#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/42/2204206.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204206_Fobs loop_ _publ_author_name 'Kostochka, Mickael L.' 'Lezina, Valentina P.' 'Stash, Adam I.' 'Vatsadze, Sergey Z.' 'Zyk, Nikolay V.' _publ_section_title ; 4a-Hydroxy-2,3,8a-trimethyl-6-oxo-8-phenylperhydroisoquinolinium chloride ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1472 _journal_page_last o1473 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.870 _cell_angle_gamma 90.000 _cell_length_a 15.1490 _cell_length_b 9.3390 _cell_length_c 12.2270 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file ob6389Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' VS01 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8088.97 8689.29 318.00 o 3 0 0 8076.47 7993.53 405.25 o 4 0 0 1507.07 1395.85 33.40 o 5 0 0 2924.19 2750.83 37.62 o 6 0 0 9876.13 9270.44 227.59 o 7 0 0 1803.93 1721.55 61.19 o 8 0 0 2706.80 3061.34 40.38 o 9 0 0 240.64 236.87 11.66 o 10 0 0 117.47 105.76 5.38 o 11 0 0 945.87 908.93 19.09 o 12 0 0 220.59 218.76 3.38 o 13 0 0 4.90 3.71 10.49 o 14 0 0 648.13 607.35 8.54 o 15 0 0 7.34 5.27 14.93 o 16 0 0 21.35 13.95 6.08 o 17 0 0 1.55 3.28 9.10 o 1 1 0 754.06 829.96 19.29 o 2 1 0 798.64 884.72 19.74 o 3 1 0 2007.32 2069.74 85.55 o 4 1 0 351.53 345.44 8.90 o 5 1 0 873.76 814.09 18.83 o 6 1 0 455.73 488.11 17.59 o 7 1 0 476.78 554.08 10.64 o 8 1 0 427.79 438.02 8.54 o 9 1 0 111.47 109.12 2.26 o 10 1 0 6.15 12.21 5.48 o 11 1 0 5.97 1.86 5.28 o 12 1 0 58.92 58.64 1.48 o 13 1 0 132.80 127.20 1.92 o 14 1 0 49.98 45.83 1.46 o 15 1 0 3.62 6.82 6.40 o 16 1 0 123.11 116.20 2.90 o 17 1 0 25.14 24.75 1.79 o 0 2 0 2060.77 1877.19 40.79 o 1 2 0 3549.02 3655.93 119.31 o 2 2 0 3025.15 3059.53 89.28 o 3 2 0 456.29 479.07 10.34 o 4 2 0 5.43 5.37 1.21 o 5 2 0 544.85 549.76 12.04 o 6 2 0 136.63 138.21 2.83 o 7 2 0 4.55 1.29 3.64 o 8 2 0 8.29 13.10 3.47 o 9 2 0 45.66 51.07 1.35 o 10 2 0 15.01 18.43 1.51 o 11 2 0 484.47 469.14 8.10 o 12 2 0 70.31 77.11 2.73 o 13 2 0 191.59 178.97 3.12 o 14 2 0 68.44 72.30 1.64 o 15 2 0 9.53 14.69 3.63 o 16 2 0 24.44 25.47 1.30 o 1 3 0 330.38 300.54 8.23 o 2 3 0 146.64 152.71 3.81 o 3 3 0 2546.01 2515.04 33.91 o 4 3 0 874.34 893.94 19.38 o 5 3 0 263.32 312.68 6.64 o 6 3 0 236.06 