#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/41/2204196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204196_Fobs loop_ _publ_author_name 'Decken, Andreas' 'Gill, Erin D.' 'Bottomley, Frank' _publ_section_title ; 2-Phenylisophosphindoline-1,3-dione ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1456 _journal_page_last o1457 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.662 _cell_angle_gamma 90.000 _cell_length_a 9.4273 _cell_length_b 14.4792 _cell_length_c 9.4762 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file lh6252Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AD in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 205.98 218.02 3.58 o 4 0 0 1083.67 1199.53 17.31 o 6 0 0 401.20 374.76 7.41 o 8 0 0 316.70 325.12 9.61 o 1 1 0 1021.14 1099.22 52.86 o 2 1 0 61.37 74.41 1.24 o 3 1 0 55.07 57.23 1.46 o 4 1 0 1839.53 1841.31 18.32 o 5 1 0 2024.68 2039.91 20.44 o 6 1 0 140.30 146.17 2.58 o 7 1 0 96.77 90.40 2.16 o 8 1 0 264.02 263.88 4.86 o 9 1 0 29.98 30.54 2.29 o 0 2 0 145.78 137.24 2.96 o 1 2 0 770.26 788.18 10.98 o 2 2 0 11468.18 13394.53 580.50 o 3 2 0 8.13 10.96 0.63 o 4 2 0 47.70 47.50 1.28 o 5 2 0 169.22 148.85 4.63 o 6 2 0 82.15 76.14 1.85 o 7 2 0 11.47 10.75 1.20 o 8 2 0 58.05 55.05 2.54 o 9 2 0 4.91 5.43 1.71 o 1 3 0 150.69 154.32 2.73 o 2 3 0 5007.92 5532.42 55.47 o 3 3 0 832.90 894.51 22.19 o 4 3 0 27.33 22.80 0.96 o 5 3 0 340.60 341.59 4.29 o 6 3 0 62.63 57.77 1.86 o 7 3 0 1289.82 1293.13 16.05 o 8 3 0 104.42 109.20 3.61 o 9 3 0 2.41 3.45 1.56 o 0 4 0 1312.60 1355.26 17.57 o 1 4 0 5.03 3.90 0.33 o 2 4 0 3447.58 3737.74 42.98 o 3 4 0 3873.86 4127.74 39.33 o 4 4 0 329.91 361.77 15.98 o 5 4 0 4.82 3.11 0.78 o 6 4 0 163.21 144.19 6.36 o 7 4 0 46.80 46.87 2.35 o 8 4 0 8.42 7.07 1.52 o 9 4 0 28.83 32.23 2.47 o 1 5 0 1269.89 1393.03 10.84 o 2 5 0 1696.56 1661.34 22.35 o 3 5 0 15.39 15.06 0.63 o 4 5 0 41.86 47.04 1.20 o 5 5 0 109.42 133.32 8.77 o 6 5 0 20.29 17.40 2.56 o 7 5 0 15.45 20.08 1.82 o 8 5 0 433.14 420.50 8.27 o 9 5 0 4.24 1.35 1.58 o 0 6 0 3138.02 3290.00 35.00 o 1 6 0 1.18 1.12 0.30 o 2 6 0 8.91 9.79 0.61 o 3 6 0 395.37 374.69 5.33 o 4 6 0 94.68 91.77 1.97 o 5 6 0 59.49 57.00 2.21 o 6 6 0 261.07 251.59 15.13 o 7 6 0 74.64 68.24 6.69 o 8 6 