#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/42/2204265.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204265_Fobs loop_ _publ_author_name 'Lewis, Thomas C.' 'Tocher, Derek A.' _publ_section_title ; Redetermination of 5,5-dihydroxybarbituric acid trihydrate (alloxan tetrahydrate) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1748 _journal_page_last o1750 _journal_volume 60 _journal_year 2004 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.465 _cell_angle_gamma 90.000 _cell_length_a 9.4614 _cell_length_b 12.2095 _cell_length_c 7.2973 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.7516 _[local]_cod_data_source_file bt6507Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 55dihydroxybarbituricacidtrihydrate in C2/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3032.96 2986.20 36.78 o 4 0 0 806.99 827.89 8.81 o 6 0 0 3670.41 3923.52 48.54 o 8 0 0 99.28 84.38 1.93 o 10 0 0 37.41 35.07 1.29 o 12 0 0 3.42 2.96 0.71 o 1 1 0 1243.98 1218.88 9.02 o 3 1 0 2326.65 2367.92 17.29 o 5 1 0 201.50 211.08 2.01 o 7 1 0 1153.44 1209.00 11.12 o 9 1 0 1.81 0.90 0.20 o 11 1 0 0.08 0.42 0.18 o 2 2 0 95.58 93.54 0.84 o 4 2 0 2410.56 2418.23 17.65 o 6 2 0 14.29 8.05 0.34 o 8 2 0 242.64 251.29 2.94 o 10 2 0 91.61 83.62 1.51 o 12 2 0 29.14 28.63 0.91 o 1 3 0 687.18 766.63 5.71 o 3 3 0 10197.58 9744.47 70.19 o 5 3 0 3551.86 3641.68 26.48 o 7 3 0 138.25 131.96 1.82 o 9 3 0 1058.52 1025.52 9.81 o 11 3 0 3.80 4.44 0.42 o 0 4 0 22.57 15.26 0.36 o 2 4 0 1537.14 1601.14 11.77 o 4 4 0 40.01 44.91 0.59 o 6 4 0 370.90 349.39 3.23 o 8 4 0 151.74 138.22 1.92 o 10 4 0 16.05 21.47 1.53 o 12 4 0 6.58 9.03 0.71 o 1 5 0 1662.68 1730.71 12.71 o 3 5 0 742.95 798.25 6.08 o 5 5 0 246.49 256.62 2.27 o 7 5 0 216.49 218.92 2.97 o 9 5 0 1266.26 1263.60 11.91 o 11 5 0 548.18 554.04 6.02 o 0 6 0 11214.85 10170.76 128.07 o 2 6 0 1206.51 1358.84 10.11 o 4 6 0 727.38 834.75 6.44 o 6 6 0 776.95 793.68 6.79 o 8 6 0 603.93 605.75 6.12 o 10 6 0 115.19 115.46 1.89 o 1 7 0 48.15 42.26 0.59 o 3 7 0 262.53 252.88 2.24 o 5 7 0 699.62 683.91 5.46 o 7 7 0 0.32 0.67 0.18 o 9 7 0 80.76 78.53 1.91 o 0 8 0 1390.77 1372.63 14.58 o 2 8 0 0.47 2.80 0.82 o 4 8 0 665.41 669.30 6.11 o 6 8 0 55.98 55.17 0.92 o 8 8 0 152.75 146.93 3.11 o 10 8 0 49.13 53.57 1.85 o 1 9 0 7.80 5.17 0.49 o 3 9 0 510.65 519.56 4.29 o 5 9 0 438.36 444.68 6.60 o 7 9 0 61.99 55.32 1.67 o 9 9 0 140.59 148.18 7.78 o 0 10 0 3652.63 