#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/40/2204028.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204028_Fobs loop_ _publ_author_name 'Gueorguieva, Petia G.' 'Stanley, George G.' 'Fronczek, Frank R.' _publ_section_title ; A mononuclear Rh^III^ tetraphosphine complex, [RhCl~2~(C~25~H~40~P~4~)]BF~4~·C~3~D~6~O, crystallized as a perdeuteroacetone solvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1043 _journal_page_last m1045 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.186 _cell_angle_gamma 90.000 _cell_length_a 10.5950 _cell_length_b 14.7500 _cell_length_c 22.2850 _exptl_crystal_F_000 1608.00 _reflns_d_resolution_high 0.7402 _[local]_cod_data_source_file hb6060Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Petia8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45775.40 46789.20 1242.92 o 4 0 0 101.24 153.65 17.60 o 6 0 0 88788.16 91268.34 2943.20 o 8 0 0 9606.96 10399.99 407.17 o 10 0 0 7305.03 7618.16 315.15 o 12 0 0 6523.76 6546.35 315.11 o 14 0 0 406.42 87.54 136.96 o 2 1 0 4879.54 4954.84 101.67 o 3 1 0 2670.76 2813.49 60.44 o 4 1 0 299.53 343.19 21.22 o 5 1 0 5641.67 5809.59 112.73 o 6 1 0 3891.00 3666.08 79.26 o 7 1 0 3919.89 4065.29 202.58 o 8 1 0 2219.75 2426.86 140.37 o 9 1 0 128.02 184.83 55.02 o 10 1 0 3275.72 3437.31 191.94 o 11 1 0 24.06 -18.38 61.99 o 12 1 0 1217.54 1305.16 103.27 o 13 1 0 560.55 637.00 101.42 o 14 1 0 2712.89 2042.13 140.86 o 0 2 0 54871.10 49568.72 8694.00 o 1 2 0 5366.60 5060.32 93.20 o 2 2 0 18943.36 20084.90 395.33 o 3 2 0 4114.38 4170.88 91.09 o 4 2 0 70.65 39.46 11.95 o 5 2 0 4283.30 4269.94 85.54 o 6 2 0 37701.33 38651.18 827.08 o 7 2 0 278.95 288.45 80.89 o 8 2 0 79.46 42.41 58.44 o 9 2 0 934.49 1085.56 66.42 o 10 2 0 2862.07 3025.21 122.60 o 11 2 0 216.61 447.77 240.86 o 12 2 0 3988.41 3936.54 147.30 o 13 2 0 230.11 273.45 183.10 o 14 2 0 26.30 106.27 141.92 o 1 3 0 17.84 22.31 5.64 o 2 3 0 1708.36 1961.07 38.34 o 3 3 0 6567.27 6429.85 126.61 o 4 3 0 10.97 -14.33 14.33 o 5 3 0 1.66 17.45 16.53 o 6 3 0 34.35 58.04 21.32 o 7 3 0 2012.09 1910.52 58.86 o 8 3 0 125.27 183.63 31.32 o 9 3 0 508.92 576.74 58.89 o 10 3 0 784.30 938.95 67.86 o 11 3 0 837.65 845.01 115.98 o 12 3 0 42.19 64.69 65.25 o 13 3 0 200.37 244.13 99.50 o 14 3 0 149.60 -33.62 91.83 o 0 4 0 