#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203746.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203746_Fobs loop_ _publ_author_name 'Ballivet-Tkatchenko, Danielle' 'Burgat, Romain' 'Plasseraud, Laurent' 'Richard, Philippe' _publ_section_title ; The ionic tin(IV) complex tri-\m~2~-methoxy-\m~3~-oxo-tris[di-tert-butyltin(IV)] tri-\m~2~-methoxy-bis[tert-butyldimethoxystannate(IV)] ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m830 _journal_page_last m832 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.719 _cell_angle_gamma 90.000 _cell_length_a 11.5912 _cell_length_b 21.7257 _cell_length_c 22.9487 _exptl_crystal_F_000 2768.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file dn6124Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in space group P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 888.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10697.06 0.00 7.39 o 2 0 0 162539.92 159896.25 2540.25 o 3 0 0 1092.72 1104.05 47.01 o 4 0 0 220425.64 204781.86 2599.67 o 5 0 0 108421.20 108047.80 1669.69 o 6 0 0 131045.09 131694.89 2283.75 o 7 0 0 23742.75 21744.26 413.64 o 8 0 0 7898.51 7150.70 206.82 o 9 0 0 23120.36 23159.65 489.16 o 10 0 0 20117.72 21140.78 483.77 o 11 0 0 26859.35 27438.82 725.99 o 12 0 0 2680.31 2818.93 344.72 o 13 0 0 2940.63 2769.33 365.61 o 14 0 0 19376.19 18711.13 1111.19 o 15 0 0 205.79 301.50 434.05 o 1 1 0 19181.07 15.98 15.08 o 2 1 0 40285.46 37553.84 438.75 o 3 1 0 1737.00 1965.52 33.65 o 4 1 0 485.11 875.36 30.68 o 5 1 0 881.34 1171.99 46.14 o 6 1 0 10831.68 9875.61 151.33 o 7 1 0 361.46 243.71 66.85 o 8 1 0 9037.80 9623.41 176.81 o 9 1 0 1107.99 939.96 82.03 o 10 1 0 817.78 848.30 85.58 o 11 1 0 1841.29 1912.87 138.08 o 12 1 0 19.29 111.74 164.34 o 13 1 0 386.52 474.01 179.42 o 14 1 0 816.99 1247.92 265.37 o 15 1 0 346.96 157.64 340.45 o 0 2 0 18536.92 -5.22 7.39 o 1 2 0 788906.25 2350.86 10805.82 o 2 2 0 14231.35 14514.99 122.95 o 3 2 0 4966.10 5508.15 57.09 o 4 2 0 27353.63 28081.07 260.46 o 5 2 0 193392.66 187032.34 1886.98 o 6 2 0 27913.94 27233.46 321.79 o 7 2 0 5835.55 6045.57 125.14 o 8 2 0 30.97 221.89 81.42 o 9 2 0 27853.59 27968.75 373.85 o 10 2 0 33205.23 35086.40 473.82 o 11 2 0 6765.75 6727.43 217.11 o 12 2 0 13759.90 13889.41 281.00 o 13 2 0 12354.09 12099.91 351.30 o 14 2 0 737.84 681.43 274.28 o 15 2 0 12131.85 11502.01 601.46 o 1 3 0 13387.55 13501.84 239.73 o 