3483.22 49.52 o 2 10 0 461.07 449.23 4.24 o 4 10 0 20.00 15.57 0.58 o 6 10 0 0.09 0.52 0.23 o 8 10 0 12.50 13.88 2.91 o 1 11 0 210.04 211.75 3.22 o 3 11 0 6.40 5.65 0.49 o 5 11 0 8.97 11.93 0.53 o 7 11 0 489.52 481.06 7.47 o 9 11 0 49.70 54.90 1.86 o 0 12 0 2249.18 2195.38 43.02 o 2 12 0 15.29 15.16 0.89 o 4 12 0 21.41 23.15 0.91 o 6 12 0 183.57 173.18 4.19 o 8 12 0 1.80 2.76 0.75 o 1 13 0 69.53 68.70 3.05 o 3 13 0 8.26 7.90 0.85 o 5 13 0 58.47 60.91 1.60 o 7 13 0 1.07 1.44 0.57 o 0 14 0 71.33 75.95 3.46 o 2 14 0 189.84 195.60 4.39 o 4 14 0 14.84 10.12 1.16 o 6 14 0 3.51 6.36 1.05 o 1 15 0 21.43 22.39 1.32 o 3 15 0 36.15 40.31 1.77 o -12 0 1 145.41 152.57 4.85 o -10 0 1 46.10 38.87 2.27 o -8 0 1 588.57 607.22 9.12 o -6 0 1 126.42 109.97 1.59 o -4 0 1 1181.38 1161.05 12.18 o -2 0 1 388.38 430.29 4.61 o 0 0 1 2688.02 2185.88 90.26 o 4 0 1 23.39 22.64 0.66 o 6 0 1 51.48 39.91 1.09 o 8 0 1 12.51 13.46 1.02 o 10 0 1 25.58 29.29 2.40 o 12 0 1 19.08 20.45 1.08 o -11 1 1 319.47 294.78 3.65 o -9 1 1 1.61 1.56 0.25 o -7 1 1 339.12 364.83 7.62 o -5 1 1 1097.59 1166.84 8.73 o -3 1 1 554.07 548.44 4.17 o -1 1 1 403.47 413.65 3.13 o 1 1 1 214.82 218.89 1.70 o 3 1 1 7380.53 7101.46 55.82 o 5 1 1 0.57 2.99 0.60 o 7 1 1 875.52 825.55 7.83 o 9 1 1 8.65 8.04 0.58 o 11 1 1 2.42 3.63 0.38 o -12 2 1 0.82 0.65 0.22 o -10 2 1 166.98 172.29 2.40 o -8 2 1 116.77 110.97 1.63 o -6 2 1 1021.92 1047.81 7.95 o -4 2 1 138.06 121.90 1.14 o -2 2 1 2050.70 1993.91 14.54 o 0 2 1 1876.92 1842.13 18.01 o 2 2 1 1126.64 1143.99 8.43 o 4 2 1 306.53 342.96 2.75 o 6 2 1 40.84 48.05 1.41 o 8 2 1 0.26 1.25 0.22 o 10 2 1 58.68 59.88 1.50 o 12 2 1 269.74 280.89 5.13 o -11 3 1 35.86 44.62 1.10 o -9 3 1 21.82 20.91 0.67 o -7 3 1 19.85 22.41 0.60 o -5 3 1 349.05 366.48 3.00 o -3 3 1 3040.88 3258.08 23.63 o -1 3 1 404.69 445.15 3.41 o 1 3 1 1583.04 1655.68 12.12 o 3 3 1 472.83 549.87 4.23 o 5 3 1 34.43 33.21 0.65 o 7 3 1 9.79 9.64 0.54 o 9 3 1 146.09 145.43 2.08 o 11 3 1 5.45 5.13 0.45 o -12 4 1 2.34 3.33 0.70 o -10 4 1 180.95 187.92 2.57 o -8 4 1 232.96 235.44 2.81 o -6 4 1 65.03 69.94 1.02 o -4 4 1 476.35 526.89 4.13 o -2 4 1 11260.08 10215.43 121.56 o 0 4 1 30.49 31.64 0.48 o 2 4 1 186.59 162.56 1.43 o 4 4 1 372.84 415.11 3.35 o 6 4 1 838.75 816.67 16.58 o 8 4 1 302.11 294.15 3.36 o 10 4 1 168.30 161.43 2.34 o 12 4 1 590.66 607.36 13.22 o -11 5 1 8.43 9.16 0.63 o -9 5 1 1314.71 1329.68 12.47 o -7 5 1 404.18 397.49 4.16 o -5 5 1 341.10 339.28 2.87 o -3 5 1 3.86 3.87 0.23 o -1 5 1 261.31 317.86 2.56 o 1 5 1 89.60 81.63 0.85 o 3 5 1 221.35 225.52 1.97 o 5 5 1 28.93 25.04 0.47 o 7 5 1 368.09 355.71 3.83 o 9 5 1 78.78 75.99 1.40 o 11 5 1 459.10 450.78 5.13 o -10 6 1 28.96 29.13 2.35 o -8 6 1 16.83 18.61 0.72 o -6 6 1 461.90 447.97 3.75 o -4 6 1 167.78 180.99 1.70 o -2 6 1 2582.81 2831.21 20.67 o 0 6 1 2618.97 2860.06 20.86 o 2 6 1 140.26 160.92 1.51 o 4 6 1 1478.50 1631.50 12.17 o 6 6 1 47.95 41.05 0.84 o 8 6 1 369.25 366.25 4.05 o 10 6 1 171.10 166.74 2.43 o -9 7 1 126.23 126.32 2.92 o -7 7 1 63.91 61.04 1.72 o -5 7 1 336.42 349.75 3.02 o -3 7 1 126.87 141.08 1.40 o -1 7 1 391.60 396.06 3.22 o 1 7 1 91.11 95.69 1.03 o 3 7 1 4042.33 4021.94 29.31 o 5 7 1 2.74 1.93 0.22 o 7 7 1 1.88 2.00 0.25 o 9 7 1 196.15 201.43 2.69 o 11 7 1 13.60 14.35 0.68 o -10 8 1 166.09 175.07 3.81 o -8 8 1 160.09 159.45 3.34 o -6 8 1 503.29 489.02 5.23 o -4 8 1 35.85 30.81 0.77 o -2 8 1 94.75 92.87 1.93 o 0 8 1 2.88 2.75 0.54 o 2 8 1 135.55 128.88 1.49 o 4 8 1 76.32 66.09 0.92 o 6 8 1 3.00 5.73 0.36 o 8 8 1 37.48 38.70 0.94 o 10 8 1 52.31 51.31 1.41 o -9 9 1 125.91 129.76 3.07 o -7 9 1 352.07 343.25 5.67 o -5 9 1 635.11 551.15 5.82 o -3 9 1 606.45 597.77 6.14 o -1 9 1 255.32 236.88 2.44 o 1 9 1 442.92 431.08 4.01 o 3 9 1 1.62 3.87 0.23 o 5 9 1 120.43 117.51 1.39 o 7 9 1 52.52 46.87 1.02 o 9 9 1 292.39 308.17 5.44 o -8 10 1 16.66 17.22 1.00 o -6 10 1 221.90 202.15 2.73 o -4 10 1 517.93 452.05 4.96 o -2 10 1 1139.90 1096.89 10.64 o 0 10 1 3325.71 3250.79 29.70 o 2 10 1 2676.67 2667.05 21.78 o 4 10 1 71.84 75.18 1.16 o 6 10 1 758.41 751.03 8.55 o 8 10 1 3.82 3.07 0.46 o -9 11 1 0.15 0.18 0.28 o -7 11 1 86.51 78.33 2.17 o -5 11 1 715.27 673.38 7.09 o -3 11 1 0.37 0.77 0.28 o -1 11 1 117.76 120.71 1.84 o 1 11 1 143.72 145.89 2.06 o 3 11 1 49.04 40.83 0.95 o 5 11 1 6.11 6.33 0.53 o 7 11 1 297.96 296.28 7.34 o 9 11 1 79.80 85.05 3.50 o -8 12 1 149.52 156.72 4.08 o -6 12 1 0.25 1.90 0.54 o -4 12 1 19.95 23.23 0.77 o -2 12 1 1.70 2.74 0.32 o 0 12 1 19.19 18.30 0.80 o 2 12 1 31.58 31.74 1.03 o 4 12 1 0.89 1.22 0.40 o 6 12 1 89.44 95.54 3.33 o 8 12 1 13.49 15.97 1.37 o -7 13 1 19.76 19.70 1.56 o -5 13 1 84.56 93.00 2.07 o -3 13 1 206.59 203.85 3.38 o -1 13 1 403.87 425.33 8.38 o 1 13 1 25.37 25.11 1.29 o 3 13 1 1519.12 1605.49 22.97 o 5 13 1 57.49 59.45 2.00 o -6 14 1 8.69 12.71 1.58 o -4 14 1 14.32 18.85 0.90 o -2 14 1 176.75 