#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204263.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204263_Fobs loop_ _publ_author_name 'Vencato, Ivo' 'Lariucci, Carlito' 'Ferreira, Katiuscia D.' 'Santana, Ricardo C.' 'Carvalho, Jesiel F.' _publ_section_title ; Redetermination of bis(L-asparaginato)copper(II) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1428 _journal_page_last m1430 _journal_volume 60 _journal_year 2004 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.210 _cell_angle_gamma 90.000 _cell_length_a 5.0360 _cell_length_b 18.9150 _cell_length_c 6.1520 _exptl_crystal_F_000 334.00 _reflns_d_resolution_high 0.8024 _[local]_cod_data_source_file bt6505Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ? _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 578.89 582.36 7.26 o 2 0 0 106.59 108.06 1.01 o 3 0 0 70.01 63.24 0.97 o 4 0 0 136.10 128.25 2.88 o 5 0 0 247.63 243.40 7.07 o 6 0 0 0.79 1.71 0.25 o 1 1 0 4411.72 3811.69 162.40 o 2 1 0 832.28 766.92 15.01 o 3 1 0 369.16 326.30 5.10 o 4 1 0 553.71 542.99 20.08 o 5 1 0 54.25 53.67 3.17 o 6 1 0 33.65 33.52 0.92 o 0 2 0 5614.91 5909.15 29.57 o 1 2 0 733.13 664.13 5.71 o 2 2 0 613.75 587.66 24.44 o 3 2 0 537.99 521.11 17.87 o 4 2 0 408.21 409.71 19.15 o 5 2 0 115.66 124.25 10.83 o 6 2 0 19.26 16.25 0.83 o 1 3 0 1474.83 1453.30 79.94 o 2 3 0 251.99 223.22 15.69 o 3 3 0 591.56 578.28 39.96 o 4 3 0 263.98 271.57 18.86 o 5 3 0 86.74 85.51 11.42 o 6 3 0 44.33 43.61 0.71 o 0 4 0 1479.46 1415.16 3.75 o 1 4 0 1189.20 1248.89 2.80 o 2 4 0 1203.24 1195.93 65.49 o 3 4 0 710.15 703.43 44.98 o 4 4 0 183.35 172.65 15.73 o 5 4 0 94.39 102.35 11.49 o 6 4 0 20.53 19.77 0.59 o 1 5 0 1050.28 987.78 10.10 o 2 5 0 35.86 31.46 1.48 o 3 5 0 577.47 538.49 35.55 o 4 5 0 143.75 147.77 9.80 o 5 5 0 33.05 31.08 4.16 o 6 5 0 18.49 15.74 1.05 o 0 6 0 1839.12 1907.61 5.31 o 1 6 0 73.46 103.99 8.95 o 2 6 0 2234.42 2292.91 41.25 o 3 6 0 140.54 139.69 1.56 o 4 6 0 24.91 23.85 1.21 o 5 6 0 27.51 28.43 1.92 o 6 6 0 10.31 9.80 0.39 o 1 7 0 2014.18 1965.50 24.38 o 2 7 0 1173.81 1169.06 4.68 o 3 7 0 375.81 336.73 10.72 o 4 7 0 35.03 33.36 1.66 o 5 7 0 21.44 22.56 1.89 o 0 8 0 223.99 197.21 1.81 o 1 8 0 2022.31 2532.21 62.56 o 2 8 0 1615.87 1624.19 19.71 o 3 8 0 133.28 