2 3 0 7833.12 8353.11 129.67 o 3 3 0 26652.22 27140.51 260.27 o 4 3 0 1699.63 1468.35 34.52 o 5 3 0 9029.47 7521.70 212.59 o 6 3 0 10602.09 9889.27 152.83 o 7 3 0 34331.12 36405.20 428.33 o 8 3 0 2879.31 2978.62 97.29 o 9 3 0 11652.97 11761.20 205.08 o 10 3 0 1361.42 1147.58 97.91 o 11 3 0 71.90 221.84 96.24 o 12 3 0 86.00 61.54 145.07 o 13 3 0 93.10 106.05 151.89 o 14 3 0 379.75 505.69 304.30 o 0 4 0 224798.72 208436.95 6831.64 o 1 4 0 8245.14 7978.90 77.29 o 2 4 0 41099.70 39966.59 440.26 o 3 4 0 1022.23 940.83 33.37 o 4 4 0 7172.11 6519.55 85.58 o 5 4 0 12361.57 13555.64 166.97 o 6 4 0 34786.66 33243.56 447.80 o 7 4 0 3885.72 3921.68 138.71 o 8 4 0 636.76 515.64 75.12 o 9 4 0 1446.56 1422.12 95.87 o 10 4 0 10171.71 10129.15 220.00 o 11 4 0 14927.20 14890.02 272.00 o 12 4 0 681.69 499.64 138.48 o 13 4 0 7543.48 7870.71 407.09 o 14 4 0 4936.86 4508.75 386.58 o 1 5 0 27.37 179.30 31.66 o 2 5 0 3167.37 3578.01 49.41 o 3 5 0 26956.20 27374.80 288.61 o 4 5 0 5633.72 5672.34 81.63 o 5 5 0 59310.50 56955.68 636.27 o 6 5 0 24349.12 22407.36 285.85 o 7 5 0 29575.58 29504.59 366.65 o 8 5 0 52475.76 55791.63 668.41 o 9 5 0 1002.12 1284.26 117.43 o 10 5 0 12329.08 12080.68 231.85 o 11 5 0 3994.59 4367.36 163.39 o 12 5 0 667.71 611.08 192.99 o 13 5 0 1701.98 1668.12 193.41 o 14 5 0 2171.74 1899.77 349.29 o 0 6 0 1577.35 1222.17 40.12 o 1 6 0 71659.55 72027.72 624.76 o 2 6 0 617.34 482.73 29.51 o 3 6 0 24862.28 24994.25 282.17 o 4 6 0 6580.87 7225.98 129.67 o 5 6 0 3728.28 3659.51 80.32 o 6 6 0 1360.56 1473.43 61.22 o 7 6 0 12796.09 11173.90 182.44 o 8 6 0 8784.90 8816.17 157.44 o 9 6 0 4649.84 5615.99 145.18 o 10 6 0 699.28 748.90 93.14 o 11 6 0 1630.55 1496.01 131.67 o 12 6 0 12248.29 11887.59 306.31 o 13 6 0 2791.95 3030.35 214.61 o 14 6 0 2955.90 3338.06 764.63 o 1 7 0 292.14 163.94 23.07 o 2 7 0 60.26 202.62 28.57 o 3 7 0 11188.44 11109.37 142.21 o 4 7 0 35953.36 38406.48 421.90 o 5 7 0 137.50 168.77 53.90 o 6 7 0 86722.71 88114.14 992.56 o 7 7 0 66707.59 66867.27 713.26 o 8 7 0 5664.98 5334.36 199.52 o 9 7 0 52355.42 53550.25 670.04 o 10 7 0 6601.12 6733.82 173.82 o 11 7 0 3652.91 4301.72 171.58 o 12 7 0 245.19 309.43 173.87 o 13 7 0 6786.60 7057.60 292.19 o 14 7 0 11493.24 10096.28 665.94 o 0 8 0 54221.69 54790.65 756.79 o 1 8 0 2563.11 2083.35 46.57 o 2 8 0 5665.99 6277.03 94.42 o 3 8 0 9332.75 9527.31 141.85 o 4 8 0 47312.60 46441.32 571.43 o 5 8 0 10801.75 