71032.98 72593.90 2276.39 o 1 4 0 3198.93 3250.80 59.95 o 2 4 0 188.47 261.16 10.34 o 3 4 0 1498.95 1590.03 67.93 o 4 4 0 847.39 994.81 59.23 o 5 4 0 728.28 753.98 30.43 o 6 4 0 11515.98 11705.37 262.57 o 7 4 0 397.57 389.79 31.93 o 8 4 0 122.95 162.22 32.31 o 9 4 0 979.48 1000.49 71.53 o 10 4 0 471.86 584.18 74.57 o 11 4 0 495.03 490.67 62.67 o 12 4 0 1213.64 1175.20 101.22 o 13 4 0 867.20 670.14 103.34 o 1 5 0 4290.64 4281.93 106.13 o 2 5 0 578.88 684.53 15.51 o 3 5 0 6222.31 5875.53 96.21 o 4 5 0 2770.20 2864.42 58.65 o 5 5 0 1492.44 1524.81 74.24 o 6 5 0 342.95 384.27 26.45 o 7 5 0 5619.19 5750.06 195.61 o 8 5 0 352.46 375.99 35.67 o 9 5 0 154.17 162.52 40.60 o 10 5 0 5146.78 5622.10 243.54 o 11 5 0 1609.16 1749.44 83.61 o 12 5 0 261.16 156.13 85.51 o 13 5 0 1253.89 1140.61 179.61 o 0 6 0 39263.36 41968.17 1425.20 o 1 6 0 49942.82 50145.73 1787.78 o 2 6 0 11503.70 10960.30 260.27 o 3 6 0 14828.99 13744.16 245.99 o 4 6 0 21155.23 21887.35 400.68 o 5 6 0 18454.40 18423.08 374.66 o 6 6 0 13845.50 13751.63 280.39 o 7 6 0 8495.07 8943.00 233.23 o 8 6 0 988.81 1098.15 49.42 o 9 6 0 7604.39 8166.44 235.05 o 10 6 0 66.69 158.48 48.72 o 11 6 0 5052.32 5269.64 248.27 o 12 6 0 2984.12 2740.49 139.24 o 13 6 0 266.66 337.99 141.47 o 1 7 0 610.69 563.13 23.47 o 2 7 0 574.45 503.80 24.71 o 3 7 0 3457.99 3509.77 123.24 o 4 7 0 6462.84 6309.00 210.44 o 5 7 0 9706.98 9720.46 235.79 o 6 7 0 1702.05 1665.89 48.67 o 7 7 0 401.18 485.16 28.22 o 8 7 0 8.74 89.78 31.67 o 9 7 0 303.61 351.98 46.94 o 10 7 0 6743.49 7851.33 429.34 o 11 7 0 5059.24 5352.67 368.34 o 12 7 0 40.49 99.50 99.50 o 13 7 0 2038.10 1897.50 132.46 o 0 8 0 1748.25 1808.27 56.08 o 1 8 0 8481.46 7856.12 152.69 o 2 8 0 262.80 300.24 17.35 o 3 8 0 35218.11 34560.50 524.00 o 4 8 0 32.20 37.87 21.32 o 5 8 0 9339.30 9411.59 216.99 o 6 8 0 3947.16 3802.67 99.54 o 7 8 0 1339.35 1365.85 56.19 o 8 8 0 461.98 566.72 40.71 o 9 8 0 8848.46 9767.65 432.12 o 10 8 0 66.83 78.97 69.94 o 11 8 0 6011.29 6630.93 263.18 o 12 8 0 1437.69 1369.21 129.97 o 1 9 0 2260.14 2088.92 128.53 o 2 9 0 1838.70 1890.17 63.30 o 3 9 0 46.83 76.49 13.31 o 4 9 0 3193.60 3260.84 65.00 o 5 9 0 2889.60 2892.28 82.21 o 6 9 0 2819.78 2737.60 72.40 o 7 9 0 48.09 49.74 29.41 o 8 9 0 637.90 697.44 57.76 o 9 9 0 63.53 209.83 85.29 o 10 9 