#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:06:39 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180962 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/42/2204280.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204280_Fobs loop_ _publ_author_name 'Ravikumar, K.' 'Swamy, G. Y. S. K.' 'Raghavan, Sadagopan' 'Kumar, Ch. Naveen' _publ_section_title ; N-[(1S,2S,3R)-2-Bromo-3-(tert-butyldiphenylsiloxy)-1-phenyl-4-(phenylsulfinyl)butyl]benzenesulfonamide ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1880 _journal_page_last o1882 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.263 _cell_angle_gamma 90.000 _cell_length_a 20.0567 _cell_length_b 8.2412 _cell_length_c 23.8154 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 0.7566 _cod_data_source_file bt6527Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Rg02m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 36715.15 36523.95 2387.31 o 3 0 0 702.11 821.72 32.00 o 4 0 0 10399.22 10674.49 283.42 o 5 0 0 7629.47 7910.53 218.06 o 6 0 0 593.59 655.23 40.80 o 7 0 0 2661.47 2833.17 97.93 o 8 0 0 3862.73 3663.79 120.84 o 9 0 0 8791.87 9635.18 273.12 o 10 0 0 7761.57 7913.79 233.17 o 11 0 0 983.05 1036.91 62.71 o 12 0 0 2099.02 2299.12 99.93 o 13 0 0 59.89 82.57 41.81 o 14 0 0 551.53 599.96 61.43 o 15 0 0 119.49 129.36 51.87 o 16 0 0 59.87 95.50 51.43 o 17 0 0 1034.34 882.53 77.52 o 18 0 0 1017.38 1117.52 143.78 o 19 0 0 923.27 829.46 141.96 o 20 0 0 145.61 258.43 84.63 o 21 0 0 1788.08 1599.73 144.69 o 22 0 0 95.97 229.31 86.45 o 23 0 0 429.01 586.02 104.65 o 24 0 0 3.15 3.64 70.98 o 1 1 0 29.88 57.68 6.35 o 2 1 0 7466.92 8351.06 179.85 o 3 1 0 2646.16 2968.66 70.57 o 4 1 0 65702.70 69965.97 1460.18 o 5 1 0 6639.38 7175.06 162.33 o 6 1 0 1715.39 2093.51 73.28 o 7 1 0 1058.86 985.42 36.25 o 8 1 0 3186.05 3272.76 76.73 o 9 1 0 25.29 -8.33 18.22 o 10 1 0 80.77 21.82 21.64 o 11 1 0 2305.99 2429.33 69.70 o 12 1 0 326.72 306.35 31.63 o 13 1 0 1311.21 1492.33 57.99 o 14 1 0 4.52 10.56 29.03 o 15 1 0 135.50 208.92 36.24 o 16 1 0 1614.86 1584.48 65.85 o 17 1 0 11.48 34.98 36.26 o 18 1 0 167.06 212.60 39.27 o 19 1 0 167.87 163.44 44.84 o 20 1 0 31.05 65.62 42.73 o 21 1 0 26.26 117.67 51.54 o 22 1 0 28.11 5.61 49.53 o 23 1 0 1.88 17.94 53.69 o 24 1 0 166.39 73.71 83.72 o 0 2 0 3648.70 