#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203950.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203950_Fobs loop_ _publ_author_name 'Reinheimer, Eric' 'Bacsa, John' 'Dunbar, Kim R.' _publ_section_title ; 1,3-Dithiolan-2-one ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1206 _journal_page_last o1207 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.426 _cell_angle_gamma 90.000 _cell_length_a 8.0397 _cell_length_b 5.2020 _cell_length_c 11.3175 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.7669 _[local]_cod_data_source_file su6116Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' er046 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 18.26 19.30 0.53 o 2 0 0 6387.63 6956.10 106.06 o 3 0 0 235.72 264.99 4.83 o 4 0 0 3517.70 3685.88 56.21 o 5 0 0 310.40 330.97 11.67 o 6 0 0 926.25 984.49 24.53 o 7 0 0 393.50 409.74 9.06 o 8 0 0 922.66 950.63 19.94 o 9 0 0 190.11 182.42 6.20 o 10 0 0 742.96 741.27 17.09 o 1 1 0 420.17 399.04 4.51 o 2 1 0 9700.13 10447.27 113.55 o 3 1 0 393.15 443.08 7.76 o 4 1 0 941.88 1046.29 11.93 o 5 1 0 623.28 649.64 12.31 o 6 1 0 1601.85 1645.21 18.69 o 7 1 0 139.04 143.74 3.09 o 8 1 0 642.90 666.37 9.55 o 9 1 0 25.07 29.16 1.95 o 10 1 0 395.11 390.10 7.57 o 0 2 0 3202.97 3199.98 71.01 o 1 2 0 711.57 740.79 9.22 o 2 2 0 2.10 27.35 19.94 o 3 2 0 1281.72 1435.86 17.66 o 4 2 0 2647.04 2881.45 32.02 o 5 2 0 0.48 2.69 2.69 o 6 2 0 807.82 859.12 11.41 o 7 2 0 307.62 314.83 5.27 o 8 2 0 209.57 218.37 4.76 o 9 2 0 5.87 7.67 1.96 o 1 3 0 2405.08 2561.01 28.66 o 2 3 0 674.48 681.62 9.84 o 3 3 0 153.29 156.64 3.13 o 4 3 0 174.73 172.69 3.49 o 5 3 0 832.26 872.55 12.87 o 6 3 0 284.78 281.35 7.54 o 7 3 0 59.28 58.37 3.62 o 8 3 0 439.29 438.61 11.48 o 9 3 0 626.93 631.87 15.65 o 0 4 0 1.06 6.42 18.08 o 1 4 0 1419.68 1499.27 17.46 o 2 4 0 7.86 9.74 1.08 o 3 4 0 2812.94 2877.89 34.08 o 4 4 0 49.46 54.29 1.97 o 5 4 0 22.83 22.74 2.30 o 6 4 0 20.62 22.42 2.48 o 7 4 0 1008.06 1027.60 22.40 o 8 4 0 31.88 30.58 3.14 o 1 5 0 1184.15 1181.18 16.29 o 2 5 0 31.19 33.64 1.44 o 3 5 0 481.21 498.03 8.17 o 4 5 0 55.32 54.09 2.45 o 5 5 0 1330.91 1367.41 21.22 o 6 5 0 0.08 -5.78 5.78 o 7 5 0 13.29 12.72 2.40 o 0 6 0 36.44 34.41 2.36 o 1 6 0 444.78 