10473.14 194.81 o 6 8 0 959.65 970.65 69.78 o 7 8 0 26.12 88.14 58.73 o 8 8 0 28191.95 27728.83 397.71 o 9 8 0 10936.88 11808.91 340.75 o 10 8 0 3094.25 2904.64 149.13 o 11 8 0 28.28 -103.14 165.85 o 12 8 0 8427.59 8262.80 270.82 o 13 8 0 4791.04 4632.40 322.66 o 14 8 0 3886.37 3896.10 611.09 o 1 9 0 5560.27 5581.82 93.13 o 2 9 0 38881.29 38163.90 409.09 o 3 9 0 1301.50 988.02 78.40 o 4 9 0 9533.08 10092.63 178.45 o 5 9 0 45446.47 44786.84 514.07 o 6 9 0 26237.88 26270.13 338.26 o 7 9 0 14775.16 15176.21 233.35 o 8 9 0 60527.37 62083.92 744.46 o 9 9 0 3493.58 3562.22 136.57 o 10 9 0 23609.18 24021.96 833.07 o 11 9 0 5376.42 6102.58 298.53 o 12 9 0 1797.54 1606.83 196.15 o 13 9 0 6674.46 6493.15 335.27 o 14 9 0 12523.23 12063.93 732.24 o 0 10 0 1901.42 1529.31 72.76 o 1 10 0 44513.22 44113.32 505.65 o 2 10 0 3632.00 3263.68 69.96 o 3 10 0 4414.40 4293.18 104.23 o 4 10 0 8131.32 7977.24 149.87 o 5 10 0 19967.78 19001.19 271.70 o 6 10 0 2540.23 2691.33 91.82 o 7 10 0 4224.70 3706.23 102.61 o 8 10 0 1170.28 1342.20 105.54 o 9 10 0 15089.73 15456.91 280.19 o 10 10 0 2970.49 3321.01 157.76 o 11 10 0 29.06 133.78 147.45 o 12 10 0 1.76 -149.75 190.60 o 13 10 0 13156.98 13037.42 561.22 o 14 10 0 4.53 -480.16 480.51 o 1 11 0 24139.25 23203.36 283.66 o 2 11 0 819.99 824.08 55.48 o 3 11 0 57788.24 60340.71 687.37 o 4 11 0 24365.58 23420.85 333.52 o 5 11 0 757.82 762.46 75.58 o 6 11 0 12659.67 13704.35 287.98 o 7 11 0 41414.53 43571.64 545.20 o 8 11 0 1727.25 1767.17 101.63 o 9 11 0 26293.30 28285.20 430.95 o 10 11 0 6490.96 6618.98 267.30 o 11 11 0 19.19 5.34 165.48 o 12 11 0 808.97 908.80 376.05 o 13 11 0 6032.38 6040.64 710.32 o 0 12 0 48489.46 47258.19 755.78 o 1 12 0 32743.09 32369.19 462.88 o 2 12 0 3041.48 3056.84 82.53 o 3 12 0 5787.22 5890.35 118.76 o 4 12 0 3305.10 3697.39 147.76 o 5 12 0 233.42 382.63 123.24 o 6 12 0 262.38 381.89 77.20 o 7 12 0 117.30 101.35 76.89 o 8 12 0 9135.19 9349.67 185.53 o 9 12 0 344.00 443.47 130.29 o 10 12 0 2181.89 2408.43 172.17 o 11 12 0 812.07 473.38 232.58 o 12 12 0 3307.32 3415.24 569.30 o 13 12 0 1567.84 1688.60 316.59 o 1 13 0 4054.56 3640.52 107.91 o 2 13 0 57867.85 56479.82 700.64 o 3 13 0 14535.20 15173.25 259.33 o 4 13 0 6639.95 6773.14 140.05 o 5 13 0 7580.27 7477.81 171.94 o 6 13 0 14915.23 16111.19 274.96 o 7 13 0 3017.51 2798.64 114.32 o 8 13 0 15847.40 16271.58 474.35 o 9 13 0 2898.80 2646.98 156.43 o 10 