#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/36/2203623.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203623_Fobs loop_ _publ_author_name 'Parrish, Damon' 'Chen, Weibin' 'Coop, Andrew' 'Deschamps, Jeffrey R.' _publ_section_title ; 7\b-Chloro-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o793 _journal_page_last o794 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7262 _cell_length_b 19.8316 _cell_length_c 23.6182 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 0.7484 _[local]_cod_data_source_file lh62003sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' coop14 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14516.82 14128.67 659.25 o 4 0 0 1408.50 1329.81 59.91 o 6 0 0 14.82 -2.01 24.21 o 8 0 0 5.43 23.15 40.04 o 1 1 0 7.68 8.12 3.18 o 2 1 0 109.80 106.96 12.89 o 3 1 0 1380.18 1395.58 42.42 o 4 1 0 721.77 621.70 29.10 o 5 1 0 23.43 35.94 14.00 o 6 1 0 983.18 1032.19 39.04 o 7 1 0 309.55 357.36 32.86 o 8 1 0 23.97 38.12 28.12 o 9 1 0 562.69 683.33 60.35 o 0 2 0 7047.60 6557.08 381.09 o 1 2 0 5630.79 5474.88 200.03 o 2 2 0 1770.77 1673.27 49.46 o 3 2 0 1489.73 1351.37 41.22 o 4 2 0 47.57 22.81 10.81 o 5 2 0 366.86 346.66 19.49 o 6 2 0 121.86 184.27 25.95 o 7 2 0 892.80 895.75 39.16 o 8 2 0 96.65 124.06 51.57 o 9 2 0 402.43 407.03 53.69 o 10 2 0 6.69 -28.84 94.22 o 1 3 0 12022.12 11698.47 390.25 o 2 3 0 1197.68 1275.54 44.42 o 3 3 0 46.93 62.03 10.60 o 4 3 0 3292.85 3661.72 114.28 o 5 3 0 3106.51 3083.18 98.27 o 6 3 0 1.93 1.03 23.73 o 7 3 0 575.00 501.95 37.07 o 8 3 0 98.71 102.86 38.53 o 9 3 0 2.03 11.00 47.86 o 10 3 0 81.35 164.66 63.51 o 0 4 0 344.40 446.31 29.67 o 1 4 0 31.25 64.04 17.60 o 2 4 0 2513.19 2218.50 82.59 o 3 4 0 194.10 193.01 12.65 o 4 4 0 549.49 529.76 28.43 o 5 4 0 666.75 640.87 33.52 o 6 4 0 26.13 40.11 23.39 o 7 4 0 6336.72 6022.81 204.34 o 8 4 0 213.97 254.37 43.83 o 9 4 0 98.21 27.56 49.13 o 10 4 0 42.15 -17.67 65.46 o 1 5 0 34953.76 34627.36 1006.35 o 2 5 0 327.36 376.17 23.02 o 3 5 0 7.72 26.59 10.67 o 4 5 0 160.25 180.10 15.62 o 5 5 0 101.43 97.81 25.38 o 6 5 0 3961.99 3918.03 147.65 o 7 5 0 208.01 183.23 40.21 o 8 5 0 2.65 64.40 34.88 o 9 5 0 0.01 -47.00 47.00 o 10 5 0 25.28 102.33 81.05 o 0 6 0 12675.12 11761.13 683.05 o 1 6 0 547.56 555.22 30.89 o 2 6 0 255.46 242.87 14.16 o 3 6 0 2970.83 3169.60 107.36 o 4 6 0 1381.81 1445.76 53.27 o 5 6 0 562.58 521.69 40.99 o 6 6 0 38.39 28.88 29.56 o 7 6 0 2031.20 1904.22 128.20 o 8 6 0 0.75 31.26 38.04 o 9 6 0 595.10 665.33 58.67 o 10 6 0 27.07 7.49 62.99 o 1 7 0 1769.58 1806.90 62.75 o 2 7 0 676.71 899.99 44.92 o 3 7 0 0.66 -8.41 13.62 o 4 7 0 1953.13 2075.35 80.06 o 5 7 0 912.98 990.81 