#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/43/2204341.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204341_Fobs loop_ _publ_author_name 'Beckmann, Jens' 'Dakternieks, Dainis' 'Duthie, Andrew' 'Jurkschat, Klaus' 'Sch\"urmann, Markus' _publ_section_title ; Octabutyl-1\k^2^C,2\k^2^C,3\k^2^C,4\k^2^C-di-\m~3~-oxo-1:2:3\k^3^O;2:3:4\k^2^O-di-\m~2~-phenoxy-1:2\k^2^O;3:4\k^2^O-diphenoxy-1\kO,4\kO-tetratin(IV) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1437 _journal_page_last m1438 _journal_volume 60 _journal_year 2004 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.070 _cell_angle_gamma 90.000 _cell_length_a 13.1456 _cell_length_b 17.1448 _cell_length_c 13.3802 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file hb6086Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2201 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 -15 0 1125.23 1029.05 231.30 o 0 -14 0 780.62 707.67 110.14 o 1 -14 0 1156.67 1159.65 125.09 o 7 -14 0 8653.73 8436.18 555.04 o 8 -14 0 571.63 439.39 217.53 o 1 -13 0 118.12 141.22 73.95 o 2 -13 0 368.45 403.20 91.65 o 3 -13 0 931.40 959.03 122.34 o 6 -13 0 20852.96 20096.80 1009.78 o 7 -13 0 724.62 931.10 176.62 o 8 -13 0 2442.45 2643.04 245.46 o 9 -13 0 542.10 586.12 229.73 o 0 -12 0 267.25 283.23 120.76 o 2 -12 0 2453.36 2405.45 111.72 o 3 -12 0 674.93 639.22 108.18 o 4 -12 0 512.31 631.75 107.39 o 5 -12 0 11622.79 11340.81 547.96 o 6 -12 0 1461.59 1283.95 153.81 o 7 -12 0 12900.40 12520.52 711.21 o 8 -12 0 1913.64 2202.47 214.39 o 9 -12 0 123.87 86.15 207.31 o 2 -11 0 2522.02 2563.58 111.72 o 3 -11 0 9253.50 9899.12 400.84 o 4 -11 0 2381.13 2425.51 92.05 o 5 -11 0 2152.44 2163.92 167.97 o 6 -11 0 15209.49 15168.29 717.90 o 7 -11 0 2485.27 2359.42 226.19 o 8 -11 0 2147.96 2270.13 230.91 o 9 -11 0 3721.25 3737.39 328.07 o 0 -10 0 797.85 786.34 85.36 o 1 -10 0 1711.59 1595.50 83.39 o 2 -10 0 8106.16 8241.07 350.10 o 3 -10 0 2077.08 2180.44 79.85 o 4 -10 0 6655.02 6453.60 176.23 o 5 -10 0 5760.40 5867.48 217.14 o 6 -10 0 746.34 775.33 133.75 o 7 -10 0 6133.36 6375.72 365.44 o 8 -10 0 7251.17 7348.12 464.17 o 9 -10 0 1909.63 1866.53 224.61 o 1 -9 0 7699.79 7909.85 305.65 o 2 -9 0 7423.14 7865.40 297.78 o 3 -9 0 13491.57 13383.97 371.34 o 4 -9 0 788.32 848.50 52.32 o 5 -9 0 6616.64 6515.36 241.13 o 