0 210.58 219.62 14.52 o 9 6 0 12.20 12.53 1.99 o 1 7 0 174.92 158.47 1.71 o 2 7 0 1572.62 1804.56 17.50 o 3 7 0 76.53 81.87 2.48 o 4 7 0 1547.74 1577.08 18.20 o 5 7 0 90.78 86.01 2.13 o 6 7 0 644.69 664.64 32.13 o 7 7 0 93.25 97.22 8.33 o 8 7 0 114.47 121.80 5.68 o 0 8 0 202.19 191.20 2.81 o 1 8 0 1173.07 1251.58 10.15 o 2 8 0 938.03 1024.85 9.18 o 3 8 0 1213.40 1212.96 12.51 o 4 8 0 164.81 166.90 2.93 o 5 8 0 199.10 200.15 5.92 o 6 8 0 345.34 323.33 6.35 o 7 8 0 0.23 0.00 1.12 o 8 8 0 27.72 29.44 2.95 o 1 9 0 513.71 490.47 4.38 o 2 9 0 348.24 378.75 4.41 o 3 9 0 31.82 35.49 1.33 o 4 9 0 1990.04 1890.96 36.70 o 5 9 0 422.26 425.10 6.07 o 6 9 0 41.70 36.00 2.07 o 7 9 0 354.91 383.55 14.93 o 8 9 0 0.01 0.00 1.33 o 0 10 0 625.55 624.93 6.74 o 1 10 0 121.35 130.32 1.55 o 2 10 0 28.70 25.35 1.11 o 3 10 0 265.71 271.07 3.49 o 4 10 0 259.81 267.49 4.17 o 5 10 0 0.03 0.10 0.84 o 6 10 0 85.11 91.45 3.63 o 7 10 0 0.01 0.23 1.22 o 1 11 0 27.36 26.38 1.07 o 2 11 0 647.14 629.50 6.16 o 3 11 0 15.71 19.16 0.99 o 4 11 0 42.25 38.93 1.48 o 5 11 0 16.41 17.77 1.34 o 6 11 0 227.62 208.98 3.96 o 7 11 0 156.25 165.75 5.86 o 0 12 0 1301.54 1284.41 15.20 o 1 12 0 178.53 184.71 2.55 o 2 12 0 190.05 187.60 2.64 o 3 12 0 291.57 287.00 3.79 o 4 12 0 25.74 24.47 1.34 o 5 12 0 0.98 0.00 0.90 o 6 12 0 342.68 341.63 6.75 o 7 12 0 0.25 0.00 1.57 o 1 13 0 242.32 239.22 3.64 o 2 13 0 28.40 33.44 1.17 o 3 13 0 17.64 16.16 1.32 o 4 13 0 384.99 365.54 8.35 o 5 13 0 50.47 50.84 2.16 o 6 13 0 124.60 105.47 2.81 o 0 14 0 871.16 859.30 18.33 o 1 14 0 91.36 86.85 1.95 o 2 14 0 227.73 227.21 3.65 o 3 14 0 38.38 43.74 2.63 o 4 14 0 103.31 103.89 3.30 o 5 14 0 1.23 1.81 1.50 o 1 15 0 0.73 0.11 0.82 o 2 15 0 21.72 23.96 1.74 o 3 15 0 18.27 16.91 1.94 o 4 15 0 8.87 11.97 1.72 o 0 16 0 121.78 124.91 3.99 o 1 16 0 0.04 0.00 1.08 o 2 16 0 0.62 0.00 1.10 o 3 16 0 6.27 7.77 1.78 o 1 17 0 33.75 42.24 4.10 o -9 0 1 79.88 83.17 4.63 o -7 0 1 1.28 0.96 1.03 o -5 0 1 2591.83 2684.96 37.45 o -3 0 1 132.69 154.08 5.49 o -1 0 1 1892.99 1984.55 27.10 o 1 0 1 1610.59 1698.28 23.34 o 3 0 1 136.77 173.41 3.43 o 5 0 1 158.35 140.20 3.44 o 7 0 1 410.36 390.00 7.54 o 9 0 1 50.67 61.77 4.40 o -10 1 1 27.05 25.81 3.21 o -9 1 1 0.91 0.00 1.17 o -8 1 1 0.64 0.00 0.94 