4185.60 148.78 o 1 2 0 110.82 44.09 11.37 o 2 2 0 15053.76 16169.70 299.01 o 3 2 0 17867.32 19433.65 414.86 o 4 2 0 319.08 308.86 21.82 o 5 2 0 269.11 278.34 21.89 o 6 2 0 37.52 24.83 16.76 o 7 2 0 8879.93 9096.07 206.98 o 8 2 0 15458.43 15831.52 348.31 o 9 2 0 24.50 27.88 22.28 o 10 2 0 3037.59 2699.18 83.46 o 11 2 0 708.34 712.38 36.81 o 12 2 0 27.25 16.91 23.97 o 13 2 0 739.93 822.72 42.68 o 14 2 0 748.34 714.28 43.98 o 15 2 0 1266.87 1054.73 60.23 o 16 2 0 178.24 252.75 45.58 o 17 2 0 310.70 226.15 38.09 o 18 2 0 1342.61 1319.71 99.03 o 19 2 0 62.25 42.35 47.52 o 20 2 0 237.08 263.03 49.99 o 21 2 0 708.98 922.82 111.93 o 22 2 0 223.77 305.78 64.38 o 23 2 0 116.54 122.71 59.20 o 24 2 0 27.89 200.19 95.55 o 1 3 0 12970.94 14269.65 240.98 o 2 3 0 5535.24 5640.78 115.66 o 3 3 0 8.76 12.66 15.56 o 4 3 0 10116.77 10746.19 240.96 o 5 3 0 1527.21 1747.32 71.89 o 6 3 0 301.82 226.12 26.27 o 7 3 0 293.41 229.13 32.00 o 8 3 0 670.69 693.11 37.57 o 9 3 0 4315.75 4253.43 113.77 o 10 3 0 756.71 674.64 41.42 o 11 3 0 2491.16 2393.94 81.70 o 12 3 0 3507.08 3499.21 112.09 o 13 3 0 865.90 733.60 49.16 o 14 3 0 134.71 138.40 30.20 o 15 3 0 459.70 409.01 42.42 o 16 3 0 37.41 -12.42 33.80 o 17 3 0 810.07 736.94 47.88 o 18 3 0 283.79 254.58 45.82 o 19 3 0 1115.77 1103.85 98.46 o 20 3 0 409.61 503.66 55.51 o 21 3 0 27.26 138.41 47.41 o 22 3 0 86.90 145.31 64.15 o 23 3 0 8.98 -9.08 68.70 o 24 3 0 30.11 111.02 98.28 o 0 4 0 5165.49 5443.22 166.01 o 1 4 0 316.18 374.90 21.99 o 2 4 0 2184.45 2193.29 59.14 o 3 4 0 1536.36 1548.63 56.91 o 4 4 0 50.44 34.06 19.92 o 5 4 0 146.80 133.28 23.87 o 6 4 0 5568.43 5577.52 141.14 o 7 4 0 160.94 160.30 51.44 o 8 4 0 1150.60 1126.84 51.73 o 9 4 0 147.20 140.50 28.98 o 10 4 0 2839.23 2804.76 90.64 o 11 4 0 1672.55 1699.29 69.43 o 12 4 0 1578.77 1398.96 65.28 o 13 4 0 1373.52 1282.67 63.38 o 14 4 0 60.49 48.85 43.26 o 15 4 0 204.18 190.54 39.86 o 16 4 0 181.72 160.25 37.83 o 17 4 0 106.37 107.47 48.71 o 18 4 0 28.40 88.08 39.33 o 19 4 0 2.14 -2.57 37.10 o 20 4 0 13.67 -36.14 36.14 o 21 4 0 236.48 217.11 91.07 o 22 4 0 148.96 175.57 68.70 o 23 4 0 1.18 19.11 103.74 o 24 4 0 0.12 -90.09 90.09 o 1 5 0 9120.26 8402.33 174.59 o 2 5 0 5006.10 4648.39 107.48 o 3 5 0 2446.63 2374.00 67.21 o 4 5 0 2951.25 2727.18 86.62 o 5 5 0 1120.62 1218.53 54.98 o 6 5 0 6928.16 