#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203776.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203776_Fobs loop_ _publ_author_name 'Walji, Dhiran V. B.' 'Storey, John M. D.' 'Harrison, William T. A.' _publ_section_title ; 5-[Bis(cyclopropanecarbonyl)amino]-4,6-dichloropyrimidine containing a short cyclopropyl C---H···O interaction ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1110 _journal_page_last o1112 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.065 _cell_angle_gamma 90.000 _cell_length_a 7.6677 _cell_length_b 26.7366 _cell_length_c 6.6477 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7694 _[local]_cod_data_source_file hg6054Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DW002 SOTON DATA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6002.54 5785.72 88.96 o 3 0 0 4286.56 4422.13 77.08 o 4 0 0 3517.19 3965.51 105.07 o 5 0 0 2234.86 2104.91 63.41 o 6 0 0 260.70 301.07 18.35 o 7 0 0 1668.11 1765.39 87.77 o 8 0 0 13.56 -20.66 41.12 o 9 0 0 21.62 41.12 61.59 o 2 1 0 195.94 199.03 6.54 o 3 1 0 5676.83 5774.87 84.99 o 4 1 0 422.36 449.45 10.43 o 5 1 0 53.75 51.81 7.32 o 6 1 0 518.49 514.63 19.70 o 7 1 0 31.79 6.89 13.06 o 8 1 0 628.26 665.47 41.17 o 9 1 0 32.40 47.88 35.56 o 2 2 0 2606.33 2380.66 33.48 o 3 2 0 8.05 10.23 8.35 o 4 2 0 1176.53 1182.39 20.68 o 5 2 0 593.52 539.39 19.08 o 6 2 0 685.96 703.38 23.24 o 7 2 0 277.02 281.91 27.05 o 8 2 0 64.95 30.86 30.84 o 9 2 0 292.17 307.03 48.85 o 2 3 0 12.89 27.28 11.81 o 3 3 0 462.64 415.12 9.40 o 4 3 0 303.05 319.41 10.38 o 5 3 0 60.39 64.85 7.99 o 6 3 0 0.82 -4.15 9.75 o 7 3 0 69.02 30.98 13.06 o 8 3 0 0.19 -24.23 24.23 o 9 3 0 64.82 31.77 38.48 o 0 4 0 4737.67 4024.52 504.60 o 1 4 0 372.06 351.58 7.17 o 2 4 0 4.05 20.66 20.66 o 3 4 0 134.29 129.12 6.86 o 4 4 0 5049.04 5126.26 68.05 o 5 4 0 480.39 454.05 14.63 o 6 4 0 1385.05 1342.88 34.92 o 7 4 0 439.72 435.25 24.84 o 8 4 0 48.93 56.62 30.84 o 9 4 0 755.52 725.27 80.29 o 1 5 0 3314.45 3213.84 50.43 o 2 5 0 1191.34 1092.81 17.82 o 3 5 0 481.82 525.92 15.52 o 4 5 0 564.36 580.89 13.03 o 5 5 0 116.63 109.50 8.59 o 6 5 0 435.75 392.36 17.76 o 7 5 0 448.58 451.61 27.24 o 8 5 0 127.04 84.33 24.20 o 9 5 0 168.97 216.91 38.54 o 0 6 0 2182.98 2200.25 50.07 o 1 6 0 2889.63 2887.90 43.15 o 2 6 0 993.14 