#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:06:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180961 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/41/2204180.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204180_Fobs loop_ _publ_author_name 'Fu, Ai-Yun' 'Wang, Da-Qi' 'Shen, Qing-Jun' 'Zhang, Cun-Lan' _publ_section_title ; Bis(\m-N-acetyl-N-phenylglycinato-\k^2^O:O')bis[triaqua(1,10-phenanthroline-\k^2^N,N')lanthanum(III)] bis(N-acetyl-N-phenylglycinate) dinitrate dihydrate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1337 _journal_page_last m1339 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 66.966 _cell_angle_beta 86.448 _cell_angle_gamma 79.303 _cell_length_a 11.4722 _cell_length_b 14.2711 _cell_length_c 14.9863 _exptl_crystal_F_000 1036.00 _reflns_d_resolution_high 0.8401 _cod_data_source_file hb6082Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 040802a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14490.65 16443.07 193.25 o 2 0 0 106.53 94.60 12.97 o 3 0 0 968.98 1038.96 16.40 o 4 0 0 200.61 179.81 8.58 o 5 0 0 9339.44 9307.79 111.46 o 6 0 0 139.01 76.34 9.63 o 7 0 0 47.50 51.87 7.87 o 8 0 0 1919.03 1916.06 53.04 o 9 0 0 2097.86 2055.58 83.35 o 10 0 0 7.20 3.96 17.09 o 11 0 0 456.72 351.44 47.61 o 12 0 0 840.17 752.40 61.55 o 13 0 0 859.57 982.00 74.30 o -13 1 0 15.61 29.29 26.31 o -12 1 0 392.91 333.23 49.16 o -11 1 0 1626.38 1789.81 88.42 o -10 1 0 1078.32 1037.42 63.96 o -9 1 0 636.28 586.82 33.50 o -8 1 0 35.78 23.92 12.54 o -7 1 0 2975.95 2816.53 60.12 o -6 1 0 2219.01 2033.99 29.56 o -5 1 0 6823.50 7676.56 96.67 o -4 1 0 27837.78 27435.11 369.46 o -3 1 0 7116.75 6984.15 101.87 o -2 1 0 7121.27 7431.99 157.40 o -1 1 0 7.90 4.27 2.10 o 1 1 0 26727.18 25041.43 294.18 o 2 1 0 27525.61 28877.96 327.93 o 3 1 0 11213.97 12721.28 114.76 o 4 1 0 536.81 591.00 20.41 o 5 1 0 1197.19 1229.93 26.91 o 6 1 0 7254.16 7662.82 87.38 o 7 1 0 14.89 13.98 8.24 o 8 1 0 567.26 593.40 43.40 o 9 1 0 981.43 890.54 56.47 o 10 1 0 1603.87 1570.18 77.65 o 11 1 0 694.06 611.42 52.56 o 12 1 0 26.88 -9.85 22.17 o 13 1 0 508.25 583.56 58.76 o -13 2 0 362.36 445.05 59.87 o -12 2 0 9.12 18.39 24.77 o -11 2 0 31.02 49.53 26.75 o -10 2 0 728.27 717.97 38.01 o -9 2 0 3070.16 3111.01 108.05 o -8 2 0 813.18 728.14 33.75 o -7 2 0 841.71 939.60 37.49 o -6 2 0 3283.47 3558.35 42.70 o -5 2 0 288.82 211.03 23.38 o -4 2 0 166.81 181.09 10.75 o -3 2 0 4434.37 4665.88 44.60 o -2 2 0 1293.86 1329.92 18.91 o -1 2 0 1132.96 1222.93 30.46 o 0 2 0 4725.01 