#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/40/2204080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204080_Fobs loop_ _publ_author_name 'Shen, Xiao-Ping' 'Yuan, Ai-Hua' _publ_section_title ; cis-Dibromobis(1,10-phenanthroline)manganese(II) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1074 _journal_page_last m1075 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.622 _cell_angle_gamma 90.000 _cell_length_a 10.4230 _cell_length_b 16.2230 _cell_length_c 13.2440 _exptl_crystal_F_000 1132.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file rn6019Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 398.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 174.00 282.26 150.38 o 2 0 0 6056.99 6033.83 164.26 o 3 0 0 980.60 1039.96 212.85 o 4 0 0 13795.27 13888.95 270.36 o 5 0 0 10562.44 10853.02 148.07 o 6 0 0 33.30 47.34 28.46 o 7 0 0 771.45 802.81 12.72 o 8 0 0 3764.50 3975.03 139.88 o 9 0 0 8027.48 7883.54 96.01 o 10 0 0 1439.95 1286.31 257.67 o 11 0 0 0.68 62.47 292.67 o 12 0 0 10.52 62.67 85.48 o 1 1 0 38816.68 36268.90 30.08 o 2 1 0 19152.19 19370.48 183.93 o 3 1 0 1067.62 1317.14 125.30 o 4 1 0 82.83 239.46 173.52 o 5 1 0 9679.44 9165.19 138.95 o 6 1 0 18101.39 18500.58 342.41 o 7 1 0 5621.80 5324.28 68.75 o 8 1 0 3946.90 4179.49 237.14 o 9 1 0 329.53 337.33 34.38 o 10 1 0 29.34 128.40 32.39 o 11 1 0 10.85 46.03 75.03 o 12 1 0 1028.84 1434.42 223.26 o 0 2 0 15577.98 15276.60 82.13 o 1 2 0 3586.41 3761.89 269.53 o 2 2 0 932.31 889.59 29.05 o 3 2 0 1967.21 2465.12 249.87 o 4 2 0 21008.04 19946.84 364.66 o 5 2 0 349.89 345.88 3.47 o 6 2 0 397.69 395.81 9.50 o 7 2 0 1626.53 2128.50 318.12 o 8 2 0 268.22 353.28 55.66 o 9 2 0 929.18 853.71 25.45 o 10 2 0 2996.03 2730.25 44.61 o 11 2 0 469.71 533.28 101.80 o 12 2 0 12.46 33.55 20.01 o 1 3 0 139.55 284.32 79.31 o 2 3 0 2935.91 2937.09 319.27 o 3 3 0 561.61 529.21 48.19 o 4 3 0 10544.84 10295.45 225.57 o 5 3 0 30859.84 29127.21 85.30 o 6 3 0 276.10 308.86 251.02 o 7 3 0 2739.35 3120.69 89.26 o 8 3 0 1416.68 1484.16 313.49 o 9 3 0 11428.33 10767.45 69.65 o 10 3 0 1310.69 1395.09 164.26 o 11 3 0 308.23 270.79 57.23 o 12 3 0 1945.32 1989.68 25.45 o 0 4 0 41.05 124.51 39.20 o 1 4 0 333.56 550.63 263.75 o 2 4 0 13798.14 14460.70 141.63 o 3 4 0 25302.06 24068.22 82.13 o 4 4 0 11649.87 11574.68 329.48 o 5 4 0 9651.16 9160.64 138.82 o 6 4 0 8748.21 8526.54 60.27 o 7 4 0 88.57 