133.25 1.62 o 4 8 0 163.25 152.01 3.68 o 5 8 0 4.56 5.17 0.41 o 1 9 0 2849.94 3076.58 16.06 o 2 9 0 837.62 817.66 17.02 o 3 9 0 399.12 376.08 9.81 o 4 9 0 97.28 98.95 2.87 o 5 9 0 71.83 66.22 1.50 o 0 10 0 486.82 436.20 3.15 o 1 10 0 365.90 464.37 16.92 o 2 10 0 292.36 271.98 7.57 o 3 10 0 144.54 134.69 2.72 o 4 10 0 274.90 280.65 10.13 o 5 10 0 136.70 129.67 3.26 o 1 11 0 614.26 558.92 4.41 o 2 11 0 100.50 97.72 1.31 o 3 11 0 430.88 438.95 10.26 o 4 11 0 225.94 221.24 6.67 o 5 11 0 33.78 30.47 0.61 o 0 12 0 169.11 153.48 2.12 o 1 12 0 476.79 512.39 9.64 o 2 12 0 1210.57 1216.98 11.19 o 3 12 0 48.39 45.16 1.51 o 4 12 0 125.28 131.14 1.67 o 5 12 0 125.21 122.70 3.67 o 1 13 0 478.15 422.87 2.72 o 2 13 0 192.16 174.57 3.51 o 3 13 0 407.75 419.04 6.84 o 4 13 0 9.67 8.99 0.52 o 5 13 0 9.32 12.07 0.82 o 0 14 0 493.59 513.44 4.32 o 1 14 0 224.97 260.80 5.13 o 2 14 0 628.07 627.71 7.64 o 3 14 0 31.87 29.27 0.63 o 4 14 0 9.74 10.56 0.34 o 5 14 0 23.44 22.64 0.54 o 1 15 0 647.23 637.46 3.66 o 2 15 0 89.12 88.16 1.43 o 3 15 0 180.06 170.90 1.91 o 4 15 0 26.32 26.77 0.54 o 0 16 0 527.30 556.44 4.84 o 1 16 0 678.53 700.76 9.12 o 2 16 0 39.48 33.26 1.13 o 3 16 0 163.75 158.16 1.80 o 4 16 0 79.03 80.78 2.72 o 1 17 0 84.16 96.61 3.99 o 2 17 0 77.59 81.98 1.36 o 3 17 0 198.57 195.03 1.86 o 4 17 0 44.80 39.45 0.47 o 0 18 0 286.14 287.97 3.52 o 1 18 0 8.60 11.43 1.00 o 2 18 0 91.62 92.08 4.33 o 3 18 0 160.87 161.16 1.58 o 4 18 0 35.58 38.47 0.57 o 1 19 0 108.51 107.98 3.55 o 2 19 0 6.50 7.05 0.30 o 3 19 0 80.56 83.37 3.10 o 0 20 0 591.73 653.36 4.93 o 1 20 0 195.23 169.39 2.07 o 2 20 0 87.17 83.79 1.30 o 3 20 0 10.61 9.83 0.25 o 1 21 0 311.62 312.02 2.15 o 2 21 0 25.11 24.14 0.82 o 0 22 0 315.95 339.21 2.93 o 1 22 0 19.70 17.58 2.88 o 2 22 0 54.27 58.26 0.74 o 1 23 0 131.70 138.20 1.08 o -6 0 1 22.41 21.71 0.63 o -5 0 1 179.67 184.21 2.52 o -4 0 1 411.89 471.51 4.60 o -3 0 1 189.36 205.84 4.39 o -2 0 1 10.07 12.70 0.47 o -1 0 1 8206.40 9059.49 188.70 o 0 0 1 26.47 29.55 0.43 o 1 0 1 74.66 119.71 1.66 o 2 0 1 53.62 59.29 0.71 o 3 0 1 58.36 57.86 2.24 o 4 0 1 42.65 37.62 0.64 o 5 0 1 3.34 5.31 0.28 o 6 0 1 29.77 25.98 0.77 o -6 1 1 59.22 57.10 1.18 o -5 1 1 276.98 295.98 2.75 o -4 1 1 202.74 199.38 2.75 o -3 1 1 54.63 63.10 1.02 o -2 1 