#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/36/2203693.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203693_Fobs loop_ _publ_author_name 'Blake, Alexander J.' 'Lippolis, Vito' 'Schr\"oder, Martin' _publ_section_title ; 10,13-Bis(p-tolylsulfonyl)-1,4,7-trithia-10,13-diazacyclopentadecane ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o901 _journal_page_last o903 _journal_volume 60 _journal_year 2004 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.3770 _cell_length_b 12.3770 _cell_length_c 18.2960 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.8381 _[local]_cod_data_source_file ya6205Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' N2S3TS #433 for VL/MS in P 41 21 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 217.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 136.52 204.25 16.67 o 1 2 0 0.29 4.87 9.52 o 2 2 0 47417.47 43586.24 449.55 o 1 3 0 21112.58 20704.46 888.85 o 2 3 0 604.70 462.52 23.19 o 3 3 0 10.33 23.06 21.48 o 0 4 0 439.65 523.51 28.66 o 1 4 0 1115.97 1023.48 57.34 o 2 4 0 7887.88 7743.72 480.49 o 3 4 0 21.78 -14.86 12.67 o 4 4 0 38.36 52.65 22.70 o 1 5 0 2494.98 2460.38 35.79 o 2 5 0 4854.98 4912.91 310.50 o 3 5 0 1704.14 1699.15 106.84 o 4 5 0 185.26 289.58 28.35 o 5 5 0 2740.87 2599.51 69.02 o 0 6 0 9007.33 9408.76 99.13 o 1 6 0 954.93 1088.32 30.19 o 2 6 0 3115.46 2994.75 166.90 o 3 6 0 1900.74 1963.78 121.90 o 4 6 0 324.92 380.62 27.18 o 5 6 0 4121.33 4047.72 94.95 o 6 6 0 48.81 49.59 26.57 o 1 7 0 1081.34 1296.05 33.00 o 2 7 0 266.54 268.01 22.85 o 3 7 0 288.18 269.57 24.92 o 4 7 0 705.53 709.97 30.79 o 5 7 0 198.19 197.00 21.64 o 6 7 0 403.07 343.64 27.76 o 7 7 0 1017.77 981.16 55.12 o 0 8 0 2910.89 3074.83 69.43 o 1 8 0 51.66 -38.24 19.12 o 2 8 0 1194.07 1280.81 28.92 o 3 8 0 0.05 31.86 15.75 o 4 8 0 177.32 230.14 26.66 o 5 8 0 18.21 -30.81 15.93 o 6 8 0 4.27 -10.20 43.73 o 7 8 0 4.60 -20.25 57.17 o 8 8 0 126.05 168.22 39.00 o 1 9 0 304.68 316.85 25.19 o 2 9 0 71.21 94.74 28.51 o 3 9 0 100.57 103.00 18.04 o 4 9 0 2411.18 2402.07 144.35 o 5 9 0 119.81 131.59 32.11 o 6 9 0 493.10 539.04 26.93 o 7 9 0 61.84 65.77 20.83 o 8 9 0 104.93 113.74 22.07 o 9 9 0 1.24 8.11 33.86 o 0 10 0 937.36 976.23 52.51 o 1 10 0 125.74 190.44 25.18 o 2 10 0 28.67 7.09 16.89 o 3 10 0 75.71 40.03 22.82 o 4 10 0 460.23 532.72 25.29 o 5 10 0 299.31 263.82 31.59 o 6 10 0 89.51 41.47 38.43 o 7 10 0 55.22 -1.86 21.21 o 8 10 0 25.36 41.44 37.42 o 9 10 0 