1005.75 19.98 o 3 6 0 1660.52 1736.66 35.33 o 4 6 0 537.70 557.47 20.10 o 5 6 0 1.53 7.75 7.28 o 6 6 0 33.00 28.94 9.74 o 7 6 0 1.67 -8.28 15.68 o 8 6 0 23.89 0.00 26.94 o 9 6 0 27.83 54.13 38.53 o 1 7 0 66.50 77.89 9.08 o 2 7 0 832.12 854.50 14.35 o 3 7 0 408.77 387.00 11.64 o 4 7 0 68.94 65.31 7.76 o 5 7 0 58.21 44.41 8.04 o 6 7 0 59.21 46.56 16.94 o 7 7 0 37.28 27.54 14.64 o 8 7 0 101.82 102.87 30.84 o 9 7 0 14.65 -38.49 38.49 o 0 8 0 14420.44 14244.83 251.28 o 1 8 0 4156.88 4273.41 66.49 o 2 8 0 3.76 16.28 9.10 o 3 8 0 17.17 10.16 7.18 o 4 8 0 1755.08 1784.88 38.38 o 5 8 0 1010.68 1001.80 31.67 o 6 8 0 2078.98 2203.44 60.37 o 7 8 0 2.82 36.33 22.30 o 8 8 0 95.60 56.59 20.56 o 9 8 0 162.61 123.27 43.55 o 1 9 0 703.29 756.87 20.44 o 2 9 0 303.69 323.97 9.11 o 3 9 0 114.85 112.69 7.18 o 4 9 0 1029.14 1062.87 33.70 o 5 9 0 1120.43 1107.05 30.14 o 6 9 0 17.79 11.79 12.46 o 7 9 0 282.62 297.67 28.91 o 8 9 0 0.03 5.60 22.14 o 9 9 0 222.27 122.98 82.05 o 0 10 0 384.20 376.88 11.24 o 1 10 0 1953.82 1904.42 30.89 o 2 10 0 2361.40 2435.78 38.22 o 3 10 0 453.14 435.49 15.37 o 4 10 0 222.96 223.49 13.75 o 5 10 0 133.33 122.81 12.48 o 6 10 0 26.88 34.37 14.55 o 7 10 0 55.12 32.84 15.20 o 8 10 0 4.09 25.70 30.84 o 9 10 0 139.38 81.86 40.93 o 1 11 0 529.93 632.03 15.30 o 2 11 0 878.50 1002.31 24.94 o 3 11 0 394.86 393.59 14.33 o 4 11 0 0.17 -3.40 8.34 o 5 11 0 8.07 -7.70 10.98 o 6 11 0 66.91 74.08 16.94 o 7 11 0 0.30 -4.12 18.42 o 8 11 0 104.91 105.15 26.97 o 0 12 0 10672.73 10654.47 209.82 o 1 12 0 0.88 -3.37 8.26 o 2 12 0 647.55 587.29 19.59 o 3 12 0 799.09 748.68 28.95 o 4 12 0 0.20 10.18 10.18 o 5 12 0 4861.14 5089.00 120.44 o 6 12 0 416.44 380.92 24.14 o 7 12 0 146.77 161.60 21.01 o 8 12 0 276.87 234.26 29.46 o 1 13 0 1236.98 1377.86 25.17 o 2 13 0 2580.75 2995.02 55.13 o 3 13 0 1087.35 1200.56 29.60 o 4 13 0 12.00 10.18 10.18 o 5 13 0 203.23 209.84 20.45 o 6 13 0 587.65 584.10 35.81 o 7 13 0 117.87 100.63 22.07 o 8 13 0 579.73 541.78 44.83 o 0 14 0 419.27 354.63 19.98 o 1 14 0 2974.11 3214.04 51.25 o 2 14 0 2660.91 2726.77 47.13 o 3 14 0 303.93 277.38 20.39 o 4 14 0 155.05 160.86 14.34 o 5 14 0 4558.10 4608.50 162.04 o 6 14 0 605.73 598.20 38.32 o 7 14 0 262.79 240.22 27.02 o 8 14 0 372.69 370.73 67.28 o 1 15 0 665.76 732.16 21.10 o 2 15 0 100.00 