246.40 98.33 o 8 4 0 7108.29 6575.10 129.94 o 9 4 0 169.42 374.80 231.36 o 10 4 0 8053.91 7612.92 53.85 o 11 4 0 3849.77 3713.30 304.24 o 12 4 0 514.02 548.54 62.48 o 1 5 0 2782.68 2667.85 57.13 o 2 5 0 712.22 763.48 215.16 o 3 5 0 463.48 433.61 45.06 o 4 5 0 13174.39 13889.60 229.04 o 5 5 0 21320.24 21147.09 121.76 o 6 5 0 190.73 384.05 223.26 o 7 5 0 1646.27 1607.04 201.90 o 8 5 0 828.27 976.33 315.80 o 9 5 0 5547.48 5253.45 148.40 o 10 5 0 2392.79 2720.78 337.78 o 11 5 0 153.92 183.74 21.80 o 12 5 0 791.18 809.75 16.20 o 0 6 0 9703.94 9138.02 63.51 o 1 6 0 177.70 241.77 180.46 o 2 6 0 1378.51 1669.99 52.90 o 3 6 0 495.36 685.98 257.96 o 4 6 0 14010.02 13076.29 211.03 o 5 6 0 1.48 12.72 10.41 o 6 6 0 1731.19 1765.95 69.93 o 7 6 0 4.85 70.56 263.75 o 8 6 0 2863.49 2815.00 38.83 o 9 6 0 432.54 439.58 17.35 o 10 6 0 3423.56 3344.22 99.85 o 11 6 0 5.85 50.90 113.37 o 12 6 0 430.83 406.45 38.20 o 1 7 0 8015.92 7594.87 27.69 o 2 7 0 976.52 1170.67 185.09 o 3 7 0 1942.59 2097.45 82.98 o 4 7 0 628.86 691.76 90.23 o 5 7 0 1175.34 1439.38 81.65 o 6 7 0 11.71 31.23 20.82 o 7 7 0 1006.65 1373.09 91.62 o 8 7 0 120.17 364.39 322.74 o 9 7 0 6.78 21.14 37.03 o 10 7 0 204.29 379.43 153.85 o 11 7 0 283.03 277.98 44.66 o 0 8 0 18421.67 17964.96 90.26 o 1 8 0 391.09 525.18 180.46 o 2 8 0 8616.61 8429.29 68.70 o 3 8 0 5775.48 5760.82 123.78 o 4 8 0 123.74 256.98 37.32 o 5 8 0 1671.87 1666.94 52.06 o 6 8 0 1637.63 1946.33 74.95 o 7 8 0 3058.35 3178.86 98.33 o 8 8 0 60.31 97.51 64.33 o 9 8 0 520.55 688.29 249.87 o 10 8 0 499.91 606.07 94.25 o 11 8 0 566.27 559.89 71.72 o 1 9 0 16451.70 15443.02 354.10 o 2 9 0 574.57 626.98 148.07 o 3 9 0 4254.76 4106.26 70.97 o 4 9 0 7766.65 7440.49 256.81 o 5 9 0 1049.43 1453.52 94.68 o 6 9 0 559.84 558.73 9.25 o 7 9 0 920.58 839.48 91.27 o 8 9 0 569.45 587.65 333.16 o 9 9 0 2661.18 2563.84 114.29 o 10 9 0 1295.46 1363.86 19.67 o 11 9 0 102.70 269.45 86.92 o 0 10 0 402.10 485.32 121.54 o 1 10 0 2412.83 2629.39 91.39 o 2 10 0 3762.72 3828.89 62.56 o 3 10 0 3561.27 3825.51 151.54 o 4 10 0 2.29 48.44 77.55 o 5 10 0 550.75 628.14 343.57 o 6 10 0 1.08 78.38 33.14 o 7 10 0 71.30 194.34 61.31 o 8 10 0 50.88 116.72 98.37 o 9 10 0 275.57 342.41 292.67 o 10 10 0 604.30 657.77 36.37 o 1 11 0 12.03 17.94 19.53 o 2 11 0 1037.80 1560.51 256.81 o 3 11 0 1809.28 1768.52 82.84 o 4 11 0 378.32 493.95 151.54 o 5 11 0 7.44 125.75 53.34 o 6 11 0 2402.26 