34.97 47.39 23.44 o 10 10 0 5.09 88.71 40.50 o 1 11 0 355.56 394.29 52.43 o 2 11 0 241.82 216.00 32.84 o 3 11 0 4.69 -27.41 37.98 o 4 11 0 3.21 12.54 23.50 o 5 11 0 29.29 21.01 20.57 o 6 11 0 79.43 55.38 78.38 o 7 11 0 6.96 52.20 36.26 o 8 11 0 85.72 154.69 55.18 o 9 11 0 0.84 39.41 22.53 o 0 12 0 363.11 400.05 45.44 o 1 12 0 0.44 -5.67 44.66 o 2 12 0 15.98 26.24 19.49 o 3 12 0 0.33 -31.46 19.54 o 4 12 0 12.76 -33.68 37.09 o 5 12 0 3.66 -42.35 38.76 o 6 12 0 35.90 43.07 26.41 o 7 12 0 98.40 101.49 23.89 o 8 12 0 0.96 7.85 22.68 o 1 13 0 0.67 -47.42 23.71 o 2 13 0 32.04 55.64 19.83 o 3 13 0 0.29 1.23 27.56 o 4 13 0 67.84 89.81 21.63 o 5 13 0 38.31 -1.51 22.02 o 6 13 0 62.59 122.56 59.90 o 0 14 0 20.74 -64.22 36.43 o 1 14 0 21.03 29.53 52.04 o 2 14 0 92.95 131.94 27.21 o 3 14 0 6.91 -51.03 47.14 o 4 14 0 0.16 -2.58 42.03 o 1 1 1 1424.28 1390.82 22.70 o 0 2 1 3180.26 3276.33 36.83 o 1 2 1 8921.00 8836.36 186.59 o 2 2 1 10568.59 10275.79 131.51 o 0 3 1 18302.09 18614.41 107.67 o 1 3 1 7562.78 8106.57 380.54 o 2 3 1 1397.30 1469.16 74.04 o 3 3 1 82.46 65.82 22.86 o 0 4 1 5310.49 5284.18 62.37 o 1 4 1 8469.53 9148.68 244.45 o 2 4 1 2208.78 2432.07 165.74 o 3 4 1 481.20 473.50 28.82 o 4 4 1 25.85 -25.63 22.62 o 0 5 1 2476.51 2492.16 51.04 o 1 5 1 2955.48 2991.16 48.59 o 2 5 1 3438.35 3432.81 295.33 o 3 5 1 1184.62 1176.49 26.68 o 4 5 1 336.74 352.50 17.79 o 5 5 1 16.54 43.56 24.16 o 0 6 1 381.37 230.70 45.33 o 1 6 1 3988.69 4035.98 48.27 o 2 6 1 3227.86 3009.64 215.22 o 3 6 1 889.26 873.54 63.35 o 4 6 1 813.22 697.97 23.23 o 5 6 1 134.67 124.25 35.94 o 6 6 1 23.45 31.09 25.67 o 0 7 1 4297.85 4883.03 80.33 o 1 7 1 240.01 232.23 51.86 o 2 7 1 2583.58 2527.39 180.47 o 3 7 1 369.64 383.12 50.50 o 4 7 1 714.69 652.71 37.91 o 5 7 1 21.54 26.76 14.63 o 6 7 1 288.53 225.63 25.68 o 7 7 1 1073.09 936.17 53.81 o 0 8 1 82.66 107.58 28.65 o 1 8 1 389.50 361.02 24.55 o 2 8 1 303.27 265.27 19.00 o 3 8 1 606.86 582.63 86.58 o 4 8 1 31.85 53.34 25.82 o 5 8 1 149.20 160.30 23.20 o 6 8 1 845.03 856.16 37.31 o 7 8 1 274.85 315.14 26.63 o 8 8 1 20.54 -4.24 32.31 o 0 9 1 89.36 45.03 30.64 o 1 9 1 948.67 992.30 34.77 o 2 9 1 7.79 24.34 21.63 o 3 9 1 223.50 229.30 19.79 o 4 9 1 77.31 74.93 19.09 o 5 9 1 504.62 466.37 33.62 o 6 9 1 38.82 -23.93 19.05 o 7 9 1 382.00 325.33 39.54 o 8 9 1 129.69 107.06 30.44 o 9 9 1 129.03 318.96 40.18 o 0 10 1 168.81 213.30 35.78 o 1 10 1 235.64 300.43 32.40 o 2 10 1 120.42 150.39 44.09 o 3 10 