#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:05:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180957 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203748.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203748_Fobs loop_ _publ_author_name 'Khan, Muhammad S.' 'Al-Suti, Mohammed K.' 'Ahrens, Birte' 'Raithby, Paul R.' 'Teat, Simon J.' _publ_section_title ; trans-(\m-5,5'-Diethynyl-2,2'-bipyridine)bis[phenylbis(triethylphosphine)platinum(II)] ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m735 _journal_page_last m737 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.130 _cell_angle_beta 90.032 _cell_angle_gamma 94.958 _cell_length_a 9.2651 _cell_length_b 16.6840 _cell_length_c 16.8258 _exptl_crystal_F_000 1212.00 _reflns_d_resolution_high 0.7090 _cod_data_source_file dn6135Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cam111 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc 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0 18903.04 18972.35 346.61 o 8 1 0 3326.36 3173.11 159.57 o 9 1 0 453.71 374.10 57.07 o 10 1 0 3076.48 3198.28 129.35 o 11 1 0 895.00 853.47 69.75 o 12 1 0 457.89 405.81 83.70 o -12 2 0 6777.91 6498.01 239.68 o -11 2 0 14389.75 14786.65 526.28 o -10 2 0 8773.85 8529.56 210.35 o -9 2 0 8548.98 8079.78 203.46 o -8 2 0 4089.44 4217.19 156.62 o -7 2 0 4084.33 4179.38 149.01 o -6 2 0 29.19 33.53 77.14 o -5 2 0 2931.97 3330.15 102.53 o -4 2 0 8441.66 8967.10 165.85 o -3 2 0 8622.01 9403.62 167.59 o -2 2 0 12399.92 12797.80 386.15 o 2 2 0 30593.23 30677.55 493.31 o 3 2 0 11769.48 11811.38 231.91 o 4 2 0 7224.08 7139.99 138.16 o 5 2 0 4971.53 5082.30 135.21 o 6 2 0 37.38 43.91 76.22 o 7 2 0 4096.03 3786.47 87.17 o 8 2 0 5764.94 5474.27 165.67 o 9 2 0 3081.41 2869.21 94.62 o 10 2 0 989.19 1069.05 72.28 o 11 2 0 955.68 913.07 73.55 o 12 2 0 336.99 426.10 95.11 o -12 3 0 4.77 136.96 181.35 o -11 3 0 90.40 64.68 180.08 o -10 3 0 2341.89 2363.08 79.22 o -9 3 0 6485.17 6745.51 173.62 o -8 3 0 13016.13 12739.21 302.84 o -7 3 0 18033.21 19352.71 432.40 o -6 3 0 47157.52 50111.82 821.08 o -5 3 0 64602.69 68012.80 1083.87 o -4 3 0 37659.50 39019.61 699.10 o -3 3 0 36903.48 38755.93 618.85 o -2 3 0 622.84 652.30 46.92 o -1 3 0 5926.93 6743.03 162.32 o 0 3 0 4315.32 4646.10 197.18 o 1 3 0 9955.36 10050.73 416.83 o 2 3 0 7545.94 7605.76 210.57 o 3 3 0 16434.35 16574.10 288.06 o 4 3 0 18112.19 17833.59 312.64 o 5 3 0 16490.02 16612.29 298.99 o 6 3 0 10427.12 10425.87 202.41 o 7 3 0 5586.99 5630.42 120.21 o 8 3 0 467.06 365.72 52.06 o 9 3 0 1667.48 1644.16 67.87 o 10 3 0 893.55 819.23 81.16 o 11 3 0 739.66 753.28 