#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/39/2203933.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203933_Fobs loop_ _publ_author_name '\"Oz\,celik, Suzan' 'Din\,cer, Muharrem' 'Y\?ild\?ir\?im, \.Ismail' 'Ak\,camur, Yunus' _publ_section_title ; 1-Ethyl-5-(4-methoxybenzoyl)-4-(4-methoxyphenyl)pyrimidine-2(1H)-thione ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1123 _journal_page_last o1125 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.4718 _cell_length_b 17.6737 _cell_length_c 17.0718 _exptl_crystal_F_000 1600.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ob6369Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' muh24 in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 388.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22557.51 21117.32 890.09 o 4 0 0 2446.83 2423.98 87.89 o 6 0 0 4797.44 4676.53 176.49 o 8 0 0 14.28 46.01 44.70 o 10 0 0 1737.28 1695.80 65.49 o 12 0 0 133.29 194.89 63.07 o 14 0 0 60.94 74.45 81.07 o 2 1 0 6664.58 6025.27 159.26 o 4 1 0 10303.25 9843.88 284.99 o 6 1 0 93.14 103.68 41.60 o 8 1 0 5098.02 5028.38 144.19 o 10 1 0 1227.22 1316.77 48.41 o 12 1 0 655.93 633.35 49.13 o 14 1 0 135.22 159.99 57.02 o 0 2 0 38353.94 36385.38 1292.49 o 2 2 0 14869.19 14489.11 207.11 o 4 2 0 9264.13 8709.42 273.84 o 6 2 0 8045.13 8071.80 236.97 o 8 2 0 260.43 217.37 37.97 o 10 2 0 10.31 55.68 39.45 o 12 2 0 360.47 279.93 44.77 o 14 2 0 215.62 220.96 48.54 o 2 3 0 50.95 131.75 46.55 o 4 3 0 3511.72 3404.89 103.05 o 6 3 0 4786.86 5206.84 140.39 o 8 3 0 240.14 204.84 40.77 o 10 3 0 1416.20 1352.79 45.52 o 12 3 0 89.12 88.83 44.13 o 14 3 0 15.30 -6.21 53.15 o 0 4 0 18688.60 17695.27 403.43 o 2 4 0 1.38 30.91 42.58 o 4 4 0 3496.48 3071.56 79.79 o 6 4 0 541.67 683.33 41.06 o 8 4 0 542.25 578.66 39.18 o 10 4 0 867.23 916.91 40.32 o 12 4 0 0.73 -7.25 44.18 o 14 4 0 70.67 88.93 42.25 o 2 5 0 4054.45 4259.68 118.73 o 4 5 0 2841.25 3120.27 86.58 o 6 5 0 6.12 7.90 38.05 o 8 5 0 255.06 221.98 44.80 o 10 5 0 594.06 610.51 39.76 o 12 5 0 1285.05 1237.19 47.87 o 14 5 0 15.99 35.94 50.80 o 0 6 0 9887.03 9174.92 202.74 o 2 6 0 4.82 10.51 45.10 o 4 6 0 14931.69 16209.58 194.95 o 6 6 0 0.06 24.67 39.57 o 8 6 0 1046.88 998.14 39.58 o 10 6 0 2470.65 2301.74 88.72 o 12 6 0 66.58 53.74 45.04 o 14 6 0 18.71 8.05 49.89 o 2 7 0 1980.46 1839.35 53.22 o 4 7 0 11302.86 11722.31 225.08 o 6 7 0 1040.23 944.63 47.95 o 8 7 0 383.80 417.33 45.66 o 10 7 0 967.94 