4810.73 68.48 o 1 2 0 19.10 20.56 6.44 o 2 2 0 132.59 159.37 15.91 o 3 2 0 1502.17 1638.11 48.17 o 4 2 0 15.16 7.54 5.23 o 5 2 0 55.81 87.32 10.47 o 6 2 0 8707.37 8918.23 254.12 o 7 2 0 2423.63 2406.55 70.74 o 8 2 0 1604.36 1710.18 72.01 o 9 2 0 4.31 -13.31 13.31 o 10 2 0 674.35 630.48 52.14 o 11 2 0 1207.35 1258.66 75.91 o 12 2 0 714.61 700.07 60.06 o 13 2 0 55.19 59.38 29.91 o -12 3 0 619.56 681.06 61.05 o -11 3 0 1249.27 1217.97 51.84 o -10 3 0 623.32 601.94 61.79 o -9 3 0 709.41 619.50 33.91 o -8 3 0 1544.60 1615.09 73.16 o -7 3 0 276.63 310.93 22.18 o -6 3 0 130.24 122.51 20.37 o -5 3 0 3993.80 4385.10 68.16 o -4 3 0 7361.62 7448.38 92.11 o -3 3 0 12637.28 12898.98 221.15 o -2 3 0 3888.60 4392.58 53.69 o -1 3 0 7200.10 7532.33 109.72 o 0 3 0 2511.95 2633.17 50.84 o 1 3 0 737.49 739.70 25.70 o 2 3 0 416.45 435.46 23.03 o 3 3 0 337.51 287.66 23.28 o 4 3 0 6909.08 7330.78 129.91 o 5 3 0 4010.43 4270.99 63.11 o 6 3 0 5.32 -1.25 7.26 o 7 3 0 1347.99 1406.64 37.23 o 8 3 0 6025.18 6220.99 88.99 o 9 3 0 1984.69 1822.57 80.50 o 10 3 0 37.47 31.33 26.44 o 11 3 0 820.15 791.65 60.50 o 12 3 0 686.15 666.76 60.93 o 13 3 0 470.16 519.97 63.65 o -12 4 0 58.13 21.30 30.15 o -11 4 0 2333.06 2453.48 109.10 o -10 4 0 282.71 404.81 50.77 o -9 4 0 16.15 -7.68 12.06 o -8 4 0 461.64 397.82 28.75 o -7 4 0 4441.53 4634.15 82.02 o -6 4 0 4391.95 4492.60 75.54 o -5 4 0 200.93 218.37 17.50 o -4 4 0 2549.42 2626.36 51.12 o -3 4 0 17573.42 17714.81 164.38 o -2 4 0 10460.88 10555.04 155.42 o -1 4 0 2384.39 2300.35 54.61 o 0 4 0 868.96 739.39 28.05 o 1 4 0 9977.15 9468.34 132.94 o 2 4 0 9651.21 9221.03 135.92 o 3 4 0 65.87 56.41 14.49 o 4 4 0 5172.23 4985.16 105.02 o 5 4 0 5528.99 5072.16 113.13 o 6 4 0 3160.22 3359.36 60.42 o 7 4 0 653.60 661.08 27.70 o 8 4 0 13.87 18.94 13.59 o 9 4 0 1861.90 1957.80 84.96 o 10 4 0 2132.10 2246.91 96.04 o 11 4 0 132.70 142.71 37.34 o 12 4 0 83.04 38.39 30.21 o 13 4 0 453.22 530.99 65.51 o -11 5 0 2.38 5.51 25.88 o -10 5 0 1911.04 1921.15 93.50 o -9 5 0 1507.32 1522.13 78.76 o -8 5 0 92.95 75.81 17.03 o -7 5 0 1007.93 946.93 36.88 o -6 5 0 1486.44 1393.08 41.46 o -5 5 0 8400.13 8751.38 165.58 o -4 5 0 34.11 30.46 9.56 o -3 5 0 33.83 33.88 19.26 o -2 5 0 17.72 -1.86 8.54 o -1 5 0 9662.99 9945.50 151.58 o 0 5 0 5780.10 5651.74 100.00 o 1 5 0 431.86 434.43 16.06 o 2 5 0 4090.39 4006.70 81.49 o 3 5 0 3233.11 2934.48 72.69 o 4 5 0 1121.78 910.23 44.03 o 5 5 0 11.27 29.29 17.21 o 6 5 0 467.12 364.13 35.36 o 7 5 0 5937.36 6122.67 146.07 o 8 5 0 2345.94 2406.66 56.85 