46.96 o 6 7 0 828.99 810.34 55.17 o 7 7 0 601.54 644.15 51.88 o 8 7 0 439.64 514.14 68.28 o 9 7 0 25.07 -14.70 48.46 o 0 8 0 87255.97 88903.34 5151.79 o 1 8 0 10298.15 10002.78 338.19 o 2 8 0 226.79 163.94 13.72 o 3 8 0 1971.02 2395.02 90.54 o 4 8 0 754.69 740.75 33.69 o 5 8 0 19.23 2.16 33.52 o 6 8 0 7.72 -30.63 64.23 o 7 8 0 167.13 84.35 64.25 o 8 8 0 3.76 -45.08 45.08 o 9 8 0 17.68 30.12 50.52 o 1 9 0 7.44 4.45 11.38 o 2 9 0 794.45 724.33 34.20 o 3 9 0 62.29 83.32 15.67 o 4 9 0 1154.49 1157.08 55.77 o 5 9 0 24.41 23.12 25.42 o 6 9 0 44.10 39.93 31.39 o 7 9 0 74.51 121.96 39.97 o 8 9 0 84.29 63.45 48.30 o 9 9 0 91.96 44.35 49.62 o 0 10 0 2170.15 2702.18 160.36 o 1 10 0 269.45 310.94 18.58 o 2 10 0 3290.51 3692.53 124.75 o 3 10 0 1853.94 1697.35 87.35 o 4 10 0 923.48 898.85 54.98 o 5 10 0 206.61 171.62 29.36 o 6 10 0 406.23 407.51 60.91 o 7 10 0 312.00 297.50 43.10 o 8 10 0 8.63 23.91 55.31 o 9 10 0 313.15 179.65 55.37 o 1 11 0 3544.61 3530.36 132.47 o 2 11 0 1852.71 1945.31 84.48 o 3 11 0 123.06 75.17 27.73 o 4 11 0 1996.66 2101.68 105.84 o 5 11 0 1311.91 1550.09 115.64 o 6 11 0 489.76 438.10 41.07 o 7 11 0 21.02 -40.70 40.70 o 8 11 0 240.54 210.77 63.53 o 9 11 0 21.77 54.95 56.44 o 0 12 0 7.09 21.75 18.77 o 1 12 0 178.62 239.62 25.01 o 2 12 0 19.60 57.23 19.18 o 3 12 0 273.13 314.77 33.10 o 4 12 0 670.42 642.57 47.34 o 5 12 0 30.70 25.96 28.08 o 6 12 0 587.97 574.76 99.70 o 7 12 0 15.26 -1.98 54.81 o 8 12 0 2.42 -36.08 50.84 o 1 13 0 2991.60 3214.25 122.34 o 2 13 0 842.51 788.21 44.36 o 3 13 0 81.05 64.74 30.19 o 4 13 0 1831.39 1592.95 106.03 o 5 13 0 34.89 5.49 30.13 o 6 13 0 272.37 309.24 43.54 o 7 13 0 3.44 44.77 49.51 o 8 13 0 28.05 60.16 69.24 o 0 14 0 1865.84 1844.08 95.63 o 1 14 0 2079.08 2051.64 90.52 o 2 14 0 0.43 25.46 24.64 o 3 14 0 1464.54 1419.28 94.91 o 4 14 0 238.95 183.70 35.65 o 5 14 0 1443.07 1353.26 79.68 o 6 14 0 74.77 56.55 37.51 o 7 14 0 59.93 141.18 45.86 o 8 14 0 43.16 76.66 66.01 o 1 15 0 449.24 513.91 52.04 o 2 15 0 405.41 388.87 33.24 o 3 15 0 554.82 539.37 47.56 o 4 15 0 1036.18 971.48 146.81 o 5 15 0 2732.94 2419.75 124.72 o 6 15 0 131.84 74.96 38.58 o 7 15 0 81.48 90.32 49.97 o 8 15 0 132.21 28.67 58.54 o 0 16 0 1505.95 1354.62 76.76 o 1 16 0 200.35 198.09 25.34 o 2 16 0 241.79 221.93 31.00 o 3 16 0 1495.89 1490.69 248.45 o 4 16 0 159.11 68.41 84.75 o 5 16 0 53.71 72.73 38.62 o 6 16 0 60.41 80.71 41.62 o 7 16 0 14.83 75.08 53.89 o 1 17 0 42.20 76.25 26.20 o 2 17 0 345.19 295.16 34.45 o 3 17 0 281.39 299.77 41.91 o 4 17 0 43.79 -44.23 44.23 o 5 17 0 158.62 131.07 56.52 o 6 17 0 0.20 -26.10 42.30 o 7 17 0 296.94 378.22 61.19 o 0 18 0 3075.91 2982.95 151.40 o 1 