13 0 64.00 -115.80 147.36 o 11 13 0 343.09 322.69 290.80 o 12 13 0 4725.06 4445.88 306.79 o 13 13 0 1349.35 820.25 306.03 o 0 14 0 110507.49 112642.71 1868.58 o 1 14 0 4153.28 4516.42 122.13 o 2 14 0 17586.63 17664.20 265.51 o 3 14 0 2552.76 2550.61 134.19 o 4 14 0 10719.81 10603.83 200.45 o 5 14 0 306.17 479.57 92.50 o 6 14 0 4222.58 4354.44 141.80 o 7 14 0 4405.01 4229.95 133.24 o 8 14 0 6067.61 5806.13 195.02 o 9 14 0 45.36 6.88 125.89 o 10 14 0 2662.54 2619.45 199.04 o 11 14 0 253.42 164.36 212.69 o 12 14 0 4163.01 3988.24 409.11 o 13 14 0 2913.52 2568.65 313.86 o 1 15 0 5882.49 6436.65 143.24 o 2 15 0 16299.59 16353.85 261.12 o 3 15 0 19669.68 19415.44 350.28 o 4 15 0 181.35 72.37 76.52 o 5 15 0 801.75 823.05 125.14 o 6 15 0 6336.46 6908.21 209.58 o 7 15 0 5210.32 5186.53 157.96 o 8 15 0 5411.27 5235.08 176.45 o 9 15 0 318.32 116.44 133.64 o 10 15 0 84.61 304.31 232.19 o 11 15 0 6650.64 6912.26 330.60 o 12 15 0 793.86 827.07 438.73 o 0 16 0 3541.93 3223.57 229.81 o 1 16 0 75509.84 75811.89 975.51 o 2 16 0 38.04 105.06 69.01 o 3 16 0 7436.34 7547.59 227.67 o 4 16 0 14683.95 15231.58 259.42 o 5 16 0 26446.11 27335.50 400.20 o 6 16 0 2850.27 2781.30 131.54 o 7 16 0 147.32 196.53 107.16 o 8 16 0 167.75 132.25 145.76 o 9 16 0 25976.65 26230.68 533.66 o 10 16 0 1279.93 1292.04 199.12 o 11 16 0 724.55 718.80 314.87 o 12 16 0 321.89 313.38 506.63 o 1 17 0 5053.90 5198.85 142.35 o 2 17 0 3944.42 3662.66 194.50 o 3 17 0 4225.21 4374.93 131.90 o 4 17 0 1488.09 1359.44 111.69 o 5 17 0 6956.30 7043.59 176.10 o 6 17 0 1270.14 1278.06 118.12 o 7 17 0 11805.64 12287.29 324.23 o 8 17 0 855.54 746.03 144.70 o 9 17 0 373.78 165.53 263.07 o 10 17 0 4189.74 3928.55 432.72 o 11 17 0 601.62 318.86 238.82 o 12 17 0 236.42 -584.97 584.97 o 0 18 0 58061.58 60006.12 1079.82 o 1 18 0 7699.71 7860.32 180.98 o 2 18 0 8213.76 8422.29 184.23 o 3 18 0 2079.66 1803.77 107.05 o 4 18 0 22958.40 23578.83 392.85 o 5 18 0 7124.70 7669.73 245.76 o 6 18 0 10784.74 10997.99 298.41 o 7 18 0 725.57 697.48 125.06 o 8 18 0 7183.67 6249.32 415.48 o 9 18 0 1427.02 1617.15 220.75 o 10 18 0 12411.97 12090.38 467.40 o 11 18 0 1341.69 1096.74 294.89 o 1 19 0 1395.30 1559.87 104.39 o 2 19 0 3414.11 3386.46 140.22 o 3 19 0 99.36 203.45 92.93 o 4 19 0 1486.10 1422.16 134.81 o 5 19 0 4157.33 3641.56 168.60 o 6 19 0 10315.18 10959.11 255.02 o 7 19 0 14324.86 13996.40 292.77 o 8 19 0 926.56 1346.27 165.97 