2361.01 68.25 o 7 11 0 3445.88 3197.32 49.18 o 8 11 0 631.18 697.55 318.12 o 9 11 0 83.29 203.31 94.09 o 10 11 0 61.69 180.46 341.25 o 0 12 0 3845.58 3800.00 128.34 o 1 12 0 4652.79 4947.60 224.42 o 2 12 0 1875.82 1692.59 35.35 o 3 12 0 1628.36 1858.96 100.64 o 4 12 0 596.54 681.41 39.35 o 5 12 0 3670.46 3363.95 16.20 o 6 12 0 1455.25 1504.96 138.14 o 7 12 0 1091.86 1376.58 104.11 o 8 12 0 2884.59 2739.82 122.57 o 9 12 0 965.94 1501.52 233.67 o 10 12 0 163.98 324.98 116.36 o 1 13 0 6116.60 6030.01 84.64 o 2 13 0 3452.33 3513.18 96.01 o 3 13 0 2837.09 2681.94 51.40 o 4 13 0 68.08 219.79 91.39 o 5 13 0 348.34 311.29 50.15 o 6 13 0 6085.66 5803.63 311.18 o 7 13 0 6428.97 5953.28 82.39 o 8 13 0 1743.12 2054.46 341.25 o 9 13 0 407.54 433.22 48.59 o 0 14 0 24486.73 23543.82 217.00 o 1 14 0 5149.40 5172.02 341.25 o 2 14 0 805.91 734.84 27.30 o 3 14 0 237.60 451.15 282.26 o 4 14 0 868.70 1047.15 53.68 o 5 14 0 817.39 883.79 230.20 o 6 14 0 110.50 152.17 33.60 o 7 14 0 238.70 423.39 277.63 o 8 14 0 820.71 849.42 45.83 o 9 14 0 2659.51 2981.05 329.69 o 1 15 0 286.45 264.09 38.74 o 2 15 0 30.38 60.15 86.76 o 3 15 0 3038.65 2933.74 37.56 o 4 15 0 2659.38 2396.87 17.35 o 5 15 0 2896.89 2707.77 118.12 o 6 15 0 1774.70 1864.75 155.01 o 7 15 0 2177.81 2267.18 60.20 o 8 15 0 63.11 245.24 314.65 o 0 16 0 95.99 153.91 80.33 o 1 16 0 511.25 580.71 296.14 o 2 16 0 4824.49 4613.61 89.74 o 3 16 0 3823.02 3746.85 54.37 o 4 16 0 1170.96 1233.24 71.63 o 5 16 0 522.94 585.34 62.47 o 6 16 0 436.90 496.87 41.29 o 7 16 0 8.54 24.29 105.27 o 1 17 0 236.98 315.91 42.49 o 2 17 0 0.36 152.70 136.50 o 3 17 0 1275.13 1140.93 98.94 o 4 17 0 3751.76 4003.66 276.47 o 5 17 0 2437.15 2270.81 57.15 o 6 17 0 243.82 204.75 54.37 o 0 18 0 198.25 310.28 82.77 o 1 18 0 1084.59 993.68 33.55 o 2 18 0 1492.47 1652.50 50.02 o 3 18 0 1702.68 1985.06 230.20 o 4 18 0 904.71 891.31 143.19 o 5 18 0 412.88 567.98 193.18 o 1 19 0 19.75 95.46 30.33 o 2 19 0 313.72 477.76 318.12 o 3 19 0 74.59 75.11 22.73 o 0 20 0 3311.50 3043.72 45.47 o -12 1 1 319.58 448.84 242.93 o -11 1 1 245.43 267.47 35.69 o -10 1 1 464.27 471.97 26.61 o -9 1 1 1620.84 1892.91 61.96 o -8 1 1 512.77 593.43 116.84 o -7 1 1 7.99 43.23 34.50 o -6 1 1 25.86 63.62 133.03 o -5 1 1 456.43 474.73 51.37 o -4 1 1 4779.50 5029.73 321.59 o -3 1 1 2387.57 3011.26 162.86 o -2 1 1 19.39 202.44 233.67 o -1 1 1 928.41 894.55 72.99 o 0 1 1 175.87 