1073.64 50.95 o 12 7 0 966.28 1053.33 47.58 o 0 8 0 2593.91 2672.95 79.95 o 2 8 0 6210.89 6192.98 145.83 o 4 8 0 5005.40 5647.01 86.57 o 6 8 0 254.13 271.60 46.30 o 8 8 0 2380.10 2310.32 76.29 o 10 8 0 71.34 124.34 39.35 o 12 8 0 295.37 323.98 44.15 o 2 9 0 1959.16 1727.50 45.63 o 4 9 0 412.24 406.40 59.00 o 6 9 0 3250.09 3132.90 103.60 o 8 9 0 62.25 94.04 44.27 o 10 9 0 0.58 36.41 50.45 o 12 9 0 555.85 569.10 46.49 o 0 10 0 124.03 162.59 74.51 o 2 10 0 1289.52 1223.01 45.82 o 4 10 0 93.93 113.84 43.41 o 6 10 0 345.93 279.41 47.31 o 8 10 0 0.37 55.96 50.70 o 10 10 0 429.90 426.19 48.54 o 12 10 0 88.83 131.62 47.76 o 2 11 0 3987.82 3908.44 63.81 o 4 11 0 2532.71 2590.48 62.96 o 6 11 0 1357.49 1338.58 58.63 o 8 11 0 5529.28 5289.18 247.11 o 10 11 0 9.74 29.18 56.11 o 12 11 0 134.68 118.42 55.71 o 0 12 0 1865.15 1891.02 88.24 o 2 12 0 1200.79 1238.71 46.00 o 4 12 0 53.56 23.34 48.91 o 6 12 0 446.72 497.37 57.73 o 8 12 0 1864.79 1975.59 85.43 o 10 12 0 62.52 135.27 52.15 o 12 12 0 5.52 5.11 53.28 o 2 13 0 1559.06 1522.86 53.02 o 4 13 0 10.39 54.93 47.41 o 6 13 0 790.29 720.02 49.65 o 8 13 0 1855.47 1705.48 98.61 o 10 13 0 557.16 615.94 56.20 o 0 14 0 26.29 125.70 80.17 o 2 14 0 657.39 696.67 46.12 o 4 14 0 443.23 386.66 53.73 o 6 14 0 30.53 88.12 51.43 o 8 14 0 23.89 92.35 83.19 o 10 14 0 5.60 54.86 68.84 o 2 15 0 956.52 990.58 51.15 o 4 15 0 744.59 775.14 59.99 o 6 15 0 572.90 560.76 51.97 o 8 15 0 942.61 841.47 77.77 o 10 15 0 144.30 173.31 62.69 o 0 16 0 376.15 460.64 70.73 o 2 16 0 103.56 109.75 53.33 o 4 16 0 402.23 329.32 52.51 o 6 16 0 87.34 66.70 55.32 o 8 16 0 181.80 173.65 66.66 o 2 17 0 34.27 34.09 50.37 o 4 17 0 86.27 104.84 52.13 o 6 17 0 809.60 810.30 65.55 o 8 17 0 0.40 -35.95 61.35 o 0 18 0 439.72 522.44 131.88 o 2 18 0 695.58 737.36 54.01 o 4 18 0 47.44 17.32 59.57 o 6 18 0 441.59 579.96 57.65 o 2 19 0 194.73 212.88 50.97 o 4 19 0 523.30 409.87 54.36 o 6 19 0 69.93 45.19 57.60 o 0 20 0 551.78 653.98 74.95 o 2 20 0 19.11 70.86 56.85 o 4 20 0 42.68 64.02 59.47 o 1 1 1 5931.15 5639.80 95.64 o 2 1 1 1818.84 1773.88 39.19 o 3 1 1 557.74 568.51 31.17 o 4 1 1 1835.23 1936.58 36.10 o 5 1 1 1324.05 1325.84 27.67 o 6 1 1 7896.12 7790.05 152.57 o 7 1 1 450.68 484.00 26.76 o 8 1 1 0.56 35.12 24.85 o 9 1 1 434.95 443.03 28.45 o 10 1 1 96.19 88.05 26.90 o 11 1 1 21.83 35.46 28.08 o 12 1 1 222.26 267.72 33.85 o 13 1 1 6.80 -5.14 32.32 o 14 1 1 93.46 128.64 35.86 o 0 2 1 12336.85 