.18 o -4 8 0 41.80 38.06 29.09 o -3 8 0 2.00 -0.57 26.97 o -3 8 0 2.36 5.60 25.10 o -2 8 0 1497.31 1328.67 67.57 o -1 8 0 124.09 113.77 30.80 o -1 8 0 105.00 113.98 31.32 o 0 8 0 1161.40 1304.30 62.07 o 0 8 0 982.77 1062.39 58.75 o 1 8 0 4531.18 4570.29 109.42 o 1 8 0 3614.27 4269.06 103.92 o 2 8 0 1423.94 1364.09 47.50 o 2 8 0 1204.93 1189.85 51.75 o 3 8 0 73.54 50.98 24.06 o 3 8 0 62.23 65.96 24.11 o 4 8 0 349.08 311.09 82.76 o 4 8 0 273.93 295.43 42.11 o 4 8 0 231.80 242.17 53.78 o 5 8 0 709.23 683.78 52.89 o 5 8 0 838.14 850.61 56.84 o 5 8 0 1097.66 1097.03 121.09 o 6 8 0 589.87 558.29 54.86 o 6 8 0 697.08 692.81 58.18 o 7 8 0 905.28 690.37 70.84 o 8 8 0 15.10 41.17 40.55 o 8 8 0 17.85 69.02 40.66 o 9 8 0 492.04 553.99 67.67 o 9 8 0 581.47 714.69 101.74 o 10 8 0 936.55 1074.68 138.92 o -11 9 0 197.94 15.25 42.89 o -11 9 0 9.70 46.05 70.27 o -10 9 0 203.41 122.54 101.12 o -9 9 0 651.17 673.52 118.96 o -8 9 0 1153.36 966.25 108.80 o -8 9 0 975.97 966.97 58.81 o -7 9 0 380.89 436.06 104.65 o -7 9 0 238.70 256.28 61.92 o -6 9 0 144.15 175.90 55.07 o -6 9 0 575.61 502.91 103.82 o -5 9 0 209.96 186.37 41.90 o -5 9 0 177.67 172.16 41.59 o -4 9 0 5.11 21.47 31.22 o -3 9 0 145.41 72.18 74.62 o -3 9 0 144.58 193.37 52.79 o -2 9 0 87.95 73.12 32.20 o -2 9 0 103.93 91.16 33.14 o -1 9 0 501.52 504.62 70.53 o -1 9 0 860.42 892.30 102.00 o 0 9 0 174.80 183.47 81.10 o 0 9 0 0.79 -11.62 36.66 o 1 9 0 369.70 357.76 46.05 o 1 9 0 436.90 375.70 46.77 o 2 9 0 777.49 721.07 102.62 o 2 9 0 776.64 649.77 74.00 o 2 9 0 657.19 737.25 81.93 o 3 9 0 1681.20 1569.44 123.37 o 3 9 0 1259.03 1329.66 93.71 o 4 9 0 499.39 531.64 54.81 o 4 9 0 590.16 579.60 55.43 o 5 9 0 3.34 15.04 43.97 o 5 9 0 12.90 1.45 87.85 o 6 9 0 596.74 634.78 100.34 o 7 9 0 462.85 463.65 83.64 o 7 9 0 391.66 397.64 80.53 o 8 9 0 205.46 275.77 81.73 o 8 9 0 173.86 240.93 76.28 o -10 10 0 77.10 142.55 80.01 o -10 10 0 91.11 145.51 77.06 o -9 10 0 4.31 34.85 66.38 o -9 10 0 5.09 34.12 62.85 o -8 10 0 723.57 902.26 119.84 o -7 10 0 1161.22 1124.41 75.14 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