188.76 4.29 o 0 14 1 187.63 199.71 4.45 o 2 14 1 39.50 41.90 1.76 o 4 14 1 78.06 87.61 2.64 o -3 15 1 34.66 29.60 2.30 o -1 15 1 86.66 84.01 2.68 o 1 15 1 24.31 26.22 1.42 o 3 15 1 21.12 21.35 1.62 o -12 0 2 67.65 67.87 2.07 o -10 0 2 0.10 0.46 0.28 o -8 0 2 248.16 261.94 4.30 o -6 0 2 480.16 458.70 5.28 o -4 0 2 171.04 178.26 2.24 o -2 0 2 7090.01 6726.48 211.60 o 0 0 2 696.19 635.83 5.77 o 4 0 2 4905.14 5234.69 53.78 o 6 0 2 2308.34 2152.81 27.11 o 8 0 2 1359.79 1338.94 17.55 o 10 0 2 233.94 226.85 4.17 o -11 1 2 6.22 4.48 0.39 o -9 1 2 143.52 123.87 1.85 o -7 1 2 170.40 158.95 2.02 o -5 1 2 6624.87 7064.20 67.98 o -3 1 2 463.76 499.80 3.86 o -1 1 2 811.74 768.45 5.72 o 1 1 2 2571.41 2531.78 19.29 o 3 1 2 801.40 760.84 5.72 o 5 1 2 2.50 0.86 0.15 o 7 1 2 353.12 363.19 4.44 o 9 1 2 695.72 665.44 6.72 o 11 1 2 62.60 58.37 1.31 o -12 2 2 44.95 48.42 1.70 o -10 2 2 355.31 342.12 3.98 o -8 2 2 34.37 33.94 0.80 o -6 2 2 10.04 9.51 0.29 o -4 2 2 24.85 28.59 0.44 o -2 2 2 6651.69 6660.28 59.42 o 0 2 2 1920.85 1917.30 17.92 o 2 2 2 423.52 487.65 3.74 o 4 2 2 574.76 558.70 5.73 o 6 2 2 128.48 126.51 2.09 o 8 2 2 109.74 112.49 1.68 o 10 2 2 124.30 127.49 2.00 o -11 3 2 28.08 29.74 1.15 o -9 3 2 6.85 5.62 0.40 o -7 3 2 641.22 647.13 7.48 o -5 3 2 724.32 740.12 5.73 o -3 3 2 103.09 97.19 1.05 o -1 3 2 8165.21 7403.30 66.02 o 1 3 2 12296.81 10815.21 403.84 o 3 3 2 1166.65 1159.45 8.63 o 5 3 2 1853.80 1926.61 15.49 o 7 3 2 43.94 46.30 0.93 o 9 3 2 90.38 88.19 2.16 o 11 3 2 19.90 15.60 0.66 o -10 4 2 130.01 128.82 2.34 o -8 4 2 6.44 5.73 0.36 o -6 4 2 1015.34 1006.66 7.72 o -4 4 2 232.14 208.56 1.85 o -2 4 2 1120.83 1100.99 8.23 o 0 4 2 9076.01 8335.88 96.39 o 2 4 2 50.09 54.03 0.90 o 4 4 2 3756.03 3779.04 27.47 o 6 4 2 88.71 95.68 1.40 o 8 4 2 44.24 49.06 1.03 o 10 4 2 114.72 106.25 1.80 o -11 5 2 0.06 0.53 0.31 o -9 5 2 520.11 527.47 8.07 o -7 5 2 3535.51 3527.26 31.52 o -5 5 2 663.80 663.08 5.22 o -3 5 2 333.94 326.52 2.75 o -1 5 2 272.44 275.52 2.93 o 1 5 2 55.75 62.80 0.81 o 3 5 2 1094.90 1168.34 8.77 o 5 5 2 301.96 289.13 2.53 o 7 5 2 138.06 125.16 1.78 o 9 5 2 292.91 278.36 3.38 o 11 5 2 50.51 50.20 1.22 o -10 6 2 62.39 63.79 2.01 o -8 6 2 503.33 510.16 7.77 o -6 6 2 608.26 590.83 10.91 o -4 6 2 2.16 1.25 0.19 o -2 6 2 2765.28 2986.35 21.86 o 0 6 2 1884.25 2047.15 16.63 o 2 6 2 956.70 922.83 7.02 o 4 6 2 27.74 35.29 0.64 o 6 6 2 1728.25 1800.84 16.28 o 8 6 2 384.39 381.27 4.23 o 