o -7 1 1 433.30 423.79 5.46 o -6 1 1 136.31 120.60 3.57 o -5 1 1 227.09 267.61 3.50 o -4 1 1 0.92 0.00 0.54 o -3 1 1 919.69 965.14 9.73 o -2 1 1 698.69 708.63 7.11 o -1 1 1 2702.40 2975.11 33.05 o 0 1 1 718.37 738.41 8.27 o 1 1 1 619.14 613.54 9.42 o 2 1 1 0.41 2.34 0.44 o 3 1 1 260.40 267.40 3.33 o 4 1 1 68.38 61.63 1.48 o 5 1 1 1563.64 1643.38 16.81 o 6 1 1 7.64 9.72 0.99 o 7 1 1 6.23 6.18 1.12 o 8 1 1 43.30 45.46 2.16 o 9 1 1 86.83 87.01 5.06 o -10 2 1 66.35 82.52 4.93 o -9 2 1 308.81 317.64 8.62 o -8 2 1 388.99 380.04 9.22 o -7 2 1 138.97 143.13 3.09 o -6 2 1 619.11 586.82 8.14 o -5 2 1 100.83 124.96 2.10 o -4 2 1 64.24 65.46 2.01 o -3 2 1 326.46 321.31 3.62 o -2 2 1 1537.63 1557.43 27.31 o -1 2 1 6333.89 6610.75 55.17 o 0 2 1 2670.94 2744.42 23.44 o 1 2 1 7472.04 8183.37 90.82 o 2 2 1 375.49 392.73 18.22 o 3 2 1 4.29 3.45 0.59 o 4 2 1 2121.96 2219.64 22.04 o 5 2 1 41.96 43.49 1.63 o 6 2 1 185.54 163.40 2.87 o 7 2 1 334.69 327.57 5.46 o 8 2 1 66.19 59.85 2.89 o 9 2 1 7.80 4.87 1.76 o -10 3 1 109.52 120.08 5.82 o -9 3 1 37.60 34.66 2.49 o -8 3 1 0.90 1.21 1.20 o -7 3 1 193.24 174.02 3.45 o -6 3 1 717.59 661.77 8.68 o -5 3 1 86.35 94.21 1.78 o -4 3 1 459.55 434.30 4.92 o -3 3 1 165.28 188.44 2.66 o -2 3 1 375.17 374.51 6.13 o -1 3 1 2360.26 2384.27 19.72 o 0 3 1 8459.05 9350.10 87.46 o 1 3 1 280.74 312.00 3.29 o 2 3 1 2165.13 2442.26 139.17 o 3 3 1 159.75 156.66 5.08 o 4 3 1 497.94 537.22 6.07 o 5 3 1 129.54 111.84 3.97 o 6 3 1 42.57 44.55 1.81 o 7 3 1 4.73 5.14 1.41 o 8 3 1 62.13 65.92 3.01 o 9 3 1 44.14 48.41 2.99 o -10 4 1 53.33 61.42 4.78 o -9 4 1 1.81 3.24 1.47 o -8 4 1 110.88 119.55 3.68 o -7 4 1 924.70 887.62 14.08 o -6 4 1 14.67 12.53 1.20 o -5 4 1 74.96 60.14 1.70 o -4 4 1 3.95 3.59 0.58 o -3 4 1 60.21 62.16 1.16 o -2 4 1 50.53 54.59 0.90 o -1 4 1 26.39 20.66 0.69 o 0 4 1 1810.25 1931.70 16.32 o 1 4 1 1069.08 1073.91 9.28 o 2 4 1 96.35 105.64 2.42 o 3 4 1 1.09 1.19 0.35 o 4 4 1 474.42 480.17 12.16 o 5 4 1 4.99 4.15 1.07 o 6 4 1 26.16 27.83 1.92 o 7 4 1 3.28 1.74 1.24 o 8 4 1 29.65 31.26 2.36 o 9 4 1 0.37 0.00 1.69 o -9 5 1 47.48 54.17 3.29 o -8 5 1 0.09 0.00 1.17 o -7 5 1 0.07 0.32 1.71 o -6 5 1 75.92 78.57 2.58 o -5 5 1 59.88 55.53 1.61 o -4 5 1 1419.00 1495.59 26.92 o -3 5 1 3561.84 