0 2217.76 2597.99 145.32 o 11 9 0 2635.71 2497.39 142.39 o 12 9 0 288.93 415.16 139.44 o 0 10 0 839.34 909.95 53.25 o 1 10 0 27.22 -12.21 21.66 o 2 10 0 599.91 536.89 59.12 o 3 10 0 9949.72 9315.91 210.93 o 4 10 0 257.11 228.11 8.57 o 5 10 0 150.82 187.04 15.57 o 6 10 0 508.74 485.76 28.56 o 7 10 0 20.66 60.69 31.81 o 8 10 0 338.39 355.59 59.11 o 9 10 0 1004.12 1189.35 85.29 o 10 10 0 5.91 6.77 101.98 o 11 10 0 491.14 655.46 133.80 o 12 10 0 568.10 494.13 133.12 o 1 11 0 416.19 511.77 39.60 o 2 11 0 2210.89 2185.16 62.28 o 3 11 0 2664.39 2588.52 101.55 o 4 11 0 3976.00 3896.95 112.62 o 5 11 0 1310.66 1289.58 30.69 o 6 11 0 2.52 9.02 17.82 o 7 11 0 1230.20 1362.21 98.16 o 8 11 0 1172.62 1192.52 118.01 o 9 11 0 348.54 434.79 99.05 o 10 11 0 537.54 483.75 77.39 o 11 11 0 2781.24 2845.82 222.95 o 0 12 0 25.71 11.55 10.94 o 1 12 0 3013.66 3132.91 84.63 o 2 12 0 727.44 756.51 68.59 o 3 12 0 23098.51 22730.57 516.09 o 4 12 0 1968.52 1731.71 106.74 o 5 12 0 3985.72 4119.35 140.16 o 6 12 0 1325.19 1324.09 76.04 o 7 12 0 2647.16 2835.72 101.10 o 8 12 0 178.49 310.46 67.01 o 9 12 0 4211.52 4582.75 212.37 o 10 12 0 422.60 557.31 125.68 o 11 12 0 1405.73 1299.93 160.88 o 1 13 0 159.77 277.97 26.85 o 2 13 0 1730.71 1584.55 56.64 o 3 13 0 1276.31 1303.33 54.83 o 4 13 0 318.98 350.18 78.29 o 5 13 0 1544.36 1672.74 85.52 o 6 13 0 637.27 645.76 62.73 o 7 13 0 53.76 17.82 58.21 o 8 13 0 3054.48 3073.38 163.38 o 9 13 0 3584.81 3531.80 192.05 o 10 13 0 212.95 324.00 92.28 o 0 14 0 3938.79 3686.23 196.13 o 1 14 0 5073.21 5098.82 142.42 o 2 14 0 6831.35 6960.69 174.50 o 3 14 0 12700.56 13193.06 327.46 o 4 14 0 6806.62 7428.01 253.95 o 5 14 0 4285.52 4602.30 174.01 o 6 14 0 2430.97 2573.89 110.80 o 7 14 0 3459.32 3599.96 148.27 o 8 14 0 3775.17 4155.62 171.51 o 9 14 0 2264.71 2211.64 160.89 o 10 14 0 327.61 368.23 92.96 o 1 15 0 751.69 817.71 43.55 o 2 15 0 3914.11 4266.83 136.54 o 3 15 0 133.29 151.40 38.58 o 4 15 0 126.96 94.76 49.86 o 5 15 0 148.26 60.69 49.64 o 6 15 0 27.48 40.61 53.92 o 7 15 0 16.68 49.41 72.20 o 8 15 0 1784.67 1731.63 122.53 o 9 15 0 845.12 444.73 162.23 o 0 16 0 347.36 284.29 88.00 o 1 16 0 35.40 27.30 59.11 o 2 16 0 2112.98 2101.31 104.48 o 3 16 0 114.15 62.95 38.36 o 4 16 0 1113.39 982.89 71.53 o 5 16 0 1.05 72.20 58.89 o 6 16 0 35.22 