o 9 5 0 17.72 11.39 25.14 o 10 5 0 440.63 534.52 58.57 o 11 5 0 402.01 449.51 53.56 o 12 5 0 561.68 615.69 60.06 o 13 5 0 44.00 5.94 27.24 o -11 6 0 21.12 1.18 22.72 o -10 6 0 25.65 3.84 20.80 o -9 6 0 737.15 673.82 54.61 o -8 6 0 638.29 543.87 47.55 o -7 6 0 2064.44 2074.73 55.86 o -6 6 0 193.89 206.86 28.88 o -5 6 0 3289.66 3339.63 63.01 o -4 6 0 4774.75 4826.04 88.48 o -3 6 0 3201.79 3355.40 56.85 o -2 6 0 1327.00 1309.19 49.97 o -1 6 0 308.95 336.95 25.57 o 1 6 0 5640.24 5441.22 67.17 o 2 6 0 759.63 768.00 36.04 o 3 6 0 5893.95 5980.72 115.98 o 4 6 0 6520.14 6792.44 133.93 o 5 6 0 31.50 1.36 14.05 o 6 6 0 2124.75 2022.82 77.59 o 7 6 0 38.89 32.63 20.87 o 8 6 0 2219.55 2335.21 59.26 o 9 6 0 1868.07 1872.11 54.26 o 10 6 0 60.84 30.90 26.62 o 11 6 0 19.03 -18.95 18.95 o 12 6 0 465.87 533.59 61.85 o 13 6 0 898.90 966.08 74.92 o -10 7 0 409.65 537.30 60.99 o -9 7 0 2.64 6.87 19.07 o -8 7 0 789.77 805.96 57.96 o -7 7 0 2090.93 2047.22 86.44 o -6 7 0 1145.73 1042.25 57.96 o -5 7 0 853.73 819.55 32.18 o -4 7 0 592.27 487.13 24.00 o -3 7 0 3533.82 3557.20 81.92 o -2 7 0 2635.47 2562.46 75.98 o -1 7 0 12.14 -6.44 9.78 o 0 7 0 2352.81 2366.42 44.91 o 1 7 0 14866.66 15596.58 164.58 o 2 7 0 6230.60 6100.35 119.26 o 3 7 0 2742.82 2835.90 79.63 o 4 7 0 1052.55 901.94 47.18 o 5 7 0 2378.20 2368.46 81.86 o 6 7 0 3039.00 2929.34 95.91 o 7 7 0 2081.77 2037.62 86.01 o 8 7 0 16.41 -7.13 12.05 o 9 7 0 385.48 395.69 30.09 o 10 7 0 897.04 963.79 68.48 o 11 7 0 150.90 149.22 41.36 o 12 7 0 0.01 -2.85 25.51 o 13 7 0 201.65 235.09 49.03 o -10 8 0 920.63 936.12 70.84 o -9 8 0 1177.02 1188.63 74.61 o -8 8 0 293.96 367.60 46.43 o -7 8 0 0.84 -15.73 17.15 o -6 8 0 2065.74 2238.00 89.41 o -5 8 0 904.56 834.50 52.08 o -4 8 0 156.53 124.11 16.35 o -3 8 0 707.05 677.35 36.32 o -2 8 0 2887.90 2759.61 83.84 o -1 8 0 4545.76 4305.21 105.45 o 0 8 0 51.17 55.06 12.66 o 1 8 0 1778.33 1696.62 39.58 o 2 8 0 3223.06 3154.73 85.70 o 3 8 0 10319.76 10691.83 183.84 o 4 8 0 5011.78 5006.28 119.01 o 5 8 0 986.96 1101.88 58.76 o 6 8 0 551.40 588.26 46.81 o 7 8 0 1541.85 1500.09 74.55 o 8 8 0 757.19 729.55 58.39 o 9 8 0 743.82 704.36 38.15 o 10 8 0 636.31 615.51 55.85 o 11 8 0 378.63 476.81 61.17 o 12 8 0 402.47 443.38 59.31 o -9 9 0 197.36 139.68 36.66 o -8 9 0 1515.54 1397.30 80.93 o -7 9 0 1054.68 1051.66 66.81 o -6 9 0 4.41 -5.57 16.41 o -5 9 0 19.10 -14.92 14.92 o -4 9 0 503.94 461.15 40.00 o -3 9 0 292.80 268.59 35.05 o -2 9 0 7.27 5.76 13.31 o -1 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-7 11 0 