465.25 8.66 o 2 6 0 0.26 -1.05 2.90 o 3 6 0 818.12 854.85 15.83 o 4 6 0 58.16 58.32 2.78 o -10 1 1 118.55 118.29 3.74 o -9 1 1 201.08 197.25 4.71 o -8 1 1 0.04 -4.21 5.85 o -7 1 1 316.60 330.08 6.00 o -6 1 1 218.82 225.25 3.95 o -5 1 1 0.18 0.27 3.11 o -4 1 1 3.04 46.11 27.17 o -3 1 1 28.08 28.96 1.08 o -2 1 1 754.65 792.68 9.21 o -1 1 1 1869.83 2022.58 24.36 o 0 1 1 132.08 116.31 1.69 o 1 1 1 4543.65 4625.37 63.18 o 2 1 1 1802.98 1928.70 21.67 o 3 1 1 462.61 505.74 6.53 o 4 1 1 1344.30 1470.91 20.14 o 5 1 1 112.74 102.04 1.98 o 6 1 1 49.20 51.24 1.50 o 7 1 1 16.93 17.98 1.13 o 8 1 1 0.30 3.26 2.83 o 9 1 1 34.29 33.96 2.03 o 10 1 1 45.82 39.55 2.78 o -9 2 1 289.16 281.20 5.89 o -8 2 1 590.59 597.86 9.81 o -7 2 1 38.19 38.90 1.89 o -6 2 1 255.29 261.21 6.01 o -5 2 1 410.40 430.12 6.83 o -4 2 1 21.36 20.74 1.08 o -3 2 1 15.09 15.72 0.97 o -2 2 1 139.23 153.46 2.80 o -1 2 1 87.56 87.85 1.85 o 0 2 1 2169.06 2250.65 28.46 o 1 2 1 1506.86 1707.59 18.04 o 2 2 1 464.30 494.70 6.53 o 3 2 1 2330.54 2490.44 29.86 o 4 2 1 733.59 792.01 9.95 o 5 2 1 62.74 70.86 1.67 o 6 2 1 516.78 546.74 7.10 o 7 2 1 347.62 334.36 6.12 o 8 2 1 43.18 43.34 2.30 o 9 2 1 11.66 12.49 1.97 o -9 3 1 109.40 117.43 5.49 o -8 3 1 30.89 30.36 3.00 o -7 3 1 98.22 104.76 4.60 o -6 3 1 532.65 510.55 21.78 o -5 3 1 323.79 295.28 5.36 o -4 3 1 28.12 27.46 1.61 o -3 3 1 746.68 700.45 10.28 o -2 3 1 804.92 804.24 11.40 o -1 3 1 153.09 166.29 2.67 o 0 3 1 338.88 349.75 4.66 o 1 3 1 977.78 998.81 11.77 o 2 3 1 655.97 656.01 8.06 o 3 3 1 4.01 5.03 0.79 o 4 3 1 660.23 658.99 9.04 o 5 3 1 636.26 631.06 8.93 o 6 3 1 30.91 33.68 2.26 o 7 3 1 78.97 78.47 3.33 o 8 3 1 189.64 193.81 6.82 o 9 3 1 54.80 56.95 3.52 o -8 4 1 34.50 32.11 3.14 o -7 4 1 82.54 82.12 4.59 o -6 4 1 13.32 14.93 2.24 o -5 4 1 87.07 94.47 4.91 o -4 4 1 278.03 287.53 5.36 o -3 4 1 61.63 58.53 1.69 o -2 4 1 119.11 120.18 2.41 o -1 4 1 196.47 194.43 3.25 o 0 4 1 56.08 54.84 1.74 o 1 4 1 5.01 10.76 19.55 o 2 4 1 70.27 67.52 1.72 o 3 4 1 99.67 98.90 2.20 o 4 4 1 62.30 65.45 2.89 o 5 4 1 5.98 7.10 1.52 o 6 4 1 137.42 137.82 6.81 o 7 4 1 127.34 121.30 5.32 o 8 4 1 0.35 -0.44 7.39 o -7 5 1 0.21 -55.10 55.10 o -6 5 1 3.89 3.65 2.05 o -5 5 1 2.45 4.91 1.64 o -4 5 1 0.33 1.22 