7048.55 177.17 o 7 5 0 77.63 97.41 48.05 o 8 5 0 2052.06 1938.10 73.54 o 9 5 0 764.18 728.05 63.08 o 10 5 0 494.81 453.12 50.63 o 11 5 0 371.50 450.92 70.02 o 12 5 0 616.33 652.69 49.59 o 13 5 0 347.23 336.16 48.35 o 14 5 0 294.27 339.51 43.58 o 15 5 0 285.65 226.03 40.34 o 16 5 0 78.90 34.15 40.01 o 17 5 0 624.65 576.24 55.11 o 18 5 0 106.41 121.27 43.50 o 19 5 0 524.55 638.22 69.57 o 20 5 0 214.92 335.16 54.90 o 21 5 0 16.91 11.25 45.12 o 22 5 0 360.32 257.79 74.99 o 23 5 0 69.77 36.40 111.02 o 0 6 0 628.33 735.00 47.45 o 1 6 0 634.27 599.75 34.55 o 2 6 0 111.91 112.32 26.28 o 3 6 0 153.34 107.30 32.70 o 4 6 0 1358.73 1398.07 92.79 o 5 6 0 465.11 466.29 42.32 o 6 6 0 42.08 83.34 34.44 o 7 6 0 32.88 4.77 43.27 o 8 6 0 522.41 409.30 46.37 o 9 6 0 305.75 369.71 42.51 o 10 6 0 721.51 819.30 55.12 o 11 6 0 113.07 100.87 70.75 o 12 6 0 267.27 280.60 42.28 o 13 6 0 6.03 45.87 36.44 o 14 6 0 418.81 409.25 49.70 o 15 6 0 17.14 61.18 46.81 o 16 6 0 31.13 11.43 48.32 o 17 6 0 307.07 368.01 66.46 o 18 6 0 308.78 356.64 70.52 o 19 6 0 27.26 3.19 43.19 o 20 6 0 2.55 35.86 48.38 o 21 6 0 40.93 85.13 82.05 o 22 6 0 119.89 140.93 67.10 o 1 7 0 2080.47 1885.34 62.87 o 2 7 0 197.18 127.38 29.58 o 3 7 0 359.68 378.80 45.31 o 4 7 0 1747.36 1724.81 119.57 o 5 7 0 32.00 37.33 31.42 o 6 7 0 2407.89 2135.67 84.40 o 7 7 0 1124.29 1002.13 60.12 o 8 7 0 855.74 897.17 103.61 o 9 7 0 1154.88 1090.39 104.08 o 10 7 0 52.87 26.75 34.58 o 11 7 0 354.03 334.94 46.21 o 12 7 0 84.21 119.61 40.51 o 13 7 0 34.12 0.47 46.44 o 14 7 0 300.01 302.95 70.33 o 15 7 0 440.59 506.94 72.13 o 16 7 0 47.49 115.11 58.53 o 17 7 0 117.44 224.20 90.09 o 18 7 0 37.75 30.18 100.55 o 19 7 0 48.88 39.47 64.52 o 20 7 0 3.60 -22.15 45.85 o 0 8 0 598.91 531.97 65.93 o 1 8 0 86.11 69.38 30.16 o 2 8 0 217.06 222.06 41.60 o 3 8 0 29.09 49.98 30.40 o 4 8 0 258.01 256.15 54.68 o 5 8 0 241.93 284.27 44.90 o 6 8 0 568.17 529.81 53.68 o 7 8 0 689.97 787.12 61.16 o 8 8 0 589.46 553.91 55.88 o 9 8 0 4.43 44.84 37.45 o 10 8 0 799.88 864.88 65.19 o 11 8 0 731.98 780.79 64.07 o 12 8 0 11.74 81.09 60.03 o 13 8 0 159.24 301.14 54.68 o 14 8 0 8.32 -45.94 70.98 o 15 8 0 99.86 81.21 62.97 o 16 8 0 3.44 -21.98 131.49 o 17 8 0 178.77 154.29 70.38 o 1 9 0 12.74 -38.91 38.91 o 2 9 0 51.36 42.58 42.63 o 3 9 0 11.83 14.26 40.43 o 4 9 0 106.03 