99.50 65.43 o 7 16 0 425.93 415.16 83.26 o 8 16 0 1347.44 1065.03 151.86 o 1 17 0 9.24 17.82 64.98 o 2 17 0 1936.61 2180.48 119.82 o 3 17 0 31.54 11.28 67.91 o 4 17 0 590.94 769.63 86.87 o 5 17 0 0.11 151.39 65.43 o 6 17 0 248.54 270.08 74.91 o 7 17 0 161.64 171.93 92.06 o 0 18 0 1000.59 991.90 152.53 o 1 18 0 1053.34 1124.58 124.33 o 2 18 0 3697.32 3497.97 191.15 o 3 18 0 39.88 62.95 76.94 o 4 18 0 771.83 475.41 138.77 o 5 18 0 32.00 72.20 133.34 o 6 18 0 488.51 262.41 73.78 o 1 19 0 513.17 421.03 91.61 o 2 19 0 1784.93 1296.57 129.97 o -13 0 1 914.01 712.56 98.83 o -11 0 1 1301.65 1134.32 131.10 o -7 0 1 17546.77 17912.24 598.11 o -5 0 1 28415.12 27453.70 741.32 o -3 0 1 11635.80 10911.14 308.17 o 3 0 1 13145.37 13695.89 367.54 o 5 0 1 38704.02 39036.55 997.59 o 9 0 1 2165.10 2497.43 142.39 o 11 0 1 9402.74 9543.64 519.95 o 13 0 1 6451.25 6739.80 390.03 o -14 1 1 14.19 -62.70 81.57 o -13 1 1 1133.38 1214.99 206.35 o -12 1 1 483.84 545.04 221.68 o -11 1 1 3820.28 4322.99 293.62 o -10 1 1 347.42 511.35 81.34 o -9 1 1 11197.98 11922.70 315.22 o -8 1 1 278.05 351.98 48.06 o -7 1 1 9264.04 9045.58 235.90 o -6 1 1 11.95 27.61 49.64 o -5 1 1 14442.95 14711.84 301.91 o -4 1 1 6578.54 6625.07 134.01 o -3 1 1 26896.95 27479.60 618.63 o -2 1 1 4039.43 4181.83 92.83 o 2 1 1 4906.14 4996.20 148.58 o 3 1 1 2429.40 2609.31 61.77 o 4 1 1 3369.15 3796.73 115.02 o 5 1 1 3095.38 3343.15 67.94 o 6 1 1 103.54 93.46 21.40 o 7 1 1 25.15 41.40 23.77 o 8 1 1 303.20 411.98 71.52 o 9 1 1 132.00 259.09 57.51 o 10 1 1 77.31 164.70 57.21 o 11 1 1 306.36 280.50 107.06 o 12 1 1 0.69 22.86 61.71 o 13 1 1 935.74 716.36 84.15 o 14 1 1 21.24 -56.41 141.92 o -14 2 1 166.34 268.50 112.14 o -13 2 1 301.69 276.24 103.90 o -12 2 1 1.72 93.86 85.85 o -11 2 1 1012.99 1125.13 77.19 o -10 2 1 1921.88 1998.98 127.83 o -9 2 1 1799.91 1935.56 91.42 o -8 2 1 275.72 290.67 50.99 o -7 2 1 572.83 522.20 38.08 o -6 2 1 4.92 -7.96 37.34 o -5 2 1 524.51 422.72 26.40 o -4 2 1 278.97 352.54 51.44 o -3 2 1 16917.98 16924.40 322.49 o -2 2 1 5109.37 4894.68 89.46 o -1 2 1 76961.42 79618.61 1871.45 o 0 2 1 49.66 116.57 16.13 o 1 2 1 46715.18 46936.66 1245.72 o 2 2 1 1638.94 1653.08 43.51 o 3 2 1 3141.63 3126.82 77.10 o 4 2 1 728.78 801.61 29.45 o 5 2 1 12521.13 12303.42 276.01 o 6 2 1 1829.28 