7.50 o -3 5 1 16.59 18.81 1.41 o -2 5 1 4.69 4.21 0.95 o -1 5 1 0.71 2.77 3.26 o 0 5 1 0.57 0.05 5.67 o 1 5 1 13.36 14.21 1.14 o 2 5 1 21.52 20.30 1.46 o 3 5 1 5.01 4.51 1.14 o 4 5 1 3.01 5.55 6.77 o 5 5 1 6.98 125.18 80.42 o 6 5 1 0.82 59.68 65.82 o 7 5 1 22.68 22.91 3.81 o -4 6 1 27.85 32.41 2.22 o -3 6 1 0.02 1.87 2.47 o -2 6 1 3.02 2.61 4.73 o -1 6 1 28.34 28.98 1.70 o 0 6 1 58.69 59.50 2.48 o 1 6 1 32.24 34.64 2.05 o 2 6 1 0.65 0.91 3.44 o 3 6 1 142.20 149.67 5.18 o 4 6 1 209.15 229.56 7.73 o -10 0 2 331.21 338.00 9.90 o -9 0 2 340.64 334.52 9.40 o -8 0 2 1958.16 1957.36 38.04 o -7 0 2 46.29 49.94 2.86 o -6 0 2 238.40 250.44 6.70 o -5 0 2 1831.47 1971.38 44.66 o -4 0 2 1749.22 1779.98 33.01 o -3 0 2 4719.86 5477.95 97.86 o -2 0 2 417.77 409.25 8.76 o 0 0 2 5006.40 4600.21 107.02 o 1 0 2 1556.76 1413.83 18.20 o 2 0 2 2480.23 2570.10 45.92 o 3 0 2 350.42 361.34 6.35 o 4 0 2 1355.43 1474.57 23.24 o 5 0 2 1278.45 1328.13 21.29 o 6 0 2 1844.30 1934.43 30.74 o 7 0 2 281.74 297.52 7.78 o 8 0 2 82.76 80.36 3.00 o 9 0 2 4.71 9.87 2.09 o 10 0 2 521.43 506.83 12.60 o -10 1 2 289.10 296.71 6.44 o -9 1 2 64.92 66.23 2.69 o -8 1 2 31.41 35.17 1.92 o -7 1 2 413.86 447.02 7.61 o -6 1 2 1293.96 1360.92 18.71 o -5 1 2 937.92 1021.47 14.21 o -4 1 2 50.51 47.24 1.85 o -3 1 2 29.19 32.98 1.09 o -2 1 2 2151.13 2126.51 23.69 o -1 1 2 883.71 886.48 10.15 o 0 1 2 23.40 24.09 0.79 o 2 1 2 6177.60 6393.24 78.44 o 3 1 2 346.19 369.07 6.01 o 4 1 2 2447.74 2520.95 37.69 o 5 1 2 4.41 3.69 0.74 o 6 1 2 388.03 395.14 5.96 o 7 1 2 411.50 402.99 5.77 o 8 1 2 1137.88 1165.13 15.26 o 9 1 2 164.80 164.02 5.00 o 10 1 2 0.94 1.47 5.29 o -9 2 2 19.56 21.97 1.84 o -8 2 2 129.54 132.24 3.63 o -7 2 2 249.77 265.82 5.26 o -6 2 2 266.28 283.08 7.71 o -5 2 2 0.05 0.87 7.69 o -4 2 2 1554.39 1548.07 19.10 o -3 2 2 631.03 610.63 8.86 o -2 2 2 96.66 89.09 2.00 o -1 2 2 11.02 10.75 0.75 o 0 2 2 1166.92 1185.66 19.57 o 1 2 2 1439.97 1453.29 17.25 o 2 2 2 145.93 140.28 2.93 o 3 2 2 694.53 736.89 11.28 o 4 2 2 1021.66 1074.02 12.50 o 5 2 2 37.04 39.47 1.26 o 6 2 2 606.27 618.26 8.20 o 7 2 2 182.73 182.81 3.82 o 8 2 2 94.28 98.57 3.28 o 9 2 2 14.44 17.01 1.83 o -9 3 2 237.84 246.83 8.40 o -8 3 2 268.43 277.09 6.46 o -7 3 2 133.74 