1 0.48 52.92 28.46 o 4 10 1 62.94 54.50 45.93 o 5 10 1 88.88 44.12 33.78 o 6 10 1 5.22 -13.82 18.87 o 7 10 1 193.40 143.19 26.98 o 8 10 1 4.96 20.07 20.31 o 9 10 1 20.78 63.19 25.88 o 10 10 1 164.53 106.16 46.33 o 0 11 1 12.84 142.01 32.27 o 1 11 1 14.84 20.00 22.82 o 2 11 1 218.83 202.62 22.63 o 3 11 1 199.18 188.62 20.43 o 4 11 1 192.60 202.09 26.17 o 5 11 1 273.34 308.70 24.29 o 6 11 1 14.51 -12.80 26.88 o 7 11 1 9.55 42.12 56.00 o 8 11 1 41.72 15.45 22.22 o 9 11 1 19.05 -3.31 39.68 o 0 12 1 4.63 -3.42 34.11 o 1 12 1 1.73 -17.07 25.82 o 2 12 1 17.69 -21.40 19.21 o 3 12 1 30.23 -0.11 23.79 o 4 12 1 49.17 -2.94 20.41 o 5 12 1 63.38 41.34 21.65 o 6 12 1 127.07 116.15 45.08 o 7 12 1 64.80 7.97 28.71 o 8 12 1 22.29 -52.35 40.54 o 0 13 1 99.64 154.00 38.59 o 1 13 1 60.99 90.92 41.59 o 2 13 1 42.76 14.77 39.21 o 3 13 1 13.16 0.07 24.06 o 4 13 1 18.73 -11.95 20.90 o 5 13 1 41.12 36.25 40.18 o 6 13 1 18.19 16.82 55.11 o 0 14 1 18.35 87.33 40.06 o 1 14 1 64.70 20.01 31.36 o 2 14 1 100.50 106.88 45.36 o 3 14 1 5.80 56.00 21.82 o 4 14 1 78.08 115.60 29.63 o 0 1 2 87.99 95.01 13.21 o 1 1 2 1408.88 1306.45 25.10 o 0 2 2 3008.97 2912.75 38.06 o 1 2 2 13897.43 13724.18 165.83 o 2 2 2 328.65 409.02 23.65 o 0 3 2 10688.89 11045.17 81.19 o 1 3 2 4228.37 4435.41 123.87 o 2 3 2 3934.87 3735.58 40.42 o 3 3 2 1105.31 1088.03 36.22 o 0 4 2 1.07 -44.66 22.33 o 1 4 2 6148.97 6012.74 194.37 o 2 4 2 2490.26 2606.27 37.26 o 3 4 2 868.43 924.43 28.04 o 4 4 2 217.54 205.41 26.61 o 0 5 2 1062.72 940.51 37.64 o 1 5 2 1479.66 1568.31 30.70 o 2 5 2 553.63 515.33 18.28 o 3 5 2 1472.98 1579.77 77.22 o 4 5 2 130.53 192.16 30.57 o 5 5 2 505.58 487.31 34.77 o 0 6 2 294.66 247.64 30.04 o 1 6 2 4723.18 4906.99 53.26 o 2 6 2 1546.68 1490.06 63.98 o 3 6 2 56.46 104.14 42.54 o 4 6 2 1816.85 1826.32 90.43 o 5 6 2 593.37 587.56 52.30 o 6 6 2 316.79 270.74 33.58 o 0 7 2 1.24 152.65 28.65 o 1 7 2 9.24 49.61 18.22 o 2 7 2 256.01 246.11 55.71 o 3 7 2 224.89 180.72 43.15 o 4 7 2 281.76 257.09 18.92 o 5 7 2 247.48 184.88 18.21 o 6 7 2 281.37 286.51 26.93 o 7 7 2 522.10 459.31 43.77 o 0 8 2 717.31 739.60 40.85 o 1 8 2 718.58 761.70 29.38 o 2 8 2 15.04 24.41 15.68 o 3 8 2 1326.08 1185.46 64.71 o 4 8 2 625.12 613.96 93.13 o 5 8 2 87.12 36.93 28.65 o 6 8 2 929.07 828.71 29.97 o 7 8 2 233.47 232.12 22.95 o 8 8 2 95.53 62.84 36.19 o 0 9 2 305.29 225.54 35.74 o 1 9 2 348.05 363.40 27.07 o 2 9 2 239.77 264.89 45.64 o 3 9 2 146.21 71.31 23.22 o 4 9 2 