271.85 55.53 o 1 1 1 4585.22 4415.41 36.45 o 2 1 1 4245.96 4002.50 2.31 o 3 1 1 1090.06 1181.51 60.51 o 4 1 1 17669.76 17844.67 148.07 o 5 1 1 3927.65 3747.49 65.78 o 6 1 1 213.28 332.00 138.82 o 7 1 1 2736.23 3087.40 93.48 o 8 1 1 8.48 27.76 160.79 o 9 1 1 526.42 506.91 52.45 o 10 1 1 1543.78 1566.30 17.35 o 11 1 1 30.86 210.68 76.31 o 12 1 1 830.04 934.69 127.25 o -12 2 1 16.71 160.10 113.83 o -11 2 1 1410.29 1408.97 286.88 o -10 2 1 2077.44 2041.50 170.00 o -9 2 1 464.60 546.01 134.19 o -8 2 1 5611.85 5364.50 56.89 o -7 2 1 1106.42 1437.89 121.46 o -6 2 1 1096.74 1018.92 84.51 o -5 2 1 4304.56 4735.91 289.20 o -4 2 1 100.68 170.34 62.79 o -3 2 1 11480.33 13226.76 314.65 o -2 2 1 41885.36 39242.39 111.94 o -1 2 1 500.55 615.41 285.73 o 0 2 1 4630.63 4782.53 69.74 o 1 2 1 513.03 551.79 79.82 o 2 2 1 1129.80 1105.11 81.96 o 3 2 1 14970.72 14561.70 136.50 o 4 2 1 307.95 292.12 63.28 o 5 2 1 3847.54 4452.49 303.08 o 6 2 1 13363.10 12686.88 342.11 o 7 2 1 517.95 533.28 72.88 o 8 2 1 1165.62 1383.77 80.44 o 9 2 1 9.76 34.70 76.35 o 10 2 1 629.70 640.53 37.83 o 11 2 1 1748.74 1742.13 78.66 o 12 2 1 205.67 411.61 80.15 o -12 3 1 68.32 57.84 11.57 o -11 3 1 151.25 308.22 67.30 o -10 3 1 1219.35 1397.40 137.66 o -9 3 1 5085.40 4991.13 91.01 o -8 3 1 940.77 1316.43 315.80 o -7 3 1 62.55 94.92 46.95 o -6 3 1 1203.48 1266.69 30.08 o -5 3 1 70.07 95.71 9.89 o -4 3 1 823.85 798.19 335.47 o -3 3 1 855.16 1077.74 88.43 o -2 3 1 2503.62 3001.88 235.99 o -1 3 1 7411.91 7279.89 129.74 o 0 3 1 47309.33 45234.04 122.62 o 1 3 1 454.09 464.60 24.65 o 2 3 1 2622.20 2620.13 18.51 o 3 3 1 2555.21 2511.00 57.58 o 4 3 1 20360.10 20780.61 160.79 o 5 3 1 4673.38 4392.62 124.08 o 6 3 1 816.38 916.18 285.73 o 7 3 1 2275.36 2161.53 33.21 o 8 3 1 58.88 217.48 200.13 o 9 3 1 9.18 54.22 37.52 o 10 3 1 334.39 421.07 303.08 o 11 3 1 317.46 291.03 38.62 o 12 3 1 1833.05 2039.42 68.25 o -12 4 1 6.35 49.91 65.17 o -11 4 1 59.46 172.36 144.60 o -10 4 1 674.63 650.82 31.48 o -9 4 1 815.11 897.67 273.00 o -8 4 1 1535.89 1811.79 51.03 o -7 4 1 82.51 174.68 313.49 o -6 4 1 4273.39 3932.57 119.53 o -5 4 1 7958.34 7551.54 31.23 o -4 4 1 804.73 883.07 98.59 o -3 4 1 272.04 327.37 37.02 o -2 4 1 9644.70 9085.23 114.09 o -1 4 1 11573.90 11891.82 152.70 o 0 4 1 2705.87 2652.92 105.94 o 1 4 1 272.97 391.00 238.30 o 2 4 1 372.69 432.37 40.80 o 3 4 1 1.76 32.39 56.68 o 4 4 1 2516.29 2571.32 109.27 