10 6 2 23.15 23.32 0.79 o -9 7 2 6.09 6.06 0.67 o -7 7 2 529.29 526.49 6.42 o -5 7 2 552.99 530.07 5.52 o -3 7 2 450.60 431.41 6.95 o -1 7 2 833.21 859.68 8.29 o 3 7 2 282.70 294.67 2.59 o 5 7 2 43.72 50.46 0.77 o 7 7 2 647.16 663.75 6.63 o 9 7 2 80.64 83.25 1.53 o -10 8 2 351.57 361.20 6.34 o -8 8 2 1.31 0.99 0.33 o -6 8 2 89.10 87.49 1.50 o -4 8 2 12.22 9.35 0.45 o -2 8 2 742.01 739.22 8.60 o 0 8 2 179.37 170.11 2.16 o 2 8 2 50.66 40.29 0.85 o 4 8 2 37.62 36.39 0.64 o 6 8 2 24.47 25.29 0.70 o 8 8 2 82.02 79.99 1.45 o 10 8 2 164.15 173.10 2.56 o -9 9 2 141.78 147.45 3.91 o -7 9 2 16.05 16.00 0.72 o -5 9 2 91.86 73.69 1.37 o -1 9 2 418.58 406.77 4.41 o 1 9 2 358.43 380.78 4.16 o 3 9 2 171.47 163.94 1.91 o 5 9 2 215.07 229.86 2.81 o 7 9 2 28.20 30.01 0.81 o 9 9 2 0.48 0.76 0.19 o -8 10 2 131.56 137.33 3.17 o -6 10 2 245.07 250.50 4.04 o -4 10 2 1.60 0.29 0.18 o -2 10 2 132.12 150.66 2.13 o 0 10 2 228.90 225.18 2.81 o 2 10 2 2382.09 2339.25 21.70 o 4 10 2 24.81 23.10 0.70 o 6 10 2 0.41 0.86 0.65 o 8 10 2 227.48 227.00 3.45 o -7 11 2 61.96 65.61 1.61 o -5 11 2 817.03 747.29 7.80 o -3 11 2 423.32 374.65 5.29 o -1 11 2 41.36 40.91 0.98 o 1 11 2 65.31 64.65 1.26 o 3 11 2 0.00 0.50 0.35 o 5 11 2 0.82 1.17 0.29 o 7 11 2 1.59 1.29 0.39 o -8 12 2 46.01 54.54 2.60 o -6 12 2 9.94 11.80 0.78 o -4 12 2 0.60 0.67 0.37 o -2 12 2 0.15 1.04 0.71 o 0 12 2 2.19 4.47 0.39 o 2 12 2 493.48 481.08 5.33 o 4 12 2 53.40 53.80 1.43 o -7 13 2 149.48 150.48 4.80 o -5 13 2 167.46 164.00 2.55 o -3 13 2 57.65 64.59 1.61 o -1 13 2 511.74 515.62 5.75 o 1 13 2 40.01 43.19 1.31 o 3 13 2 22.05 23.27 0.94 o 5 13 2 155.50 172.04 5.67 o -4 14 2 41.03 45.44 1.43 o -2 14 2 10.91 7.76 0.66 o 0 14 2 219.03 229.27 3.75 o 2 14 2 39.53 41.36 1.75 o 4 14 2 144.18 152.11 3.70 o -3 15 2 30.66 37.95 1.58 o -1 15 2 177.01 182.06 5.35 o 1 15 2 68.48 71.09 2.44 o 3 15 2 13.12 15.19 1.03 o -12 0 3 4.26 6.64 1.02 o -10 0 3 30.17 34.56 1.30 o -8 0 3 752.30 733.86 10.19 o -6 0 3 34.10 31.84 0.78 o -4 0 3 34.00 34.04 0.73 o -2 0 3 3911.37 4302.44 53.19 o 0 0 3 1253.16 1309.52 14.17 o 2 0 3 5905.38 5991.04 61.08 o 4 0 3 2616.76 3028.93 31.23 o 6 0 3 1369.62 1414.33 18.21 o 8 0 3 138.58 125.14 4.17 o 10 0 3 3.79 5.42 0.63 o -11 1 3 127.99 124.60 2.38 o -9 1 3 437.70 396.69 4.38 o -7 1 3 35.99 41.75 0.68 o -5 1 3 182.11 151.79 1.49 o -1 1 3 8.49 8.56 0.30 o 3 1 3 207.12 245.94 2.07 o 5 1 3 901.29 894.35 8.31 o 7 1 3 38.10 40.84 0.88 