12145.62 769.10 o 1 2 1 156.78 186.56 36.81 o 2 2 1 3313.82 3303.82 49.06 o 3 2 1 78.93 87.20 34.29 o 4 2 1 82.45 105.65 28.48 o 5 2 1 722.16 735.07 27.16 o 6 2 1 1665.82 1700.40 48.58 o 7 2 1 902.22 975.21 29.19 o 8 2 1 721.52 591.35 28.35 o 9 2 1 192.08 215.05 27.36 o 10 2 1 4605.85 4644.29 92.47 o 11 2 1 5.62 8.85 30.59 o 12 2 1 139.72 146.46 33.82 o 13 2 1 1.17 36.82 33.83 o 14 2 1 185.07 199.38 36.92 o 1 3 1 26502.86 24462.76 441.46 o 2 3 1 2483.94 2487.00 41.89 o 3 3 1 2697.10 2804.37 44.69 o 4 3 1 6367.17 5827.84 78.99 o 5 3 1 3110.11 3279.18 47.83 o 6 3 1 173.28 196.53 24.91 o 7 3 1 10.39 5.16 26.76 o 8 3 1 1694.87 1741.18 37.13 o 9 3 1 1292.09 1279.05 30.99 o 10 3 1 4380.69 4479.72 99.05 o 11 3 1 396.19 411.44 26.71 o 12 3 1 189.72 161.86 29.72 o 13 3 1 75.92 63.30 32.01 o 14 3 1 143.95 163.38 37.70 o 0 4 1 25956.15 26117.72 739.05 o 1 4 1 122.37 177.39 35.29 o 2 4 1 1470.48 1490.64 39.42 o 3 4 1 5340.49 5215.65 64.32 o 4 4 1 1108.67 1200.27 35.59 o 5 4 1 2261.09 2499.06 35.11 o 6 4 1 13115.13 13830.84 223.92 o 7 4 1 408.11 443.74 24.25 o 8 4 1 1504.85 1280.11 28.22 o 9 4 1 3410.51 3405.32 57.77 o 10 4 1 572.74 541.41 27.75 o 11 4 1 500.24 473.61 27.07 o 12 4 1 49.20 85.43 29.01 o 13 4 1 28.92 36.78 33.70 o 14 4 1 9.08 23.84 32.44 o 1 5 1 466.69 481.81 38.91 o 2 5 1 1068.66 1140.35 43.06 o 3 5 1 2557.32 2452.77 38.55 o 4 5 1 7080.57 6482.80 98.56 o 5 5 1 47.68 27.11 28.73 o 6 5 1 1422.75 1500.02 35.27 o 7 5 1 0.15 15.72 28.35 o 8 5 1 20.74 40.15 26.74 o 9 5 1 722.17 677.85 29.31 o 10 5 1 379.98 356.73 27.56 o 11 5 1 301.13 321.08 29.27 o 12 5 1 670.29 624.85 29.98 o 13 5 1 369.29 348.26 30.58 o 14 5 1 176.56 262.67 36.13 o 0 6 1 6098.81 5984.28 130.38 o 1 6 1 2151.98 2244.50 48.48 o 2 6 1 1287.22 1343.04 35.74 o 3 6 1 2161.77 2114.94 37.19 o 4 6 1 469.44 543.82 31.98 o 5 6 1 17.39 15.62 31.58 o 6 6 1 460.96 488.91 31.08 o 7 6 1 126.80 128.43 36.69 o 8 6 1 1433.21 1305.20 30.88 o 9 6 1 105.92 106.51 27.95 o 10 6 1 1272.94 1310.13 31.71 o 11 6 1 96.14 122.60 32.08 o 12 6 1 186.96 191.63 33.39 o 13 6 1 81.79 97.19 32.77 o 14 6 1 127.74 145.02 36.97 o 1 7 1 0.01 2.22 36.94 o 2 7 1 3359.55 3641.09 58.42 o 3 7 1 621.49 653.17 32.94 o 4 7 1 832.77 688.51 32.84 o 5 7 1 62.22 100.39 31.14 o 6 7 1 13.67 13.33 31.38 o 7 7 1 4.87 32.52 29.98 o 8 7 1 0.18 20.97 28.62 o 9 7 1 6.05 5.85 31.35 o 10 7 1 1096.90 1162.51 38.15 o 11 7 1 136.23 138.41 30.34 o 12 7 1 135.53 200.25 32.77 o 13 7 