#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:06:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/40/2204017.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204017_Fobs loop_ _publ_author_name 'Sun, Qiao-Zhen' 'Sun, Qiao-Hong' 'Zhang, Han-Hui' 'Huang, Chang-Cang' 'Cao, Yan-Ning' 'Sun, Rui-Qing' _publ_section_title ; Bis(ethylenediammonium) tetra-\m-oxo-tetrakis[(nitrilotriacetato)titanate(IV)] monohydrate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1084 _journal_page_last m1086 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.483 _cell_angle_beta 90.796 _cell_angle_gamma 104.374 _cell_length_a 10.8082 _cell_length_b 10.9099 _cell_length_c 19.6832 _exptl_crystal_F_000 1180.00 _reflns_d_resolution_high 0.7687 _cod_data_source_file dn6144Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in space group P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17.41 10.40 9.80 o 3 0 0 34.87 53.25 14.69 o 4 0 0 3281.45 3068.09 33.67 o 5 0 0 256.65 343.42 31.22 o 6 0 0 274.26 220.37 34.89 o 7 0 0 0.01 -20.82 20.82 o 8 0 0 323.17 290.77 26.32 o 9 0 0 94.24 77.74 20.20 o 10 0 0 1224.70 1201.65 37.96 o 11 0 0 8.93 17.75 34.89 o 12 0 0 569.94 563.18 31.83 o 13 0 0 47.59 32.45 22.04 o -13 1 0 66.87 118.76 30.00 o -12 1 0 76.62 56.32 37.96 o -11 1 0 2001.83 2020.70 25.71 o -10 1 0 134.97 157.94 34.29 o -9 1 0 732.53 771.92 54.48 o -8 1 0 217.74 212.42 22.65 o -7 1 0 41.27 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