#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203787_Fobs loop_ _publ_author_name 'Lebel, H\'el\`ene' 'del Salvatori, Maria' 'B\'elanger-Gari\'epy, Francine' _publ_section_title ; (R)-Bis[1,3-bis(1-phenylethyl)imidazolin-2-ylidene]dichloropalladium(II) dichloromethane solvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m755 _journal_page_last m757 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6567 _cell_length_b 13.6627 _cell_length_c 24.1997 _exptl_crystal_F_000 1672.00 _reflns_d_resolution_high 0.8066 _[local]_cod_data_source_file na6322Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' helen6 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 44906.80 46395.86 250.83 o 4 0 0 78.87 75.87 10.72 o 6 0 0 15210.77 15181.26 116.79 o 8 0 0 8204.60 8281.59 178.64 o 1 1 0 65662.77 68423.41 345.37 o 2 1 0 34080.14 36457.04 356.83 o 3 1 0 1332.37 1760.11 36.41 o 4 1 0 28.08 21.83 5.74 o 5 1 0 811.62 689.83 19.25 o 6 1 0 86.36 56.29 10.00 o 7 1 0 4919.21 4661.22 89.54 o 8 1 0 2229.05 2178.23 75.95 o 9 1 0 11021.02 11030.37 363.34 o 0 2 0 23086.62 25372.34 170.55 o 1 2 0 25164.65 25967.76 167.97 o 2 2 0 62372.60 62290.70 818.12 o 3 2 0 1487.67 1522.90 25.36 o 4 2 0 1466.13 1547.31 35.60 o 5 2 0 6864.48 7627.99 87.90 o 6 2 0 1520.27 1446.73 34.25 o 7 2 0 2045.30 2030.23 60.51 o 8 2 0 8764.62 8903.18 167.63 o 9 2 0 3264.32 2832.66 146.90 o 10 2 0 4544.55 5356.27 374.04 o 11 2 0 5.81 -28.63 82.33 o 1 3 0 5613.60 6062.07 59.58 o 2 3 0 76.49 97.58 6.90 o 3 3 0 4685.23 5000.17 51.15 o 4 3 0 25065.42 26724.83 425.46 o 5 3 0 5355.23 5676.62 154.99 o 6 3 0 3754.56 3743.83 61.90 o 7 3 0 584.19 627.01 40.58 o 8 3 0 835.09 609.35 45.50 o 9 3 0 4188.86 4132.09 156.26 o 10 3 0 1.06 -23.00 56.78 o 11 3 0 719.69 687.60 166.68 o 12 3 0 1013.30 764.38 124.28 o 0 4 0 8242.23 8405.50 106.74 o 1 4 0 12.95 48.79 5.97 o 2 4 0 705.94 660.03 16.28 o 3 4 0 28924.13 30377.76 241.27 o 4 4 0 39.04 47.93 10.83 o 5 4 0 27389.56 28096.72 400.37 o 6 4 0 2645.99 2521.36 84.28 o 7 4 0 1569.95 1361.19 55.52 o 8 4 0 3093.20 2973.92 84.82 o 9 4 0 15.67 18.11 38.76 o 10 4 0 759.29 734.81 78.95 o 11 4 0 325.32 297.26 61.49 o 12 4 0 147.64 147.86 58.11 o 13 4 0 2457.99 2429.04 168.35 o 1 5 0 923.13 837.36 18.35 o 2 5 0 20820.02 20904.72 199.92 o 3 5 0 2974.91 2769.64 43.18 o 4 5 0 28406.44 29038.16 228.67 o 5 5 0 2109.99 2245.02 53.46 o 6 5 0 6792.84 6529.50 123.84 o 7 5 0 3.45 27.45 22.51 o 8 5 0 172.23 129.29 35.22 