100.45 71.47 22.07 o 5 9 2 236.25 162.59 33.42 o 6 9 2 560.33 551.99 27.62 o 7 9 2 147.33 153.76 23.73 o 8 9 2 227.84 218.70 23.99 o 9 9 2 55.40 -58.44 35.62 o 0 10 2 325.10 328.12 39.21 o 1 10 2 245.96 276.90 60.11 o 2 10 2 22.62 48.74 22.77 o 3 10 2 74.15 38.67 34.53 o 4 10 2 87.43 121.73 20.12 o 5 10 2 21.53 10.20 19.23 o 6 10 2 28.93 35.40 19.23 o 7 10 2 246.97 232.77 25.21 o 8 10 2 225.28 213.99 24.12 o 9 10 2 35.75 -24.98 36.25 o 10 10 2 18.33 32.19 41.85 o 0 11 2 10.55 32.52 32.80 o 1 11 2 146.77 213.15 26.21 o 2 11 2 234.10 137.29 30.24 o 3 11 2 36.01 31.78 44.06 o 4 11 2 66.38 71.37 47.20 o 5 11 2 6.38 -39.34 19.67 o 6 11 2 82.41 44.63 29.11 o 7 11 2 18.56 30.44 25.56 o 8 11 2 28.27 27.62 21.78 o 9 11 2 25.06 105.83 24.04 o 0 12 2 3.94 -33.29 33.13 o 1 12 2 354.13 437.74 49.72 o 2 12 2 91.34 120.47 31.21 o 3 12 2 128.55 203.16 42.55 o 4 12 2 78.07 103.31 34.09 o 5 12 2 3.31 10.76 21.73 o 6 12 2 2.80 -12.17 21.03 o 7 12 2 0.95 -5.53 74.75 o 8 12 2 45.24 -20.10 23.95 o 0 13 2 1.09 79.13 35.00 o 1 13 2 82.55 87.27 67.85 o 2 13 2 68.00 81.48 21.30 o 3 13 2 69.91 68.61 26.21 o 4 13 2 2.53 -18.67 22.82 o 5 13 2 32.61 -50.11 59.90 o 6 13 2 10.80 -22.25 37.41 o 0 14 2 0.46 -38.14 36.67 o 1 14 2 27.97 59.11 28.29 o 2 14 2 19.11 13.81 29.00 o 3 14 2 9.77 16.50 22.09 o 4 14 2 13.64 12.24 38.66 o 0 1 3 13806.58 13866.03 76.50 o 1 1 3 30637.30 31645.71 135.24 o 0 2 3 3133.69 3002.24 41.19 o 1 2 3 4429.45 4245.55 100.21 o 2 2 3 5349.88 5294.10 59.19 o 0 3 3 2041.13 2120.63 40.73 o 1 3 3 2265.86 2182.89 85.53 o 2 3 3 714.71 652.95 17.28 o 3 3 3 94.72 114.92 22.86 o 0 4 3 7756.65 7624.91 78.21 o 1 4 3 621.64 742.08 56.76 o 2 4 3 1362.83 1234.08 22.06 o 3 4 3 1613.02 1472.63 44.61 o 4 4 3 817.90 795.16 35.88 o 0 5 3 5370.83 5624.18 74.16 o 1 5 3 3830.15 3937.85 139.68 o 2 5 3 68.62 153.75 21.38 o 3 5 3 2176.55 2562.09 39.73 o 4 5 3 1759.13 1660.90 29.88 o 5 5 3 494.67 518.11 35.83 o 0 6 3 1391.69 1569.69 47.23 o 1 6 3 3221.80 3583.26 47.50 o 2 6 3 750.73 864.18 22.84 o 3 6 3 736.31 680.58 34.35 o 4 6 3 16.11 53.33 14.74 o 5 6 3 699.69 655.07 41.06 o 6 6 3 682.93 638.15 40.44 o 0 7 3 63.07 -26.20 26.49 o 1 7 3 1703.42 1726.65 37.14 o 2 7 3 152.06 113.48 16.13 o 3 7 3 3013.23 2967.07 67.79 o 4 7 3 609.72 613.69 74.57 o 5 7 3 0.03 8.51 16.61 o 6 7 3 842.24 837.87 28.84 o 7 7 3 394.09 367.78 41.69 o 0 8 3 235.55 260.70 34.40 o 1 8 3 174.49 185.56 22.62 o 2 8 3 781.48 773.38 25.13 o 3 8 3 221.08 204.04 20.30 