o 9 19 0 5181.95 5611.50 329.27 o 10 19 0 8.91 -238.89 263.27 o 11 19 0 0.27 -301.15 301.15 o 0 20 0 4052.31 3884.77 250.81 o 1 20 0 14472.88 15738.52 285.51 o 2 20 0 1775.24 1928.83 126.86 o 3 20 0 2392.10 2478.22 180.15 o 4 20 0 2339.81 2697.50 235.21 o 5 20 0 11942.47 11978.63 385.98 o 6 20 0 1965.54 2244.30 172.83 o 7 20 0 264.78 180.61 158.31 o 8 20 0 73.43 0.11 185.36 o 9 20 0 7049.95 7274.63 394.53 o 10 20 0 1758.04 1641.78 314.18 o 1 21 0 44.13 111.46 115.10 o 2 21 0 14014.35 14347.19 292.77 o 3 21 0 74.76 287.19 135.88 o 4 21 0 217.59 209.24 312.01 o 5 21 0 3078.17 3186.94 194.26 o 6 21 0 19789.94 19491.46 515.98 o 7 21 0 749.25 936.90 180.85 o 8 21 0 13236.34 14262.26 556.42 o 9 21 0 493.87 582.28 248.12 o 10 21 0 28.39 393.97 312.84 o 0 22 0 33.74 63.26 123.38 o 1 22 0 1752.28 2202.30 140.60 o 2 22 0 4.61 202.09 142.76 o 3 22 0 1153.34 995.38 154.58 o 4 22 0 965.31 998.77 232.95 o 5 22 0 38.08 282.86 187.90 o 6 22 0 909.87 969.51 238.79 o 7 22 0 1013.90 1159.18 224.13 o 8 22 0 126.32 570.29 285.48 o 9 22 0 19.66 -86.86 354.32 o 1 23 0 6614.96 6158.04 277.42 o 2 23 0 580.21 502.49 179.11 o 3 23 0 12495.45 13245.41 437.11 o 4 23 0 7.21 235.66 196.98 o 5 23 0 4609.59 4285.02 319.37 o 6 23 0 66.94 -198.08 288.87 o 7 23 0 16690.14 17964.55 668.93 o 8 23 0 424.23 617.23 312.16 o 0 24 0 678.83 -73.12 355.16 o 1 24 0 7210.86 7210.14 346.92 o 2 24 0 1762.94 1357.07 202.72 o 3 24 0 135.28 245.45 446.87 o 4 24 0 3344.80 3703.67 405.16 o 5 24 0 710.78 369.73 242.10 o 6 24 0 3.62 24.27 277.36 o 7 24 0 583.76 659.41 446.29 o 1 25 0 16.80 -67.04 245.38 o 2 25 0 7959.61 7894.76 391.92 o 3 25 0 0.37 -334.20 334.20 o 4 25 0 312.58 419.84 361.46 o 5 25 0 51.73 588.00 303.14 o 6 25 0 5851.11 5546.23 652.33 o 0 26 0 17089.72 16911.96 908.80 o 1 26 0 255.68 93.23 285.61 o 2 26 0 1919.83 2024.84 312.55 o 3 26 0 2386.68 2597.53 343.90 o 4 26 0 1610.36 1903.28 336.01 o 5 26 0 1323.41 1037.39 320.09 o 1 27 0 657.64 933.20 376.82 o 2 27 0 352.27 -309.01 382.12 o 3 27 0 939.57 335.22 292.53 o 4 27 0 804.42 435.57 421.77 o 0 28 0 154.89 -365.61 501.40 o 1 28 0 9791.79 10069.32 1645.23 o -15 1 1 2027.98 1889.33 437.66 o -14 1 1 51.60 244.77 239.22 o -13 1 1 3160.85 3107.23 186.66 o -12 1 1 2715.07 2427.52 152.28 o -11 1 1 8570.31 8047.69 195.82 o -10 1 1 3234.80 3245.27 131.47 o -9 1 1 2077.45 2151.83 93.31 o -8 1 1 754.02 888.00 67.30 o -7 1 1 2433.31 2148.35 83.32 