235.86 4.79 o 7 3 0 448.03 420.88 9.30 o 8 3 0 894.57 943.73 34.74 o 9 3 0 102.31 97.84 2.64 o 10 3 0 313.03 330.40 5.63 o 11 3 0 374.80 388.07 6.33 o 12 3 0 317.27 284.72 11.35 o 13 3 0 9.87 13.62 3.94 o 14 3 0 20.23 21.57 1.19 o 15 3 0 265.41 298.42 4.97 o 16 3 0 22.21 29.42 1.35 o 0 4 0 171.01 185.12 5.87 o 1 4 0 1329.27 1316.51 23.41 o 2 4 0 637.88 649.05 11.65 o 3 4 0 87.80 88.27 1.87 o 4 4 0 2175.44 2418.95 96.85 o 5 4 0 157.77 195.29 7.15 o 6 4 0 5.95 7.52 4.22 o 7 4 0 47.11 46.71 1.33 o 8 4 0 82.87 77.00 2.14 o 9 4 0 415.08 414.92 7.63 o 10 4 0 54.57 58.84 1.49 o 11 4 0 713.21 729.34 17.66 o 12 4 0 1.07 3.07 8.47 o 13 4 0 39.42 40.71 1.39 o 14 4 0 4.00 4.06 6.50 o 15 4 0 17.08 18.82 3.33 o 16 4 0 22.76 10.95 7.34 o 1 5 0 1925.09 1878.41 31.65 o 2 5 0 43.98 60.24 1.44 o 3 5 0 44.39 37.45 2.96 o 4 5 0 111.31 118.40 2.92 o 5 5 0 678.60 711.25 25.87 o 6 5 0 172.23 151.79 2.78 o 7 5 0 28.26 29.41 1.19 o 8 5 0 110.16 106.77 1.77 o 9 5 0 384.29 391.19 10.76 o 10 5 0 8.06 11.14 5.87 o 11 5 0 193.24 191.28 3.50 o 12 5 0 0.09 1.25 1.39 o 13 5 0 61.46 66.99 1.61 o 14 5 0 1.75 9.23 6.38 o 15 5 0 62.59 61.98 2.54 o 0 6 0 97.93 123.11 3.47 o 1 6 0 2.77 3.04 4.68 o 2 6 0 0.05 3.77 4.61 o 3 6 0 582.57 621.63 11.40 o 4 6 0 180.98 175.27 5.91 o 5 6 0 95.36 92.28 2.04 o 6 6 0 65.28 76.21 2.43 o 7 6 0 0.86 1.91 5.40 o 8 6 0 687.23 683.11 11.89 o 9 6 0 62.37 50.89 1.43 o 10 6 0 335.36 347.95 7.69 o 11 6 0 45.56 46.19 2.38 o 12 6 0 12.65 13.29 1.19 o 13 6 0 210.00 225.66 11.49 o 14 6 0 0.05 2.23 6.31 o 1 7 0 176.43 170.94 2.81 o 2 7 0 200.52 193.64 3.30 o 3 7 0 74.92 81.80 2.03 o 4 7 0 0.84 1.84 5.21 o 5 7 0 8.11 11.15 1.42 o 6 7 0 93.94 101.85 1.77 o 7 7 0 4.31 4.91 7.34 o 8 7 0 1.32 4.42 7.46 o 9 7 0 0.75 2.12 6.00 o 10 7 0 83.84 81.44 1.71 o 11 7 0 41.07 39.31 1.39 o 12 7 0 223.07 225.06 2.94 o 13 7 0 9.00 11.06 6.72 o 0 8 0 1050.17 1015.41 20.42 o 1 8 0 9.01 9.28 5.65 o 2 8 0 1130.93 1131.82 32.28 o 3 8 0 181.35 176.30 2.62 o 4 8 0 195.44 178.87 2.63 o 5 8 0 99.79 105.60 2.15 o 6 8 0 66.26 49.64 1.43 o 7 8 0 32.27 27.05 1.25 o 8 8 0 355.16 346.17 4.70 o 9 8 0 85.41 81.35 2.57 o 10 8 0 5.99 10.34 6.44 o 11 8 0 15.01 11.62 6.79 o 1 9 0 370.13 375.42 5.38 o 2 9 0 334.72 322.42 5.73 o 3 9 0 245.27 246.18 3.51 o 4 9 0 5.12 5.82 6.27 o 5 9 0 18.96 21.86 