1 95.28 77.83 35.49 o 0 8 1 630.52 813.43 49.27 o 1 8 1 1090.49 1110.00 42.90 o 2 8 1 1882.31 2294.30 38.17 o 3 8 1 166.45 121.42 33.80 o 4 8 1 23.06 -2.74 30.48 o 5 8 1 502.34 551.27 30.37 o 6 8 1 34.24 28.15 30.04 o 7 8 1 81.88 55.56 33.51 o 8 8 1 696.13 706.01 35.70 o 9 8 1 18.74 37.59 29.94 o 10 8 1 88.26 89.14 31.51 o 11 8 1 409.53 407.18 32.48 o 12 8 1 18.49 20.49 31.68 o 13 8 1 21.06 56.95 33.37 o 1 9 1 131.45 177.10 33.69 o 2 9 1 7250.01 7649.33 138.21 o 3 9 1 489.36 541.80 30.48 o 4 9 1 643.14 542.69 39.68 o 5 9 1 30.27 24.01 34.03 o 6 9 1 67.95 150.88 33.59 o 7 9 1 30.77 61.87 31.54 o 8 9 1 186.87 223.18 33.79 o 9 9 1 149.48 97.55 38.78 o 10 9 1 6.96 -0.29 32.34 o 11 9 1 3.31 5.12 33.12 o 12 9 1 0.58 2.66 34.03 o 13 9 1 4.39 22.40 37.55 o 0 10 1 1708.25 1781.71 59.50 o 1 10 1 356.32 393.26 38.25 o 2 10 1 5044.29 5207.28 101.99 o 3 10 1 0.03 -19.03 29.04 o 4 10 1 16.24 20.46 33.93 o 5 10 1 399.33 390.69 34.36 o 6 10 1 5.47 30.60 31.34 o 7 10 1 191.54 220.62 35.54 o 8 10 1 52.89 29.15 37.57 o 9 10 1 47.68 52.53 33.90 o 10 10 1 210.34 237.90 38.75 o 11 10 1 63.05 96.93 38.47 o 12 10 1 67.31 88.55 33.98 o 13 10 1 124.77 162.54 38.46 o 1 11 1 163.39 181.45 36.13 o 2 11 1 295.70 404.16 34.25 o 3 11 1 81.14 87.74 32.15 o 4 11 1 1781.27 1981.11 37.30 o 5 11 1 203.05 197.82 34.08 o 6 11 1 2122.15 1922.86 42.21 o 7 11 1 194.83 208.32 36.84 o 8 11 1 1056.33 1033.49 38.02 o 9 11 1 0.99 40.37 33.97 o 10 11 1 0.44 -17.87 36.83 o 11 11 1 22.53 43.33 32.80 o 12 11 1 42.15 58.63 35.23 o 0 12 1 90.87 119.88 50.33 o 1 12 1 555.70 598.38 37.28 o 2 12 1 385.90 312.29 33.96 o 3 12 1 44.52 83.44 29.84 o 4 12 1 51.68 61.48 33.10 o 5 12 1 188.44 214.81 34.11 o 6 12 1 1.02 60.28 36.09 o 7 12 1 1286.33 1273.82 61.25 o 8 12 1 2477.51 2418.60 47.34 o 9 12 1 217.28 228.87 35.61 o 10 12 1 106.31 130.50 40.57 o 11 12 1 93.92 91.75 33.95 o 12 12 1 0.04 -0.16 36.64 o 1 13 1 14.89 17.06 37.56 o 2 13 1 202.68 182.77 31.75 o 3 13 1 242.52 265.94 34.66 o 4 13 1 226.87 243.83 34.18 o 5 13 1 431.12 386.64 37.06 o 6 13 1 1028.72 927.79 38.82 o 7 13 1 11.69 -8.95 39.74 o 8 13 1 55.28 39.66 42.39 o 9 13 1 5.63 23.48 40.13 o 10 13 1 20.02 20.82 38.30 o 11 13 1 1.48 -48.00 41.16 o 0 14 1 605.03 706.25 59.77 o 1 14 1 49.39 75.88 35.84 o 2 14 1 4307.87 4139.70 89.51 o 3 14 1 4.85 19.70 36.37 o 4 14 1 305.18 305.35 34.93 o 5 14 1 344.26 381.03 39.96 o 6 14 1 332.48 288.21 36.41 o 7 14 1 503.68 477.50 38.19 o 8 14 1 