o 4 8 3 846.64 780.97 48.37 o 5 8 3 323.05 382.04 69.85 o 6 8 3 24.87 -1.14 26.12 o 7 8 3 430.38 371.44 66.83 o 8 8 3 112.43 29.22 36.59 o 0 9 3 798.41 823.45 47.57 o 1 9 3 1498.01 1552.92 41.16 o 2 9 3 491.06 510.79 27.69 o 3 9 3 324.70 315.34 30.23 o 4 9 3 174.71 147.16 32.07 o 5 9 3 680.93 620.08 29.12 o 6 9 3 229.17 198.14 22.37 o 7 9 3 321.54 319.51 38.59 o 8 9 3 31.94 33.37 38.07 o 9 9 3 70.76 81.09 38.02 o 0 10 3 27.66 19.32 30.64 o 1 10 3 32.97 -30.50 29.22 o 2 10 3 450.89 481.92 24.56 o 3 10 3 254.67 254.56 22.45 o 4 10 3 75.75 82.78 27.75 o 5 10 3 311.17 335.07 23.62 o 6 10 3 3.70 46.86 19.36 o 7 10 3 149.22 100.47 25.56 o 8 10 3 44.63 37.15 45.01 o 9 10 3 57.81 62.97 22.60 o 10 10 3 144.71 76.20 45.03 o 0 11 3 218.23 187.79 37.08 o 1 11 3 120.96 161.88 52.32 o 2 11 3 122.05 124.24 24.86 o 3 11 3 84.43 72.16 46.01 o 4 11 3 98.94 80.79 20.83 o 5 11 3 283.22 229.84 24.32 o 6 11 3 170.86 260.43 35.71 o 7 11 3 55.28 35.62 22.63 o 8 11 3 39.71 11.62 21.95 o 9 11 3 9.74 -60.44 37.74 o 0 12 3 51.58 -70.42 35.21 o 1 12 3 77.12 4.38 32.36 o 2 12 3 57.98 105.90 39.83 o 3 12 3 59.08 65.48 29.15 o 4 12 3 66.70 42.97 28.75 o 5 12 3 91.02 136.50 24.36 o 6 12 3 25.24 53.49 27.52 o 7 12 3 2.65 43.81 39.51 o 8 12 3 4.03 46.36 23.25 o 0 13 3 20.83 -5.79 35.90 o 1 13 3 40.20 46.54 25.72 o 2 13 3 13.05 30.23 19.63 o 3 13 3 9.05 -28.14 20.00 o 4 13 3 9.12 41.03 35.94 o 5 13 3 26.97 14.43 41.04 o 6 13 3 50.27 3.68 29.38 o 0 14 3 1.78 28.85 39.32 o 1 14 3 101.47 119.95 30.87 o 2 14 3 4.30 -1.06 21.59 o 3 14 3 19.55 48.45 44.82 o 4 14 3 4.62 42.43 58.70 o 0 0 4 20061.98 20442.40 99.86 o 0 1 4 25843.54 27747.73 123.83 o 1 1 4 7491.13 8089.68 66.01 o 0 2 4 6670.56 6493.72 62.51 o 1 2 4 11023.58 11596.99 90.47 o 2 2 4 74.09 148.46 23.39 o 0 3 4 298.93 353.69 25.48 o 1 3 4 376.78 414.84 15.55 o 2 3 4 1542.05 1328.98 60.10 o 3 3 4 920.69 999.67 34.83 o 0 4 4 334.61 307.26 26.41 o 1 4 4 560.59 623.30 22.05 o 2 4 4 2572.63 2326.67 28.60 o 3 4 4 1881.34 1929.14 42.29 o 4 4 4 782.54 783.79 36.94 o 0 5 4 64.48 36.88 24.41 o 1 5 4 780.19 739.26 29.07 o 2 5 4 1223.85 1161.81 24.41 o 3 5 4 98.50 149.92 23.86 o 4 5 4 878.95 827.69 22.43 o 5 5 4 132.80 133.34 27.43 o 0 6 4 804.79 766.78 38.24 o 1 6 4 1022.41 951.24 28.38 o 2 6 4 597.54 614.02 20.94 o 3 6 4 150.04 130.67 16.02 o 4 6 4 562.37 615.94 25.00 o 5 6 4 962.55 1005.25 30.73 o 6 6 4 0.70 -36.55 28.04 o 0 7 4 6961.88 7055.68 98.97 o 1 7 4 1161.25 1055.87 41.94 o 2 7 