84.99 11.34 o 3 15 0 7.00 10.18 10.18 o 4 15 0 378.52 369.46 30.77 o 5 15 0 399.10 367.28 20.87 o 6 15 0 11.36 -20.50 20.50 o 7 15 0 404.51 420.41 40.33 o 8 15 0 44.50 70.65 38.36 o 0 16 0 29.23 35.26 10.17 o 1 16 0 3227.92 3141.73 71.08 o 2 16 0 21.78 0.00 9.05 o 3 16 0 124.77 139.96 12.30 o 4 16 0 1231.02 1246.57 75.36 o 5 16 0 180.26 198.83 20.45 o 6 16 0 1014.04 1036.05 53.82 o 7 16 0 153.18 115.38 20.50 o 8 16 0 1.99 9.28 38.31 o 1 17 0 267.48 272.55 18.95 o 2 17 0 106.25 94.26 10.77 o 3 17 0 85.32 74.87 15.60 o 4 17 0 12.25 36.91 13.73 o 5 17 0 172.46 147.65 22.75 o 6 17 0 4.14 -15.40 20.50 o 7 17 0 257.33 253.08 32.51 o 8 17 0 70.95 44.08 49.53 o 0 18 0 454.49 473.10 28.54 o 1 18 0 285.97 266.60 18.08 o 2 18 0 119.19 110.00 9.80 o 3 18 0 85.60 80.81 12.74 o 4 18 0 288.00 332.88 21.99 o 5 18 0 5.73 20.43 12.89 o 6 18 0 22.95 16.72 21.98 o 7 18 0 3.15 -1.88 22.02 o 8 18 0 4.90 100.79 80.52 o 1 19 0 57.33 71.09 14.49 o 2 19 0 163.14 163.90 15.22 o 3 19 0 132.32 134.59 20.22 o 4 19 0 39.08 40.60 15.36 o 5 19 0 73.78 45.91 20.41 o 6 19 0 3.35 -16.35 26.64 o 7 19 0 0.13 -1.90 24.45 o 0 20 0 4529.33 4969.31 242.14 o 1 20 0 1166.28 1193.13 40.80 o 2 20 0 769.90 834.73 35.00 o 3 20 0 96.64 106.23 20.22 o 4 20 0 11.68 -8.12 15.41 o 5 20 0 1509.24 1622.97 108.34 o 6 20 0 197.29 133.13 30.69 o 7 20 0 96.98 34.77 24.09 o 1 21 0 0.15 0.00 11.20 o 2 21 0 445.66 437.05 30.14 o 3 21 0 731.09 746.66 56.94 o 4 21 0 130.10 103.33 20.32 o 5 21 0 4.79 36.74 24.03 o 6 21 0 3.87 -6.86 26.87 o 7 21 0 74.26 81.82 31.57 o 0 22 0 79.42 120.68 40.16 o 1 22 0 490.82 474.00 26.32 o 2 22 0 40.05 20.15 12.73 o 3 22 0 36.98 40.45 12.77 o 4 22 0 11.37 12.21 15.41 o 5 22 0 3.37 -16.67 29.51 o 6 22 0 22.47 13.58 23.51 o 7 22 0 1.22 35.86 33.67 o 1 23 0 8.77 -10.04 28.27 o 2 23 0 56.46 47.08 12.76 o 3 23 0 142.96 97.91 20.22 o 4 23 0 65.10 62.87 21.87 o 5 23 0 62.65 84.67 24.03 o 6 23 0 0.25 6.32 31.54 o 7 23 0 38.64 -40.36 40.36 o 0 24 0 880.64 975.96 100.60 o 1 24 0 23.32 20.14 15.21 o 2 24 0 28.78 36.18 15.23 o 3 24 0 455.81 458.52 48.69 o 4 24 0 6.73 -16.25 23.92 o 5 24 0 1263.81 1406.14 65.89 o 6 24 0 36.67 5.13 33.62 o 1 25 0 28.43 34.79 21.72 o 2 25 0 172.96 177.91 20.18 o 3 25 0 297.73 261.97 21.82 o 4 25 0 9.68 9.28 21.93 o 5 25 0 1.07 25.23 27.98 o 6 25 0 20.14 36.54 