82.43 o 12 3 0 4.16 -46.92 237.14 o -12 4 0 10405.56 10104.63 365.23 o -11 4 0 17021.94 17926.59 620.13 o -10 4 0 11932.56 11583.75 281.35 o -9 4 0 9881.16 9443.32 235.49 o -8 4 0 3969.32 4090.35 110.32 o -7 4 0 3180.76 3238.06 90.75 o -6 4 0 2123.85 2459.09 72.18 o -5 4 0 9277.75 10429.44 193.18 o -4 4 0 10297.89 11299.73 203.90 o -3 4 0 46629.76 51886.01 1015.51 o -1 4 0 7273.17 7980.36 339.83 o 0 4 0 11105.26 12201.40 434.73 o 1 4 0 36026.53 37138.35 593.87 o 2 4 0 14883.66 15871.39 297.00 o 3 4 0 1877.73 1933.27 47.50 o 4 4 0 652.97 727.69 48.78 o 5 4 0 3601.14 3389.28 99.65 o 6 4 0 425.93 433.30 39.57 o 7 4 0 2166.66 2034.87 56.74 o 8 4 0 2872.68 2607.16 84.71 o 9 4 0 853.81 830.70 84.33 o 10 4 0 241.27 196.56 74.82 o 11 4 0 59.11 300.55 221.93 o 12 4 0 41.36 150.91 235.88 o -12 5 0 142.19 441.32 194.03 o -11 5 0 405.73 424.93 238.41 o -10 5 0 2484.98 2416.92 124.91 o -9 5 0 9279.95 9547.55 240.81 o -8 5 0 14140.46 14523.37 344.22 o -7 5 0 15842.14 16238.38 372.49 o -6 5 0 31885.64 33278.43 988.52 o -5 5 0 31392.14 31918.23 530.84 o -4 5 0 33075.98 32342.54 530.97 o -3 5 0 5083.44 5500.39 137.59 o -2 5 0 6483.78 7597.39 221.22 o -1 5 0 12383.71 13064.38 226.22 o 0 5 0 45.60 139.84 45.12 o 1 5 0 8352.09 8709.92 160.93 o 2 5 0 10356.07 10316.41 189.97 o 3 5 0 12722.72 12452.24 239.36 o 4 5 0 7884.92 8197.08 160.89 o 5 5 0 2319.56 2391.86 60.44 o 6 5 0 639.66 717.01 41.45 o 7 5 0 413.20 405.62 75.46 o 8 5 0 563.49 554.72 56.42 o 9 5 0 10.42 -59.00 133.93 o 10 5 0 3.75 100.18 237.14 o 11 5 0 237.41 607.44 228.27 o 12 5 0 177.94 429.90 261.24 o -12 6 0 7707.07 7460.54 273.92 o -11 6 0 12971.62 13180.59 319.82 o -10 6 0 10135.91 10145.95 252.18 o -9 6 0 6642.45 6553.37 169.13 o -8 6 0 3236.27 3496.76 96.65 o -7 6 0 1672.02 1695.57 59.00 o -6 6 0 1459.75 1445.94 53.71 o -5 6 0 33.83 141.51 95.87 o -4 6 0 6683.44 6841.29 240.95 o -3 6 0 43057.11 46970.95 753.65 o -2 6 0 26763.81 28692.24 667.23 o -1 6 0 21693.24 24150.46 460.37 o 0 6 0 7263.72 8010.93 221.29 o 1 6 0 17142.79 18655.74 554.46 o 2 6 0 3895.19 4377.82 109.44 o 3 6 0 31.71 162.44 72.73 o 4 6 0 15.01 96.99 78.28 o 5 6 0 109.09 196.07 82.57 o 6 6 0 1058.82 994.97 54.23 o 7 6 0 10.73 22.26 113.50 o 8 6 0 9.47 24.32 119.59 o 9 6 0 41.43 20.96 149.01 o 10 6 0 598.22 667.76 180.71 o 11 6 0 640.69 734.26 101.45 o 12 6 0 865.87 939.70 110.33 o -12 7 0 395.18 445.12 78.63 o -11 7 0 399.65 344.25 57.60 o -10 7 0 1624.95 1578.14 64.27 o -9 7 0 4166.08 4213.54 113.37 o -8 7 0 10930.58 11033.12 270.86 o -7 7 0 13344.62 13592.37 324.57 o -6 7 0 17615.95 18577.98 420.69 o -5 7 0 23645.59 25848.37 557.70 o -4 7 0 