#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203798.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203798_Fobs loop_ _publ_author_name 'Terasaki, Yukiko' 'Fujihara, Takashi' 'Nagasawa, Akira' 'Kaizaki, Sumio' _publ_section_title ; fac-Triaqua[tris(2-pyridyl)amine-\k^3^N]chromium(III) tris(trifluoromethanesulfonate) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m854 _journal_page_last m856 _journal_volume 60 _journal_year 2004 _space_group_IT_number 147 _symmetry_space_group_name_Hall '-P 3' _symmetry_space_group_name_H-M 'P -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 13.0562 _cell_length_b 13.0562 _cell_length_c 10.4754 _exptl_crystal_F_000 806.00 _reflns_d_resolution_high 0.7497 _[local]_cod_data_source_file ob6366Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Crtpaaq in P-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 142.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 610.34 604.44 8.02 o -1 2 0 20.30 30.58 4.34 o 0 2 0 922.88 941.29 17.68 o -2 3 0 18679.43 14235.15 507.25 o -1 3 0 967.56 1066.38 21.30 o 0 3 0 16666.10 12850.84 983.93 o -3 4 0 6145.88 5781.42 80.24 o -2 4 0 12289.40 11806.91 194.48 o -1 4 0 8498.93 8635.41 125.05 o 0 4 0 9316.85 9079.46 104.18 o -4 5 0 10.06 11.72 0.45 o -3 5 0 5395.56 5083.59 66.22 o -2 5 0 4410.25 4746.20 92.03 o -1 5 0 47.52 43.12 0.80 o 0 5 0 123.82 182.11 2.38 o -5 6 0 2160.74 2230.69 36.88 o -4 6 0 584.33 577.00 8.44 o -3 6 0 18571.01 16413.26 381.57 o -2 6 0 805.30 831.39 13.87 o -1 6 0 579.80 611.80 6.18 o 0 6 0 8111.11 8106.33 129.96 o -6 7 0 4643.46 4612.57 64.75 o -5 7 0 66.43 93.61 2.43 o -4 7 0 123.39 98.59 1.78 o -3 7 0 125.28 119.12 2.49 o -2 7 0 738.22 698.35 11.88 o -1 7 0 2154.35 2215.61 23.02 o 0 7 0 5632.71 5644.71 81.20 o -7 8 0 285.03 247.19 6.46 o -6 8 0 5.94 8.85 0.50 o -5 8 0 268.02 270.92 5.81 o -4 8 0 50.32 37.55 1.06 o -3 8 0 247.76 251.75 4.05 o -2 8 0 501.62 484.08 11.16 o -1 8 0 1824.14 1986.12 59.70 o 0 8 0 152.60 134.94 2.70 o -8 9 0 726.22 783.32 20.42 o -7 9 0 5.43 8.90 2.01 o -6 9 0 329.16 340.83 15.07 o -5 9 0 1935.84 1943.42 37.62 o -4 9 0 41.23 23.16 1.05 o -3 9 0 1281.23 1313.07 42.24 o -2 9 0 4095.61 4085.65 61.83 o -1 9 0 128.28 133.69 1.80 o 0 9 0 3950.76 4056.43 104.05 o -9 10 0 213.53 215.43 4.16 o -8 10 0 468.81 475.61 8.60 o -7 10 0 715.41 652.26 8.32 o -6 10 0 911.47 879.82 28.74 o -5 