1 138.66 128.66 1.42 o -1 1 1 540.77 555.74 13.53 o 0 1 1 2502.17 2066.43 9.67 o 1 1 1 5769.99 5496.92 58.63 o 2 1 1 1053.08 1056.40 2.55 o 3 1 1 39.50 33.03 0.56 o 4 1 1 180.14 167.96 4.76 o 5 1 1 148.82 135.60 6.65 o 6 1 1 3.86 6.04 0.34 o -6 2 1 52.63 58.83 1.15 o -5 2 1 23.87 26.48 0.47 o -4 2 1 680.27 771.77 3.30 o -3 2 1 403.81 446.13 5.79 o -2 2 1 1033.95 1087.76 14.59 o -1 2 1 663.60 678.43 10.83 o 0 2 1 306.64 291.13 1.82 o 1 2 1 6278.32 5925.14 76.28 o 2 2 1 405.30 421.01 3.85 o 3 2 1 962.96 925.22 24.02 o 4 2 1 8.20 11.39 0.34 o 5 2 1 29.39 25.26 2.53 o 6 2 1 53.61 45.09 0.97 o -6 3 1 2.28 2.51 0.15 o -5 3 1 81.96 89.97 1.18 o -4 3 1 87.98 90.03 1.35 o -3 3 1 1072.22 1111.31 3.34 o -2 3 1 2304.45 2596.45 33.23 o -1 3 1 178.53 168.73 2.14 o 0 3 1 2342.14 1649.74 9.52 o 1 3 1 2672.14 1971.89 16.30 o 2 3 1 1258.96 1299.91 36.67 o 3 3 1 81.26 86.06 3.00 o 4 3 1 153.62 142.74 5.04 o 5 3 1 90.67 85.68 4.65 o 6 3 1 8.82 9.06 0.36 o -6 4 1 57.62 54.79 2.47 o -5 4 1 50.92 57.91 1.06 o -4 4 1 591.29 654.07 4.35 o -3 4 1 471.92 573.59 8.18 o -2 4 1 1295.83 1437.49 16.62 o -1 4 1 932.13 982.99 9.42 o 0 4 1 38.99 39.60 0.70 o 1 4 1 4484.94 3454.70 51.76 o 2 4 1 181.11 177.55 5.47 o 3 4 1 787.24 717.34 42.37 o 4 4 1 97.86 96.99 7.20 o 5 4 1 84.45 72.15 3.34 o 6 4 1 17.76 13.57 0.40 o -6 5 1 11.15 11.34 0.26 o -5 5 1 94.82 101.96 1.52 o -4 5 1 82.92 77.75 1.11 o -3 5 1 991.71 1004.66 6.20 o -2 5 1 1047.74 1028.34 6.39 o -1 5 1 541.88 510.84 3.30 o 0 5 1 1837.28 1870.27 12.48 o 1 5 1 661.77 605.06 4.93 o 2 5 1 1666.37 1647.26 58.72 o 3 5 1 247.34 240.13 9.73 o 4 5 1 276.10 273.33 15.56 o 5 5 1 28.81 27.02 0.85 o -6 6 1 69.41 62.57 0.76 o -5 6 1 98.98 96.05 2.50 o -4 6 1 135.10 141.31 1.46 o -3 6 1 853.52 1001.21 8.46 o -2 6 1 1278.75 1328.27 4.68 o -1 6 1 1627.38 1625.73 5.19 o 0 6 1 97.00 91.79 0.64 o 1 6 1 547.91 505.79 6.46 o 2 6 1 514.28 511.39 11.95 o 3 6 1 543.48 517.66 13.11 o 4 6 1 80.78 76.65 3.52 o 5 6 1 67.47 60.35 3.84 o -5 7 1 100.73 105.63 2.02 o -4 7 1 258.17 240.90 3.48 o -3 7 1 828.75 819.69 9.31 o -2 7 1 971.40 930.46 13.59 o -1 7 1 525.60 475.07 1.67 o 0 7 1 247.32 196.89 1.01 o 1 7 1 85.56 83.55 0.89 o 2 7 1 2187.64 2229.91 11.04 o 3 7 1 64.11 63.97 0.96 o 4 7 1 206.67 199.49 5.12 o 5 7 1 54.20 58.56 