3892.41 63.86 o -2 5 1 0.25 0.24 0.26 o -1 5 1 36.26 38.14 0.89 o 0 5 1 245.74 254.32 2.94 o 1 5 1 901.97 1018.41 8.92 o 2 5 1 2453.00 2690.48 20.86 o 3 5 1 0.11 1.44 0.36 o 4 5 1 47.90 40.96 3.75 o 5 5 1 281.17 285.20 25.30 o 6 5 1 265.29 264.68 12.54 o 7 5 1 52.05 43.02 2.46 o 8 5 1 76.06 81.07 3.33 o -9 6 1 39.97 47.90 2.84 o -8 6 1 19.99 22.87 2.31 o -7 6 1 679.58 683.62 34.29 o -6 6 1 20.40 18.16 1.53 o -5 6 1 1038.64 976.25 14.61 o -4 6 1 387.10 375.77 5.07 o -3 6 1 1589.08 1708.98 16.77 o -2 6 1 558.75 574.77 4.93 o -1 6 1 0.22 4.55 1.13 o 0 6 1 533.73 550.60 4.65 o 1 6 1 1085.95 1111.17 9.76 o 2 6 1 15.55 7.30 0.88 o 3 6 1 2104.22 2185.65 36.35 o 4 6 1 134.08 161.77 8.19 o 5 6 1 465.46 446.54 10.85 o 6 6 1 58.85 48.25 2.37 o 7 6 1 0.89 0.00 1.16 o 8 6 1 6.97 6.34 1.70 o -9 7 1 14.42 18.33 2.09 o -8 7 1 155.98 149.01 5.54 o -7 7 1 4.96 1.91 1.19 o -6 7 1 31.37 32.45 1.86 o -5 7 1 98.12 93.56 2.13 o -4 7 1 443.85 422.48 5.65 o -3 7 1 801.08 905.60 10.69 o -2 7 1 3.00 3.32 0.53 o -1 7 1 40.98 28.70 0.91 o 0 7 1 583.89 593.87 5.05 o 1 7 1 25.04 32.63 0.84 o 2 7 1 1005.81 991.50 12.54 o 3 7 1 90.73 84.41 1.55 o 4 7 1 33.78 37.83 1.52 o 5 7 1 2.27 1.76 1.45 o 6 7 1 220.22 219.09 4.99 o 7 7 1 1.65 1.87 1.40 o 8 7 1 280.54 291.91 21.41 o -8 8 1 160.72 161.96 10.57 o -7 8 1 485.08 500.80 22.46 o -6 8 1 23.31 28.23 1.78 o -5 8 1 134.35 116.81 2.46 o -4 8 1 125.68 120.40 2.35 o -3 8 1 66.72 70.42 1.41 o -2 8 1 351.81 319.75 3.41 o -1 8 1 38.44 37.65 1.03 o 0 8 1 83.04 80.34 1.31 o 1 8 1 110.87 131.49 1.61 o 2 8 1 0.18 0.00 0.51 o 3 8 1 18.78 13.71 0.97 o 4 8 1 527.69 514.13 6.85 o 5 8 1 0.05 0.00 1.01 o 6 8 1 6.22 7.26 1.46 o 7 8 1 60.42 52.81 2.73 o -8 9 1 31.39 35.79 2.36 o -7 9 1 108.69 99.47 3.22 o -6 9 1 16.81 16.02 1.50 o -5 9 1 43.85 44.78 1.60 o -4 9 1 233.08 220.95 4.30 o -3 9 1 333.80 357.25 3.79 o -2 9 1 37.53 44.05 0.99 o -1 9 1 42.90 45.26 1.64 o 0 9 1 537.51 512.21 5.67 o 1 9 1 61.68 59.98 1.07 o 2 9 1 252.85 222.76 2.94 o 3 9 1 384.42 385.44 5.33 o 4 9 1 4.31 2.38 0.82 o 5 9 1 56.29 48.61 2.22 o 6 9 1 8.03 9.55 1.56 o 7 9 1 9.63 7.77 1.70 o -8 10 1 46.36 54.37 2.82 o -7 10 1 12.21 10.19 1.59 o -6 10 1 178.66 168.80 3.34 o -5 10 1 369.20 358.81 5.34 o -4 10 1 12.51 12.20 0.89 o -3 10 1 526.07 