18 0 832.79 879.02 64.24 o 2 18 0 79.65 101.79 33.53 o 3 18 0 1089.47 1084.19 88.01 o 4 18 0 713.05 720.88 67.85 o 5 18 0 83.23 21.76 43.77 o 6 18 0 31.62 1.11 50.07 o 7 18 0 35.10 7.96 56.05 o 1 19 0 562.10 663.76 40.08 o 2 19 0 780.43 757.68 55.86 o 3 19 0 110.08 92.02 45.96 o 4 19 0 15.24 -23.31 47.94 o 5 19 0 2.54 45.49 47.25 o 6 19 0 6.41 -20.88 51.65 o 0 20 0 221.26 312.44 50.98 o 1 20 0 55.56 12.60 33.22 o 2 20 0 244.91 289.23 41.76 o 3 20 0 0.09 -7.99 70.16 o 4 20 0 0.01 -52.00 52.00 o 5 20 0 199.37 209.07 53.09 o 6 20 0 187.59 160.48 56.63 o 1 21 0 652.50 681.53 46.36 o 2 21 0 481.75 484.50 56.63 o 3 21 0 236.09 297.96 54.93 o 4 21 0 2.33 43.72 69.90 o 5 21 0 150.35 135.56 55.16 o 6 21 0 280.58 266.31 62.20 o 0 22 0 926.71 971.04 164.46 o 1 22 0 153.11 277.59 40.50 o 2 22 0 13.79 9.60 58.74 o 3 22 0 312.65 145.25 56.73 o 4 22 0 4.87 1.80 61.92 o 5 22 0 778.54 794.23 70.22 o 1 23 0 3.84 -4.09 41.74 o 2 23 0 54.38 36.05 49.17 o 3 23 0 189.37 176.24 63.26 o 4 23 0 234.59 315.27 82.90 o 5 23 0 46.69 10.52 59.11 o 0 24 0 1052.86 1493.86 175.87 o 1 24 0 138.57 197.26 75.38 o 2 24 0 190.97 118.01 83.66 o 3 24 0 2.99 -21.34 65.71 o 4 24 0 80.65 55.38 71.09 o 1 25 0 4.10 152.28 81.87 o 2 25 0 271.40 232.09 85.47 o 0 26 0 524.47 720.29 141.46 o 1 26 0 15.14 41.10 91.19 o 1 0 1 4226.66 4104.69 125.69 o 2 0 1 1884.77 1950.32 61.08 o 3 0 1 518.15 639.52 39.32 o 4 0 1 709.91 856.43 40.08 o 5 0 1 225.94 235.76 17.14 o 6 0 1 17.03 22.48 17.91 o 7 0 1 801.45 819.18 36.29 o 8 0 1 9.41 -6.37 27.65 o 9 0 1 344.14 431.95 56.12 o -9 1 1 8.80 -28.56 56.91 o -8 1 1 30.70 -20.09 28.66 o -7 1 1 681.90 635.03 30.26 o -6 1 1 2005.49 2019.00 62.06 o -5 1 1 54.88 48.29 19.57 o -4 1 1 768.38 755.21 27.04 o -3 1 1 4190.48 4088.66 127.07 o -2 1 1 3229.47 2986.09 98.86 o -1 1 1 15523.73 15487.86 473.30 o 0 1 1 542.06 -2.04 4.59 o 1 1 1 15755.85 15315.09 626.93 o 2 1 1 3184.22 2944.43 86.10 o 3 1 1 4199.06 4120.51 119.06 o 4 1 1 746.82 750.95 29.72 o 5 1 1 61.15 34.90 14.72 o 6 1 1 1966.21 1891.16 62.32 o 7 1 1 684.80 665.62 31.33 o 8 1 1 32.02 -31.07 31.07 o 9 1 1 9.15 -27.78 60.81 o -10 2 1 16.83 234.11 125.27 o -9 2 1 11.69 -30.92 49.74 o -8 2 1 221.27 233.55 42.49 o -7 2 1 853.20 885.74 38.30 o -6 2 1 183.79 192.03 23.12 o -5 2 1 2184.45 2156.41 67.13 o -4 2 1 194.77 191.14 14.55 o -3 2 1 90.83 119.61 9.06 o -2 2 1 434.09 435.62 17.94 o -1 2 1 374.53 374.84 13.29 o 0 2 1 19311.70 19433.50 1117.19 o 1 2 1 386.18 378.96 19.65 o 2 2 1 413.54 463.35 18.49 o 3 2 1 88.49 80.96 11.80 o 4 2 1 175.02 181.55 15.58 o 5 2 1 2170.55 2219.82 71.16 o 6 2 1 188.50 199.70 23.40 o 7 2 1 864.43 810.76 43.03 o 8 2 1 224.76 203.21 33.45 