34.73 o 0 26 0 1158.23 1129.66 71.14 o 1 26 0 7.26 4.05 23.27 o 2 26 0 179.78 186.60 33.28 o 3 26 0 349.98 386.49 34.27 o 4 26 0 134.71 83.26 21.93 o 5 26 0 148.32 149.52 30.60 o 6 26 0 73.79 68.54 38.15 o 1 27 0 9.37 8.03 33.28 o 2 27 0 53.55 43.97 21.70 o 3 27 0 0.11 -0.02 20.22 o 4 27 0 0.37 -1.82 21.87 o 5 27 0 5.74 -2.06 24.02 o 0 28 0 30.96 60.44 60.44 o 1 28 0 1973.08 2276.62 100.15 o 2 28 0 248.95 195.47 23.74 o 3 28 0 136.69 156.59 25.19 o 4 28 0 661.35 634.50 40.69 o 5 28 0 49.82 65.67 34.63 o 1 29 0 4.72 16.11 33.60 o 2 29 0 142.11 110.71 25.99 o 3 29 0 30.09 28.85 26.36 o 4 29 0 209.99 245.87 30.50 o 5 29 0 23.94 70.96 57.34 o 0 30 0 46.68 50.30 30.22 o 1 30 0 151.21 164.84 32.05 o 2 30 0 121.18 122.12 27.50 o 3 30 0 24.82 11.58 35.11 o 4 30 0 209.11 176.92 32.30 o 1 31 0 5.89 -10.09 20.13 o 2 31 0 39.47 25.26 29.03 o 3 31 0 63.28 8.52 24.70 o 4 31 0 78.08 69.49 29.47 o 0 32 0 204.76 183.90 50.30 o 1 32 0 21.16 -3.19 29.07 o 2 32 0 33.08 24.24 23.74 o 3 32 0 10.64 -28.85 29.33 o 1 33 0 46.15 60.61 31.07 o 2 33 0 325.10 373.60 103.57 o 0 34 0 188.19 69.05 48.34 o 1 34 0 47.09 38.73 30.90 o -9 1 1 1.20 -20.58 51.54 o -8 1 1 1093.02 1188.02 59.70 o -7 1 1 1.62 20.69 15.64 o -6 1 1 0.64 11.53 6.92 o -5 1 1 450.36 387.59 11.57 o -4 1 1 42.00 43.26 6.24 o -3 1 1 2062.19 2028.05 24.60 o -2 1 1 15658.32 14449.58 176.79 o -1 1 1 173.53 169.39 12.26 o 0 1 1 1794.70 1555.29 34.54 o 1 1 1 6274.79 6161.13 84.99 o 2 1 1 3524.00 3381.00 46.67 o 3 1 1 607.09 576.05 12.55 o 4 1 1 576.16 616.37 15.55 o 5 1 1 27.42 26.56 11.93 o 6 1 1 57.43 82.53 20.66 o 7 1 1 310.97 294.25 23.82 o 8 1 1 483.59 514.48 41.07 o -9 2 1 1.23 -20.62 43.68 o -8 2 1 19.43 15.49 20.66 o -7 2 1 34.60 41.54 9.80 o -6 2 1 595.76 617.29 18.03 o -5 2 1 836.37 797.23 15.51 o -4 2 1 289.17 311.67 8.37 o -3 2 1 678.16 683.03 11.11 o -2 2 1 1914.02 1794.85 24.89 o -1 2 1 1701.62 1550.17 53.67 o 0 2 1 5351.26 4939.26 58.73 o 1 2 1 2818.27 2684.01 36.44 o 2 2 1 1769.46 1684.88 23.68 o 3 2 1 3434.62 3516.47 44.78 o 4 2 1 486.17 498.48 12.84 o 5 2 1 1586.45 1584.09 45.61 o 6 2 1 21.71 20.66 11.93 o 7 2 1 17.03 30.91 20.61 o 8 2 1 118.95 150.39 30.79 o -9 3 1 48.31 92.79 71.91 o -8 3 1 761.43 786.22 41.36 o -7 3 1 99.09 86.01 13.90 o -6 3 1 723.71 714.66 25.38 o -5 3 1 162.90 167.54 