1.70 o 6 9 0 69.28 85.07 2.11 o 7 9 0 94.73 86.03 1.76 o 8 9 0 213.42 233.98 3.79 o 9 9 0 6.40 2.63 7.44 o 10 9 0 52.35 52.67 1.56 o 0 10 0 11.77 2.88 11.46 o 1 10 0 0.43 3.89 6.41 o 2 10 0 104.83 98.25 2.12 o 3 10 0 234.29 253.63 5.88 o 4 10 0 169.82 172.85 2.34 o 5 10 0 74.38 84.64 1.89 o 6 10 0 12.91 16.05 3.82 o 7 10 0 74.68 76.42 1.72 o 1 11 0 61.26 57.05 1.61 o 2 11 0 33.90 32.68 8.69 o -17 1 1 138.49 163.71 3.25 o -16 1 1 132.63 123.33 2.90 o -15 1 1 2.17 16.26 9.92 o -14 1 1 11.37 2.12 8.47 o -13 1 1 16.28 6.15 7.83 o -12 1 1 15.55 20.41 1.59 o -11 1 1 275.05 277.33 6.27 o -10 1 1 89.45 78.56 2.20 o -9 1 1 75.29 86.26 2.24 o -8 1 1 169.79 133.97 3.51 o -7 1 1 284.79 345.92 12.05 o -6 1 1 4741.42 4581.93 61.37 o -5 1 1 1270.22 1278.91 32.98 o -4 1 1 2069.64 1945.75 41.06 o -3 1 1 611.33 628.95 23.66 o -2 1 1 9236.29 9157.80 456.20 o -1 1 1 89.14 64.09 3.12 o 0 1 1 4068.00 4079.23 223.73 o 1 1 1 272.34 199.10 9.76 o 2 1 1 777.72 803.01 26.94 o 3 1 1 1597.44 1551.40 36.86 o 4 1 1 2560.99 2497.33 45.82 o 5 1 1 2415.69 2421.16 44.54 o 6 1 1 9965.88 9086.98 311.71 o 7 1 1 27.60 26.59 1.57 o 8 1 1 2600.22 2622.04 45.40 o 9 1 1 671.49 700.08 16.94 o 10 1 1 35.87 35.10 1.77 o 11 1 1 0.87 1.86 7.50 o 12 1 1 135.67 149.65 2.92 o 13 1 1 76.29 69.43 2.30 o 14 1 1 19.28 2.34 9.34 o 15 1 1 29.63 31.14 1.88 o 16 1 1 0.10 4.28 17.13 o -17 2 1 39.58 56.56 2.22 o -16 2 1 0.21 9.08 9.04 o -15 2 1 106.91 107.20 2.66 o -14 2 1 77.25 72.05 2.36 o -13 2 1 1032.28 1013.30 20.28 o -12 2 1 10.89 1.98 7.95 o -11 2 1 182.70 171.21 3.99 o -10 2 1 347.25 372.57 8.77 o -9 2 1 1657.94 1745.69 37.21 o -8 2 1 27.81 31.93 1.61 o -7 2 1 108.60 95.15 2.90 o -6 2 1 548.52 567.03 15.25 o -5 2 1 8.46 3.47 6.56 o -4 2 1 1384.92 1383.01 34.27 o -3 2 1 551.82 593.43 16.26 o -2 2 1 16009.53 16164.70 624.91 o -1 2 1 181.15 155.39 5.66 o 0 2 1 0.63 1.51 6.05 o 1 2 1 1095.53 1043.88 30.36 o 2 2 1 155.79 165.59 6.51 o 3 2 1 101.19 112.43 4.07 o 4 2 1 426.18 460.01 14.14 o 5 2 1 671.34 694.55 17.01 o 6 2 1 331.03 311.34 9.41 o 7 2 1 0.57 1.31 5.27 o 8 2 1 294.38 296.68 9.21 o 9 2 1 30.83 28.64 1.65 o 10 2 1 472.93 460.35 11.23 o 11 2 1 89.07 77.55 2.26 o 12 2 1 66.55 69.79 2.22 o 13 2 1 4.97 7.06 8.45 o 14 2 1 0.83 3.33 13.31 o 15 2 1 15.67 8.73 10.07 o 16 2 1 45.11 45.79 2.12 o -16 3 1 50.59 59.91 2.24 o -15 3 1 0.04 2.10 8.43 o -14 3 1 110.90 119.38 2.76 o -13 3 1 115.26 116.72 2.66 o -12 3 1 78.27 70.92 2.26 o -11 3 1 20.95 17.07 1.63 o -10 3 1 531.91 520.92 11.99 o -9 3 1 413.61 403.05 10.64 o -8 3 1 761.27 772.59 17.70 o -7 3 1 1.64 3.33 5.59 o -6 3 1 129.06 132.61 3.47 o -5 3 1 185.45 188.04 5.77 o -4 3 1 27.05 31.39 1.55 o -3 3 1 4370.52 4353.16 154.09 o -2 3 1 73.32 79.80 2.80 o -1 3 1 29.86 33.16 1.63 o 0 3 1 295.33 323.56 12.13 o 1 3 1 13.54 13.74 1.35 o 2 3 1 1953.65 1986.95 40.96 o 3 3 1 1217.78 1166.71 31.36 o 4 3 1 74.16 66.78 2.20 o 5 3 1 684.10 704.91 16.83 o 6 3 1 437.19 400.73 12.96 o 7 3 1 194.35 196.31 5.30 o 8 3 1 23.64 26.59 1.57 o 9 3 1 121.18 120.04 2.92 o 10 3 1 244.82 286.40 7.04 o 11 3 1 4.87 2.02 8.11 o 12 3 1 3.03 5.37 8.13 o 13 3 1 5.82 9.06 1.49 o 14 3 1 31.70 29.81 1.86 o 15 3 1 0.71 7.08 10.65 o 16 3 1 19.29 22.27 9.62 o -16 4 1 0.45 2.22 8.90 o -15 4 1 9.28 6.13 8.98 o -14 4 1 66.26 60.61 2.22 o -13 4 1 12.07 11.84 1.59 o -12 4 1 733.07 774.76 17.71 o -11 4 1 111.31 110.02 2.66 o -10 4 1 1244.12 1229.33 21.98 o -9 4 1 469.27 428.38 11.00 o -8 4 1 49.82 45.81 1.86 o -7 4 1 618.59 592.89 15.55 o -6 4 1 0.40 5.12 5.22 o -5 4 1 251.54 238.63 7.20 o -3 4 1 206.76 204.34 5.95 o -2 4 1 674.35 616.26 15.96 o -1 4 1 0.53 2.38 9.52 o 0 4 1 1624.70 1705.29 37.55 o 1 4 1 14.10 12.10 1.29 o 2 4 1 7174.09 7690.71 227.95 o 3 4 1 2869.96 3090.92 49.42 o 4 4 1 3758.63 3935.95 55.51 o 5 4 1 2070.09 2082.77 40.47 o 6 4 1 8.81 1.51 6.07 o 7 4 1 41.65 39.45 1.75 o 8 4 1 493.28 510.96 11.81 o 9 4 1 1054.54 1080.18 20.64 o 10 4 1 1316.54 1245.87 22.20 o 11 4 1 527.02 532.89 12.21 o 12 4 1 4.56 2.97 1.41 o 13 4 1 22.11 23.68 1.71 o 14 4 1 24.44 27.51 1.84 o 15 4 1 11.30 12.91 9.26 o -15 5 1 11.16 15.75 9.30 o -14 5 1 0.43 6.64 8.45 o -13 5 1 10.26 11.22 1.59 o -12 5 1 5.24 2.14 8.59 o -11 5 1 194.61 194.34 4.07 o -10 5 1 408.75 410.90 8.37 o -9 5 1 6.94 8.90 1.43 o -8 5 1 41.53 35.48 1.78 o -7 5 1 184.67 205.80 5.48 o -6 5 1 1.47 13.92 7.16 o -5 5 1 173.18 180.62 4.48 o -4 5 1 312.95 339.30 9.66 o -3 5 1 270.33 272.88 7.62 o -2 5 1 10.20 3.49 6.27 o -1 5 1 331.64 371.41 10.20 o 0 5 1 162.69 179.84 5.18 o 1 5 1 1235.17 1245.69 31.85 o 2 5 1 2088.52 2144.29 41.13 o 3 5 1 1962.77 2088.68 40.70 o 4 5 1 99.35 