o 9 5 0 9.76 18.52 33.57 o 10 5 0 171.83 111.94 40.70 o 11 5 0 46.02 44.87 45.17 o 12 5 0 1619.48 1746.53 98.60 o 13 5 0 76.65 40.74 61.53 o 0 6 0 114.83 71.15 11.72 o 1 6 0 1583.26 1442.60 26.69 o 2 6 0 332.65 287.64 17.63 o 3 6 0 22029.88 22636.10 309.99 o 4 6 0 23.24 19.66 12.28 o 5 6 0 18907.42 19356.65 349.36 o 6 6 0 1883.16 1890.75 59.78 o 7 6 0 4419.35 4233.05 166.91 o 8 6 0 35.19 18.72 32.89 o 9 6 0 0.25 -16.69 31.25 o 10 6 0 290.05 273.54 43.14 o 11 6 0 1680.70 1721.44 77.42 o 12 6 0 340.47 342.42 57.17 o 13 6 0 2905.80 3115.41 125.12 o 1 7 0 116.37 135.56 14.29 o 2 7 0 140.33 127.16 16.01 o 3 7 0 605.43 453.25 26.94 o 4 7 0 11939.15 11559.40 123.01 o 5 7 0 4223.52 4409.68 89.43 o 6 7 0 8473.28 8455.34 169.92 o 7 7 0 110.64 132.23 34.13 o 8 7 0 531.55 531.37 47.70 o 9 7 0 1684.03 1630.61 70.83 o 10 7 0 20.45 26.35 30.34 o 11 7 0 1155.47 1014.08 79.75 o 12 7 0 2448.09 2725.67 104.74 o 0 8 0 231.39 309.93 36.69 o 1 8 0 7.45 1.27 12.15 o 2 8 0 54.12 39.59 14.66 o 3 8 0 2764.37 2656.37 62.18 o 4 8 0 1662.35 1567.34 51.09 o 5 8 0 11094.52 10624.77 133.13 o 6 8 0 20.09 40.73 26.34 o 7 8 0 422.20 468.49 48.27 o 8 8 0 395.02 361.47 42.95 o 9 8 0 125.52 122.93 33.24 o 10 8 0 2174.58 2035.63 73.87 o 11 8 0 440.41 471.50 43.77 o 12 8 0 278.35 299.61 42.06 o 1 9 0 7239.17 6899.00 180.73 o 2 9 0 206.52 191.59 24.89 o 3 9 0 2291.55 2053.93 66.99 o 4 9 0 2495.81 2298.90 64.80 o 5 9 0 149.75 156.26 25.44 o 6 9 0 458.22 507.84 45.80 o 7 9 0 674.65 593.78 48.14 o 8 9 0 6.25 19.05 26.50 o 9 9 0 2043.84 1933.21 73.15 o 10 9 0 138.95 117.94 33.06 o 11 9 0 1020.61 1007.49 54.09 o 12 9 0 296.84 345.31 51.10 o 0 10 0 12080.22 10814.45 821.77 o 1 10 0 527.09 467.63 49.68 o 2 10 0 3625.51 3348.97 113.87 o 3 10 0 934.18 924.07 56.04 o 4 10 0 23.03 31.60 33.82 o 5 10 0 683.98 710.31 53.88 o 6 10 0 101.92 92.98 32.78 o 7 10 0 2.78 2.17 25.71 o 8 10 0 4227.55 4307.20 102.29 o 9 10 0 36.56 61.73 28.91 o 10 10 0 1637.49 1576.64 61.25 o 11 10 0 19.71 -2.32 26.72 o 1 11 0 12339.96 12781.23 250.29 o 2 11 0 669.92 532.50 58.91 o 3 11 0 126.55 162.29 39.15 o 4 11 0 176.00 214.55 41.25 o 5 11 0 240.93 246.19 41.05 o 6 11 0 522.22 518.88 47.40 o 7 11 0 2758.62 2938.54 80.05 o 8 11 0 196.08 196.31 34.96 o 9 11 0 2310.99 2433.11 73.39 o 10 11 0 29.06 12.28 25.72 o 0 12 0 4423.53 4641.42 239.96 o 1 12 0 361.99 339.10 67.71 o 2 12 0 4849.82 5560.72 136.66 o 3 12 0 128.90 94.65 40.11 o 4 12 0 123.76 132.08 35.44 o 5 12 0 332.22 