36.64 72.61 42.59 o 9 14 1 30.94 72.26 46.35 o 10 14 1 503.28 555.92 49.14 o 11 14 1 2.17 -16.93 45.55 o 1 15 1 260.37 282.69 30.36 o 2 15 1 5264.60 5025.29 93.41 o 3 15 1 7.34 23.76 34.67 o 4 15 1 3.16 12.63 34.32 o 5 15 1 1.34 12.75 39.72 o 6 15 1 48.24 90.57 40.15 o 7 15 1 422.90 402.32 40.40 o 8 15 1 25.72 39.29 40.56 o 9 15 1 1.98 19.76 42.73 o 10 15 1 79.77 84.88 50.41 o 0 16 1 426.95 505.43 61.52 o 1 16 1 211.32 177.13 34.49 o 2 16 1 254.08 299.80 35.12 o 3 16 1 127.27 152.24 35.24 o 4 16 1 9.39 11.61 36.06 o 5 16 1 17.01 27.70 47.84 o 6 16 1 61.57 24.02 39.11 o 7 16 1 0.18 2.62 42.76 o 8 16 1 6.84 51.18 53.17 o 9 16 1 28.19 36.36 50.07 o 1 17 1 157.14 194.07 32.83 o 2 17 1 580.86 567.14 33.24 o 3 17 1 0.51 16.06 33.26 o 4 17 1 523.91 548.32 35.33 o 5 17 1 315.38 317.53 48.13 o 6 17 1 40.76 21.56 40.70 o 7 17 1 24.58 -32.02 50.31 o 8 17 1 28.35 18.03 45.61 o 0 18 1 392.17 352.32 58.64 o 1 18 1 128.07 172.52 39.16 o 2 18 1 128.58 136.29 37.18 o 3 18 1 32.84 14.38 39.11 o 4 18 1 80.62 78.98 41.17 o 5 18 1 150.68 160.04 44.87 o 6 18 1 12.58 27.98 45.60 o 7 18 1 0.02 -20.93 43.92 o 1 19 1 14.47 5.97 40.23 o 2 19 1 6.19 6.01 36.80 o 3 19 1 221.91 206.84 40.31 o 4 19 1 231.51 93.96 45.38 o 5 19 1 1.93 27.35 49.97 o 6 19 1 14.24 41.33 50.70 o 0 20 1 75.98 60.24 57.70 o 1 20 1 48.59 19.46 40.21 o 2 20 1 76.50 72.84 42.42 o 3 20 1 0.52 27.50 42.88 o 4 20 1 59.20 51.42 41.00 o 0 0 2 9350.28 9867.75 203.22 o 1 0 2 88.65 93.74 44.68 o 2 0 2 6370.63 5974.50 184.20 o 3 0 2 1744.89 1805.78 53.91 o 4 0 2 142.29 175.93 34.32 o 5 0 2 642.18 737.65 37.84 o 6 0 2 446.21 479.74 35.23 o 7 0 2 43.40 52.06 35.16 o 8 0 2 2172.65 1998.63 61.55 o 9 0 2 3763.07 3560.35 143.91 o 10 0 2 153.06 190.82 42.05 o 11 0 2 697.40 731.89 53.03 o 12 0 2 0.20 14.91 44.09 o 13 0 2 116.47 93.26 44.18 o 14 0 2 116.90 129.29 48.87 o 1 1 2 397.76 468.89 34.51 o 2 1 2 17905.77 17743.09 343.73 o 3 1 2 762.42 819.18 33.68 o 4 1 2 15978.42 16619.20 316.18 o 5 1 2 112.71 95.29 25.76 o 6 1 2 1773.45 1837.61 39.09 o 7 1 2 153.91 101.29 28.26 o 8 1 2 0.01 -2.35 24.22 o 9 1 2 56.08 62.64 26.89 o 10 1 2 247.53 277.14 26.56 o 11 1 2 314.59 372.00 28.00 o 12 1 2 178.97 142.19 31.46 o 13 1 2 177.86 152.68 37.80 o 14 1 2 350.23 390.13 36.79 o 0 2 2 1941.46 1928.98 86.96 o 1 2 2 6719.76 6368.56 107.57 o 2 2 2 9755.87 8977.95 153.51 o 3 2 2 4914.62 5064.04 80.83 o 4 2 2 3399.93 3341.59 59.73 o 5 2 2 6.95 9.94 25.64 o 6 2 2 326.60 333.54 