1790.67 67.93 o 7 2 1 30168.78 30894.81 707.25 o 8 2 1 42.12 -52.12 56.18 o 9 2 1 116.87 127.49 38.54 o 10 2 1 151.68 84.74 56.88 o 11 2 1 5373.32 5931.32 203.07 o 12 2 1 198.07 350.74 79.77 o 13 2 1 3557.12 3597.49 184.96 o 14 2 1 6.34 -47.38 117.10 o -14 3 1 3.34 184.56 150.94 o -13 3 1 57.09 29.33 128.61 o -12 3 1 48.66 49.97 93.75 o -11 3 1 643.72 705.38 64.79 o -10 3 1 257.46 268.71 55.81 o -9 3 1 2007.10 2138.87 99.18 o -8 3 1 504.56 519.51 53.02 o -7 3 1 2520.36 2496.06 110.25 o -6 3 1 5170.80 5128.98 124.56 o -5 3 1 429.43 372.27 19.29 o -4 3 1 2082.37 2208.49 52.01 o -3 3 1 1543.52 1653.33 34.26 o -2 3 1 1386.41 1301.73 31.27 o -1 3 1 48.94 68.87 10.04 o 0 3 1 28968.60 28710.90 646.17 o 1 3 1 3339.51 3355.27 60.75 o 2 3 1 5069.34 4951.08 95.22 o 3 3 1 714.10 725.93 32.16 o 4 3 1 145.49 139.35 41.52 o 5 3 1 3409.08 3588.12 78.43 o 6 3 1 7054.66 7572.86 170.79 o 7 3 1 571.78 631.26 83.37 o 8 3 1 26.41 29.16 28.73 o 9 3 1 314.26 345.05 57.31 o 10 3 1 1887.70 1859.00 85.40 o 11 3 1 2.31 76.87 62.35 o 12 3 1 2184.85 2266.20 145.19 o 13 3 1 21.24 -65.64 65.64 o 14 3 1 103.75 139.89 165.16 o -13 4 1 1006.30 901.20 151.18 o -12 4 1 1325.27 1325.01 141.25 o -11 4 1 20.62 111.50 53.29 o -10 4 1 3193.12 3492.46 110.15 o -9 4 1 496.26 530.58 75.59 o -8 4 1 3.62 21.11 28.53 o -7 4 1 1852.26 1793.88 58.99 o -6 4 1 357.32 368.23 34.75 o -5 4 1 2187.31 2133.37 51.09 o -4 4 1 5470.12 5455.84 115.62 o -3 4 1 30.90 30.57 11.28 o -2 4 1 11464.24 11081.48 325.56 o -1 4 1 944.99 1020.69 42.54 o 0 4 1 18778.00 18074.87 460.39 o 1 4 1 13494.53 13316.33 325.14 o 2 4 1 837.79 895.52 21.04 o 3 4 1 4705.76 5041.53 92.93 o 4 4 1 1564.04 1648.10 40.93 o 5 4 1 3920.49 3705.84 94.13 o 6 4 1 16622.36 16096.15 375.67 o 7 4 1 7913.04 8064.16 219.46 o 8 4 1 145.46 131.76 47.04 o 9 4 1 188.24 190.66 61.93 o 10 4 1 683.46 869.65 79.96 o 11 4 1 320.52 324.12 116.65 o 12 4 1 408.56 476.01 52.02 o 13 4 1 1643.66 1611.12 144.86 o -13 5 1 1092.13 1147.15 170.58 o -12 5 1 2257.67 1989.61 182.33 o -11 5 1 1967.84 2209.21 127.85 o -10 5 1 2534.98 2674.51 97.90 o -9 5 1 2513.34 2506.15 130.21 o -8 5 1 18.32 44.56 27.06 o -7 5 1 172.47 202.54 26.17 o -6 5 1 13393.77 13774.48 313.05 o -5 5 1 4012.29 4063.74 120.09 o -4 5 1 2562.45 2771.08 57.66 o -3 5 1 4822.11 4813.96 115.16 o -2 