128.63 3.86 o -6 3 2 139.21 136.20 3.77 o -5 3 2 152.77 153.56 3.83 o -4 3 2 364.22 349.21 5.95 o -3 3 2 115.83 108.43 2.54 o -2 3 2 1051.84 1051.30 14.62 o -1 3 2 835.66 832.95 9.99 o 0 3 2 54.85 55.81 1.36 o 1 3 2 1381.83 1430.62 19.92 o 2 3 2 74.59 72.00 1.76 o 3 3 2 195.72 215.88 4.96 o 5 3 2 1545.90 1562.95 23.21 o 6 3 2 292.61 290.97 6.83 o 7 3 2 95.87 96.61 3.75 o 8 3 2 46.14 44.57 2.84 o 9 3 2 265.03 265.77 6.24 o -8 4 2 27.64 29.46 2.99 o -7 4 2 569.09 555.30 13.77 o -6 4 2 391.90 373.87 7.66 o -5 4 2 975.10 950.17 16.41 o -4 4 2 0.09 -3.69 7.74 o -3 4 2 103.53 109.91 2.38 o -2 4 2 872.03 863.21 10.69 o -1 4 2 1151.25 1157.05 13.82 o 0 4 2 576.46 577.96 7.48 o 1 4 2 58.24 65.25 1.66 o 2 4 2 30.99 32.86 1.31 o 3 4 2 1331.84 1403.53 19.07 o 4 4 2 133.01 144.79 4.38 o 5 4 2 13.01 11.80 1.66 o 6 4 2 28.55 25.95 2.61 o 7 4 2 731.67 745.14 31.36 o 8 4 2 143.47 131.98 5.71 o -6 5 2 0.61 0.69 12.72 o -5 5 2 297.16 304.74 8.79 o -4 5 2 372.44 360.46 6.05 o -3 5 2 764.09 769.73 10.79 o -2 5 2 75.75 76.90 2.26 o -1 5 2 101.01 105.17 2.42 o 0 5 2 167.91 172.99 3.23 o 1 5 2 1061.36 1056.73 14.39 o 2 5 2 61.64 61.55 2.54 o 3 5 2 26.31 26.68 1.61 o 4 5 2 109.40 109.98 3.13 o 5 5 2 1349.18 1405.67 25.39 o 6 5 2 63.95 68.98 4.09 o -4 6 2 22.67 24.06 2.04 o -3 6 2 166.19 164.36 6.03 o -2 6 2 104.14 106.16 3.44 o -1 6 2 510.64 510.24 8.30 o 0 6 2 50.61 51.32 2.37 o 1 6 2 37.01 32.90 2.02 o 2 6 2 93.83 94.35 3.83 o 3 6 2 644.61 704.58 25.72 o 4 6 2 162.29 184.28 10.77 o -10 1 3 46.28 48.03 2.61 o -9 1 3 37.15 39.89 2.39 o -8 1 3 49.45 56.34 2.35 o -7 1 3 567.92 595.48 9.57 o -6 1 3 238.12 252.79 5.87 o -5 1 3 284.41 314.16 8.42 o -4 1 3 1504.22 1611.89 23.92 o -3 1 3 210.52 219.10 3.86 o -2 1 3 560.90 570.26 7.42 o -1 1 3 777.69 767.47 8.88 o 0 1 3 29.18 29.12 0.73 o 1 1 3 1.67 0.93 0.58 o 2 1 3 23.09 23.19 1.09 o 3 1 3 25.63 22.30 1.17 o 4 1 3 319.01 308.87 4.12 o 5 1 3 136.02 140.69 2.44 o 6 1 3 34.08 34.77 1.29 o 7 1 3 119.44 120.96 2.52 o 8 1 3 71.70 70.84 2.39 o 9 1 3 4.88 5.48 1.50 o 10 1 3 6.77 5.53 1.78 o -9 2 3 98.37 91.52 3.19 o -8 2 3 87.00 91.08 3.02 o -7 2 3 0.09 2.67 5.26 o -6 2 3 264.83 266.85 6.35 o -5 2 3 839.65 866.96 12.50 o -4 2 3 205.35 196.85 3.79 o -3 2 3 464.68 449.26 