6.81 o -4 3 1 0.03 -6.98 8.55 o -3 3 1 6540.84 6319.57 75.95 o -2 3 1 2291.95 2224.05 39.64 o -1 3 1 4650.42 3807.31 297.48 o 0 3 1 1760.47 1616.08 23.53 o 1 3 1 361.77 345.20 7.18 o 2 3 1 3821.62 3748.15 47.10 o 3 3 1 937.28 941.79 15.62 o 4 3 1 901.14 919.20 19.23 o 5 3 1 546.08 516.41 20.61 o 6 3 1 187.90 180.66 20.61 o 7 3 1 512.33 517.02 42.72 o 8 3 1 141.89 104.74 24.98 o -9 4 1 5.81 20.66 51.54 o -8 4 1 74.83 78.45 18.48 o -7 4 1 75.60 77.68 13.89 o -6 4 1 4.72 2.58 7.31 o -5 4 1 209.08 204.89 9.72 o -4 4 1 172.53 184.01 7.56 o -3 4 1 10.61 0.00 20.08 o -2 4 1 140.65 141.71 6.44 o -1 4 1 1878.61 1940.06 30.83 o 0 4 1 6601.31 6258.03 79.66 o 1 4 1 473.87 477.98 9.71 o 2 4 1 10.87 23.95 8.38 o 3 4 1 357.89 338.01 14.50 o 4 4 1 1135.31 1225.08 32.79 o 5 4 1 202.43 186.01 11.99 o 6 4 1 27.59 37.02 15.58 o 7 4 1 220.20 183.54 24.23 o 8 4 1 161.31 186.27 32.62 o -9 5 1 350.01 370.64 49.48 o -8 5 1 35.52 27.51 14.61 o -7 5 1 343.53 369.09 19.75 o -6 5 1 70.39 78.57 8.78 o -5 5 1 1675.91 1672.93 31.74 o -4 5 1 2688.72 2795.52 41.51 o -3 5 1 75.40 85.92 6.85 o -2 5 1 13580.42 13445.34 172.68 o -1 5 1 3837.83 3713.80 63.81 o 0 5 1 2029.67 2067.05 30.82 o 1 5 1 3541.66 3285.36 54.98 o 2 5 1 67.24 87.04 7.23 o 3 5 1 419.25 379.32 12.43 o 4 5 1 21.57 5.91 7.78 o 5 5 1 17.07 9.41 9.04 o 6 5 1 522.97 512.24 26.94 o 7 5 1 69.45 26.15 22.15 o 8 5 1 201.32 225.41 34.87 o -9 6 1 95.94 102.97 34.26 o -8 6 1 40.27 28.86 18.44 o -7 6 1 25.55 57.91 14.68 o -6 6 1 2568.08 2597.27 52.58 o -5 6 1 115.50 122.80 8.22 o -4 6 1 746.60 745.03 21.72 o -3 6 1 701.20 789.96 14.67 o -2 6 1 3563.72 3716.48 51.58 o -1 6 1 4660.72 4475.20 65.35 o 1 6 1 5894.98 5725.49 79.46 o 2 6 1 1567.34 1601.62 26.26 o 3 6 1 72.11 79.09 7.23 o 4 6 1 495.72 427.22 15.35 o 5 6 1 81.55 83.38 8.44 o 6 6 1 955.10 950.28 39.76 o 7 6 1 122.39 135.63 26.93 o 8 6 1 48.96 24.88 25.02 o -9 7 1 885.86 1114.15 87.50 o -8 7 1 24.16 35.36 24.15 o -7 7 1 2163.87 2311.60 64.66 o -6 7 1 192.71 179.26 14.54 o -5 7 1 1021.82 975.71 27.03 o -4 7 1 3730.96 3770.36 52.39 o -3 7 1 76.17 73.72 6.79 o -2 7 1 6152.58 6361.16 100.78 o -1 7 1 3234.55 3267.85 56.48 o 0 7 1 2264.83 2270.92 42.65 o 1 7 1 4407.85 4343.51 60.56 o 2 7 1 514.26 523.99 12.46 o 3 7 1 1713.37 1734.51 36.37 o 4 7 1 9.14 8.20 9.17 o 5 7 1 3.56 