504.46 5.08 o -2 10 1 100.51 82.99 1.39 o -1 10 1 63.41 57.37 1.14 o 0 10 1 21.70 22.38 1.04 o 1 10 1 660.02 663.59 5.82 o 2 10 1 61.86 59.27 1.39 o 3 10 1 118.50 115.25 2.39 o 4 10 1 303.84 292.85 5.83 o 5 10 1 57.56 48.67 1.81 o 6 10 1 47.93 52.31 2.85 o 7 10 1 268.55 289.37 6.48 o -7 11 1 183.59 193.18 4.75 o -6 11 1 0.22 0.00 0.92 o -5 11 1 402.05 380.71 5.63 o -4 11 1 67.14 68.92 1.62 o -3 11 1 645.12 642.65 6.31 o -2 11 1 0.18 0.00 0.50 o -1 11 1 106.28 100.87 1.59 o 0 11 1 4.53 3.50 0.65 o 1 11 1 27.23 25.62 0.90 o 2 11 1 0.09 0.00 0.79 o 3 11 1 650.26 660.55 8.48 o 4 11 1 15.71 14.46 1.19 o 5 11 1 476.73 449.52 8.03 o 6 11 1 14.49 12.78 1.71 o -7 12 1 136.10 134.17 3.89 o -6 12 1 15.91 19.19 1.45 o -5 12 1 240.46 246.98 6.10 o -4 12 1 73.28 73.70 2.13 o -3 12 1 0.06 0.00 0.66 o -2 12 1 980.58 996.85 9.32 o -1 12 1 209.78 214.54 2.52 o 0 12 1 241.83 260.71 3.25 o 1 12 1 674.80 655.98 7.38 o 2 12 1 24.31 26.70 2.25 o 3 12 1 68.41 72.63 2.14 o 4 12 1 4.05 5.33 0.99 o 5 12 1 67.29 62.91 2.13 o 6 12 1 0.46 0.18 1.76 o -6 13 1 27.39 26.52 1.63 o -5 13 1 33.91 37.71 3.30 o -4 13 1 18.25 24.37 3.21 o -3 13 1 11.13 8.63 1.06 o -2 13 1 86.98 88.79 1.80 o -1 13 1 229.63 218.23 2.46 o 0 13 1 15.88 16.43 0.95 o 1 13 1 134.42 139.10 2.27 o 2 13 1 220.72 217.84 5.84 o 3 13 1 57.35 53.78 2.55 o 4 13 1 53.70 50.79 1.92 o 5 13 1 158.65 165.37 3.47 o -6 14 1 6.31 8.11 2.47 o -5 14 1 51.94 52.09 2.75 o -4 14 1 154.66 162.18 5.75 o -3 14 1 1.28 0.30 0.77 o -2 14 1 697.53 701.35 6.62 o -1 14 1 232.61 231.09 3.34 o 0 14 1 354.66 335.64 4.66 o 1 14 1 155.69 153.44 2.95 o 3 14 1 4.98 4.14 1.35 o 4 14 1 79.07 93.67 4.77 o 5 14 1 20.83 24.51 1.99 o -5 15 1 0.87 0.00 1.23 o -4 15 1 25.09 29.30 1.80 o -3 15 1 4.66 5.76 1.37 o -2 15 1 1.79 0.30 0.85 o -1 15 1 115.60 118.90 2.81 o 0 15 1 321.13 327.11 4.29 o 1 15 1 1.83 3.95 1.47 o 2 15 1 0.06 0.00 1.30 o 3 15 1 85.56 84.94 4.53 o 4 15 1 11.16 14.14 2.83 o -4 16 1 35.33 26.57 3.28 o -3 16 1 17.17 14.00 1.57 o -2 16 1 0.07 0.00 0.88 o -1 16 1 147.69 145.32 2.74 o 0 16 1 9.24 9.27 1.26 o 1 16 1 11.88 14.17 2.42 o 2 16 1 4.06 2.52 2.27 o -1 17 1 0.01 0.00 1.94 o 0 17 1 10.87 11.09 2.66 o -10 0 2 156.17 148.96 6.27 o -8 0 2 240.35 212.53 6.85 o -6 0 2 15.85 22.19 1.53 o -4 