8.29 o -2 2 3 1537.58 1474.52 19.76 o -1 2 3 377.52 370.63 5.07 o 0 2 3 0.01 0.06 0.86 o 1 2 3 353.99 327.30 5.12 o 2 2 3 796.19 768.80 11.61 o 3 2 3 607.59 608.10 9.59 o 4 2 3 0.85 3.54 9.22 o 5 2 3 634.60 647.42 9.42 o 6 2 3 934.72 949.55 16.84 o 7 2 3 34.16 31.87 1.63 o 8 2 3 291.96 278.54 5.95 o 9 2 3 269.17 260.07 5.97 o -9 3 3 6.73 7.74 2.37 o -8 3 3 84.27 90.50 4.55 o -7 3 3 322.82 311.00 7.62 o -6 3 3 223.96 217.14 5.06 o -5 3 3 48.01 45.53 2.05 o -4 3 3 888.00 866.67 13.88 o -3 3 3 952.27 991.79 14.02 o -2 3 3 1.94 2.63 0.74 o -1 3 3 1413.26 1429.67 16.47 o 0 3 3 968.28 985.59 10.84 o 1 3 3 3.62 4.91 0.62 o 2 3 3 113.66 115.56 2.33 o 3 3 3 100.94 89.85 2.64 o 4 3 3 175.15 179.97 4.14 o 5 3 3 124.66 126.60 3.53 o 6 3 3 0.02 -2.32 10.56 o 7 3 3 198.14 203.61 5.71 o 8 3 3 373.24 347.26 8.27 o 9 3 3 6.45 8.14 2.03 o -8 4 3 11.40 9.72 2.37 o -7 4 3 15.45 13.52 2.29 o -6 4 3 10.47 11.12 1.58 o -5 4 3 80.49 83.49 3.13 o -4 4 3 100.36 98.76 3.07 o -3 4 3 39.73 43.27 1.62 o -2 4 3 229.82 224.10 3.67 o -1 4 3 119.66 118.09 2.39 o 0 4 3 2.81 3.31 0.80 o 1 4 3 198.85 194.34 3.71 o 2 4 3 185.70 199.07 4.53 o 3 4 3 0.67 0.43 1.61 o 4 4 3 5.93 6.96 1.11 o 5 4 3 38.85 37.03 2.13 o 6 4 3 121.85 120.23 3.79 o 7 4 3 4.34 53.25 64.75 o 8 4 3 39.31 36.84 4.50 o -6 5 3 0.10 3.05 5.58 o -5 5 3 4.57 4.45 1.99 o -4 5 3 64.89 64.68 2.21 o -3 5 3 42.06 43.50 2.49 o -2 5 3 59.15 58.13 2.00 o -1 5 3 62.11 62.29 2.00 o 0 5 3 0.01 -2.26 5.25 o 1 5 3 32.01 29.86 1.80 o 2 5 3 36.44 35.61 1.90 o 3 5 3 32.24 31.44 3.04 o 4 5 3 67.97 70.46 3.32 o 5 5 3 40.69 36.76 2.69 o 6 5 3 55.48 52.72 3.74 o -4 6 3 23.07 24.27 2.12 o -3 6 3 1.81 2.18 2.00 o -2 6 3 205.52 197.40 5.13 o -1 6 3 142.54 148.08 4.07 o 0 6 3 22.69 24.69 2.19 o 1 6 3 68.31 68.80 3.23 o 2 6 3 29.16 29.98 2.46 o 3 6 3 65.95 65.09 3.38 o 4 6 3 2.19 36.13 73.04 o -10 0 4 53.82 52.46 3.85 o -9 0 4 20.80 23.34 2.65 o -8 0 4 525.80 535.72 12.92 o -7 0 4 833.91 862.43 21.39 o -6 0 4 864.04 877.37 18.18 o -4 0 4 340.40 323.33 7.50 o -3 0 4 2997.66 3205.22 58.04 o -2 0 4 3872.50 4072.37 104.13 o -1 0 4 2040.83 1963.27 35.66 o 0 0 4 232.50 238.21 5.12 o 1 0 4 540.03 531.81 10.42 o 2 0 4 1674.92 1634.73 25.39 o 3 0 4 1043.64 1009.43 19.52 o 4 0 4 0.08 -0.47 