o -6 1 1 1461.50 1093.18 61.24 o -5 1 1 24579.22 21517.32 259.33 o -4 1 1 63836.25 63116.27 560.02 o -3 1 1 39239.11 38907.56 335.48 o -2 1 1 128160.15 123207.71 1851.51 o -1 1 1 38089.34 13.93 9.05 o 0 1 1 29.12 -2.61 5.22 o 1 1 1 20058.92 -6.72 8.62 o 2 1 1 73566.18 71018.38 901.63 o 3 1 1 4955.75 5514.64 62.68 o 4 1 1 2977.38 3073.72 48.58 o 5 1 1 2247.19 1785.00 79.91 o 6 1 1 21980.79 21592.03 283.32 o 7 1 1 503.40 632.84 63.89 o 8 1 1 13.27 95.20 55.67 o 9 1 1 18556.60 18154.60 262.34 o 10 1 1 29717.64 29840.78 485.49 o 11 1 1 10484.96 10153.49 217.05 o 12 1 1 21978.10 23457.53 395.24 o 13 1 1 524.26 759.34 223.73 o 14 1 1 123.15 -155.27 294.02 o 15 1 1 176.38 -277.86 480.74 o -15 2 1 1397.94 1508.48 347.23 o -14 2 1 696.04 1030.76 223.02 o -13 2 1 2197.03 2339.57 212.26 o -12 2 1 3867.43 3536.55 165.11 o -11 2 1 17045.88 16532.82 283.78 o -10 2 1 68.81 190.33 86.06 o -9 2 1 1000.06 941.09 87.17 o -8 2 1 23108.87 23477.11 305.72 o -7 2 1 10592.83 10016.51 158.10 o -6 2 1 10619.87 10806.21 152.86 o -5 2 1 14993.12 15118.78 181.68 o -4 2 1 47030.09 46159.57 406.74 o -3 2 1 44114.60 46627.80 390.83 o -2 2 1 70682.22 68781.76 814.18 o -1 2 1 22519.21 8840.22 4874.52 o 0 2 1 833.33 8.95 6.03 o 1 2 1 64464.61 6989.59 16276.84 o 2 2 1 8512.26 9298.81 123.63 o 3 2 1 63333.08 64535.42 509.17 o 4 2 1 10655.95 9936.83 102.89 o 5 2 1 1501.37 1692.03 73.88 o 6 2 1 27262.49 26661.45 321.75 o 7 2 1 6596.45 7357.30 173.39 o 8 2 1 608.36 856.40 73.43 o 9 2 1 76.83 22.93 78.40 o 10 2 1 3288.15 3083.16 121.55 o 11 2 1 865.62 616.04 109.39 o 12 2 1 753.58 1075.56 152.95 o 13 2 1 0.94 -45.94 141.42 o 14 2 1 26.11 156.31 311.51 o -14 3 1 122.77 -97.55 251.97 o -13 3 1 142.20 -55.14 187.63 o -12 3 1 13760.79 13932.57 289.49 o -11 3 1 981.94 789.78 115.55 o -10 3 1 896.59 730.35 96.50 o -9 3 1 1055.68 1113.74 110.07 o -8 3 1 751.25 870.92 73.50 o -7 3 1 260.18 217.75 51.26 o -6 3 1 305.80 504.93 63.33 o -5 3 1 13119.96 12452.27 154.39 o -4 3 1 19809.58 19321.52 198.72 o -3 3 1 72021.81 69306.38 567.25 o -2 3 1 12129.52 12069.12 115.25 o -1 3 1 58310.50 57254.02 695.91 o 0 3 1 952.40 1127.22 81.42 o 1 3 1 103713.67 96401.71 1126.72 o 2 3 1 78.54 241.53 19.60 o 3 3 1 36020.07 35772.24 339.20 o 4 3 1 72.11 189.45 28.37 o 5 3 1 19921.88 21045.52 232.49 o 6 3 1 2593.12 2523.25 73.88 o 7 3 1 56471.35 59509.93 701.35 o 8 3 1 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