3316.74 3377.84 93.55 o -3 7 0 7538.57 8483.52 164.50 o -2 7 0 2103.35 2412.76 56.26 o -1 7 0 1894.63 2055.11 61.87 o 0 7 0 4097.74 4761.32 176.91 o 1 7 0 372.17 374.53 29.64 o 2 7 0 1244.56 1349.83 39.56 o 3 7 0 1203.99 1310.86 43.07 o 4 7 0 3904.42 3874.25 85.50 o 5 7 0 264.63 433.11 53.64 o 6 7 0 916.63 905.83 97.65 o 7 7 0 238.94 328.00 57.04 o 8 7 0 794.80 712.70 60.87 o 9 7 0 628.55 632.74 64.38 o 10 7 0 284.62 477.29 157.33 o 11 7 0 3.41 -62.14 246.02 o -12 8 0 7739.68 8150.41 262.51 o -11 8 0 7426.74 7547.46 188.66 o -10 8 0 8417.49 8438.40 213.75 o -9 8 0 3756.27 3779.43 105.89 o -8 8 0 427.74 414.39 49.34 o -7 8 0 397.92 372.69 46.92 o -6 8 0 2673.29 2581.61 75.26 o -5 8 0 59.31 258.99 101.44 o -4 8 0 6241.92 7321.01 185.17 o -3 8 0 158.38 249.49 81.38 o -2 8 0 7906.02 8345.12 192.63 o -1 8 0 3720.04 4025.23 87.12 o 0 8 0 2266.37 2644.24 132.98 o 1 8 0 244.42 282.08 32.65 o 2 8 0 758.72 900.77 37.72 o 3 8 0 4.56 28.92 85.63 o 4 8 0 855.26 889.81 46.74 o 5 8 0 48.01 142.68 98.14 o 6 8 0 1.47 15.15 119.52 o 7 8 0 408.55 428.50 54.21 o 8 8 0 1174.47 1193.83 181.35 o 9 8 0 1837.14 1850.70 79.06 o 10 8 0 3358.28 3502.28 247.92 o 11 8 0 3271.81 3335.24 207.98 o -12 9 0 405.23 422.29 125.55 o -11 9 0 46.55 -22.32 153.66 o -10 9 0 320.92 399.67 55.82 o -9 9 0 1350.30 1311.74 54.23 o -8 9 0 5068.81 4844.82 128.79 o -7 9 0 7167.56 6950.77 179.28 o -6 9 0 7836.97 8294.79 210.76 o -5 9 0 2663.72 2551.05 138.86 o -4 9 0 2465.16 2651.63 79.36 o -3 9 0 455.74 552.55 51.33 o -2 9 0 32.80 179.87 71.38 o -1 9 0 110.83 287.66 73.58 o 0 9 0 12.72 -5.15 95.05 o 1 9 0 77.13 209.90 77.83 o 2 9 0 370.28 455.68 74.03 o 3 9 0 1863.98 2080.00 55.70 o 4 9 0 5936.39 5592.24 142.05 o 5 9 0 5658.02 5374.05 197.83 o 6 9 0 551.36 519.79 142.03 o 7 9 0 1890.94 1939.20 78.59 o 8 9 0 1391.44 1238.22 69.87 o 9 9 0 698.67 739.61 141.40 o 10 9 0 71.53 39.31 237.14 o 11 9 0 0.63 -38.04 277.73 o -12 10 0 3077.90 3108.24 144.57 o -11 10 0 4645.81 4502.50 119.65 o -10 10 0 3439.71 3441.77 95.95 o -9 10 0 1941.27 1879.94 65.36 o -8 10 0 96.43 286.38 120.82 o -7 10 0 30.95 127.04 119.51 o -6 10 0 23.75 87.77 117.14 o -5 10 0 132.82 184.61 110.80 o -4 10 0 8.66 88.16 103.83 o -3 10 0 7.20 22.55 80.72 o -2 10 0 46.54 192.73 91.77 o -1 10 0 498.36 604.35 82.03 o 0 10 0 2417.91 2634.41 176.27 o 1 10 0 3527.91 3632.18 145.82 o 2 10 0 3546.23 3735.35 84.13 o 3 10 0 86.41 240.42 93.17 o 4 10 0 236.87 441.99 105.85 o 5 10 0 73.07 162.73 128.07 o 6 10 0 18.49 21.81 135.06 o 7 10 0 846.29 862.43 171.83 o 8 10 0 1790.31 1729.12 80.44 o 9 10 0 3244.59 3087.95 152.18 o 10 10 0 5653.02 5747.26 223.19 o 11 