10 0 61.26 43.43 1.40 o -4 10 0 992.94 987.41 19.60 o -3 10 0 2922.58 2909.60 56.86 o -2 10 0 4234.19 4285.56 72.02 o -1 10 0 58.58 56.82 1.63 o 0 10 0 1024.96 1012.00 26.32 o -10 11 0 1530.22 1539.33 43.66 o -9 11 0 227.17 231.58 4.99 o -8 11 0 155.82 133.52 3.46 o -7 11 0 986.11 934.51 21.34 o -6 11 0 312.55 317.33 7.43 o -5 11 0 542.42 517.01 12.43 o -4 11 0 371.27 362.74 7.96 o -3 11 0 22.42 21.08 1.26 o -2 11 0 233.62 249.62 6.40 o -1 11 0 956.99 960.03 25.39 o 0 11 0 79.53 74.29 3.24 o -11 12 0 314.11 312.06 9.13 o -10 12 0 6.76 5.46 0.92 o -9 12 0 17.14 13.28 0.98 o -8 12 0 40.52 45.00 1.56 o -7 12 0 224.74 226.15 5.19 o -6 12 0 0.87 0.79 0.59 o -5 12 0 34.15 30.69 1.32 o -4 12 0 200.69 208.96 4.91 o -3 12 0 0.70 0.30 0.60 o -2 12 0 199.13 219.10 9.23 o -1 12 0 0.35 1.19 0.81 o 0 12 0 45.04 35.53 1.73 o -12 13 0 0.61 1.16 1.01 o -11 13 0 0.46 1.48 0.85 o -10 13 0 36.83 41.75 1.79 o -9 13 0 226.37 240.68 5.53 o -8 13 0 22.62 21.74 1.19 o -7 13 0 13.10 13.31 1.02 o -6 13 0 374.59 354.41 6.56 o -5 13 0 371.33 378.94 10.42 o -4 13 0 22.54 26.52 1.54 o -3 13 0 50.65 56.87 2.55 o -2 13 0 394.34 344.56 11.51 o -1 13 0 208.20 192.06 8.48 o 0 13 0 215.80 204.99 6.56 o -13 14 0 365.95 393.39 10.86 o -12 14 0 43.47 46.82 2.53 o -11 14 0 84.20 87.53 2.61 o -10 14 0 1074.89 1104.03 27.89 o -9 14 0 57.14 48.21 1.76 o -8 14 0 236.13 238.91 4.17 o -7 14 0 786.07 803.38 17.85 o -6 14 0 34.69 24.52 1.56 o -5 14 0 84.80 78.62 2.40 o -4 14 0 67.52 59.40 3.44 o -3 14 0 235.91 241.88 4.86 o -2 14 0 83.02 90.64 4.03 o -1 14 0 202.41 193.30 4.53 o 0 14 0 78.55 91.05 3.34 o -14 15 0 66.86 70.72 3.09 o -13 15 0 27.07 29.73 2.86 o -12 15 0 1.65 1.71 0.97 o -11 15 0 68.79 66.57 2.40 o -10 15 0 0.03 1.43 0.88 o -9 15 0 8.80 12.11 1.14 o -8 15 0 34.17 37.41 1.71 o -7 15 0 0.49 2.23 0.96 o -6 15 0 47.78 51.35 2.17 o -5 15 0 52.18 47.36 2.49 o -4 15 0 81.91 89.13 5.18 o -3 15 0 8.23 4.31 1.34 o -2 15 0 0.19 1.77 1.21 o -1 15 0 1.37 5.25 1.52 o 0 15 0 17.92 15.47 2.44 o -13 16 0 65.37 75.67 2.71 o -12 16 0 1.34 0.74 1.02 o -11 16 0 266.24 287.85 4.70 o -10 16 0 135.82 153.21 5.16 o -9 16 0 405.80 412.69 7.64 o -8 16 0 328.24 325.13 5.97 o -7 16 0 136.09 148.42 4.93 o -6 16 0 68.06 64.17 3.13 o -5 16 0 130.62 133.08 3.98 o -4 16 0 7.40 8.06 1.58 o -3 16 0 5.63 4.56 1.51 o -11 17 0 135.72 149.75 5.40 o -10 17 0 1126.24 1259.38 21.92 o -9 17 0 