3.07 o -5 8 1 123.91 117.89 1.23 o -4 8 1 23.23 26.90 1.49 o -3 8 1 300.74 317.65 4.10 o -2 8 1 727.65 739.80 4.44 o -1 8 1 506.33 414.14 12.63 o 0 8 1 455.47 424.61 2.04 o 1 8 1 1342.69 1219.71 3.07 o 2 8 1 77.04 75.28 0.88 o 3 8 1 401.51 395.25 8.60 o 4 8 1 40.23 38.85 0.87 o 5 8 1 95.51 89.00 5.81 o -5 9 1 184.75 184.33 1.45 o -4 9 1 330.47 326.41 2.33 o -3 9 1 326.35 292.58 2.75 o -2 9 1 1229.66 1225.20 8.12 o -1 9 1 211.46 188.68 1.19 o 0 9 1 1514.36 1473.55 5.32 o 1 9 1 13.32 9.68 0.26 o 2 9 1 174.08 156.29 2.10 o 3 9 1 188.92 177.10 3.55 o 4 9 1 46.54 47.45 1.46 o 5 9 1 25.61 28.17 1.46 o -5 10 1 11.68 12.29 0.39 o -4 10 1 126.92 132.84 1.44 o -3 10 1 8.99 20.66 2.62 o -2 10 1 86.15 118.24 4.89 o -1 10 1 1896.10 1855.70 20.30 o 0 10 1 27.35 30.37 1.14 o 1 10 1 518.52 472.89 2.92 o 2 10 1 92.12 94.30 3.33 o 3 10 1 277.40 259.30 6.83 o 4 10 1 254.62 254.35 7.36 o 5 10 1 25.81 26.33 2.16 o -5 11 1 234.00 236.43 1.87 o -4 11 1 34.77 34.64 0.59 o -3 11 1 59.58 61.10 0.98 o -2 11 1 197.86 175.60 1.67 o -1 11 1 245.62 220.46 1.46 o 0 11 1 2142.19 2241.82 18.70 o 1 11 1 6.78 10.65 0.29 o 2 11 1 112.54 97.82 1.98 o 3 11 1 321.02 315.82 9.67 o 4 11 1 49.97 52.11 3.54 o 5 11 1 47.20 45.92 3.43 o -5 12 1 0.22 -0.29 0.29 o -4 12 1 126.50 127.21 2.00 o -3 12 1 546.70 606.58 11.16 o -2 12 1 157.86 159.58 3.16 o -1 12 1 338.22 316.03 2.74 o 0 12 1 36.13 36.35 5.37 o 1 12 1 713.79 669.73 6.21 o 2 12 1 25.16 28.92 0.66 o 3 12 1 67.47 63.80 2.83 o 4 12 1 219.89 222.27 7.91 o 5 12 1 27.32 29.51 1.39 o -5 13 1 21.18 19.99 0.36 o -4 13 1 161.42 151.76 1.46 o -3 13 1 632.12 626.82 3.78 o -2 13 1 259.47 239.15 1.82 o -1 13 1 61.81 63.91 0.90 o 0 13 1 868.77 816.26 6.02 o 1 13 1 47.22 45.41 0.71 o 2 13 1 161.88 164.65 1.90 o 3 13 1 14.39 15.33 0.60 o 4 13 1 156.03 163.74 7.43 o 5 13 1 38.52 37.08 2.24 o -5 14 1 6.92 7.85 0.22 o -4 14 1 55.35 64.36 1.10 o -3 14 1 485.14 556.52 10.58 o -2 14 1 173.34 216.84 5.72 o -1 14 1 318.27 328.98 3.54 o 0 14 1 331.59 304.40 2.46 o 1 14 1 558.37 530.95 5.10 o 2 14 1 18.66 15.06 0.45 o 3 14 1 136.24 136.04 3.30 o 4 14 1 67.41 65.15 1.28 o -4 15 1 109.95 107.88 1.07 o -3 15 1 47.84 47.25 0.76 o -2 15 1 490.82 500.80 4.14 o -1 15 1 129.24 120.12 1.33 o 0 15 1 412.11 391.79 2.33 o 1 15 1 29.01 26.78 