284.23 39.77 o 6 12 0 112.18 103.00 31.87 o 7 12 0 26.69 26.60 25.94 o 8 12 0 2194.78 2303.76 73.30 o 9 12 0 10.02 3.77 25.46 o 10 12 0 1684.21 1747.94 78.60 o 1 13 0 2996.87 3190.51 144.36 o 2 13 0 549.13 395.56 71.91 o 3 13 0 743.04 790.62 64.86 o 4 13 0 440.22 398.64 46.82 o 5 13 0 230.90 185.02 36.85 o 6 13 0 518.53 512.39 46.86 o 7 13 0 855.05 924.64 54.10 o 8 13 0 363.41 377.94 43.01 o 9 13 0 1423.31 1596.07 75.96 o 0 14 0 1003.18 1019.06 137.78 o 1 14 0 8.61 25.49 49.65 o 2 14 0 63.57 57.58 46.34 o 3 14 0 1043.04 965.40 64.29 o 4 14 0 935.62 1046.20 66.45 o 5 14 0 207.30 234.88 37.92 o 6 14 0 165.38 183.89 33.88 o 7 14 0 441.77 529.81 45.08 o 8 14 0 353.73 388.43 72.70 o 1 15 0 20.29 40.66 51.04 o 2 15 0 306.06 398.88 93.92 o 3 15 0 63.45 80.45 52.57 o 4 15 0 981.09 968.56 95.74 o 5 15 0 41.53 89.49 33.27 o 6 15 0 1306.17 1435.73 98.54 o 0 16 0 85.03 130.47 79.78 o 1 16 0 237.93 313.07 62.97 o 2 16 0 92.87 141.11 57.96 o 3 16 0 562.53 672.20 79.63 o 4 16 0 58.25 22.51 56.20 o 1 0 1 1053.11 1278.93 13.01 o 2 0 1 1365.44 1446.59 16.05 o 3 0 1 2533.61 2564.04 25.87 o 4 0 1 1968.99 1692.59 28.57 o 5 0 1 604.03 600.96 18.20 o 6 0 1 1985.47 1871.18 32.71 o 7 0 1 9613.75 8295.35 293.13 o 8 0 1 1725.22 1850.45 72.43 o 9 0 1 310.59 457.01 131.65 o -10 1 1 1601.20 1710.88 171.56 o -9 1 1 1055.60 973.34 105.34 o -8 1 1 4757.80 4528.34 156.70 o -7 1 1 3704.49 3819.47 66.12 o -6 1 1 7373.00 7603.25 116.24 o -5 1 1 9368.39 8828.41 97.19 o -4 1 1 6368.53 6782.44 90.05 o -3 1 1 4523.76 4414.74 53.11 o -2 1 1 635.87 630.44 11.62 o -1 1 1 2949.08 3327.00 26.15 o 0 1 1 5506.08 5644.07 45.60 o 1 1 1 2630.98 3027.23 32.92 o 2 1 1 781.72 738.50 11.98 o 3 1 1 4653.48 4486.76 60.71 o 4 1 1 7846.74 8560.50 92.07 o 5 1 1 10303.37 9969.19 67.31 o 6 1 1 7163.28 7437.43 75.14 o 7 1 1 3905.08 4139.52 119.47 o 8 1 1 5261.21 5165.77 135.36 o 9 1 1 1151.53 1248.08 137.59 o -12 2 1 382.31 31.46 76.95 o -11 2 1 1711.10 1443.59 169.34 o -10 2 1 166.17 176.21 81.00 o -9 2 1 4349.69 4067.41 141.30 o -8 2 1 1780.00 1650.32 64.32 o -7 2 1 6993.78 6899.58 104.72 o -6 2 1 5848.93 6052.14 107.20 o -5 2 1 1360.59 1301.90 27.13 o -4 2 1 3794.73 3597.57 38.89 o -3 2 1 6089.03 6537.70 92.52 o -2 2 1 11914.41 12658.80 90.86 o -1 2 1 5970.04 6549.76 64.85 o 0 2 1 147.18 179.37 5.97 o 1 2 1 4931.13 5519.88 94.71 o 2 2 1 13070.27 13397.99 239.84 o 3 2 1 5920.37 6191.54 62.44 o 4 2 1 3880.87 3681.34 57.41 o 5 2 1 1957.07 2005.60 33.37 o 6 2 