4 1165.72 1052.23 74.75 o 3 7 4 28.28 35.84 30.41 o 4 7 4 470.68 442.82 38.59 o 5 7 4 855.97 799.59 26.15 o 6 7 4 1000.64 1007.21 29.96 o 7 7 4 3.08 -7.91 30.97 o 0 8 4 2.86 -40.83 27.87 o 1 8 4 229.54 211.97 34.15 o 2 8 4 353.43 358.43 28.68 o 3 8 4 525.33 560.89 23.09 o 4 8 4 957.86 916.28 37.35 o 5 8 4 320.61 371.45 22.47 o 6 8 4 30.91 21.18 33.92 o 7 8 4 169.53 128.74 48.11 o 8 8 4 846.18 724.47 55.31 o 0 9 4 716.13 683.59 43.17 o 1 9 4 57.51 71.79 23.35 o 2 9 4 1523.58 1538.48 34.13 o 3 9 4 857.98 786.30 33.79 o 4 9 4 581.23 658.63 31.20 o 5 9 4 229.17 270.44 22.75 o 6 9 4 198.72 170.70 22.04 o 7 9 4 18.19 15.09 36.46 o 8 9 4 78.81 27.26 29.81 o 9 9 4 23.69 -24.29 38.92 o 0 10 4 797.24 793.70 50.67 o 1 10 4 23.06 20.22 21.76 o 2 10 4 282.44 285.15 30.33 o 3 10 4 288.14 396.07 23.80 o 4 10 4 137.10 157.78 20.53 o 5 10 4 21.53 27.16 45.47 o 6 10 4 192.91 238.21 52.73 o 7 10 4 111.39 81.23 21.66 o 8 10 4 11.06 3.81 22.10 o 9 10 4 2.78 -58.83 29.41 o 10 10 4 33.04 -29.10 39.20 o 0 11 4 6.70 102.08 33.62 o 1 11 4 59.87 89.55 24.33 o 2 11 4 24.65 45.36 18.64 o 3 11 4 95.93 71.40 20.42 o 4 11 4 177.80 169.14 22.16 o 5 11 4 43.39 64.82 52.95 o 6 11 4 2.89 -0.03 20.85 o 7 11 4 34.58 20.24 21.44 o 8 11 4 69.36 38.32 39.25 o 9 11 4 180.74 192.03 26.46 o 0 12 4 88.21 42.42 36.27 o 1 12 4 29.51 -46.14 25.00 o 2 12 4 54.62 69.43 20.86 o 3 12 4 12.74 -34.18 22.83 o 4 12 4 12.12 -25.72 20.48 o 5 12 4 164.44 196.29 24.25 o 6 12 4 8.78 34.90 24.29 o 7 12 4 56.63 129.08 23.59 o 8 12 4 35.54 41.79 25.23 o 0 13 4 7.03 7.21 35.17 o 1 13 4 130.25 73.01 45.89 o 2 13 4 130.97 58.85 22.36 o 3 13 4 44.63 133.79 22.56 o 4 13 4 57.33 75.72 22.69 o 5 13 4 58.20 42.04 22.47 o 6 13 4 6.08 29.24 33.37 o 0 14 4 2.35 0.00 38.71 o 1 14 4 7.73 34.80 29.28 o 2 14 4 58.85 94.47 24.68 o 3 14 4 73.48 51.68 27.14 o 0 1 5 6.10 -1.14 20.82 o 1 1 5 7207.17 7577.80 70.11 o 0 2 5 30.55 43.81 21.27 o 1 2 5 3332.12 3543.35 39.08 o 2 2 5 2033.17 1958.26 42.46 o 0 3 5 257.09 344.86 27.15 o 1 3 5 1705.93 1630.22 26.00 o 2 3 5 1722.80 1449.33 23.52 o 3 3 5 1154.90 1310.23 40.99 o 0 4 5 2108.13 1919.86 47.15 o 1 4 5 2617.11 2501.82 36.48 o 2 4 5 1853.78 1853.18 55.05 o 3 4 5 712.94 616.83 39.25 o 4 4 5 0.82 30.52 23.72 o 0 5 5 15.76 -12.55 23.06 o 1 5 5 422.51 406.13 41.94 o 2 5 5 557.23 526.73 32.46 o 3 5 5 160.64 198.97 20.87 o 4 5 5 781.87 780.38 39.28 o 5 5 5 314.24 335.95 33.09 o 0 6 5 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