5 1 2424.50 2319.08 33.82 o -1 5 1 4520.32 4737.93 161.01 o 0 5 1 23408.38 22818.70 777.08 o 1 5 1 2075.40 2155.94 38.60 o 2 5 1 1509.65 1581.54 29.97 o 3 5 1 639.52 619.51 36.10 o 4 5 1 3.63 8.14 13.56 o 5 5 1 720.02 597.24 77.62 o 6 5 1 147.43 94.76 26.85 o 7 5 1 66.42 36.88 55.28 o 8 5 1 98.22 60.55 33.66 o 9 5 1 1386.77 1458.59 112.37 o 10 5 1 287.78 338.98 61.77 o 11 5 1 136.93 182.83 70.13 o 12 5 1 2027.71 2162.66 128.17 o 13 5 1 16.51 -11.28 113.49 o -13 6 1 628.74 641.02 105.82 o -12 6 1 97.43 239.84 119.13 o -11 6 1 0.70 218.18 70.17 o -10 6 1 9533.38 9734.97 325.63 o -9 6 1 383.63 450.62 45.87 o -8 6 1 1245.36 1032.60 50.15 o -7 6 1 13089.62 13195.36 277.80 o -6 6 1 1009.07 1006.19 90.26 o -5 6 1 3424.83 3244.03 92.55 o -4 6 1 11277.15 11000.34 205.72 o -3 6 1 4829.32 4914.18 103.46 o -2 6 1 6733.79 6058.17 96.13 o -1 6 1 3488.27 3589.75 90.87 o 0 6 1 33527.06 33511.46 982.58 o 1 6 1 7536.48 7468.41 210.20 o 2 6 1 11351.19 10917.54 169.93 o 3 6 1 6920.51 6687.88 313.13 o 4 6 1 14481.76 14540.80 416.91 o 5 6 1 4459.96 4504.07 118.74 o 6 6 1 15517.63 15432.36 357.68 o 7 6 1 5845.67 6000.27 188.95 o 8 6 1 5056.12 5281.72 160.72 o 9 6 1 2495.46 2602.61 126.94 o 10 6 1 10399.65 10776.22 293.36 o 11 6 1 865.37 886.98 96.12 o 12 6 1 3325.85 3331.35 175.57 o 13 6 1 3036.68 2871.35 183.24 o -13 7 1 777.96 680.06 113.95 o -12 7 1 7781.37 7893.64 439.05 o -11 7 1 3157.59 3287.57 223.41 o -10 7 1 9216.31 10572.54 605.74 o -9 7 1 2634.70 2701.55 101.60 o -8 7 1 3046.32 3100.63 157.52 o -7 7 1 30.51 44.35 26.96 o -6 7 1 17257.47 17365.62 383.29 o -5 7 1 4542.01 4641.95 123.02 o -4 7 1 5889.79 5878.55 172.49 o -3 7 1 6389.22 6224.54 113.46 o -2 7 1 297.57 491.45 45.01 o -1 7 1 2168.82 1936.03 35.12 o 0 7 1 7700.88 7602.49 144.90 o 1 7 1 3022.09 3183.39 53.57 o 2 7 1 6432.65 5845.15 81.37 o 3 7 1 1992.64 1971.53 41.37 o 4 7 1 2319.12 2140.42 68.92 o 5 7 1 553.74 534.76 26.00 o 6 7 1 106.66 116.44 19.03 o 7 7 1 2217.66 2211.59 67.16 o 8 7 1 904.84 898.49 50.88 o 9 7 1 1729.95 1785.78 83.71 o 10 7 1 36.09 158.39 60.92 o 11 7 1 269.63 313.85 80.77 o 12 7 1 1588.97 1580.88 117.11 o 13 7 1 1123.19 962.12 117.78 o -13 8 1 1038.28 947.45 128.61 o -12 8 1 429.55 382.89 115.30 o -11 8 1 112.07 113.26 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