0 2 12772.69 14192.56 191.32 o -2 0 2 4966.60 5054.20 55.93 o 0 0 2 10606.12 11699.99 177.10 o 2 0 2 408.65 453.40 7.15 o 4 0 2 2055.87 2201.66 31.20 o 6 0 2 241.15 231.24 5.22 o 8 0 2 131.60 136.99 5.99 o -10 1 2 27.37 16.99 1.92 o -9 1 2 395.81 399.46 14.79 o -8 1 2 25.72 34.11 1.70 o -7 1 2 69.59 67.51 1.75 o -6 1 2 79.84 57.88 1.50 o -5 1 2 388.54 359.20 4.33 o -4 1 2 18.80 15.49 0.73 o -3 1 2 245.54 252.21 2.97 o -2 1 2 317.83 324.10 3.07 o -1 1 2 6047.71 6456.81 83.63 o 0 1 2 6875.84 7379.76 88.13 o 1 1 2 3350.89 3693.13 139.81 o 2 1 2 194.36 226.43 2.60 o 3 1 2 217.28 195.00 2.78 o 4 1 2 22.26 17.77 0.99 o 5 1 2 124.64 132.05 2.50 o 6 1 2 408.41 400.95 5.36 o 7 1 2 12.84 12.27 1.43 o 8 1 2 59.14 59.16 3.05 o -10 2 2 30.55 28.91 3.19 o -9 2 2 254.07 249.27 6.06 o -8 2 2 29.28 31.81 1.70 o -7 2 2 213.04 185.18 3.99 o -6 2 2 610.38 611.99 6.95 o -5 2 2 313.47 295.73 6.93 o -4 2 2 519.20 570.35 6.18 o -3 2 2 963.29 973.74 9.81 o -2 2 2 1786.03 1760.49 13.56 o -1 2 2 1474.30 1508.28 13.18 o 0 2 2 10309.53 11300.35 95.48 o 1 2 2 871.38 941.86 8.37 o 2 2 2 1184.40 1319.57 11.49 o 3 2 2 1.11 0.77 0.55 o 4 2 2 750.33 806.03 8.81 o 5 2 2 889.29 912.93 10.06 o 6 2 2 208.18 208.49 3.99 o 7 2 2 104.96 86.64 3.35 o 8 2 2 54.11 56.02 2.97 o -10 3 2 32.52 36.98 3.49 o -9 3 2 0.90 0.60 1.27 o -8 3 2 82.33 70.45 2.44 o -7 3 2 176.46 171.85 3.34 o -6 3 2 16.95 20.18 1.18 o -5 3 2 124.70 108.03 1.87 o -4 3 2 1583.76 1675.42 16.65 o -3 3 2 917.40 923.51 13.39 o -2 3 2 18.54 18.79 0.97 o -1 3 2 36.82 41.86 0.72 o 0 3 2 451.08 440.14 4.63 o 1 3 2 1780.88 1919.17 17.21 o 2 3 2 1266.32 1639.78 108.97 o 3 3 2 1517.94 1673.36 71.25 o 4 3 2 15.91 11.62 0.89 o 5 3 2 37.46 35.53 2.11 o 6 3 2 18.47 21.61 3.41 o 7 3 2 5.72 4.04 1.48 o 8 3 2 0.01 0.00 1.27 o -10 4 2 22.88 22.60 2.30 o -9 4 2 61.77 63.09 2.89 o -8 4 2 308.82 274.11 5.87 o -7 4 2 812.41 797.66 10.78 o -6 4 2 468.88 460.18 8.90 o -5 4 2 57.79 63.74 1.67 o -4 4 2 10.73 21.67 0.83 o -3 4 2 60.89 58.73 1.56 o -2 4 2 226.57 235.38 2.00 o -1 4 2 666.43 617.43 5.01 o 0 4 2 375.71 362.15 3.51 o 1 4 2 475.00 492.62 4.66 o 2 4 2 1207.89 1189.55 12.05 o 3 4 2 11.25 6.95 0.92 o 4 4 2 14.69 21.67 1.89 o 5 4 2 436.10 437.98 7.82 o 6 4 2 38.84 40.13 2.36 o 7 4 2 125.80 