#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203603.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203603_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Yokoyama, Yoshimi' 'Hama, Hideki' 'Kato, Kaoru' 'Ikuta, Yoshie' 'Tsubomura, Taro' 'Tanase, Tomoaki' _publ_section_title ; Bis[\m-3-(N'-methyl-4,4'-bipyridinium-1-yl)propionamidato]bis[cis-diammineplatinum(II)] hexaperchlorate dihydrate: a head-to-tail isomer ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m664 _journal_page_last m667 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.116 _cell_angle_beta 79.305 _cell_angle_gamma 74.210 _cell_length_a 10.0927 _cell_length_b 11.0827 _cell_length_c 24.4798 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.7689 _[local]_cod_data_source_file hb6032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mvc2 in P-1 2004/03/13 11:26:17 010 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 422.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35580.84 33876.52 598.04 o 2 0 0 62909.36 68313.44 1105.60 o 3 0 0 11491.43 12039.98 332.95 o 4 0 0 2799.14 3330.35 223.99 o 5 0 0 293.68 337.98 199.21 o 6 0 0 2112.62 2204.13 327.05 o 7 0 0 3333.94 3903.53 481.27 o 8 0 0 239.32 16.27 366.46 o 9 0 0 467.83 1185.11 751.01 o 10 0 0 37.56 -380.76 725.10 o 11 0 0 17.44 598.07 893.85 o 12 0 0 7.38 -445.76 1498.50 o -12 1 0 379.65 865.02 1126.18 o -11 1 0 1448.04 359.43 918.11 o -10 1 0 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6 28 116.98 303.49 1451.08 o -1 6 28 16.45 673.38 1451.08 o 0 6 28 53.57 -1507.98 1507.98 o 1 6 28 670.15 1223.46 1621.79 o 2 6 28 517.67 1441.59 1640.76 o 3 6 28 16.48 -588.02 1403.66 o 4 6 28 700.81 208.65 1564.89 o 5 6 28 808.18 1223.46 1517.47 o 6 6 28 97.86 -1022.42 1030.26 o 7 6 28 258.95 656.06 1156.13 o 8 6 28 439.24 2437.43 1944.26 o -1 7 28 67.34 -47.42 1697.67 o 0 7 28 128.26 -910.48 1754.57 o 1 7 28 0.44 493.18 1602.83 o 2 7 28 9.28 -758.73 1479.53 o 3 7 28 57.01 654.41 1659.73 o 4 7 28 91.84 -872.54 1612.31 o 5 7 28 21.09 113.81 1621.79 o 6 7 28 222.82 569.05 1593.34 o 7 7 28 256.27 544.00 1243.36 o 1 8 28 0.13 -1242.43 1773.54 o 2 8 28 360.46 -569.05 1688.18 o 3 8 28 420.83 -1005.32 1849.41 o 4 8 28 4.04 104.33 1839.93 o 5 8 28 11.88 1394.17 1735.60 o 6 8 28 9.13 -625.96 1602.83 o 3 9 28 196.99 -1820.96 1953.74 o 4 9 28 141.61 1289.85 2209.81 o 5 9 28 500.43 2380.53 1934.77 o 0 -3 29 192.19 180.20 1602.83 o 1 -3 29 149.33 -1545.92 1545.92 o -1 -2 29 184.27 1237.73 1012.28 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832.41 1451.08 1356.24 o 1 5 29 764.12 417.30 1517.47 o 2 5 29 46.05 654.41 1545.92 o 3 5 29 853.16 2646.08 1583.86 o 4 5 29 653.80 2257.23 1612.31 o 5 5 29 15.00 -425.35 1101.34 o 6 5 29 224.73 1473.93 1162.37 o 7 5 29 74.24 509.07 1327.78 o -1 6 29 161.87 1052.74 1441.59 o 0 6 29 343.87 1128.62 1659.73 o 1 6 29 26.70 -711.31 1574.37 o 2 6 29 730.04 1062.23 1593.34 o 3 6 29 789.21 -882.03 1697.67 o 4 6 29 94.74 18.97 1574.37 o 5 6 29 356.86 720.80 1745.09 o 6 6 29 1073.54 616.47 1688.18 o 7 6 29 