108.24 2.48 o 5 5 1 12.36 12.89 1.39 o 6 5 1 38.13 47.42 1.88 o 7 5 1 731.28 759.19 17.57 o 8 5 1 44.40 45.75 1.96 o 9 5 1 19.88 12.00 8.35 o 10 5 1 145.56 148.68 3.37 o 11 5 1 52.04 52.85 2.08 o 12 5 1 26.21 33.83 1.92 o 13 5 1 58.72 54.99 2.16 o 14 5 1 8.00 2.30 9.20 o -14 6 1 7.18 9.42 1.59 o -13 6 1 4.74 2.22 8.84 o -12 6 1 33.42 35.24 1.90 o -11 6 1 417.07 423.66 8.47 o -10 6 1 0.42 2.10 8.45 o -9 6 1 705.02 729.94 17.11 o -8 6 1 1.66 1.84 1.35 o -7 6 1 604.72 580.48 15.44 o -6 6 1 89.98 81.38 2.30 o -5 6 1 538.82 515.80 14.59 o -4 6 1 792.23 858.75 18.47 o -3 6 1 1175.78 1230.77 31.51 o -2 6 1 23.72 23.92 1.55 o -1 6 1 142.79 144.23 3.83 o 0 6 1 735.49 744.00 17.40 o 1 6 1 48.75 52.50 1.92 o 2 6 1 31.88 23.28 1.51 o 3 6 1 23.53 17.17 1.45 o 4 6 1 51.22 42.10 1.82 o 5 6 1 356.56 383.60 8.93 o 6 6 1 220.22 227.17 5.34 o 7 6 1 406.77 435.52 9.47 o 8 6 1 20.60 23.76 1.65 o 9 6 1 206.96 194.28 4.25 o 10 6 1 244.31 239.72 4.19 o 11 6 1 42.30 43.59 2.02 o 12 6 1 0.04 2.48 9.90 o 13 6 1 12.19 2.62 10.49 o 14 6 1 0.82 11.82 12.77 o -13 7 1 115.71 123.88 2.88 o -12 7 1 57.74 55.27 2.24 o -11 7 1 117.62 113.89 2.76 o -10 7 1 0.11 2.34 9.32 o -9 7 1 32.45 26.71 1.75 o -8 7 1 30.15 32.17 1.82 o -7 7 1 3.57 1.86 7.48 o -6 7 1 529.61 510.42 11.87 o -5 7 1 0.22 5.51 9.97 o -4 7 1 28.20 30.44 1.77 o -3 7 1 19.38 18.64 1.57 o -2 7 1 7.79 5.41 8.35 o -1 7 1 72.76 72.33 2.18 o 0 7 1 13.15 6.46 7.58 o 1 7 1 150.53 136.59 3.31 o 2 7 1 138.89 147.44 3.43 o 3 7 1 114.60 110.74 2.56 o 4 7 1 1.00 1.84 7.40 o 5 7 1 0.37 1.80 7.20 o 6 7 1 2.11 1.94 7.79 o 7 7 1 14.05 13.82 1.53 o 8 7 1 309.21 318.55 6.77 o 9 7 1 0.00 2.24 8.94 o 10 7 1 214.90 229.82 4.56 o 11 7 1 0.01 11.84 12.18 o 12 7 1 0.21 2.30 9.18 o -12 8 1 41.31 39.15 2.04 o -11 8 1 40.20 42.84 2.08 o -10 8 1 87.80 95.55 2.60 o -9 8 1 63.16 59.64 2.24 o -8 8 1 16.25 23.00 1.76 o -7 8 1 22.65 2.26 9.08 o -6 8 1 0.89 2.20 8.82 o -5 8 1 282.48 295.54 6.59 o -4 8 1 336.31 333.27 7.58 o -3 8 1 191.20 186.40 4.09 o -2 8 1 89.74 95.40 2.46 o -1 8 1 447.39 441.15 9.64 o 0 8 1 12.40 14.18 1.55 o 1 8 1 93.59 90.58 2.36 o 2 8 1 0.15 1.84 7.36 o 3 8 1 0.03 2.00 7.99 o 4 8 1 18.03 11.58 1.49 o 5 8 1 58.30 48.61 2.02 o 6 8 1 12.32 16.80 1.59 o 7 8 1 269.32 250.89 5.00 o 8 8 1 530.81 522.32 10.44 o 9 8 1 1.02 2.20 8.80 