0.47 o 2 15 1 112.39 124.49 1.38 o 3 15 1 40.65 38.78 1.83 o 4 15 1 147.28 149.70 5.10 o -4 16 1 66.85 67.12 1.01 o -3 16 1 83.46 85.43 1.32 o -2 16 1 266.04 274.98 4.45 o -1 16 1 375.76 386.30 9.21 o 0 16 1 146.65 129.37 4.32 o 1 16 1 216.21 206.34 2.13 o 2 16 1 21.80 18.85 0.59 o 3 16 1 240.91 251.71 2.18 o 4 16 1 0.54 1.02 0.18 o -4 17 1 12.06 11.45 0.26 o -3 17 1 71.62 74.50 1.17 o -2 17 1 150.98 155.31 3.66 o -1 17 1 171.85 168.12 3.57 o 0 17 1 80.63 76.91 1.55 o 1 17 1 26.81 23.94 0.50 o 2 17 1 559.66 554.31 3.63 o 3 17 1 24.63 19.88 0.47 o 4 17 1 58.27 59.86 2.74 o -4 18 1 127.61 131.24 2.21 o -3 18 1 116.42 132.68 2.17 o -2 18 1 43.99 47.02 2.20 o -1 18 1 320.02 336.61 5.90 o 0 18 1 8.68 4.18 2.36 o 1 18 1 249.91 244.87 2.27 o 2 18 1 283.73 271.15 4.20 o 3 18 1 48.72 44.34 0.82 o -3 19 1 86.34 85.66 1.67 o -2 19 1 240.53 233.64 2.01 o -1 19 1 14.38 14.81 0.37 o 0 19 1 145.05 146.58 1.82 o 1 19 1 93.66 88.68 2.04 o 2 19 1 203.80 200.31 3.21 o 3 19 1 26.23 26.52 0.61 o -3 20 1 39.00 46.11 0.69 o -2 20 1 32.00 41.41 0.82 o -1 20 1 223.79 217.58 4.92 o 0 20 1 184.18 185.97 1.84 o 1 20 1 94.43 92.94 1.27 o 2 20 1 35.40 30.77 1.06 o 3 20 1 17.45 20.30 0.39 o -2 21 1 35.99 37.20 0.67 o -1 21 1 8.71 7.92 0.32 o 0 21 1 208.09 206.83 1.76 o 1 21 1 6.39 7.19 0.56 o 2 21 1 39.21 42.79 0.85 o -2 22 1 4.84 6.14 0.74 o -1 22 1 53.15 52.03 0.82 o 0 22 1 6.62 5.38 0.71 o 1 22 1 109.62 111.99 1.79 o 2 22 1 2.39 2.85 0.22 o -1 23 1 13.35 14.69 0.31 o 0 23 1 126.97 134.51 1.10 o 1 23 1 0.40 1.47 0.19 o -6 0 2 9.15 14.04 0.33 o -5 0 2 201.83 225.19 4.01 o -4 0 2 11.02 14.23 0.41 o -3 0 2 780.97 809.23 25.01 o -2 0 2 4311.56 5465.43 203.19 o -1 0 2 423.13 368.82 3.37 o 0 0 2 69.43 71.09 0.81 o 1 0 2 383.24 351.85 6.59 o 2 0 2 613.01 563.63 2.54 o 3 0 2 36.60 40.45 0.79 o 4 0 2 125.62 112.83 2.32 o 5 0 2 87.39 81.06 1.78 o -6 1 2 113.65 109.89 1.06 o -5 1 2 23.08 25.81 1.23 o -4 1 2 273.77 294.68 2.67 o -3 1 2 306.95 288.73 9.49 o -2 1 2 2046.79 2214.94 51.02 o -1 1 2 1253.82 1332.18 7.93 o 0 1 2 2671.47 3330.58 709.24 o 1 1 2 4098.83 3319.48 23.27 o 2 1 2 722.79 704.14 2.86 o 3 1 2 223.83 222.26 2.96 o 4 1 2 111.70 119.98 1.76 o 5 1 2 9.08 11.94 0.53 o -6 2 2 26.12 27.76 0.74 o -5 2 2 196.52 223.27 8.24 o -4 2 2 100.67 101.44 