6 -9 0 5070.69 4734.98 302.50 o 7 -9 0 6100.73 6015.00 387.07 o 8 -9 0 1357.38 1451.92 205.34 o 9 -9 0 5607.22 5446.58 371.73 o 1 -8 0 2192.24 2400.73 125.48 o 2 -8 0 14881.66 15171.83 313.91 o 3 -8 0 7608.70 7601.84 210.45 o 4 -8 0 20409.74 21023.97 443.33 o 5 -8 0 1637.75 1628.15 130.99 o 6 -8 0 75.37 47.60 112.90 o 7 -8 0 2209.36 1891.32 163.64 o 8 -8 0 10383.07 10713.39 544.82 o 9 -8 0 4894.32 4850.63 344.98 o 10 -8 0 6543.38 6362.73 442.93 o 1 -7 0 286.02 335.94 46.81 o 2 -7 0 8870.12 9161.94 200.62 o 3 -7 0 21105.78 20743.89 423.26 o 4 -7 0 7918.83 7937.78 228.55 o 5 -7 0 3809.44 3528.91 219.11 o 6 -7 0 790.43 810.34 125.09 o 7 -7 0 9803.82 9226.06 462.60 o 8 -7 0 3285.35 3059.62 264.74 o 9 -7 0 13149.16 13911.87 653.39 o 10 -7 0 6527.75 6625.90 424.05 o 0 -6 0 8172.07 8688.33 303.68 o 1 -6 0 4331.55 4642.14 209.67 o 2 -6 0 1065.85 990.11 38.94 o 3 -6 0 24749.75 24463.19 604.21 o 4 -6 0 23584.04 23435.71 576.28 o 5 -6 0 6126.21 5747.11 181.34 o 6 -6 0 410.39 337.90 82.21 o 7 -6 0 2630.17 2621.41 203.76 o 8 -6 0 14932.47 13871.75 691.94 o 9 -6 0 7060.29 7595.16 415.79 o 10 -6 0 4160.09 4230.68 343.80 o 1 -5 0 30148.56 30490.78 715.54 o 2 -5 0 12930.33 13367.45 272.21 o 3 -5 0 8185.84 7406.34 319.02 o 4 -5 0 21507.46 22184.80 442.93 o 5 -5 0 14701.05 14346.15 380.39 o 6 -5 0 9814.84 9770.88 452.37 o 7 -5 0 4674.67 4701.93 289.13 o 8 -5 0 7002.49 7045.23 222.65 o 9 -5 0 9002.73 9456.18 284.80 o 10 -5 0 3150.17 3369.59 134.53 o 11 -5 0 1158.69 1107.33 77.89 o 12 -5 0 453.60 497.61 62.55 o 0 -4 0 45722.31 46259.73 1467.66 o 1 -4 0 33916.20 33659.36 813.88 o 2 -4 0 1255.51 1243.04 38.55 o 3 -4 0 34770.26 35733.98 887.44 o 4 -4 0 21535.78 21836.67 446.47 o 5 -4 0 8519.04 8619.10 195.11 o 6 -4 0 1988.20 2068.33 83.39 o 7 -4 0 8913.09 8911.76 271.42 o 8 -4 0 9660.04 9521.88 290.70 o 9 -4 0 8685.79 8537.67 276.14 o 10 -4 0 195.78 211.63 51.53 o 11 -4 0 3267.27 3140.65 189.60 o 12 -4 0 4709.42 4618.93 254.90 o 13 -4 0 2104.89 1956.22 151.84 o 1 -3 0 46527.90 45516.66 1042.03 o 2 -3 0 177.10 156.17 16.52 o 3 -3 0 1747.60 1732.39 64.91 o 4 -3 0 13981.08 14379.98 302.89 o 5 -3 0 9494.07 9168.63 254.12 o 6 -3 0 3380.19 3499.80 126.66 o 7 -3 0 3120.15 3034.05 118.80 o 8 -3 0 8684.04 8459.00 281.65 o 9 -3 0 3131.26 3159.93 137.68 o 10 -3 0 232.08 208.09 57.04 o 11 -3 0 3991.12 3862.48 203.37 o 12 -3 0 3313.61 3105.25 180.95 o 13 -3 0 6313.12 6153.46 370.16 o 14 -3 0 1873.44 1752.85 175.44 o 2 -2 0 4608.57 4688.95 83.39 o 3 -2 0 6764.20 6508.67 120.37 o 4 -2 0 14523.84 14379.98 299.35 o 5 -2 0 2553.49 2629.67 99.92 o 6 -2 0 18.46 83.79 35.40 o 7 -2 0 3981.92 3974.99 154.99 o 8 -2 0 3672.56 3777.91 151.45 o 9 -2 0 2483.47 2314.97 115.26 o 10 -2 0 274.01 313.12 70.02 o 11 -2 0 2156.76 1971.17 135.71 o 12 -2 0 17842.29 17085.96 903.96 o 13 -2 0 3507.21 3149.31 273.78 o 14 -2 0 1996.56 1793.37 214.39 o 2 -1 0 3471.82 3456.14 62.55 o 3 -1 0 581.96 645.12 23.21 o 4 -1 0 3146.64 3278.73 74.74 o 5 -1 0 2684.97 2684.35 73.17 o 6 -1 0 164.55 212.81 20.85 o 7 -1 0 504.82 570.38 30.68 o 8 -1 0 942.98 997.98 40.91 o 9 -1 0 133.98 179.38 23.21 o 10 -1 0 200.31 193.54 75.92 o 11 -1 0 7884.96 7942.50 341.84 o 12 -1 0 6847.60 6549.58 436.25 o 13 -1 0 9402.49 9034.10 542.06 o 14 -1 0 899.33 922.84 168.76 o 15 -1 0 136.32 87.33 190.39 o 2 0 0 18660.88 18316.02 308.01 o 3 0 0 402.50 293.06 25.96 o 4 0 0 4438.30 4792.01 102.67 o 5 0 0 56.10 65.69 20.06 o 6 0 0 730.97 722.22 35.80 o 7 0 0 44.14 62.15 28.72 o 8 0 0 3798.49 3726.38 106.21 o 9 0 0 27.89 99.13 32.26 o 10 0 0 264.87 295.42 45.24 o 11 0 0 2322.08 2218.99 84.18 o 12 0 0 23418.76 23542.31 628.60 o 13 0 0 3144.30 3318.06 254.51 o 14 0 0 1824.16 1851.98 210.06 o 15 0 0 11.88 -7.47 174.26 o 2 1 0 3479.93 3307.84 73.17 o 3 1 0 583.94 639.22 25.57 o 4 1 0 3137.02 3119.41 68.05 o 5 1 0 2653.60 2580.10 66.09 o 6 1 0 163.14 208.09 30.68 o 7 1 0 509.52 559.76 39.73 o 8 1 0 944.55 932.68 53.89 o 9 1 0 128.10 108.57 45.24 o 10 1 0 213.50 222.65 46.02 o 11 1 0 7920.96 8337.44 232.48 o 12 1 0 6860.58 6891.81 228.55 o 13 1 0 9390.07 9284.68 304.07 o 14 1 0 898.24 918.91 202.58 o 15 1 0 133.77 314.69 196.68 o 2 2 0 4642.76 4761.33 105.03 o 3 2 0 6816.04 6325.36 132.17 o 4 2 0 14461.25 14213.98 248.22 o 5 2 0 2569.14 2569.48 65.69 o 6 2 0 21.67 43.27 35.01 o 7 2 0 3987.54 4098.51 103.85 o 8 2 0 3660.99 3814.10 117.22 o 9 2 0 2488.89 2469.17 91.26 o 10 2 0 275.23 295.81 60.19 o 11 2 0 2127.97 2036.08 107.39 o 12 2 0 17818.38 17633.53 533.41 o 13 2 0 3496.06 3325.54 160.89 o 14 2 0 2001.08 1936.55 231.30 o 15 2 0 948.58 947.62 238.77 o 16 2 0 1575.56 1418.09 309.97 o 1 3 0 46530.77 46154.32 