27.66 o 7 2 2 3162.58 2878.30 51.37 o 8 2 2 1929.50 1862.88 45.03 o 9 2 2 526.77 509.89 26.45 o 10 2 2 1377.53 1351.39 33.65 o 11 2 2 32.66 11.69 29.66 o 12 2 2 15.37 0.16 28.67 o 13 2 2 5.36 2.06 34.98 o 14 2 2 94.41 142.26 35.95 o 1 3 2 2099.70 2391.80 59.32 o 2 3 2 2.62 7.73 40.75 o 3 3 2 16262.77 15457.80 260.54 o 4 3 2 1124.81 1124.71 30.88 o 5 3 2 2385.94 2359.33 53.05 o 6 3 2 55.23 37.44 24.55 o 7 3 2 139.19 181.18 28.39 o 8 3 2 8.81 -1.60 27.20 o 9 3 2 735.78 672.35 29.71 o 10 3 2 696.00 758.33 29.87 o 11 3 2 131.53 141.86 29.97 o 12 3 2 112.82 107.75 29.63 o 13 3 2 0.01 17.48 32.86 o 14 3 2 34.22 9.50 33.67 o 0 4 2 261.97 246.48 54.59 o 1 4 2 8038.46 8010.43 184.85 o 2 4 2 4380.70 4191.56 61.52 o 3 4 2 4539.00 4607.66 70.67 o 4 4 2 6853.21 6534.59 104.27 o 5 4 2 19.19 43.06 25.69 o 6 4 2 565.75 472.80 28.65 o 7 4 2 33.89 40.97 26.08 o 8 4 2 748.20 785.73 28.11 o 9 4 2 32.29 49.69 27.09 o 10 4 2 1.89 23.19 26.45 o 11 4 2 285.52 253.55 31.10 o 12 4 2 186.83 153.30 29.12 o 13 4 2 86.39 92.04 29.81 o 14 4 2 22.52 62.23 37.19 o 1 5 2 2920.35 2602.07 63.21 o 2 5 2 1058.94 1034.46 37.50 o 3 5 2 1.63 2.30 33.39 o 4 5 2 1185.79 1184.10 36.54 o 5 5 2 541.44 559.68 34.10 o 6 5 2 3827.31 3638.50 64.77 o 7 5 2 125.63 173.10 29.72 o 8 5 2 468.03 528.37 28.01 o 9 5 2 10.99 29.54 26.55 o 10 5 2 46.21 39.19 27.81 o 11 5 2 761.54 700.32 31.27 o 12 5 2 112.17 157.75 32.15 o 13 5 2 124.84 88.74 32.18 o 14 5 2 31.25 25.15 33.70 o 0 6 2 19.89 67.95 57.72 o 1 6 2 3385.37 3445.32 74.89 o 2 6 2 3630.92 3435.20 82.09 o 3 6 2 902.57 856.84 31.19 o 4 6 2 1060.35 1232.41 33.17 o 5 6 2 41.34 71.36 31.76 o 6 6 2 309.21 346.10 33.11 o 7 6 2 5.74 23.57 28.45 o 8 6 2 168.53 194.70 26.08 o 9 6 2 400.32 383.15 27.06 o 10 6 2 71.47 105.49 30.46 o 11 6 2 112.64 85.33 29.40 o 12 6 2 287.92 244.09 29.43 o 13 6 2 1.61 30.59 31.06 o 14 6 2 31.84 30.15 35.71 o 1 7 2 389.19 332.75 38.46 o 2 7 2 635.11 591.13 32.57 o 3 7 2 117.20 122.71 34.03 o 4 7 2 174.17 238.34 33.22 o 5 7 2 2116.64 2103.19 36.31 o 6 7 2 2004.28 1785.11 51.80 o 7 7 2 52.50 50.81 29.43 o 8 7 2 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7 214.71 180.55 31.15 o 3 6 7 1595.57 1564.14 33.34 o 4 6 7 31.80 79.94 28.75 o 5 6 7 473.00 484.47 29.81 o 6 6 7 746.41 757.87 33.27 o 7 6 7 124.30 151.91 31.36 o 8 6 7 696.42 719.78 32.96 o 9 6 7 488.80 510.83 30.80 o 10 6 7 88.72 105.69 30.71 o 11 6 7 2.61 -9.35 34.90 o 12 6 7 47.10 36.33 33.99 o 13 6 7 