1.58 o -3 2 2 860.47 887.43 21.36 o -2 2 2 1252.42 1285.82 29.72 o -1 2 2 1648.36 1844.46 25.08 o 0 2 2 1495.45 1604.54 16.65 o 1 2 2 973.96 1006.66 20.30 o 2 2 2 1177.41 1310.82 19.83 o 3 2 2 96.31 86.96 1.29 o 4 2 2 108.41 105.99 4.07 o 5 2 2 51.52 50.20 1.38 o -6 3 2 43.73 40.55 0.93 o -5 3 2 155.78 156.44 2.81 o -4 3 2 334.77 370.05 5.24 o -3 3 2 570.70 541.96 10.92 o -2 3 2 1317.93 1404.63 23.50 o -1 3 2 507.69 530.48 12.42 o 0 3 2 933.41 937.95 4.83 o 1 3 2 1481.86 1602.54 18.33 o 2 3 2 345.76 377.07 13.40 o 3 3 2 529.32 597.75 24.89 o 4 3 2 27.42 24.00 1.69 o 5 3 2 89.21 77.95 8.81 o -6 4 2 9.82 11.08 0.38 o -5 4 2 136.15 155.63 1.78 o -4 4 2 196.67 204.46 4.77 o -3 4 2 580.84 601.01 8.93 o -2 4 2 747.88 761.12 10.31 o -1 4 2 3795.26 4761.59 100.42 o 0 4 2 774.69 757.43 3.51 o 1 4 2 658.07 751.20 9.53 o 2 4 2 1279.98 1394.09 28.78 o 3 4 2 280.04 281.47 17.49 o 4 4 2 106.49 110.11 12.50 o 5 4 2 12.45 10.18 2.01 o -6 5 2 92.82 81.20 1.16 o -5 5 2 44.13 42.08 1.61 o -4 5 2 183.81 193.05 6.11 o -3 5 2 650.48 629.04 12.97 o -2 5 2 1465.97 1543.13 24.88 o -1 5 2 3129.62 3796.29 19.07 o 0 5 2 206.55 194.28 1.24 o 1 5 2 448.76 441.98 2.06 o 2 5 2 534.07 568.25 7.43 o 3 5 2 535.15 604.66 48.43 o 4 5 2 2.87 4.99 0.83 o 5 5 2 50.11 45.28 8.96 o -5 6 2 50.43 55.82 1.07 o -4 6 2 197.56 200.84 2.13 o -3 6 2 586.79 616.54 9.65 o -2 6 2 1068.54 1071.31 12.75 o -1 6 2 427.20 392.40 4.24 o 0 6 2 116.92 109.80 0.98 o 1 6 2 159.79 143.95 1.23 o 2 6 2 1160.71 1173.60 44.65 o 3 6 2 162.63 151.93 12.73 o 4 6 2 70.30 64.11 8.81 o 5 6 2 5.99 5.87 0.27 o -5 7 2 21.83 20.39 0.44 o -4 7 2 525.78 549.25 3.54 o -3 7 2 576.78 552.97 5.15 o -2 7 2 320.80 299.35 2.02 o -1 7 2 1845.32 1937.71 13.10 o 0 7 2 129.49 116.84 1.42 o 1 7 2 1038.64 1049.60 10.31 o 2 7 2 87.98 90.27 1.20 o 3 7 2 243.09 247.04 16.28 o 4 7 2 89.50 93.76 9.23 o 5 7 2 3.38 3.72 0.44 o -5 8 2 101.01 107.44 1.79 o -4 8 2 20.38 25.72 1.97 o -3 8 2 787.95 803.07 4.97 o -2 8 2 452.20 411.57 2.50 o -1 8 2 389.35 351.96 2.15 o 0 8 2 2488.74 2727.59 42.74 o 1 8 2 105.86 97.86 1.13 o 2 8 2 399.48 375.85 10.23 o 3 8 2 20.01 19.75 1.34 o 4 8 2 99.55 90.28 5.12 o 5 8 2 101.77 86.69 5.32 o -5 9 2 11.79 12.60 0.55 o -4 9 2 474.63 474.29 3.28 o -3 9 2 219.20 211.79 5.64 o -2 9 2 255.80 