240.72 274.22 4.83 o -8 17 0 121.46 131.69 5.78 o -7 17 0 280.87 305.66 7.12 o -6 17 0 212.49 226.01 5.24 o -1 1 1 6062.49 5845.15 103.16 o 0 1 1 3669.29 3694.93 59.52 o 1 1 1 11705.29 9607.74 989.63 o -3 2 1 381.04 421.58 6.53 o -2 2 1 14267.17 11909.65 342.51 o -1 2 1 3771.01 4271.21 57.36 o 0 2 1 3463.86 3498.34 68.71 o 1 2 1 1724.48 1892.19 27.98 o 2 2 1 1075.93 1095.95 16.17 o -5 3 1 596.83 614.18 9.27 o -4 3 1 131.37 122.92 4.95 o -3 3 1 890.88 991.50 16.08 o -2 3 1 1263.64 1347.53 27.84 o -1 3 1 8215.63 7930.12 211.10 o 0 3 1 207.03 157.28 2.62 o 1 3 1 124.67 152.63 2.80 o 2 3 1 6463.39 6964.10 136.23 o 3 3 1 423.57 377.59 5.84 o -7 4 1 2.55 1.14 0.28 o -6 4 1 217.81 324.97 4.50 o -5 4 1 21.35 5.94 0.52 o -4 4 1 17.30 10.32 1.91 o -3 4 1 14351.75 13049.51 476.23 o -2 4 1 1076.43 1084.94 22.38 o -1 4 1 300.80 288.75 4.56 o 0 4 1 3.91 16.75 8.03 o 1 4 1 1526.29 1453.15 23.44 o 2 4 1 2937.68 3181.29 43.35 o 3 4 1 9.46 10.97 0.63 o 4 4 1 1827.26 1892.74 46.00 o -9 5 1 344.21 325.04 9.33 o -8 5 1 595.83 554.42 11.55 o -7 5 1 2787.83 3107.73 56.39 o -6 5 1 161.61 143.55 2.64 o -5 5 1 4007.74 3954.23 73.81 o -4 5 1 339.77 382.85 8.19 o -3 5 1 4.42 42.78 2.70 o -2 5 1 8239.61 8022.10 174.28 o -1 5 1 295.59 267.63 3.21 o 0 5 1 737.46 793.56 12.30 o 1 5 1 122.94 59.96 0.97 o 2 5 1 1660.05 1952.90 29.58 o 3 5 1 1557.79 1590.25 18.75 o 4 5 1 611.13 605.70 17.23 o 5 5 1 1190.36 1112.66 30.50 o -11 6 1 1707.62 1668.66 24.59 o -10 6 1 322.57 336.29 8.85 o -9 6 1 1543.67 1569.52 29.03 o -8 6 1 358.40 382.72 7.18 o -7 6 1 1082.73 1045.12 17.28 o -6 6 1 2379.49 2253.04 34.83 o -5 6 1 1134.09 1038.35 17.90 o -4 6 1 790.05 835.59 14.15 o -3 6 1 5431.21 5444.68 111.63 o -2 6 1 941.85 996.39 19.76 o -1 6 1 1336.03 1356.88 18.82 o 0 6 1 124.35 154.17 2.03 o 1 6 1 663.67 604.11 7.03 o 2 6 1 1673.25 1739.14 20.92 o 3 6 1 361.53 395.73 9.92 o 4 6 1 22.83 18.50 1.38 o 5 6 1 86.84 86.67 1.85 o 6 6 1 6.01 7.11 0.79 o -13 7 1 286.16 278.09 3.53 o -12 7 1 171.83 166.97 2.64 o -11 7 1 2.41 2.85 0.69 o -10 7 1 1823.14 1868.24 47.94 o -9 7 1 814.22 821.15 16.05 o -8 7 1 48.26 43.99 1.05 o -7 7 1 8.79 18.44 0.69 o -6 7 1 663.85 711.25 14.15 o -5 7 1 4104.35 4254.27 105.87 o -4 7 1 550.49 589.65 10.74 o -3 7 1 665.26 759.97 10.07 o -2 7 1 6378.04 6640.07 83.14 o -1 7 1 402.20 471.48 7.04 o 0 7 1 912.55 925.52 13.64 o 1 7 1 10.96 21.53 0.87 o 2 7 1 