2.70 32.64 37.58 o 1 7 7 121.11 114.17 34.82 o 2 7 7 980.11 929.93 33.31 o 3 7 7 489.47 457.04 34.38 o 4 7 7 297.66 273.50 31.07 o 5 7 7 39.11 20.04 29.11 o 6 7 7 342.79 334.38 32.69 o 7 7 7 29.73 28.10 29.95 o 8 7 7 1135.35 1044.24 31.85 o 9 7 7 1273.79 1263.20 34.53 o 10 7 7 26.48 48.22 30.96 o 11 7 7 20.91 8.91 35.65 o 12 7 7 40.37 63.87 36.05 o 13 7 7 36.92 19.73 40.57 o 0 8 7 1395.84 1546.85 60.56 o 1 8 7 295.08 348.19 31.53 o 2 8 7 2208.39 2171.36 40.94 o 3 8 7 334.77 346.84 32.41 o 4 8 7 707.45 816.41 35.63 o 5 8 7 87.64 69.88 32.13 o 6 8 7 562.70 577.46 32.00 o 7 8 7 0.31 -6.15 30.34 o 8 8 7 588.53 627.48 31.70 o 9 8 7 109.98 139.49 29.63 o 10 8 7 65.46 70.86 32.41 o 11 8 7 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33.35 o 13 2 8 46.50 61.07 33.36 o 1 3 8 3734.27 3716.86 54.40 o 2 3 8 807.13 830.39 31.08 o 3 3 8 170.32 221.86 28.95 o 4 3 8 563.98 493.97 28.38 o 5 3 8 1035.14 1043.04 29.37 o 6 3 8 313.24 358.11 29.56 o 7 3 8 1292.24 1360.83 31.56 o 8 3 8 215.75 224.30 30.56 o 9 3 8 72.98 85.04 29.12 o 10 3 8 36.59 57.29 28.66 o 11 3 8 108.32 125.05 31.64 o 12 3 8 77.22 77.65 35.33 o 13 3 8 74.47 57.53 37.09 o 0 4 8 3433.39 3455.49 99.42 o 1 4 8 4360.87 4356.41 86.90 o 2 4 8 1063.64 1035.29 30.61 o 3 4 8 131.00 151.19 30.94 o 4 4 8 24.87 37.30 29.17 o 5 4 8 16.45 19.75 24.87 o 6 4 8 168.63 172.27 31.09 o 7 4 8 851.37 810.43 31.30 o 8 4 8 136.94 115.04 26.69 o 9 4 8 7.71 37.84 30.97 o 10 4 8 818.92 805.46 35.61 o 11 4 8 114.12 98.62 30.87 o 12 4 8 15.60 10.58 32.11 o 13 4 8 1.23 12.55 36.34 o 1 5 8 7878.51 7850.96 143.75 o 2 5 8 2577.30 2528.87 45.91 o 3 5 8 380.51 399.20 32.92 o 4 5 8 281.11 225.18 29.65 o 5 5 8 25.47 43.71 29.94 o 6 5 8 1.03 46.38 30.24 o 7 5 8 34.63 43.50 28.87 o 8 5 8 12.35 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361.10 29.82 o 6 8 8 1186.03 1200.21 33.90 o 7 8 8 1725.53 1732.46 37.93 o 8 8 8 392.79 426.24 36.74 o 9 8 8 21.95 18.42 33.38 o 10 8 8 0.14 36.90 33.11 o 11 8 8 25.13 15.08 35.94 o 12 8 8 11.29 32.98 37.62 o 1 9 8 345.65 304.92 37.15 o 2 9 8 634.18 610.87 34.18 o 3 9 8 14.57 35.83 31.21 o 4 9 8 1581.05 1498.19 40.01 o 5 9 8 35.66 67.84 35.33 o 6 9 8 1737.54 1740.14 40.23 o 7 9 8 249.40 262.90 30.90 o 8 9 8 73.06 77.87 35.33 o 9 9 8 118.19 96.39 34.97 o 10 9 8 0.24 -4.82 34.99 o 11 9 8 15.64 33.36 34.05 o 12 9 8 243.16 276.91 37.36 o 0 10 8 96.47 47.52 52.27 o 1 10 8 4.05 6.49 35.67 o 2 10 8 494.43 580.66 39.66 o 3 10 8 