o 9 2 1 11.18 -22.38 45.25 o 10 2 1 17.23 -139.04 139.04 o -10 3 1 107.39 164.77 158.41 o -9 3 1 210.83 289.56 51.66 o -8 3 1 203.06 241.90 36.64 o -7 3 1 1041.80 1137.28 69.10 o -6 3 1 5934.22 5662.30 165.06 o -5 3 1 1165.81 1182.15 43.56 o -4 3 1 369.45 395.02 17.23 o -3 3 1 149.31 108.84 9.67 o -2 3 1 589.56 637.45 21.03 o -1 3 1 11801.39 11493.10 421.68 o 0 3 1 5952.67 5893.48 278.70 o 1 3 1 11909.97 11604.96 421.66 o 2 3 1 593.22 594.55 26.27 o 3 3 1 161.86 157.78 21.50 o 4 3 1 356.46 360.78 19.76 o 5 3 1 1165.58 1169.37 51.20 o 6 3 1 5945.59 5623.65 208.99 o 7 3 1 1013.72 1034.84 64.31 o 8 3 1 211.93 169.22 56.23 o 9 3 1 205.48 183.14 47.31 o 10 3 1 105.10 121.62 63.91 o -10 4 1 4.93 -17.86 63.02 o -9 4 1 55.31 89.21 47.44 o -8 4 1 95.50 133.70 38.74 o -7 4 1 14.23 38.20 38.69 o -6 4 1 440.78 544.78 32.45 o -5 4 1 2337.06 2454.23 85.78 o -4 4 1 2515.94 2657.59 90.35 o -3 4 1 1872.93 1771.20 62.41 o -2 4 1 179.83 181.02 11.09 o -1 4 1 1775.33 1553.18 54.74 o 0 4 1 8608.73 8243.05 300.87 o 1 4 1 1847.28 1621.21 54.11 o 2 4 1 183.92 255.09 26.65 o 3 4 1 1882.15 1828.68 68.39 o 4 4 1 2506.17 2604.44 98.77 o 5 4 1 2395.29 2463.17 86.23 o 6 4 1 429.83 480.50 39.94 o 7 4 1 14.78 -12.94 29.08 o 8 4 1 96.97 149.21 67.01 o 9 4 1 56.46 47.05 54.58 o 10 4 1 3.96 -18.07 63.59 o -10 5 1 41.21 -14.74 64.21 o -9 5 1 18.47 -44.62 48.54 o -8 5 1 416.14 397.30 43.51 o -7 5 1 1631.38 1508.34 75.92 o -6 5 1 7215.89 7050.85 256.46 o -5 5 1 1672.09 1574.96 59.26 o -4 5 1 102.46 195.43 20.04 o -3 5 1 2000.70 2068.28 70.16 o -2 5 1 537.11 516.01 27.18 o -1 5 1 2389.46 2347.87 79.79 o 0 5 1 11390.15 11168.57 407.73 o 1 5 1 2356.89 2329.58 79.17 o 2 5 1 512.71 512.81 21.95 o 3 5 1 2001.45 1987.11 76.52 o 4 5 1 96.88 157.22 24.63 o 5 5 1 1669.73 1615.81 59.29 o 6 5 1 7147.29 6893.27 256.47 o 7 5 1 1661.22 1483.78 86.57 o 8 5 1 404.13 430.67 42.05 o 9 5 1 17.38 -27.64 50.33 o 10 5 1 38.37 21.35 72.31 o -10 6 1 77.15 69.87 64.77 o -9 6 1 38.45 68.71 48.71 o -8 6 1 700.10 735.11 51.56 o -7 6 1 257.73 248.67 49.58 o -6 6 1 1056.46 1068.61 58.85 o -5 6 1 899.84 869.41 39.17 o -4 6 1 481.02 450.19 23.22 o -3 6 1 4982.91 5278.32 173.98 o -2 6 1 239.17 223.83 14.36 o -1 6 1 2318.46 2398.50 82.49 o 0 6 1 518.82 533.31 22.90 o 1 6 1 2316.88 2428.42 76.47 o 2 6 1 255.48 264.86 17.46 o 3 6 1 4974.58 5060.55 213.18 o 4 6 1 471.80 487.72 27.30 o 5 6 1 889.01 902.35 43.47 o 6 6 1 1042.33 1037.65 56.59 o 7 6 1 266.18 296.07 39.27 o 8 6 1 698.28 643.94 61.64 o 9 6 1 37.54 8.92 70.25 o 10 6 1 79.16 118.13 62.61 o -9 7 1 0.08 -36.35 49.02 o -8 7 1 16.89 -1.60 39.77 o -7 7 1 1234.33 1239.94 79.36 o -6 7 1 933.15 964.34 60.93 o -5 7 1 