187.49 200.43 3.19 o 3 7 1 589.54 544.59 7.29 o 4 7 1 455.91 436.28 11.37 o 5 7 1 337.01 304.23 4.44 o 6 7 1 506.38 478.45 8.15 o 7 7 1 255.36 276.85 5.41 o -15 8 1 1.51 0.90 0.83 o -14 8 1 130.78 121.54 4.00 o -13 8 1 138.38 133.37 3.30 o -12 8 1 30.62 34.37 3.66 o -11 8 1 974.73 975.73 21.87 o -10 8 1 98.60 91.31 2.10 o -9 8 1 41.11 54.65 1.14 o -8 8 1 6244.51 6308.94 150.39 o -7 8 1 783.88 781.10 15.86 o -6 8 1 386.35 418.90 7.72 o -5 8 1 1656.17 1624.77 32.45 o -4 8 1 190.03 230.90 6.78 o -3 8 1 1.30 7.04 1.75 o -2 8 1 3662.42 3671.02 40.49 o -1 8 1 950.70 876.09 13.15 o 0 8 1 2126.91 2246.61 19.37 o 1 8 1 1933.09 1891.33 25.33 o 2 8 1 184.59 168.31 5.95 o 3 8 1 108.53 111.27 2.31 o 4 8 1 370.00 372.03 7.07 o 5 8 1 628.36 584.53 9.40 o 6 8 1 408.26 397.37 7.01 o 7 8 1 9.50 5.97 1.00 o 8 8 1 483.44 477.31 6.01 o -17 9 1 549.12 568.21 11.53 o -16 9 1 324.23 319.20 5.83 o -15 9 1 12.56 11.16 1.51 o -14 9 1 371.05 358.55 5.71 o -13 9 1 828.84 835.35 30.31 o -12 9 1 333.85 321.00 9.22 o -11 9 1 1449.42 1531.11 42.50 o -10 9 1 971.48 995.50 24.47 o -9 9 1 2443.03 2383.58 58.68 o -8 9 1 1260.47 1256.22 23.36 o -7 9 1 31.04 14.78 0.85 o -6 9 1 278.89 278.12 4.99 o -5 9 1 32.42 38.03 1.42 o -4 9 1 219.96 202.46 5.38 o -3 9 1 553.75 595.24 7.46 o -2 9 1 69.91 82.25 1.57 o -1 9 1 430.14 492.18 6.86 o 0 9 1 155.72 184.74 3.02 o 1 9 1 207.44 176.20 4.03 o 2 9 1 255.64 228.69 2.92 o 3 9 1 99.71 96.55 2.49 o 4 9 1 287.53 311.43 3.70 o 5 9 1 738.64 744.86 9.38 o 6 9 1 5.25 7.10 1.17 o 7 9 1 98.71 103.44 2.67 o 8 9 1 158.18 160.12 4.46 o -17 10 1 24.73 28.56 2.26 o -16 10 1 144.63 152.57 4.22 o -15 10 1 107.51 100.04 3.48 o -14 10 1 132.48 106.51 5.25 o -13 10 1 13.88 12.02 1.53 o -12 10 1 77.84 78.96 5.40 o -11 10 1 403.09 356.86 10.62 o -10 10 1 231.33 194.34 8.88 o -9 10 1 131.05 151.78 3.13 o -8 10 1 55.04 40.65 2.12 o -7 10 1 7.51 9.60 0.78 o -6 10 1 56.50 61.19 1.88 o -5 10 1 747.93 668.72 12.06 o -4 10 1 21.84 15.61 0.83 o -3 10 1 113.13 107.47 2.31 o -2 10 1 2402.11 2468.47 38.07 o -1 10 1 1578.47 1563.09 26.87 o 0 10 1 350.49 338.53 4.05 o 1 10 1 268.55 272.23 7.55 o 2 10 1 184.89 177.00 4.49 o 3 10 1 200.69 197.41 4.27 o 4 10 1 229.35 213.76 5.98 o 5 10 1 0.05 0.09 1.06 o 6 10 1 612.59 645.67 9.69 o 7 10 1 85.93 87.93 3.52 o -17 11 1 4.20 7.59 1.58 o -16 11 1 2.40 2.92 1.28 o -15 11 1 13.50 13.35 1.65 o -14 11 1 167.57 