o 10 8 1 22.46 19.49 9.98 o 11 8 1 37.18 37.36 2.06 o -10 9 1 21.39 26.12 1.84 o -9 9 1 68.32 74.69 2.46 o -8 9 1 138.01 143.30 2.98 o -7 9 1 51.10 51.68 2.10 o -6 9 1 0.97 2.56 10.25 o -5 9 1 15.33 12.99 9.44 o -4 9 1 8.92 9.24 1.49 o -3 9 1 85.18 83.12 2.42 o -2 9 1 12.55 11.30 1.55 o -1 9 1 353.54 359.49 7.98 o 0 9 1 43.68 34.73 1.90 o 1 9 1 70.80 73.98 2.34 o 2 9 1 430.91 429.58 8.47 o 3 9 1 89.10 90.16 2.50 o 4 9 1 155.01 137.46 2.90 o 5 9 1 52.58 57.53 2.18 o 6 9 1 99.34 92.50 2.56 o 7 9 1 129.05 157.62 3.07 o 8 9 1 416.21 454.06 8.93 o 9 9 1 37.07 39.72 2.10 o -7 10 1 2.07 2.22 8.90 o -6 10 1 0.08 4.28 17.11 o -5 10 1 142.97 156.55 3.07 o -4 10 1 13.28 14.24 1.69 o -3 10 1 86.06 85.30 2.52 o -2 10 1 0.07 10.43 11.24 o -1 10 1 75.75 81.89 2.64 o 0 10 1 42.99 39.35 2.00 o 1 10 1 17.70 17.29 9.10 o 2 10 1 0.56 2.24 8.96 o 3 10 1 6.73 2.40 9.64 o 4 10 1 0.08 2.10 8.41 o 5 10 1 0.05 2.86 11.38 o 6 10 1 7.01 8.37 1.57 o 7 10 1 3.40 17.51 13.72 o -2 11 1 20.39 19.08 1.88 o -1 11 1 43.58 47.60 2.24 o 0 11 1 52.03 44.50 2.22 o 1 11 1 13.21 4.98 9.74 o -17 0 2 35.86 37.26 1.90 o -16 0 2 24.76 27.64 1.86 o -15 0 2 220.62 230.86 5.10 o -14 0 2 15.05 19.91 1.63 o -13 0 2 75.86 77.75 2.30 o -12 0 2 399.93 396.99 9.09 o -11 0 2 379.10 357.42 8.67 o -10 0 2 159.97 172.80 4.42 o -9 0 2 1053.29 1054.28 28.96 o -8 0 2 120.04 142.41 3.73 o -7 0 2 126.96 131.31 3.91 o -6 0 2 0.33 3.17 12.67 o -5 0 2 1499.08 1573.12 36.54 o -4 0 2 835.90 979.25 29.17 o -3 0 2 1292.34 1401.39 35.19 o -2 0 2 16199.84 16597.11 618.64 o -1 0 2 7929.35 8716.73 444.69 o 0 0 2 774.81 644.73 24.10 o 1 0 2 5471.64 5241.32 244.82 o 2 0 2 3525.80 3649.01 144.60 o 3 0 2 8347.80 7828.28 299.46 o 4 0 2 5683.31 5502.06 201.29 o 5 0 2 1993.44 2235.08 43.10 o 6 0 2 7549.22 8107.31 235.23 o 8 0 2 60.19 81.00 2.20 o 9 0 2 167.04 142.89 3.63 o 10 0 2 337.77 327.90 8.37 o 11 0 2 395.03 428.84 10.85 o 12 0 2 340.81 397.60 8.19 o 13 0 2 317.88 263.04 4.80 o 14 0 2 5.30 2.14 8.55 o 15 0 2 8.63 11.48 1.59 o 16 0 2 6.77 8.31 9.08 o -17 1 2 1.74 2.42 9.70 o -16 1 2 13.28 11.82 1.61 o -15 1 2 26.19 20.84 1.73 o -14 1 2 91.16 87.60 2.46 o -13 1 2 8.21 9.84 1.49 o -12 1 2 3.26 1.94 7.77 o -11 1 2 54.96 50.73 1.94 o -10 1 2 57.19 44.31 1.86 o -9 1 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