#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204212.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204212_Fobs loop_ _publ_author_name 'Gao, Fei' 'Meng, Bian-Hong' 'Zhu, Miao-Li' _publ_section_title ; An Na--O--Zn--O--Zn bridging complex of Cl-HXTA, where Cl-HXTA is 2,6-bis{[bis(carboxylatomethyl)amino]methyl}-4-chlorophenolate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1225 _journal_page_last m1227 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.781 _cell_angle_beta 109.593 _cell_angle_gamma 103.043 _cell_length_a 10.2810 _cell_length_b 11.7333 _cell_length_c 13.9745 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file ob6403Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' M01 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15907.97 16927.84 330.08 o 2 0 0 603.69 741.38 31.81 o 3 0 0 1975.26 1909.23 54.95 o 4 0 0 4651.59 4642.02 255.83 o 5 0 0 19.89 19.94 25.14 o 6 0 0 930.71 687.63 137.39 o 7 0 0 21.63 106.49 89.38 o 8 0 0 65.68 191.17 84.48 o 9 0 0 727.88 730.48 140.43 o 10 0 0 599.33 685.19 145.22 o 11 0 0 7.70 313.75 103.86 o -11 1 0 17.26 128.02 106.69 o -10 1 0 0.46 161.12 86.66 o -9 1 0 8.56 211.63 90.79 o -8 1 0 625.65 738.75 126.72 o -7 1 0 461.49 435.30 58.12 o -6 1 0 279.67 362.82 127.48 o -5 1 0 11382.94 12928.16 308.85 o -4 1 0 6234.59 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