149.83 3.91 o -13 11 1 29.00 24.04 1.78 o -12 11 1 211.13 202.87 4.81 o -11 11 1 452.20 464.94 13.56 o -10 11 1 8.48 7.12 0.91 o -9 11 1 18.47 20.71 1.09 o -8 11 1 86.70 90.78 1.96 o -7 11 1 233.39 230.17 4.76 o -6 11 1 58.48 49.43 1.49 o -5 11 1 1149.54 1156.16 26.25 o -4 11 1 0.61 2.08 0.72 o -3 11 1 258.37 264.14 5.52 o -2 11 1 2041.75 2192.11 40.47 o -1 11 1 113.43 94.95 2.79 o 0 11 1 600.18 595.90 10.70 o 1 11 1 1.23 2.45 0.82 o 2 11 1 125.70 120.88 2.85 o 3 11 1 277.51 276.08 6.85 o 4 11 1 51.26 53.92 4.01 o 5 11 1 135.74 133.89 3.95 o 6 11 1 262.42 277.60 5.71 o -16 12 1 177.20 176.04 6.93 o -15 12 1 244.12 248.33 5.20 o -14 12 1 113.78 115.20 3.53 o -13 12 1 317.51 310.35 7.31 o -12 12 1 647.30 653.61 17.41 o -11 12 1 15.16 14.77 1.23 o -10 12 1 111.27 107.30 3.16 o -9 12 1 1069.06 1073.29 25.42 o -8 12 1 9.64 7.89 0.84 o -7 12 1 444.03 421.61 10.67 o -6 12 1 97.70 96.94 3.37 o -5 12 1 16.60 19.90 1.02 o -4 12 1 132.17 137.76 2.64 o -3 12 1 54.00 47.41 1.59 o -2 12 1 134.37 144.74 4.22 o -1 12 1 64.09 61.84 2.10 o 0 12 1 635.94 579.98 14.26 o 1 12 1 22.02 19.01 1.42 o 2 12 1 135.40 138.79 4.40 o 3 12 1 286.75 284.34 8.26 o 4 12 1 71.81 69.93 4.97 o -16 13 1 73.45 70.13 3.16 o -15 13 1 0.64 -0.33 1.07 o -14 13 1 72.88 62.68 2.81 o -13 13 1 67.65 72.62 2.91 o -12 13 1 505.43 509.90 16.77 o -11 13 1 48.30 38.92 1.81 o -10 13 1 0.12 -0.05 0.74 o -9 13 1 3.97 3.86 0.78 o -8 13 1 49.13 35.56 1.46 o -7 13 1 27.82 18.65 1.14 o -6 13 1 1.24 3.75 1.76 o -5 13 1 236.08 231.87 4.90 o -4 13 1 108.60 101.06 3.90 o -3 13 1 173.51 177.70 7.02 o -2 13 1 107.63 94.93 4.57 o -1 13 1 18.02 15.89 1.36 o 0 13 1 85.87 81.83 3.05 o 1 13 1 207.25 227.77 5.29 o 2 13 1 1.96 2.16 1.28 o 3 13 1 1.22 1.23 1.29 o -15 14 1 37.51 28.65 2.23 o -14 14 1 238.79 238.71 8.11 o -13 14 1 107.89 99.11 7.07 o -12 14 1 36.43 35.15 1.87 o -11 14 1 683.17 707.05 16.38 o -10 14 1 218.82 223.71 6.91 o -9 14 1 68.77 68.20 2.13 o -8 14 1 825.32 882.62 23.25 o -7 14 1 118.89 103.32 3.14 o -6 14 1 6.73 7.32 1.10 o -5 14 1 837.85 880.02 22.78 o -4 14 1 194.16 180.94 8.69 o -3 14 1 53.59 49.94 2.87 o -2 14 1 1160.71 1190.63 20.50 o -1 14 1 296.63 307.27 5.61 o 0 14 1 6.37 9.91 1.33 o 1 14 1 111.34 125.73 7.32 o -15 15 1 573.84 604.00 8.57 o -14 15 1 65.86 77.22 3.22 o -13 15 1 178.32 187.90 4.56 o -12 15 1 658.28 706.54 20.71 o -11 15 1 22.94 27.62 1.75 o -10 15 