32.41 -1.36 21.36 o -6 11 0 774.87 656.42 54.92 o -5 11 0 1838.60 1890.00 88.73 o -4 11 0 1388.19 1457.30 74.80 o -3 11 0 218.39 140.18 30.59 o -2 11 0 838.27 909.18 58.02 o -1 11 0 2727.53 2852.22 63.79 o 0 11 0 472.06 441.99 25.77 o 1 11 0 45.92 65.75 24.40 o 2 11 0 869.77 907.07 56.35 o 3 11 0 3405.93 3365.01 107.68 o 4 11 0 727.04 750.79 55.42 o 5 11 0 259.38 256.21 41.85 o 6 11 0 333.97 344.69 48.79 o 7 11 0 997.97 995.13 68.92 o 8 11 0 1137.29 1073.27 74.43 o 9 11 0 122.31 104.19 24.06 o 10 11 0 157.17 177.58 41.33 o 11 11 0 466.19 552.29 67.86 o -6 12 0 11.54 -7.49 20.93 o -5 12 0 490.73 487.71 56.96 o -4 12 0 1815.20 1769.26 86.69 o -3 12 0 563.53 582.75 51.14 o -2 12 0 31.09 25.32 16.07 o -1 12 0 1302.63 1222.66 44.09 o 0 12 0 718.91 661.73 54.39 o 1 12 0 1021.45 1090.73 63.10 o 2 12 0 517.92 567.77 48.04 o 3 12 0 7.97 25.26 21.30 o 4 12 0 2839.32 3033.55 108.86 o 5 12 0 1408.47 1350.98 75.11 o 6 12 0 430.10 415.52 52.81 o 7 12 0 245.52 281.84 46.68 o 8 12 0 292.70 315.89 52.19 o 9 12 0 667.54 731.28 68.92 o 10 12 0 185.65 151.71 31.59 o -5 13 0 167.32 69.96 30.34 o -4 13 0 55.21 -10.77 21.49 o -3 13 0 850.04 792.21 61.05 o -2 13 0 1846.13 1904.73 60.29 o -1 13 0 120.05 165.98 23.61 o 0 13 0 28.81 -12.68 12.68 o 1 13 0 1366.02 1323.24 72.26 o 2 13 0 1347.30 1239.46 69.78 o 3 13 0 1044.06 1013.52 66.01 o 4 13 0 103.24 135.22 34.43 o 5 13 0 878.50 834.75 64.95 o 6 13 0 1019.86 892.89 69.47 o 7 13 0 508.97 585.73 60.24 o 8 13 0 105.82 53.99 34.43 o 9 13 0 146.78 122.41 41.79 o -3 14 0 0.44 -18.20 18.20 o -2 14 0 460.92 570.42 41.50 o -1 14 0 1570.85 1464.19 56.94 o 0 14 0 991.75 998.72 68.55 o 1 14 0 1.54 -10.28 24.33 o 2 14 0 291.27 289.45 45.38 o 3 14 0 1100.17 1064.11 71.33 o 4 14 0 1439.05 1427.83 83.72 o 5 14 0 137.36 131.45 40.31 o 6 14 0 51.95 -2.48 28.23 o 7 14 0 1293.61 1281.51 86.87 o 8 14 0 562.13 608.02 73.56 o -1 15 0 164.73 196.23 30.41 o 0 15 0 931.06 1039.58 74.18 o 1 15 0 1091.49 1218.91 77.46 o 2 15 0 180.98 198.13 44.02 o 3 15 0 198.13 213.61 44.27 o 4 15 0 1023.69 1207.76 79.82 o 5 15 0 1036.00 1106.83 80.68 o 6 15 0 209.96 268.10 54.86 o -4 -15 1 475.31 576.19 67.36 o -3 -15 1 438.43 626.02 61.12 o -2 -15 1 204.15 178.69 43.90 o -1 -15 1 76.40 37.89 34.05 o 0 -15 1 495.73 578.91 57.08 o -7 -14 1 155.96 229.40 50.77 o -6 -14 1 648.95 714.19 75.48 o -5 -14 1 123.03 208.53 46.25 o -4 -14 1 11.11 8.61 25.32 o -3 -14 1 270.87 270.95 45.13 o -2 -14 1 941.11 999.34 69.54 o -1 -14 1 782.41 832.15 62.29 o 0 -14 1 6.90 20.99 27.92 o 1 -14 1 448.80 537.08 