1 6098.84 5905.39 70.19 o 7 2 1 6758.99 6856.73 100.89 o 8 2 1 1756.05 1692.14 73.18 o 9 2 1 4144.52 3978.91 267.97 o 10 2 1 176.29 259.39 90.10 o 11 2 1 1969.56 2004.48 317.71 o -12 3 1 434.62 355.12 98.77 o -11 3 1 1425.24 979.24 295.19 o -10 3 1 1370.01 1416.45 99.52 o -9 3 1 961.10 952.46 88.45 o -8 3 1 1860.28 1555.33 59.19 o -7 3 1 4218.17 4151.83 85.31 o -6 3 1 6957.09 7522.34 100.80 o -5 3 1 7183.35 7599.67 138.90 o -4 3 1 3272.89 3347.45 56.17 o -3 3 1 40092.20 43361.30 426.13 o -2 3 1 26547.42 28247.87 200.81 o -1 3 1 9000.28 9701.54 81.91 o 0 3 1 6831.69 6276.95 36.55 o 1 3 1 9063.68 9710.93 53.89 o 2 3 1 25052.47 27009.04 272.73 o 3 3 1 39488.92 41074.87 318.79 o 4 3 1 2713.00 2631.39 51.73 o 5 3 1 6406.99 6453.16 139.61 o 6 3 1 6694.53 7078.31 131.18 o 7 3 1 4287.80 4345.97 123.64 o 8 3 1 1944.82 1747.13 74.15 o 9 3 1 1358.83 1439.97 87.51 o 10 3 1 1460.42 1475.49 104.89 o 11 3 1 1519.82 1427.86 105.43 o 12 3 1 414.51 5.79 67.31 o -13 4 1 95.64 122.30 75.25 o -12 4 1 1161.78 994.54 260.29 o -11 4 1 1515.79 1616.89 95.98 o -10 4 1 1403.92 1464.75 81.71 o -9 4 1 2919.46 3029.78 109.44 o -8 4 1 871.09 757.67 48.35 o -7 4 1 2597.47 2418.64 64.19 o -6 4 1 3276.78 3430.06 75.08 o -5 4 1 1924.34 2025.15 44.29 o -4 4 1 17384.32 19277.38 316.82 o -3 4 1 14222.99 15290.37 140.46 o -2 4 1 13137.97 13404.86 76.81 o -1 4 1 12759.64 12890.24 128.18 o 0 4 1 1908.62 2523.07 29.21 o 1 4 1 11270.56 10932.82 100.96 o 2 4 1 13956.72 14175.26 77.01 o 3 4 1 13531.42 14193.09 107.38 o 4 4 1 16627.44 18944.59 217.79 o 5 4 1 1459.36 1625.87 45.09 o 6 4 1 3071.67 2988.01 90.41 o 7 4 1 2692.72 2658.93 70.41 o 8 4 1 684.48 638.92 54.51 o 9 4 1 2606.41 2570.73 108.27 o 10 4 1 1387.21 1583.62 107.01 o 11 4 1 1612.82 1626.20 101.59 o 12 4 1 1033.50 974.17 85.31 o -13 5 1 78.70 30.10 62.44 o -12 5 1 1078.09 1140.66 85.55 o -11 5 1 1530.88 1297.73 87.38 o -10 5 1 615.95 610.00 59.31 o -9 5 1 1067.14 1176.06 67.36 o -8 5 1 1802.39 1681.17 72.83 o -7 5 1 1397.60 1205.48 50.44 o -6 5 1 2437.36 2473.87 62.37 o -5 5 1 1973.22 2232.88 55.75 o -4 5 1 393.95 494.12 24.30 o -3 5 1 7453.89 7733.98 76.88 o -2 5 1 14208.64 15299.89 117.00 o -1 5 1 1303.45 1230.03 21.07 o 0 5 1 3484.27 3111.44 32.31 o 1 5 1 1654.03 1633.91 25.33 o 2 5 1 12898.85 13774.37 143.89 o 3 5 1 8869.40 9360.92 106.39 o 4 5 1 379.90 460.65 27.69 o 5 5 1 1971.71 2122.73 56.20 o 6 5 1 2153.62 2041.64 61.37 o 7 5 1 1292.54 1142.96 69.24 o 8 5 1 1838.56 