1 5.48 4.64 1.08 o -9 15 1 183.79 199.93 5.09 o -8 15 1 7.71 7.03 1.12 o -7 15 1 4.81 9.32 1.23 o -6 15 1 104.11 112.82 2.96 o -5 15 1 69.54 67.78 2.86 o -4 15 1 69.04 65.38 2.86 o -3 15 1 0.74 0.61 1.13 o -2 15 1 8.17 4.93 1.40 o -1 15 1 120.85 118.34 3.84 o 0 15 1 226.93 222.51 6.61 o -13 16 1 0.01 -0.71 0.98 o -12 16 1 49.70 53.29 2.35 o -11 16 1 3.50 1.47 1.03 o -10 16 1 90.41 91.05 3.67 o -9 16 1 387.52 373.86 11.54 o -8 16 1 0.79 1.45 1.01 o -7 16 1 45.49 46.92 2.19 o -6 16 1 16.84 15.66 1.77 o -5 16 1 185.38 187.27 5.07 o -4 16 1 182.58 195.89 4.77 o -3 16 1 52.98 56.70 2.88 o -11 17 1 339.70 363.07 10.21 o -10 17 1 209.74 208.03 10.39 o -9 17 1 3.76 4.04 1.27 o -8 17 1 572.12 607.66 14.45 o -7 17 1 70.87 74.99 3.25 o -6 17 1 3.45 0.66 1.23 o -1 1 2 3546.36 3651.93 31.85 o 0 1 2 1143.75 1097.46 12.93 o 1 1 2 20359.30 16393.42 605.25 o -3 2 2 55.00 76.39 1.32 o -2 2 2 1509.68 1521.23 31.28 o -1 2 2 1015.45 1211.81 22.60 o 0 2 2 1120.20 1229.43 22.22 o 1 2 2 380.88 393.04 5.41 o 2 2 2 554.19 628.73 9.56 o -5 3 2 301.62 279.41 5.16 o -4 3 2 205.67 266.55 7.65 o -3 3 2 56.69 66.64 4.10 o -2 3 2 8745.34 8568.90 245.12 o -1 3 2 4388.95 4378.91 71.96 o 0 3 2 1895.03 1977.75 27.13 o 1 3 2 650.90 631.85 8.39 o 2 3 2 264.08 234.90 4.22 o 3 3 2 1429.33 1341.27 19.64 o -7 4 2 257.71 296.53 6.07 o -6 4 2 1934.05 1971.95 41.74 o -5 4 2 3324.87 3551.98 89.81 o -4 4 2 771.24 738.78 15.59 o -3 4 2 3.47 2.89 0.33 o -2 4 2 4445.46 4626.63 64.08 o -1 4 2 1782.43 1894.74 32.71 o 0 4 2 1184.46 1324.27 21.52 o 1 4 2 2185.27 2376.18 26.03 o 2 4 2 3714.09 4076.64 62.12 o 3 4 2 166.17 232.32 6.89 o 4 4 2 843.00 902.37 14.92 o -9 5 2 6.80 10.60 1.60 o -8 5 2 535.47 519.37 11.88 o -7 5 2 58.40 49.65 1.33 o -6 5 2 193.26 225.94 7.12 o -5 5 2 4964.89 5007.49 100.53 o -4 5 2 2817.29 3122.62 71.14 o -3 5 2 2014.91 2039.72 42.34 o -2 5 2 8328.02 8410.07 166.78 o -1 5 2 318.41 308.44 5.93 o 0 5 2 258.72 208.73 2.69 o 1 5 2 119.17 111.26 1.48 o 2 5 2 25.31 19.94 0.93 o 3 5 2 884.00 861.73 12.95 o 4 5 2 1312.35 1322.09 27.75 o 5 5 2 335.77 338.33 3.44 o -11 6 2 2795.10 2792.47 38.68 o -10 6 2 208.53 196.97 4.39 o -9 6 2 11.26 6.74 0.60 o -8 6 2 2449.68 2313.90 81.22 o -7 6 2 430.22 348.06 5.80 o -6 6 2 10.51 11.29 0.74 o -5 6 2 5270.95 5302.21 103.79 o -4 6 2 3330.72 3293.03 71.63 o -3 6 2 2726.77 2828.96 69.68 o -2 6 2 2349.27 2504.14 46.88 o -1 