150.41 876.44 1192.90 o 0 7 29 20.87 -616.47 1745.09 o 1 7 29 10.13 -578.53 1887.35 o 2 7 29 67.66 -417.30 1688.18 o 3 7 29 5.75 104.33 1764.06 o 4 7 29 54.77 -1583.86 1697.67 o 5 7 29 408.31 910.48 1707.15 o 6 7 29 134.65 910.48 1678.70 o 2 8 29 2.96 218.14 1839.93 o 3 8 29 65.91 -1062.23 1953.74 o 4 8 29 32.32 730.28 1934.77 o 5 8 29 17.79 -28.45 2010.64 o 0 -1 30 306.91 1644.96 1143.06 o 1 -1 30 345.94 1425.75 1119.41 o 2 -1 30 1.46 -85.36 1470.05 o 3 -1 30 295.71 -701.83 1517.47 o -1 0 30 48.35 1365.72 1697.67 o 0 0 30 16.14 1489.02 1574.37 o 1 0 30 2.35 1235.78 1021.78 o 2 0 30 16.58 966.13 1034.16 o 3 0 30 68.70 -66.39 1526.95 o 4 0 30 87.02 426.79 1536.44 o 5 0 30 14.03 113.81 1621.79 o -1 1 30 524.36 2797.83 1801.99 o 0 1 30 12.69 -47.42 1659.73 o 1 1 30 205.22 499.75 1030.26 o 2 1 30 548.27 -243.21 988.76 o 3 1 30 172.76 653.99 1063.98 o 4 1 30 93.13 -331.95 1574.37 o 5 1 30 85.20 1403.66 1650.25 o -1 2 30 25.08 331.95 1612.31 o 0 2 30 341.01 -237.10 1564.89 o 1 2 30 959.33 2598.66 1640.76 o 2 2 30 413.79 977.62 1096.10 o 3 2 30 114.63 -114.40 1084.78 o 4 2 30 861.22 -48.56 1089.64 o 5 2 30 432.46 -218.14 1555.40 o 6 2 30 9.63 -606.99 1621.79 o -1 3 30 2.47 -1470.05 1470.05 o 0 3 30 199.77 -1109.65 1384.69 o 1 3 30 105.82 2001.16 1688.18 o 2 3 30 71.64 -825.12 1944.26 o 3 3 30 746.23 1321.95 1079.47 o 4 3 30 581.72 1517.19 1026.65 o 5 3 30 1.82 -150.31 1082.68 o 6 3 30 284.68 616.47 1726.12 o -1 4 30 278.44 -104.33 1470.05 o 0 4 30 71.17 -1157.07 1564.89 o 1 4 30 46.60 227.62 1498.50 o 2 4 30 70.72 1280.36 1498.50 o 3 4 30 4.19 1005.32 1583.86 o 4 4 30 0.58 976.87 1716.64 o 5 4 30 68.60 -157.13 1143.90 o 6 4 30 64.40 641.15 1465.30 o 0 5 30 4.60 1612.31 1650.25 o 1 5 30 813.61 -322.46 1574.37 o 2 5 30 585.25 1783.02 1697.67 o 3 5 30 3.23 -360.40 1745.09 o 4 5 30 187.67 -75.87 1849.41 o 5 5 30 379.54 -1327.78 1612.31 o 6 5 30 6.11 610.57 1190.24 o 1 6 30 530.93 682.86 1754.57 o 2 6 30 99.37 208.65 1896.83 o 3 6 30 329.53 3006.48 1820.96 o 4 6 30 1282.16 379.37 1754.57 o 5 6 30 292.76 -275.04 1792.51 o 6 6 30 158.84 2314.14 1925.29 o 2 7 30 1.02 -512.15 1783.02 o 3 7 30 134.51 2968.55 1991.68 o 4 7 30 103.89 -1451.08 1839.93 o 5 7 30 45.46 -1109.65 1801.99 o 1 0 31 8.71 218.99 1150.00 o 2 0 31 3.96 -1139.84 1139.84 o 0 1 31 350.45 4495.50 2096.00 o 1 1 31 109.92 407.82 1564.89 o 2 1 31 26.08 -423.21 1503.24 o 3 1 31 171.58 -29.78 1152.55 o 4 1 31 4.21 -322.46 1688.18 o 0 2 31 161.30 625.96 1593.34 o 1 2 31 58.97 -218.14 1726.12 o 2 2 31 668.12 2295.17 1707.15 o 3 2 31 629.44 1913.50 1227.53 o 4 2 31 0.52 436.22 1716.64 o 0 3 31 29.82 -1498.50 1650.25 o 1 3 31 215.80 2105.49 1593.34 o 2 3 31 303.10 1659.73 1877.87 o 3 3 31 7.86 2418.46 1498.50 o 4 3 31 466.78 1580.48 1203.57 o 5 3 31 441.50 424.33 1211.12 o 1 4 31 3.71 1925.29 1991.68 o 2 4 31 1.33 -294.01 1451.08 o 3 4 31 10.26 891.51 1830.45 o 4 4 31 12.33 -208.65 1631.28 o 5 4 31 6.33 180.20 1745.09 o 1 5 31 3.98 -170.72 1688.18 o 2 5 31 294.98 -559.57 1612.31 o 3 5 31 349.74 1470.05 1830.45 o 4 5 31 97.18 2352.07 2124.45 o