1656.37 71.78 o 9 5 1 1476.92 1591.24 79.02 o 10 5 1 382.28 399.02 49.85 o 11 5 1 1823.43 1549.94 241.92 o 12 5 1 1078.21 1184.36 84.25 o 13 5 1 72.46 113.10 64.26 o -13 6 1 200.04 300.40 68.84 o -12 6 1 974.67 1052.91 80.33 o -11 6 1 1592.99 1781.94 82.04 o -10 6 1 1221.44 1105.13 63.86 o -9 6 1 736.84 703.87 54.86 o -8 6 1 551.74 596.57 54.94 o -7 6 1 1423.02 1325.67 62.59 o -6 6 1 948.91 889.84 41.24 o -5 6 1 726.02 819.08 34.74 o -4 6 1 1718.17 1689.92 42.82 o -3 6 1 10764.54 11253.54 115.62 o -2 6 1 9102.48 9765.57 91.05 o -1 6 1 10277.55 10400.27 80.52 o 0 6 1 2861.31 2871.36 34.24 o 1 6 1 11243.67 11506.99 72.95 o 2 6 1 10074.26 10868.60 129.88 o 3 6 1 10545.50 11162.63 104.22 o 4 6 1 1472.23 1375.16 44.62 o 5 6 1 506.89 500.02 34.06 o 6 6 1 863.04 796.54 48.02 o 7 6 1 1661.90 1539.57 59.89 o 8 6 1 608.36 631.61 51.77 o 9 6 1 1145.88 1171.57 64.91 o 10 6 1 985.76 1031.31 65.26 o 11 6 1 1527.55 1620.06 75.11 o 12 6 1 931.00 899.00 71.61 o 13 6 1 179.75 183.77 60.62 o -12 7 1 562.96 555.95 52.13 o -11 7 1 982.35 943.24 62.34 o -10 7 1 2322.69 2365.36 83.50 o -9 7 1 295.64 305.80 43.02 o -8 7 1 622.21 606.46 51.76 o -7 7 1 1828.72 1767.53 68.82 o -6 7 1 2622.37 2490.29 88.07 o -5 7 1 3251.98 3138.94 102.13 o -4 7 1 2766.69 2698.16 60.58 o -3 7 1 5898.20 6171.48 84.29 o -2 7 1 5425.91 4879.65 69.80 o -1 7 1 722.52 566.20 25.54 o 0 7 1 1410.03 1350.03 38.36 o 1 7 1 1346.61 1211.88 29.26 o 2 7 1 6170.76 5722.90 74.14 o 3 7 1 5754.95 5742.19 79.72 o 4 7 1 2888.06 2811.59 61.43 o 5 7 1 3123.33 2985.72 68.38 o 6 7 1 2758.95 2639.25 71.73 o 7 7 1 1855.10 1735.04 69.05 o 8 7 1 835.69 791.53 57.38 o 9 7 1 200.26 167.00 37.51 o 10 7 1 2336.34 2313.88 152.23 o 11 7 1 1085.55 1102.23 61.94 o 12 7 1 530.80 544.66 60.76 o -12 8 1 699.64 777.03 71.64 o -11 8 1 987.11 1027.61 57.11 o -10 8 1 417.53 388.74 43.91 o -9 8 1 691.11 731.76 53.23 o -8 8 1 169.19 189.04 38.15 o -7 8 1 873.00 796.91 53.61 o -6 8 1 4904.23 4626.60 108.80 o -5 8 1 2822.85 2677.27 84.17 o -4 8 1 5988.80 5865.67 160.41 o -3 8 1 3258.04 3078.26 65.21 o -2 8 1 6265.32 6093.69 90.33 o -1 8 1 8793.73 8877.35 277.38 o 0 8 1 976.85 924.97 42.37 o 1 8 1 8729.87 8689.20 241.09 o 2 8 1 6095.33 5866.33 111.83 o 3 8 1 3016.31 2724.77 60.49 o 4 8 1 5966.62 5855.36 92.81 o 5 8 1 2746.06 2698.92 70.52 o 6 8 1 5101.82 4655.68 151.51 o 7 8 1 1326.61 1318.98 66.04 o 8 8 1 67.35 62.30 30.43 o 9 8 1 690.47 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