1.87 9.02 o 6 7 1 795.20 822.19 57.45 o 7 7 1 286.21 280.78 26.67 o 8 7 1 27.31 35.87 30.74 o -9 8 1 8.24 4.18 34.26 o -8 8 1 0.01 -4.15 18.97 o -7 8 1 65.47 58.04 13.71 o -6 8 1 356.17 326.95 15.54 o -5 8 1 427.97 404.18 14.04 o -4 8 1 1182.68 1171.05 20.39 o -3 8 1 0.36 13.66 8.36 o -2 8 1 1320.79 1406.30 28.56 o -1 8 1 1299.06 1146.89 20.02 o 0 8 1 5526.05 5446.66 86.96 o 1 8 1 2876.66 2906.65 43.09 o 2 8 1 597.56 550.94 13.71 o 3 8 1 642.42 592.66 17.19 o 4 8 1 482.18 457.56 18.37 o 5 8 1 1569.38 1570.75 40.31 o 6 8 1 8.33 8.85 12.44 o 7 8 1 453.82 483.25 32.68 o 8 8 1 162.43 134.02 28.09 o -9 9 1 237.12 288.63 49.49 o -8 9 1 1140.33 1199.91 53.66 o -7 9 1 301.87 286.10 16.80 o -6 9 1 29.39 37.77 8.42 o -5 9 1 2083.28 2107.56 40.92 o -4 9 1 549.45 582.10 13.71 o -3 9 1 3171.45 3285.97 49.29 o -2 9 1 3592.61 3882.59 65.15 o -1 9 1 2449.04 2433.00 48.52 o 0 9 1 1781.74 1756.00 33.17 o 1 9 1 56.93 64.31 7.15 o 2 9 1 8206.74 8789.16 118.70 o 3 9 1 669.87 736.40 25.73 o 4 9 1 1265.85 1309.21 40.92 o 5 9 1 1129.37 1155.04 49.81 o 6 9 1 646.33 602.17 24.77 o 7 9 1 54.66 22.86 26.95 o 8 9 1 165.42 193.07 37.57 o -9 10 1 43.67 47.12 49.55 o -8 10 1 66.41 72.19 24.29 o -7 10 1 151.11 154.56 16.76 o -6 10 1 37.04 45.26 9.66 o -5 10 1 898.72 905.52 28.04 o -4 10 1 903.19 937.72 22.02 o -3 10 1 1711.06 1831.68 36.07 o -2 10 1 811.25 864.02 18.01 o -1 10 1 33.78 20.08 20.08 o 0 10 1 8.08 6.74 8.25 o 1 10 1 484.19 513.40 18.20 o 2 10 1 69.94 97.81 7.67 o 3 10 1 658.40 681.21 20.15 o 4 10 1 17.95 26.24 11.26 o 5 10 1 3991.42 4220.03 107.04 o 6 10 1 302.52 307.46 24.73 o 7 10 1 230.08 270.90 32.61 o 8 10 1 435.10 393.70 45.93 o -9 11 1 20.94 0.00 41.22 o -8 11 1 835.18 876.60 45.57 o -7 11 1 41.24 12.35 19.81 o -6 11 1 177.63 156.85 18.38 o -5 11 1 3130.17 3201.54 67.20 o -4 11 1 0.04 0.00 7.71 o -3 11 1 3340.01 3263.02 56.80 o -2 11 1 2177.61 2589.16 41.97 o -1 11 1 2497.32 2569.28 45.51 o 0 11 1 133.88 136.93 7.62 o 1 11 1 561.86 624.83 15.30 o 2 11 1 4254.14 4486.93 68.53 o 3 11 1 1651.48 1703.88 37.05 o 4 11 1 50.99 44.31 12.93 o 5 11 1 116.61 138.08 14.62 o 6 11 1 2.14 -8.77 13.23 o 7 11 1 57.49 63.49 22.18 o 8 11 1 29.44 24.90 34.84 o -9 12 1 50.75 83.01 62.16 o -8 12 1 10.95 28.80 24.32 o -7 12 1 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