159.97 168.56 30.24 o 4 10 8 122.13 201.41 32.40 o 5 10 8 10.25 48.12 34.36 o 6 10 8 1.89 27.48 42.26 o 7 10 8 117.86 84.23 36.33 o 8 10 8 349.17 428.44 32.16 o 9 10 8 294.24 289.19 37.67 o 10 10 8 320.97 340.42 36.19 o 11 10 8 128.82 160.73 36.09 o 1 11 8 67.54 71.05 32.85 o 2 11 8 1973.29 1963.73 38.75 o 3 11 8 343.13 338.32 34.93 o 4 11 8 1221.78 1226.18 36.66 o 5 11 8 195.64 213.41 36.59 o 6 11 8 63.78 70.14 37.35 o 7 11 8 152.46 134.98 35.75 o 8 11 8 27.12 42.37 35.46 o 9 11 8 163.45 115.47 40.15 o 10 11 8 63.57 63.22 43.08 o 11 11 8 2.66 10.98 34.85 o 0 12 8 278.31 217.40 52.33 o 1 12 8 204.70 209.40 35.55 o 2 12 8 25.79 4.97 31.48 o 3 12 8 90.47 123.97 36.12 o 4 12 8 10.06 22.93 37.36 o 5 12 8 178.11 171.13 38.09 o 6 12 8 69.45 45.59 37.08 o 7 12 8 1.84 -13.47 38.33 o 8 12 8 91.61 98.41 36.09 o 9 12 8 63.92 81.58 44.66 o 10 12 8 0.13 -12.93 40.07 o 1 13 8 125.32 99.74 32.88 o 2 13 8 156.30 170.09 34.74 o 3 13 8 14.06 25.97 36.60 o 4 13 8 417.48 391.47 35.49 o 5 13 8 167.93 186.23 35.63 o 6 13 8 106.45 152.51 39.70 o 7 13 8 105.06 133.48 38.80 o 8 13 8 29.33 46.35 41.99 o 9 13 8 0.47 35.16 43.15 o 10 13 8 131.08 121.84 43.62 o 0 14 8 178.88 238.89 51.43 o 1 14 8 59.10 118.99 37.95 o 2 14 8 163.03 133.27 34.85 o 3 14 8 47.42 98.11 34.58 o 4 14 8 77.44 79.85 34.34 o 5 14 8 0.20 9.50 39.89 o 6 14 8 0.09 5.92 38.33 o 7 14 8 24.10 51.87 41.96 o 8 14 8 0.01 12.43 40.43 o 9 14 8 0.10 23.77 42.66 o 1 15 8 94.24 103.77 37.54 o 2 15 8 191.25 150.88 35.35 o 3 15 8 169.14 195.38 36.05 o 4 15 8 72.83 93.24 39.85 o 5 15 8 62.05 72.23 46.42 o 6 15 8 37.83 44.71 44.33 o 7 15 8 4.25 -12.20 45.85 o 8 15 8 47.95 7.71 46.99 o 0 16 8 25.67 -38.88 57.09 o 1 16 8 0.82 4.68 38.49 o 2 16 8 191.06 178.60 38.98 o 3 16 8 3.94 25.90 41.46 o 4 16 8 33.75 57.58 39.15 o 5 16 8 3.45 14.34 45.25 o 6 16 8 13.59 -4.17 41.24 o 7 16 8 122.31 117.76 40.57 o 1 17 8 148.23 221.73 38.58 o 2 17 8 32.58 37.34 38.56 o 3 17 8 18.45 44.68 41.25 o 4 17 8 243.61 290.67 42.71 o 5 17 8 0.20 19.56 45.89 o 6 17 8 64.83 63.61 42.98 o 0 18 8 971.18 1067.07 50.97 o 1 18 8 111.62 116.04 40.50 o 2 18 8 6.09 4.99 41.62 o 3 18 8 14.37 24.32 42.94 o 4 18 8 17.62 5.16 46.50 o 1 19 8 180.97 125.34 40.73 o 2 19 8 187.85 149.25 39.21 o 1 1 9 543.14 580.00 32.52 o 2 1 9 429.79 444.09 27.54 o 3 1 9 6.55 26.52 28.66 o 4 1 9 401.31 418.34 28.97 o 5 1 9 99.79 91.47 31.04 o 6 1 9 145.95 150.09 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