125.02 3.98 o 8 4 2 37.66 39.82 2.79 o -10 5 2 0.21 0.00 1.51 o -9 5 2 236.32 236.65 8.65 o -8 5 2 17.72 17.55 1.76 o -7 5 2 207.20 202.01 4.62 o -6 5 2 99.57 83.39 2.13 o -5 5 2 40.65 40.68 1.39 o -4 5 2 99.33 120.94 2.22 o -3 5 2 92.99 88.93 1.32 o -2 5 2 6753.32 7390.81 58.44 o -1 5 2 208.01 216.78 2.15 o 0 5 2 77.26 68.13 2.95 o 1 5 2 887.30 975.70 9.78 o 2 5 2 31.77 26.96 0.89 o 3 5 2 175.19 212.14 6.20 o 4 5 2 472.98 471.05 11.30 o 5 5 2 40.20 41.23 4.22 o 6 5 2 589.63 575.70 14.79 o 7 5 2 17.26 16.85 1.99 o 8 5 2 15.11 13.39 3.12 o -10 6 2 69.49 63.81 4.91 o -9 6 2 10.80 6.39 1.86 o -8 6 2 68.10 68.84 2.78 o -7 6 2 640.74 618.17 10.38 o -6 6 2 766.85 750.13 11.84 o -5 6 2 13.99 15.87 1.24 o -4 6 2 1120.26 1060.17 13.27 o -3 6 2 327.89 346.47 3.53 o -2 6 2 32.95 21.82 1.02 o -1 6 2 1.24 0.36 0.37 o 0 6 2 270.95 301.57 2.83 o 1 6 2 419.53 451.35 5.68 o 2 6 2 18.73 33.56 1.23 o 3 6 2 192.66 199.53 3.22 o 4 6 2 195.79 186.90 5.81 o 5 6 2 34.84 32.16 3.79 o 6 6 2 506.61 525.87 13.30 o 7 6 2 5.78 2.80 1.85 o 8 6 2 120.92 130.70 4.38 o -9 7 2 63.93 68.86 3.02 o -8 7 2 111.65 124.99 3.74 o -7 7 2 186.01 191.71 8.82 o -6 7 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304.14 3.36 o -1 9 2 143.86 127.99 1.71 o 0 9 2 1935.75 1982.25 22.50 o 1 9 2 163.66 149.55 2.27 o 2 9 2 278.17 267.92 4.03 o 3 9 2 1402.19 1432.12 23.89 o 4 9 2 36.21 33.10 1.93 o 5 9 2 9.31 6.03 1.34 o 6 9 2 33.01 34.42 4.32 o -8 10 2 57.40 59.50 2.77 o -7 10 2 312.50 328.82 6.53 o -6 10 2 23.96 24.98 1.85 o -5 10 2 52.00 47.07 1.61 o -4 10 2 493.92 470.32 6.29 o -3 10 2 29.58 31.30 1.25 o -2 10 2 20.28 28.21 0.86 o -1 10 2 39.24 31.02 1.01 o 0 10 2 1.17 0.60 0.57 o 1 10 2 41.49 36.10 1.19 o 2 10 2 641.23 636.87 8.12 o 3 10 2 12.41 16.55 1.19 o 4 10 2 147.05 143.26 3.64 o 5 10 2 34.47 34.13 2.70 o 6 10 2 0.01 0.48 1.39 o -8 11 2 50.48 53.81 3.56 o -7 11 2 28.12 30.05 2.06 o -6 11 2 41.98 40.71 2.20 o -5 11 2 187.85 183.01 3.32 o -4 11 2 152.94 148.61 2.80 o -3 11 2 17.98 17.62 0.98 o -2 11 2 1115.46 1060.26 9.60 o -1 11 2 166.46 153.73 3.37 o 0 11 2 160.52 141.47 2.41 o 1 11 2 20.21 20.94 1.01 o 2 11 2 451.95 446.17 6.12 o 3 11 2 18.99 16.53 1.21 o 4 11 2 1.48 3.05 1.15 o 5 11 2 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