142.08 43.38 o 5 9 0 394.77 435.59 47.26 o 6 9 0 3.38 -53.02 55.96 o 7 9 0 1078.32 1145.29 75.55 o 8 9 0 8.31 -32.26 41.51 o 9 9 0 422.56 347.73 55.26 o 10 9 0 0.10 5.14 47.54 o 11 9 0 179.42 184.06 52.54 o 12 9 0 86.62 122.96 66.89 o 13 9 0 66.36 119.07 65.56 o 14 9 0 425.17 358.53 103.74 o 0 10 0 686.01 667.01 117.39 o 1 10 0 64.20 51.67 45.95 o 2 10 0 588.67 542.78 62.84 o 3 10 0 364.43 402.04 58.28 o 4 10 0 167.84 128.82 48.75 o 5 10 0 315.98 341.58 56.71 o 6 10 0 3.15 -3.28 44.97 o 7 10 0 204.11 192.57 44.30 o 8 10 0 182.69 186.88 44.54 o 9 10 0 0.73 68.25 77.35 o 10 10 0 171.41 154.69 88.27 o -23 1 1 255.90 315.76 95.55 o -22 1 1 6.64 -42.11 45.99 o -21 1 1 7.59 3.43 44.35 o -20 1 1 510.41 480.57 54.38 o -19 1 1 534.17 486.42 52.02 o -18 1 1 254.11 322.04 41.33 o -17 1 1 250.58 204.55 40.70 o -16 1 1 717.09 909.39 60.06 o -15 1 1 805.41 857.59 63.18 o -14 1 1 452.76 461.23 43.97 o -13 1 1 4443.21 4340.37 108.45 o -12 1 1 2466.39 2329.38 70.73 o -11 1 1 1390.99 1355.43 53.46 o -10 1 1 13473.94 14363.39 279.12 o -9 1 1 1526.55 1666.21 60.55 o -8 1 1 9164.00 9071.27 180.05 o -7 1 1 103.34 98.72 20.49 o -6 1 1 1329.20 1178.37 38.68 o -5 1 1 329.65 420.01 43.66 o -4 1 1 677.70 702.84 30.76 o -3 1 1 18148.45 19667.91 415.92 o -2 1 1 36379.80 38848.29 812.57 o -1 1 1 259.44 258.81 15.48 o 0 1 1 4088.80 4086.75 63.70 o 1 1 1 6881.88 7238.02 121.26 o 2 1 1 24530.31 25455.65 466.36 o 3 1 1 2451.24 2498.08 52.62 o 4 1 1 7829.42 8465.89 186.65 o 5 1 1 19270.41 19555.06 418.00 o 6 1 1 18131.37 18308.72 394.36 o 7 1 1 13073.86 13878.18 305.22 o 8 1 1 28996.81 31763.64 586.11 o 9 1 1 168.20 190.87 30.93 o 10 1 1 3087.61 3054.07 78.17 o 11 1 1 2659.69 2833.47 76.56 o 12 1 1 2418.00 2512.63 72.60 o 13 1 1 5318.66 5142.09 121.95 o 14 1 1 314.48 292.25 35.64 o 15 1 1 5430.72 5434.32 132.41 o 16 1 1 378.66 347.02 42.04 o 17 1 1 56.47 125.11 37.30 o 18 1 1 639.67 616.05 56.56 o 19 1 1 0.45 59.91 41.05 o 20 1 1 17.83 32.88 50.08 o 21 1 1 6.52 31.94 56.87 o 22 1 1 87.63 77.13 52.99 o 23 1 1 36.42 48.34 52.19 o 24 1 1 296.72 419.11 183.36 o 25 1 1 59.90 171.07 90.09 o -23 2 1 16.14 19.11 80.99 o -22 2 1 746.63 892.80 82.46 o -21 2 1 350.65 262.44 50.10 o -20 2 1 75.75 84.01 42.44 o -19 2 1 4.28 -9.09 32.30 o -18 2 1 755.32 858.97 52.45 o -17 2 1 156.34 127.02 36.22 o -16 2 1 783.86 