o 9 1 3 21.33 21.10 0.70 o 11 1 3 13.92 14.81 0.64 o -10 2 3 18.19 25.14 3.49 o -8 2 3 194.67 197.44 2.48 o -6 2 3 136.04 133.96 1.91 o -4 2 3 713.61 692.19 5.35 o -2 2 3 403.94 458.84 3.58 o 0 2 3 155.89 165.51 1.33 o 2 2 3 1219.93 1252.70 9.29 o 4 2 3 1225.15 1365.46 10.17 o 6 2 3 391.44 399.70 4.76 o 8 2 3 11.52 10.58 0.52 o 10 2 3 52.01 49.59 1.29 o -11 3 3 62.60 61.08 1.96 o -9 3 3 6.30 5.70 0.48 o -7 3 3 536.88 521.69 11.78 o -5 3 3 11.66 15.87 0.60 o -3 3 3 1256.79 1258.39 9.38 o -1 3 3 123.51 116.59 1.22 o 1 3 3 560.03 561.71 4.32 o 3 3 3 1042.43 1032.00 7.76 o 5 3 3 683.95 699.48 7.66 o 7 3 3 853.64 834.40 8.03 o 9 3 3 34.49 30.49 0.85 o 11 3 3 13.20 12.55 0.60 o -10 4 3 104.24 108.44 3.30 o -8 4 3 70.79 66.80 1.87 o -6 4 3 5.81 6.67 0.30 o -4 4 3 46.23 42.05 0.68 o -2 4 3 5.78 4.80 0.50 o 0 4 3 985.04 1025.09 7.70 o 2 4 3 7.11 7.72 0.34 o 4 4 3 596.73 602.47 5.28 o 6 4 3 51.77 53.37 1.00 o 8 4 3 189.17 186.26 2.46 o 10 4 3 0.68 0.47 0.22 o -11 5 3 215.69 242.29 6.76 o -9 5 3 5.55 5.52 0.65 o -7 5 3 3012.53 3022.51 27.72 o -5 5 3 3343.81 3224.96 44.32 o -3 5 3 36.19 40.49 0.80 o -1 5 3 102.16 104.47 1.42 o 1 5 3 5.90 2.65 0.18 o 3 5 3 279.20 282.29 2.44 o 5 5 3 0.55 1.08 0.20 o 7 5 3 321.86 318.08 3.58 o 9 5 3 0.02 0.18 0.17 o 11 5 3 41.41 48.96 2.34 o -10 6 3 0.17 0.26 0.30 o -8 6 3 245.30 250.96 7.92 o -6 6 3 2.96 2.04 0.27 o -4 6 3 0.18 0.67 0.18 o -2 6 3 1970.52 1953.23 18.00 o 0 6 3 1497.90 1548.44 14.38 o 2 6 3 0.52 3.45 0.54 o 4 6 3 225.10 226.52 2.10 o 6 6 3 0.02 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33.98 35.63 1.95 o 5 5 8 26.50 27.36 1.25 o -4 6 8 36.64 40.20 1.10 o -2 6 8 27.32 25.65 0.86 o 0 6 8 5.74 7.47 0.53 o 2 6 8 92.84 94.74 1.74 o 4 6 8 12.10 12.21 0.82 o -3 7 8 35.73 37.02 1.07 o -1 7 8 1.52 1.87 0.32 o 1 7 8 7.40 7.99 0.79 o 3 7 8 25.67 27.81 1.26 o -2 8 8 467.62 490.63 7.88 o 0 8 8 10.29 12.02 0.60 o 2 8 8 91.54 94.66 2.08 o 1 9 8 45.02 48.10 2.30 o -2 0 9 6.20 6.27 0.98 o 0 0 9 73.90 72.10 3.05 o 2 0 9 4.06 2.38 0.49 o -3 1 9 104.39 98.82 2.70 o -1 1 9 2.87 3.01 0.49 o 1 1 9 6.43 7.46 0.73 o -2 2 9 45.05 42.36 1.64 o 0 2 9 237.42 234.08 4.64 o 2 2 9 179.00 183.54 5.32 o -1 3 9 20.33 22.80 1.17 o 1 3 9 15.00 16.25 0.96 o 3 3 9 24.36 26.40 1.68 o -2 4 9 63.05 67.69 1.73 o 0 4 9 13.60 15.61 0.78 o 2 4 9 295.52 301.83 7.60 o -3 5 9 54.52 58.94 2.82 o -1 5 9 238.95 258.34 6.89 o 1 5 9 427.85 441.30 5.18 o 0 6 9 64.69 64.38 2.65 o