6 2 4455.59 4686.18 81.77 o 0 6 2 37.81 38.70 3.11 o 1 6 2 551.71 517.14 3.10 o 2 6 2 1739.82 1671.86 12.32 o 3 6 2 22.28 25.02 0.95 o 4 6 2 743.38 768.54 10.71 o 5 6 2 1053.76 1118.74 11.76 o 6 6 2 9.00 10.68 1.28 o -13 7 2 331.75 319.25 6.39 o -12 7 2 563.56 588.68 10.68 o -11 7 2 12.71 15.25 0.98 o -10 7 2 52.91 48.99 1.55 o -9 7 2 55.93 66.35 2.31 o -8 7 2 1124.75 1012.30 17.09 o -7 7 2 17.38 35.76 0.87 o -6 7 2 0.62 2.38 0.36 o -5 7 2 813.03 860.28 23.03 o -4 7 2 548.41 540.32 14.65 o -3 7 2 107.47 124.39 2.49 o -2 7 2 2627.31 2793.56 60.08 o -1 7 2 113.26 148.68 5.02 o 0 7 2 693.41 743.61 7.96 o 1 7 2 158.46 154.70 2.17 o 2 7 2 36.96 36.54 1.01 o 3 7 2 64.49 55.81 1.47 o 4 7 2 75.94 76.91 2.30 o 5 7 2 78.78 74.81 2.68 o 6 7 2 141.79 139.56 2.63 o 7 7 2 148.41 132.16 2.70 o -15 8 2 23.26 23.57 1.44 o -14 8 2 2.55 3.02 0.87 o -13 8 2 20.70 14.79 1.10 o -12 8 2 388.33 340.41 8.62 o -11 8 2 203.98 190.48 3.79 o -10 8 2 254.31 228.79 6.66 o -9 8 2 151.06 160.77 3.77 o -8 8 2 160.05 159.32 2.94 o -7 8 2 206.48 223.96 4.38 o -6 8 2 120.43 123.34 4.68 o -5 8 2 2823.72 2949.09 77.68 o -4 8 2 343.54 347.58 8.49 o -3 8 2 372.97 390.58 9.17 o -2 8 2 896.85 923.91 29.15 o -1 8 2 1.43 2.07 0.36 o 0 8 2 1136.97 1078.69 20.21 o 1 8 2 1591.72 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5.19 o -7 6 12 24.00 29.96 2.64 o -6 6 12 129.20 124.22 4.84 o -5 6 12 411.43 419.46 17.38 o -4 6 12 27.04 30.65 2.80 o -3 6 12 265.11 241.03 6.46 o -2 6 12 78.59 75.71 4.37 o -1 6 12 220.93 212.74 13.41 o 0 6 12 192.72 193.94 4.76 o 1 6 12 5.18 8.18 1.52 o 2 6 12 6.87 5.59 1.30 o -8 7 12 10.99 10.53 2.12 o -7 7 12 55.51 62.60 3.70 o -6 7 12 128.82 132.18 4.98 o -5 7 12 7.27 7.88 1.51 o -4 7 12 4.55 4.70 1.69 o -3 7 12 366.86 411.98 18.35 o -2 7 12 9.69 9.08 2.00 o -1 7 12 5.57 3.83 1.37 o 0 7 12 275.43 305.47 8.11 o 1 7 12 32.54 34.57 1.88 o -7 8 12 2.30 3.31 1.33 o -6 8 12 21.92 18.87 1.93 o -5 8 12 139.43 145.99 8.87 o -4 8 12 107.82 84.64 4.24 o -3 8 12 55.77 53.27 3.64 o -2 8 12 187.93 199.39 6.27 o -1 8 12 3.10 5.05 1.49 o 0 0 13 327.86 363.27 8.64 o -1 1 13 2.70 1.70 1.18 o 0 1 13 5.05 7.10 1.11 o 1 1 13 30.54 25.16 1.59 o -3 2 13 32.28 39.85 2.42 o -2 2 13 29.54 28.69 1.89 o -1 2 13 49.45 49.36 2.77 o 0 2 13 22.61 17.89 1.42 o 1 2 13 154.10 169.49 3.64 o 2 2 13 1.07 1.90 0.98 o 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