718.87 47.88 o -15 2 1 2.54 30.64 30.79 o -14 2 1 1601.44 1617.46 91.81 o -13 2 1 53.90 22.34 26.79 o -12 2 1 1048.87 1053.84 45.41 o -11 2 1 37.51 -5.40 20.39 o -10 2 1 283.80 330.60 26.76 o -9 2 1 1856.44 2097.75 68.21 o -8 2 1 16.21 35.69 19.84 o -7 2 1 495.32 489.54 43.32 o -6 2 1 4903.88 4958.86 119.78 o -5 2 1 579.14 637.26 30.37 o -4 2 1 9127.97 9727.08 215.40 o -3 2 1 21613.19 23809.37 505.76 o -2 2 1 19572.75 21680.02 397.51 o -1 2 1 2190.32 2314.66 74.64 o 0 2 1 9340.50 9425.31 206.47 o 1 2 1 54282.77 58538.36 944.46 o 2 2 1 240.58 309.05 21.28 o 3 2 1 17450.41 18869.30 350.54 o 4 2 1 23.72 40.21 15.55 o 5 2 1 2081.47 2028.02 59.28 o 6 2 1 10273.96 10764.11 240.06 o 7 2 1 462.07 468.50 35.14 o 8 2 1 724.78 756.67 85.91 o 9 2 1 595.19 571.48 45.90 o 10 2 1 312.85 317.79 31.73 o 11 2 1 1198.22 1176.13 45.41 o 12 2 1 843.88 1027.00 44.63 o 13 2 1 645.58 662.28 39.60 o 14 2 1 106.72 124.97 30.77 o 15 2 1 323.32 321.00 36.92 o 16 2 1 91.51 76.58 34.21 o 17 2 1 1702.51 1745.66 72.53 o 18 2 1 1310.53 1219.64 69.24 o 19 2 1 18.62 74.92 40.62 o 20 2 1 7.45 -19.56 68.70 o 21 2 1 7.37 51.76 70.98 o 22 2 1 24.21 -47.10 47.10 o 23 2 1 10.79 -46.84 112.84 o 24 2 1 142.64 179.22 95.09 o 25 2 1 22.63 236.59 102.83 o -23 3 1 262.67 341.24 106.47 o -22 3 1 16.52 14.76 57.46 o -21 3 1 368.65 355.76 56.40 o -20 3 1 53.34 42.56 72.12 o -19 3 1 294.34 387.26 50.28 o -18 3 1 189.74 221.79 37.99 o -17 3 1 1.92 -28.19 28.19 o -16 3 1 1406.32 1367.21 59.97 o -15 3 1 5.03 -31.33 43.61 o -14 3 1 198.82 162.31 32.60 o -13 3 1 1336.09 1496.04 67.10 o -12 3 1 1279.70 1362.49 61.95 o -11 3 1 869.49 786.80 46.48 o -10 3 1 294.20 299.10 32.61 o -9 3 1 207.30 198.98 28.50 o -8 3 1 23.10 10.96 21.52 o -7 3 1 59.34 36.82 20.46 o -6 3 1 12.27 6.03 18.43 o -5 3 1 7556.45 7639.22 177.57 o -4 3 1 4751.59 4942.85 121.35 o -3 3 1 103.97 106.00 16.13 o -2 3 1 12001.05 12317.55 234.75 o -1 3 1 64.42 55.93 16.95 o 0 3 1 38580.25 40715.62 859.15 o 1 3 1 150.80 158.00 15.38 o 2 3 1 12700.45 13431.02 207.71 o 3 3 1 2992.75 3105.52 68.31 o 4 3 1 3334.77 3568.52 97.50 o 5 3 1 614.14 599.14 39.98 o 6 3 1 12.03 16.81 18.68 o 7 3 1 2400.74 2212.65 68.54 o 8 3 1 197.75 143.17 24.45 o 9 3 1 3.37 -9.46 21.64 o 10 3 1 76.28 49.63 36.56 o 11 3 1 20.84 24.28 27.82 o 12 3 1 355.77 285.13 36.90 o 13 3 1 12.90 