10 0 3805.27 4397.95 216.85 o -11 11 0 61.00 266.97 160.83 o -10 11 0 13.40 34.96 140.72 o -9 11 0 55.14 162.39 130.94 o -8 11 0 887.03 889.81 51.49 o -7 11 0 1109.30 1062.40 72.28 o -6 11 0 231.53 359.04 59.60 o -5 11 0 1151.69 1155.31 51.99 o -4 11 0 65.21 282.22 116.00 o -3 11 0 53.09 168.92 107.43 o -2 11 0 4.37 21.64 85.85 o -1 11 0 84.08 239.50 90.06 o 0 11 0 66.20 157.53 88.95 o 1 11 0 48.37 177.54 91.84 o 2 11 0 436.48 518.06 62.32 o 3 11 0 3206.46 3205.16 97.87 o 4 11 0 14137.54 13662.21 263.05 o 5 11 0 7962.93 7505.49 267.58 o 6 11 0 9882.78 9747.43 248.00 o 7 11 0 5264.14 5064.75 115.24 o 8 11 0 3075.74 3294.66 148.37 o 9 11 0 599.64 518.67 133.16 o 10 11 0 9.15 72.28 248.56 o -11 12 0 1668.58 1579.70 70.69 o -10 12 0 420.74 462.73 57.27 o -9 12 0 167.58 366.03 131.85 o -8 12 0 477.15 510.88 49.95 o -7 12 0 67.68 106.74 117.35 o -6 12 0 117.67 302.05 116.70 o -5 12 0 63.33 143.59 118.45 o -4 12 0 775.76 833.51 48.82 o -3 12 0 145.68 229.02 159.79 o -2 12 0 1413.29 1516.88 48.78 o -1 12 0 8435.45 8732.76 327.96 o 0 12 0 8548.89 8550.45 215.65 o 1 12 0 8759.21 8696.12 278.78 o 2 12 0 6901.81 6887.66 209.76 o 3 12 0 1095.13 1063.01 50.05 o 4 12 0 392.38 389.15 78.80 o 5 12 0 87.56 170.70 133.38 o 6 12 0 829.29 867.83 78.00 o 7 12 0 1267.10 1324.27 88.76 o 8 12 0 1932.21 2081.04 131.89 o 9 12 0 3820.78 3819.67 168.66 o 10 12 0 4646.52 5071.34 206.71 o -10 13 0 22.48 -44.40 150.81 o -9 13 0 15.46 98.56 138.89 o -8 13 0 364.11 424.91 53.45 o -7 13 0 1588.68 1572.03 119.21 o -6 13 0 489.98 475.55 48.57 o -5 13 0 1943.95 1953.01 62.99 o -4 13 0 1691.77 1700.57 95.11 o -3 13 0 2814.32 3052.78 88.30 o -2 13 0 24.17 172.12 113.21 o -1 13 0 648.40 719.06 45.58 o 0 13 0 1770.91 1729.41 100.18 o 1 13 0 971.94 992.87 82.52 o 2 13 0 1660.35 1762.47 92.72 o 3 13 0 3876.52 4026.19 202.40 o 4 13 0 6546.97 6662.16 459.71 o 5 13 0 12842.01 11824.29 601.10 o 6 13 0 11095.52 9564.40 350.01 o 7 13 0 7726.73 8329.22 303.09 o 8 13 0 1680.67 1796.97 130.62 o 9 13 0 1340.10 1431.74 139.50 o -10 14 0 123.22 470.10 157.84 o -9 14 0 133.22 414.65 146.46 o -8 14 0 109.33 472.54 136.68 o -7 14 0 152.07 445.28 129.29 o -6 14 0 1475.84 1456.20 57.83 o -5 14 0 284.69 323.26 48.82 o -4 14 0 966.72 988.32 98.28 o -3 14 0 4015.12 4118.99 111.62 o -2 14 0 8192.94 8540.96 212.07 o -1 14 0 11688.58 11575.57 224.23 o 0 14 0 10733.52 11502.00 677.83 o 1 14 0 9877.76 10628.72 247.28 o 2 14 0 3850.09 3806.33 185.18 o 3 14 0 4395.17 4411.35 142.03 o 4 14 0 342.81 397.61 75.18 o 5 14 0 514.89 563.06 111.60 o 6 14 0 1394.09 1339.17 119.21 o 7 14 0 1814.28 1866.72 150.91 o 8 14 0 2017.84 1742.44 