39.53 o 2 -14 1 1196.88 1326.05 54.29 o 3 -14 1 428.19 501.93 68.11 o -8 -13 1 419.58 456.72 46.34 o -7 -13 1 47.17 52.63 34.18 o -6 -13 1 170.55 247.29 46.87 o -5 -13 1 283.71 331.99 50.52 o -4 -13 1 1474.77 1661.89 86.32 o -3 -13 1 0.69 -16.35 16.35 o -2 -13 1 879.82 904.47 62.48 o -1 -13 1 1161.94 1062.99 66.87 o 0 -13 1 1009.31 1060.08 66.75 o 1 -13 1 318.33 356.67 32.17 o 2 -13 1 83.20 104.26 21.79 o 3 -13 1 1265.85 1558.85 58.34 o 4 -13 1 996.77 936.80 67.93 o -10 -12 1 315.43 328.03 46.96 o -9 -12 1 170.62 131.23 33.65 o -8 -12 1 756.07 744.12 45.47 o -7 -12 1 390.59 492.29 61.42 o -6 -12 1 365.69 364.38 50.52 o -5 -12 1 1.24 -18.14 23.78 o -4 -12 1 1850.07 1910.06 87.31 o -3 -12 1 660.45 761.87 55.48 o -2 -12 1 19.43 29.10 20.68 o -1 -12 1 250.75 239.43 37.52 o 0 -12 1 1841.03 1838.69 53.44 o 1 -12 1 1920.47 1954.38 56.52 o 2 -12 1 1518.44 1697.74 67.56 o 3 -12 1 60.72 -7.06 20.74 o 4 -12 1 328.67 266.67 41.48 o 5 -12 1 1291.63 1354.57 78.76 o 6 -12 1 295.39 195.04 40.25 o -10 -11 1 950.17 995.64 51.88 o -9 -11 1 327.39 340.82 36.50 o -8 -11 1 3.56 -5.98 17.16 o -7 -11 1 309.40 344.50 51.26 o -6 -11 1 915.16 890.48 62.73 o -5 -11 1 1138.90 1250.24 71.21 o -4 -11 1 33.03 18.70 21.05 o -3 -11 1 2479.93 2238.61 86.63 o -2 -11 1 982.52 994.26 57.09 o -1 -11 1 1903.45 1925.48 78.33 o 0 -11 1 3.90 -11.44 11.44 o 1 -11 1 272.95 266.35 24.80 o 2 -11 1 2744.71 2660.98 98.08 o 3 -11 1 735.98 740.82 53.99 o 4 -11 1 282.30 219.99 38.64 o 5 -11 1 161.76 140.73 34.80 o 6 -11 1 669.41 663.11 56.16 o 7 -11 1 486.48 529.20 53.06 o -11 -10 1 3.96 -1.24 25.70 o -10 -10 1 285.66 338.62 72.63 o -9 -10 1 1496.72 1527.87 59.91 o -8 -10 1 723.60 730.75 58.95 o -7 -10 1 334.63 352.30 50.34 o -6 -10 1 179.57 161.23 37.77 o -5 -10 1 2056.11 2014.09 86.01 o -4 -10 1 4524.47 4528.93 124.40 o -3 -10 1 419.04 401.15 43.28 o -2 -10 1 1053.63 1134.08 57.28 o -1 -10 1 3105.94 3071.69 93.81 o 0 -10 1 1642.78 1562.94 44.05 o 1 -10 1 1907.84 1839.30 48.57 o 2 -10 1 402.91 284.63 36.53 o 3 -10 1 954.09 892.40 56.10 o 4 -10 1 770.42 723.67 52.51 o 5 -10 1 447.16 481.70 45.51 o 6 -10 1 9.21 -12.01 20.25 o 7 -10 1 1144.91 1200.95 74.92 o 8 -10 1 692.55 646.70 59.82 o -12 -9 1 516.39 678.03 74.61 o -11 -9 1 1316.08 1321.69 84.89 o -10 -9 1 137.97 128.26 24.92 o -9 -9 1 573.74 578.30 37.35 o -8 -9 1 1563.51 1594.97 57.01 o -7 -9 1 1608.27 1468.69 76.41 o -6 -9 1 604.38 518.36 46.68 o -5 -9 1 412.12 423.07 42.10 o -4 -9 1 2970.54 2935.84 93.81 o -3 -9 1 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