37.41 31.48 o 14 3 1 92.17 100.78 29.80 o 15 3 1 380.96 510.33 40.94 o 16 3 1 3.34 -27.98 27.98 o 17 3 1 168.85 96.65 45.09 o 18 3 1 162.36 157.27 42.86 o 19 3 1 135.60 128.90 42.58 o 20 3 1 42.07 95.42 43.14 o 21 3 1 264.59 328.55 65.17 o 22 3 1 115.18 108.17 58.16 o 23 3 1 243.48 201.62 66.65 o 24 3 1 8.84 55.51 61.65 o 25 3 1 56.51 115.57 102.83 o -23 4 1 9.94 68.25 95.55 o -22 4 1 159.51 234.74 66.46 o -21 4 1 245.12 303.84 53.53 o -20 4 1 12.08 4.45 39.21 o -19 4 1 111.41 12.65 38.91 o -18 4 1 65.51 26.43 36.47 o -17 4 1 1173.24 1234.11 58.95 o -16 4 1 33.24 -11.18 29.12 o -15 4 1 1336.91 1278.50 57.18 o -14 4 1 1638.09 1682.11 92.84 o -13 4 1 28.15 -24.46 30.56 o -12 4 1 3816.26 3517.89 140.59 o -11 4 1 1226.22 1143.56 57.60 o -10 4 1 23.52 64.25 29.35 o -9 4 1 1965.99 1848.18 69.98 o -8 4 1 172.70 141.73 38.77 o -7 4 1 3607.92 3432.98 97.84 o -6 4 1 4786.96 4921.83 127.49 o -5 4 1 5359.07 5540.81 139.56 o -4 4 1 16359.22 17225.96 380.19 o -3 4 1 300.64 248.82 22.49 o -2 4 1 1261.80 1056.75 39.70 o -1 4 1 85.90 40.08 16.30 o 0 4 1 1544.77 1677.92 44.34 o 1 4 1 3338.45 3538.56 74.06 o 2 4 1 1501.58 1606.90 50.79 o 3 4 1 282.84 220.57 26.30 o 4 4 1 17043.39 17166.38 379.30 o 5 4 1 67.48 79.71 23.07 o 6 4 1 4201.49 3980.06 107.85 o 7 4 1 2137.02 1989.05 68.93 o 8 4 1 11.63 41.56 24.51 o 9 4 1 4841.64 4845.68 159.34 o 10 4 1 994.75 844.71 48.17 o 11 4 1 2466.43 2455.51 84.60 o 12 4 1 70.34 63.95 31.61 o 13 4 1 1145.34 1127.04 59.64 o 14 4 1 1836.36 1778.07 134.05 o 15 4 1 788.73 774.16 53.73 o 16 4 1 1334.40 1214.26 66.63 o 17 4 1 1099.34 1067.19 66.53 o 18 4 1 112.81 87.82 39.53 o 19 4 1 156.18 203.49 46.75 o 20 4 1 77.45 69.80 55.19 o 21 4 1 48.95 68.53 54.50 o 22 4 1 26.81 54.64 58.77 o 23 4 1 62.22 -7.44 57.83 o 24 4 1 129.73 232.95 115.57 o -23 5 1 14.38 145.60 112.84 o -22 5 1 0.59 -39.06 60.88 o -21 5 1 49.94 121.63 66.88 o -20 5 1 2.42 -49.79 49.79 o -19 5 1 184.25 237.80 52.91 o -18 5 1 21.29 -26.83 40.64 o -17 5 1 19.94 -30.81 38.58 o -16 5 1 41.32 17.48 36.07 o -15 5 1 127.09 55.53 35.18 o -14 5 1 306.29 259.94 42.12 o -13 5 1 4.50 26.41 32.20 o -12 5 1 224.87 243.65 39.58 o -11 5 1 165.20 185.75 37.23 o -10 5 1 109.43 160.79 34.69 o -9 5 1 1731.15 1859.51 106.92 o -8 5 1 51.83 74.91 29.34 o -7 5 1 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