o 5 4 1 13478.91 14048.08 207.07 o 6 4 1 2206.74 2429.19 68.58 o 7 4 1 1099.38 1172.99 122.62 o 8 4 1 1446.84 1347.61 80.63 o 9 4 1 1989.65 2062.56 137.66 o 10 4 1 180.34 277.00 40.62 o 11 4 1 925.68 1245.86 104.11 o 12 4 1 349.97 490.56 82.48 o -12 5 1 1023.33 1448.30 303.08 o -11 5 1 549.04 626.25 46.73 o -10 5 1 2685.94 2625.92 98.33 o -9 5 1 48.52 234.39 98.07 o -8 5 1 2091.30 2393.40 297.30 o -7 5 1 1931.40 2080.12 58.21 o -6 5 1 5801.98 5376.77 26.61 o -5 5 1 770.52 732.02 66.04 o -4 5 1 10539.71 10297.76 321.59 o -3 5 1 447.80 484.47 45.83 o -2 5 1 127.67 178.15 16.20 o -1 5 1 752.42 872.24 76.24 o 0 5 1 6892.71 7012.47 282.26 o 1 5 1 14538.45 13896.30 340.86 o 2 5 1 16047.69 16919.24 269.53 o 3 5 1 4413.59 4310.55 86.26 o 4 5 1 7149.67 6591.40 16.20 o 5 5 1 363.28 369.99 36.31 o 6 5 1 16.50 84.45 330.84 o 7 5 1 3564.88 3362.34 79.46 o 8 5 1 1375.64 1783.77 152.70 o 9 5 1 1679.08 1567.75 62.21 o 10 5 1 4384.25 4606.35 276.47 o 11 5 1 454.82 525.40 52.89 o 12 5 1 130.09 366.70 296.14 o -12 6 1 2048.21 2140.32 67.94 o -11 6 1 28.01 48.59 245.24 o -10 6 1 2485.28 2739.27 95.44 o -9 6 1 2243.20 2164.36 92.54 o -8 6 1 1789.41 2013.77 86.48 o -7 6 1 519.88 631.61 158.48 o -6 6 1 8431.21 7804.67 84.57 o -5 6 1 38564.06 36994.21 135.34 o -4 6 1 10016.44 9556.31 211.30 o -3 6 1 24.84 50.90 160.79 o -2 6 1 1801.87 1971.32 101.29 o -1 6 1 7651.08 7666.06 211.69 o 0 6 1 15456.89 14650.96 600.83 o 1 6 1 543.92 706.80 318.12 o 2 6 1 407.06 459.22 33.68 o 3 6 1 5787.91 5668.28 33.55 o 4 6 1 8051.15 7702.43 75.85 o 5 6 1 175.65 248.71 248.71 o 6 6 1 255.25 330.05 66.61 o 7 6 1 1714.75 1992.00 106.42 o 8 6 1 10351.08 9396.15 91.02 o 9 6 1 8966.51 8353.20 168.89 o 10 6 1 494.35 468.27 54.41 o 11 6 1 287.69 429.17 300.77 o -11 7 1 5536.47 4974.19 137.92 o -10 7 1 2550.55 2445.46 26.61 o -9 7 1 57.80 227.31 83.83 o -8 7 1 1059.74 980.96 189.71 o -7 7 1 4442.01 4536.49 117.31 o -6 7 1 16467.84 16427.61 202.44 o -5 7 1 894.28 976.45 116.43 o -4 7 1 3204.57 3058.56 112.21 o -3 7 1 16954.94 16839.48 99.33 o -2 7 1 152.38 230.20 108.74 o -1 7 1 6.95 112.66 38.66 o 0 7 1 16631.87 17185.30 256.81 o 1 7 1 14910.85 14118.98 159.12 o 2 7 1 10846.10 10268.84 4.63 o 3 7 1 12448.81 11592.39 245.53 o 4 7 1 352.12 415.29 187.40 o 5 7 1 794.36 847.66 61.74 o 6 7 1 1476.62 1422.85 327.37 o 7 7 1 5811.76 5466.17 15.91 o 8 7 1 3436.29 2978.74 201.28 o 9 7 1 2817.98 2833.77 