1.01 o 5 0 4 88.11 92.66 2.67 o 6 0 4 1389.31 1292.80 21.24 o 7 0 4 188.13 200.11 4.90 o 8 0 4 199.75 186.83 4.89 o 9 0 4 33.69 33.22 4.44 o 10 0 4 327.05 310.60 14.48 o -9 1 4 430.27 427.27 8.12 o -8 1 4 27.81 28.79 1.88 o -7 1 4 17.89 15.94 1.48 o -6 1 4 850.97 909.23 13.36 o -5 1 4 536.70 553.48 13.49 o -4 1 4 1380.81 1413.86 29.74 o -2 1 4 496.55 457.16 6.06 o -1 1 4 2363.77 2326.34 27.74 o 0 1 4 5237.24 5125.16 56.32 o 1 1 4 1098.78 1005.29 13.21 o 2 1 4 124.79 131.90 4.35 o 3 1 4 365.42 358.48 5.23 o 4 1 4 1263.58 1212.99 13.71 o 5 1 4 607.64 598.23 7.42 o 6 1 4 92.25 91.58 2.03 o 7 1 4 20.25 21.43 1.41 o 8 1 4 439.72 409.79 6.88 o 9 1 4 211.53 213.24 5.13 o -9 2 4 2.96 60.48 72.48 o -8 2 4 219.22 216.55 4.99 o -7 2 4 417.30 403.10 7.23 o -6 2 4 6.95 5.93 1.13 o -5 2 4 309.84 302.07 5.84 o -4 2 4 832.96 853.08 26.29 o -3 2 4 152.41 157.48 2.89 o -2 2 4 745.89 740.21 8.93 o -1 2 4 400.59 386.31 7.22 o 1 2 4 283.47 275.77 4.40 o 2 2 4 690.74 660.28 12.59 o 3 2 4 1147.00 1111.97 22.24 o 4 2 4 13.90 14.60 1.07 o 5 2 4 59.20 55.71 1.72 o 6 2 4 417.06 397.18 6.42 o 7 2 4 123.63 123.42 3.07 o 8 2 4 8.79 8.88 1.52 o 9 2 4 6.41 8.20 2.45 o -8 3 4 7.41 6.65 1.69 o -7 3 4 191.56 186.62 4.91 o -6 3 4 213.58 215.61 5.76 o -5 3 4 146.73 143.52 4.82 o -4 3 4 40.89 38.50 1.86 o -3 3 4 1183.19 1177.42 19.08 o -2 3 4 677.99 642.28 9.51 o -1 3 4 132.22 121.72 2.08 o 0 3 4 3.83 3.61 0.64 o 1 3 4 512.45 501.84 5.95 o 2 3 4 690.91 678.55 10.16 o 3 3 4 218.48 207.41 5.20 o 4 3 4 194.77 180.15 4.20 o 5 3 4 236.51 236.34 5.21 o 6 3 4 107.69 111.06 3.30 o 7 3 4 228.89 219.18 5.14 o 8 3 4 125.22 129.88 5.18 o -7 4 4 0.07 -1.92 6.16 o -6 4 4 131.21 132.17 3.99 o -5 4 4 543.03 504.93 9.43 o -4 4 4 398.03 383.42 7.46 o -3 4 4 76.18 74.14 2.10 o -2 4 4 294.43 298.91 4.86 o -1 4 4 828.97 811.85 10.79 o 0 4 4 1462.24 1414.50 16.90 o 1 4 4 588.88 553.42 7.39 o 2 4 4 114.62 107.16 2.48 o 3 4 4 103.11 108.15 2.85 o 4 4 4 168.31 175.11 4.42 o 5 4 4 105.14 105.37 3.44 o 6 4 4 24.56 22.31 1.96 o 7 4 4 346.04 333.41 8.26 o -6 5 4 176.79 169.51 6.39 o -5 5 4 17.46 15.58 1.81 o -4 5 4 128.48 130.66 3.22 o -3 5 4 1083.24 1071.90 14.41 o -2 5 4 289.89 280.77 4.94 o 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