230.11 5.73 o -1 9 2 635.40 568.18 5.67 o 0 9 2 91.40 82.14 1.05 o 1 9 2 86.80 83.40 6.74 o 2 9 2 127.36 128.30 1.53 o 3 9 2 207.19 197.97 2.92 o 4 9 2 90.44 94.57 3.75 o 5 9 2 47.35 41.21 3.60 o -5 10 2 329.73 346.72 12.96 o -4 10 2 9.26 13.72 2.48 o -3 10 2 48.13 49.46 0.95 o -2 10 2 42.78 50.16 2.62 o -1 10 2 482.89 447.26 2.60 o 0 10 2 2067.55 2198.47 6.83 o 1 10 2 263.81 247.54 1.97 o 2 10 2 150.81 143.29 3.58 o 3 10 2 89.82 86.11 2.54 o 4 10 2 164.81 145.27 4.32 o 5 10 2 18.32 16.06 0.61 o -5 11 2 31.82 32.07 0.64 o -4 11 2 303.00 301.21 2.55 o -3 11 2 27.81 25.50 0.56 o -2 11 2 405.99 375.90 3.08 o -1 11 2 1438.45 1417.00 22.44 o 0 11 2 116.31 104.11 1.32 o 1 11 2 211.12 189.53 6.37 o 2 11 2 11.64 16.59 0.91 o 3 11 2 115.70 130.48 1.75 o 4 11 2 12.07 17.08 0.41 o 5 11 2 96.81 88.28 1.29 o -5 12 2 203.02 212.28 3.12 o -4 12 2 118.67 119.46 12.93 o -3 12 2 65.70 60.58 2.57 o -2 12 2 95.42 76.22 1.30 o -1 12 2 323.86 295.90 3.43 o 0 12 2 1655.29 1633.72 15.36 o 1 12 2 128.17 119.84 1.52 o 2 12 2 34.60 43.64 0.90 o 3 12 2 1.93 4.09 0.51 o 4 12 2 58.78 57.50 2.60 o -5 13 2 4.12 3.69 0.28 o -4 13 2 262.05 269.06 2.25 o -3 13 2 17.96 18.95 1.34 o -2 13 2 19.68 21.47 0.46 o -1 13 2 1004.26 992.18 13.89 o 0 13 2 527.09 508.75 14.35 o 1 13 2 416.62 410.18 15.73 o 2 13 2 35.94 35.03 1.65 o 3 13 2 55.37 61.49 2.52 o 4 13 2 26.46 29.39 1.18 o -4 14 2 28.12 28.41 7.53 o -3 14 2 162.47 163.98 2.77 o -2 14 2 309.88 311.31 8.78 o -1 14 2 267.92 261.29 2.36 o 0 14 2 788.15 745.54 22.24 o 1 14 2 34.27 33.07 0.69 o 2 14 2 125.04 122.82 4.67 o 3 14 2 58.54 56.33 2.03 o 4 14 2 72.38 72.22 5.57 o -4 15 2 83.48 81.41 1.70 o -3 15 2 156.85 151.34 1.79 o -2 15 2 323.56 327.16 7.32 o -1 15 2 371.52 357.12 2.85 o 0 15 2 332.63 321.43 7.71 o 1 15 2 130.44 132.10 5.22 o 2 15 2 9.18 20.48 3.62 o 3 15 2 178.17 191.66 7.22 o 4 15 2 43.52 45.53 3.28 o -4 16 2 1.50 2.08 0.32 o -3 16 2 331.18 321.43 3.53 o -2 16 2 680.54 679.12 5.54 o -1 16 2 186.16 163.00 2.70 o 0 16 2 25.84 27.59 0.84 o 1 16 2 64.37 62.85 1.73 o 2 16 2 415.81 401.58 4.10 o 3 16 2 65.58 61.93 1.46 o 4 16 2 50.05 47.65 0.93 o -4 17 2 58.68 61.04 1.12 o -3 17 2 148.30 156.66 2.29 o -2 17 2 278.08 281.75 3.39 o -1 17 2 42.28 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