74.55 o 10 7 1 4186.30 4327.56 220.95 o 11 7 1 810.51 769.47 42.98 o -11 8 1 1615.61 1507.30 34.70 o -10 8 1 379.51 429.95 51.11 o -9 8 1 2690.88 2431.58 12.72 o -8 8 1 178.07 165.48 61.09 o -7 8 1 450.45 639.71 296.14 o -6 8 1 4873.55 4583.46 159.72 o -5 8 1 13447.01 13216.35 69.41 o -4 8 1 5332.18 5373.34 140.07 o -3 8 1 4019.79 3838.24 197.81 o -2 8 1 3970.61 4132.04 59.33 o -1 8 1 15989.98 14614.91 5.78 o 0 8 1 1630.96 1729.86 24.23 o 1 8 1 386.14 461.56 70.56 o 2 8 1 15.48 64.69 49.16 o 3 8 1 417.32 617.73 343.57 o 4 8 1 4170.17 4202.63 131.32 o 5 8 1 3372.03 3251.74 122.62 o 6 8 1 20.04 20.07 30.57 o 7 8 1 5972.48 5377.93 54.37 o 8 8 1 3002.26 2902.54 141.27 o 9 8 1 5058.34 5256.46 313.49 o 10 8 1 385.68 326.44 70.48 o 11 8 1 9.62 21.98 20.82 o -11 9 1 94.84 242.98 118.87 o -10 9 1 4806.41 4708.14 146.91 o -9 9 1 3319.96 3532.08 106.98 o -8 9 1 217.29 311.18 84.45 o -7 9 1 884.20 880.05 134.32 o -6 9 1 819.23 854.87 301.92 o -5 9 1 58.01 85.81 38.75 o -4 9 1 687.47 705.64 167.73 o -3 9 1 231.87 277.98 35.29 o -2 9 1 577.86 676.72 139.97 o -1 9 1 13272.81 12242.74 724.66 o 0 9 1 19636.15 18613.94 17.35 o 1 9 1 1905.88 1838.78 57.29 o 2 9 1 251.42 264.91 314.65 o 3 9 1 2575.26 2474.90 110.90 o 4 9 1 20622.63 20088.85 238.30 o 5 9 1 5380.04 5482.96 95.67 o 6 9 1 10.24 77.51 99.48 o 7 9 1 831.95 828.06 34.30 o 8 9 1 266.07 377.11 252.18 o 9 9 1 165.01 192.89 22.65 o 10 9 1 297.87 526.34 298.45 o 11 9 1 280.56 238.02 57.83 o -11 10 1 800.20 865.28 126.09 o -10 10 1 1186.76 1309.58 84.91 o -9 10 1 1053.66 1013.35 345.88 o -8 10 1 4021.71 3697.70 85.48 o -7 10 1 1675.40 1950.35 124.93 o -6 10 1 814.60 1092.07 174.63 o -5 10 1 1739.16 1712.05 200.13 o -4 10 1 195.15 223.48 32.51 o -3 10 1 5073.19 5259.93 275.32 o -2 10 1 13779.61 13754.15 409.76 o -1 10 1 6913.22 6506.96 109.90 o 0 10 1 1436.14 1592.89 59.70 o 1 10 1 12827.18 13116.87 198.97 o 2 10 1 4023.10 3925.89 83.77 o 3 10 1 3975.49 4223.45 341.25 o 4 10 1 970.60 951.32 118.21 o 5 10 1 16906.10 15660.65 49.74 o 6 10 1 4870.49 4676.95 31.08 o 7 10 1 309.22 384.05 229.04 o 8 10 1 1746.56 1749.72 42.40 o 9 10 1 33.54 30.08 19.67 o 10 10 1 412.16 452.18 28.64 o -10 11 1 2458.06 2330.94 39.33 o -9 11 1 3136.51 3195.68 117.16 o -8 11 1 681.58 651.27 137.66 o -7 11 1 216.20 242.75 75.52 o -6 11 1 241.38 230.20 5.78 o -5 11 1 13.22 22.21 11.78 o 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