131.89 o -10 15 0 20.96 55.80 207.98 o -9 15 0 237.77 299.99 58.18 o -8 15 0 2077.14 2060.99 70.35 o -7 15 0 3078.62 2947.60 82.48 o -6 15 0 2563.30 2611.68 79.26 o -5 15 0 3245.05 3045.70 86.76 o -4 15 0 5172.26 5451.29 452.73 o -3 15 0 2199.52 2310.97 70.39 o -2 15 0 1311.09 1261.32 151.54 o -1 15 0 201.34 476.13 116.77 o 0 15 0 1054.18 1120.87 76.56 o 1 15 0 4604.51 4506.37 115.23 o 2 15 0 3913.82 4154.63 202.02 o 3 15 0 4560.60 4449.66 549.74 o 4 15 0 9999.90 9148.45 344.94 o 5 15 0 8206.20 7747.14 281.53 o 6 15 0 6271.10 5861.40 224.46 o 7 15 0 2786.63 2800.08 143.30 o 8 15 0 1607.47 1810.92 142.03 o -9 16 0 1051.03 1005.92 91.94 o -8 16 0 499.52 467.46 59.51 o -7 16 0 245.10 348.03 55.14 o -6 16 0 976.71 937.43 54.50 o -5 16 0 1232.51 1309.17 58.27 o -4 16 0 1182.59 1275.19 157.25 o -3 16 0 4843.26 4764.25 199.73 o -2 16 0 13330.61 13490.88 388.69 o -1 16 0 15482.02 15658.55 918.78 o 0 16 0 12161.17 13012.58 856.64 o 1 16 0 5155.62 5354.47 97.60 o 2 16 0 4825.43 4253.38 167.40 o 3 16 0 3232.13 2778.52 130.62 o 4 16 0 587.53 701.29 115.40 o 5 16 0 144.19 305.62 180.08 o 6 16 0 612.68 743.26 97.27 o 7 16 0 1884.48 2111.47 135.69 o -9 17 0 1286.86 1312.54 91.31 o -8 17 0 3702.20 3663.90 164.23 o -7 17 0 5834.64 5849.85 444.49 o -6 17 0 4979.04 4989.58 304.36 o -5 17 0 4256.21 4046.70 167.40 o -4 17 0 2995.31 2882.71 301.82 o -3 17 0 2566.46 2398.70 75.07 o -2 17 0 1495.25 1514.98 67.59 o -1 17 0 0.52 -79.61 164.46 o 0 17 0 699.77 752.79 86.23 o 1 17 0 2424.45 2494.82 273.92 o 2 17 0 3851.68 3264.22 149.64 o 3 17 0 6623.46 5780.24 213.05 o 4 17 0 10001.60 8565.10 306.89 o 5 17 0 8775.63 8548.61 310.70 o 6 17 0 3267.82 3748.66 182.61 o 7 17 0 859.16 892.78 131.89 o -8 18 0 565.63 560.35 65.44 o -7 18 0 21.58 -39.69 156.24 o -6 18 0 1063.30 1036.08 88.77 o -5 18 0 1035.03 1135.67 60.06 o -4 18 0 1742.03 1667.56 119.84 o -3 18 0 4994.54 4866.38 317.67 o -2 18 0 11974.97 12110.24 715.87 o -1 18 0 12148.40 12302.60 287.70 o 1 18 0 4172.27 3956.63 178.81 o 2 18 0 1186.84 1046.23 125.55 o 3 18 0 1328.80 1123.58 130.62 o 4 18 0 442.07 467.95 128.08 o 5 18 0 10.97 88.01 150.15 o 6 18 0 465.54 569.40 136.96 o -8 19 0 3220.48 3044.83 126.82 o -7 19 0 7197.23 7013.91 625.83 o -6 19 0 7403.81 7088.50 301.82 o -5 19 0 3837.78 3643.89 238.41 o -4 19 0 1565.43 1388.24 136.96 o -3 19 0 1404.49 1437.72 123.01 o -2 19 0 983.23 1030.68 73.78 o -1 19 0 1.69 41.85 261.24 o 0 19 0 515.42 292.94 300.55 o 1 19 0 694.55 771.04 147.11 o 2 19 0 2202.59 2032.85 142.03 o 3 19 0 3255.34 3327.63 166.13 o 4 19 0 4700.38 4732.74 187.69 o 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