544.67 594.18 36.10 o -4 7 1 1778.19 1786.39 64.36 o -3 7 1 3.98 4.23 11.95 o -2 7 1 1426.80 1443.67 56.75 o -1 7 1 3678.24 3639.11 122.19 o 0 7 1 702.34 694.56 48.04 o 1 7 1 3658.86 3565.49 113.21 o 2 7 1 1449.65 1484.71 52.01 o 3 7 1 6.36 26.15 15.13 o 4 7 1 1785.25 1822.45 70.62 o 5 7 1 542.53 554.55 31.62 o 6 7 1 982.89 832.18 60.53 o 7 7 1 1221.08 1287.19 79.11 o 8 7 1 19.11 51.49 51.01 o 9 7 1 0.12 6.52 50.60 o -9 8 1 22.99 1.85 67.18 o -8 8 1 37.49 -35.79 54.80 o -7 8 1 235.90 243.56 40.49 o -6 8 1 490.91 525.65 79.59 o -5 8 1 1063.98 1101.85 60.32 o -4 8 1 475.23 526.19 26.27 o -3 8 1 2900.00 3109.20 105.92 o -2 8 1 5323.15 5406.73 199.22 o -1 8 1 3012.43 3113.89 105.38 o 0 8 1 962.01 856.19 38.84 o 1 8 1 2942.86 3065.18 97.62 o 2 8 1 5310.64 5430.98 182.40 o 3 8 1 2902.82 3133.95 129.76 o 4 8 1 470.84 515.02 27.05 o 5 8 1 1063.24 972.87 139.55 o 6 8 1 486.53 543.11 44.45 o 7 8 1 232.87 204.66 40.62 o 8 8 1 37.46 10.80 46.01 o 9 8 1 23.56 -42.81 49.89 o -9 9 1 15.81 -31.93 52.00 o -8 9 1 11.13 -6.04 46.86 o -7 9 1 277.13 281.78 41.03 o -6 9 1 530.04 501.92 41.09 o -5 9 1 146.93 130.02 36.03 o -4 9 1 433.03 436.26 29.64 o -3 9 1 2967.89 2961.73 113.46 o -2 9 1 1374.70 1300.05 59.04 o -1 9 1 3447.17 3773.82 128.30 o 0 9 1 459.67 858.93 96.12 o 1 9 1 3523.23 3758.26 128.80 o 2 9 1 1382.73 1338.66 52.85 o 3 9 1 2975.54 3087.44 126.16 o 4 9 1 426.65 402.38 35.43 o 5 9 1 155.78 113.63 27.93 o 6 9 1 512.36 493.71 41.28 o 7 9 1 275.63 186.35 41.68 o 8 9 1 10.62 -13.66 48.58 o 9 9 1 15.18 19.41 53.09 o -9 10 1 259.66 184.37 55.09 o -8 10 1 116.64 110.17 51.22 o -7 10 1 248.63 218.92 72.51 o -6 10 1 291.87 220.89 34.77 o -5 10 1 3040.39 2817.61 136.67 o -4 10 1 29.37 62.28 23.32 o -3 10 1 380.45 387.22 28.14 o -2 10 1 310.37 332.54 25.19 o -1 10 1 3893.28 3851.27 169.90 o 0 10 1 4350.79 4920.71 205.15 o 1 10 1 4028.64 4266.11 152.52 o 2 10 1 299.13 334.67 19.92 o 3 10 1 390.86 310.18 32.76 o 4 10 1 34.34 77.62 29.83 o 5 10 1 3037.06 2732.42 137.15 o 6 10 1 292.41 262.20 42.04 o 7 10 1 246.18 331.48 43.78 o 8 10 1 114.40 54.99 51.23 o 9 10 1 255.20 314.97 173.03 o -9 11 1 175.74 310.64 57.76 o -8 11 1 107.54 246.61 76.81 o -7 11 1 542.00 524.87 51.91 o -6 11 1 403.57 379.50 39.98 o -5 11 1 26.47 -18.21 27.39 o -4 11 1 225.63 225.36 25.06 o -3 11 1 574.19 536.38 40.09 o -2 11 1 1079.32 1121.56 51.29 o -1 11 1 3614.98 3660.39 136.72 o 0 11 1 651.46 839.23 34.44 o 1 11 1 3544.18 3616.21 136.95 o 2 11 1 1049.09 988.79 50.34 o 3 11 1 581.76 612.80 49.41 o 4 11 1 234.58 253.33 33.14 o 5 11 1 27.15 6.14 36.52 o 6 11 1 392.07 429.05 41.46 o 7 11 1 542.31 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