847.32 o 2 3 0 206.14 202.58 18.49 o 3 3 0 1747.00 1765.04 43.27 o 4 3 0 14043.41 14452.36 310.37 o 5 3 0 9474.11 9430.62 215.17 o 6 3 0 3384.86 3398.31 105.03 o 7 3 0 3124.23 3105.64 88.51 o 8 3 0 8676.78 8888.95 199.44 o 9 3 0 3130.81 3135.15 120.37 o 10 3 0 220.74 163.64 59.01 o 11 3 0 4023.85 4144.92 154.99 o 12 3 0 3300.19 3034.44 160.89 o 13 3 0 6327.84 6055.12 261.20 o 14 3 0 1869.53 2005.79 261.20 o 15 3 0 1125.46 1118.35 270.64 o 16 3 0 1981.37 1819.33 336.72 o 0 4 0 45532.90 45644.51 1050.29 o 1 4 0 33930.73 33472.11 805.23 o 2 4 0 1257.47 1269.01 34.22 o 3 4 0 34656.76 35320.95 592.81 o 4 4 0 21547.04 21326.08 370.55 o 5 4 0 8528.68 8594.31 164.82 o 6 4 0 1981.46 2095.47 76.71 o 7 4 0 8941.64 9082.09 195.90 o 8 4 0 9645.77 9714.23 217.93 o 9 4 0 8685.05 8639.16 243.50 o 10 4 0 192.08 211.63 68.05 o 11 4 0 3235.87 3168.19 139.25 o 12 4 0 4722.41 4625.62 214.39 o 13 4 0 2093.48 1936.95 164.82 o 14 4 0 1138.40 1035.74 260.80 o 15 4 0 1982.19 1922.79 333.58 o 16 4 0 2664.12 2740.20 368.59 o 1 5 0 30168.34 30726.80 597.92 o 2 5 0 13022.10 13529.91 361.90 o 3 5 0 8219.38 7971.22 156.95 o 4 5 0 21485.95 22400.37 394.94 o 5 5 0 14726.51 14927.55 259.23 o 6 5 0 9816.69 9829.88 233.66 o 7 5 0 4654.91 4679.12 135.71 o 8 5 0 7020.09 7165.99 176.62 o 9 5 0 9034.16 9302.77 265.13 o 10 5 0 3145.73 3208.31 140.43 o 11 5 0 1172.63 1044.00 97.95 o 12 5 0 444.83 501.54 147.91 o 13 5 0 2217.14 2040.01 166.39 o 14 5 0 2183.27 2557.68 316.27 o 15 5 0 2241.87 2247.31 356.79 o 16 5 0 1924.89 2017.98 374.88 o 0 6 0 8102.91 8584.87 323.35 o 1 6 0 4282.28 4289.29 122.34 o 2 6 0 1054.96 945.66 55.46 o 3 6 0 24779.04 25168.90 385.11 o 4 6 0 23586.99 24097.75 431.53 o 5 6 0 6114.92 5891.87 114.86 o 6 6 0 417.45 385.89 31.08 o 7 6 0 2633.42 2846.41 103.06 o 8 6 0 14921.03 14875.62 319.02 o 9 6 0 7034.20 6902.44 191.96 o 10 6 0 4161.76 4244.05 173.48 o 11 6 0 1132.41 1143.92 115.65 o 12 6 0 263.89 284.80 120.37 o 13 6 0 1491.96 1471.59 153.41 o 14 6 0 747.38 951.95 299.35 o 15 6 0 2788.09 2635.18 427.20 o 16 6 0 2234.55 1900.36 407.53 o 1 7 0 277.23 367.41 36.19 o 2 7 0 8946.89 8721.77 190.39 o 3 7 0 21078.50 21144.74 345.77 o 4 7 0 7914.76 7781.61 136.11 o 5 7 0 3821.36 3919.52 100.31 o 6 7 0 797.25 848.10 40.12 o 7 7 0 9816.59 9787.01 186.85 o 8 7 0 3293.85 3181.56 117.62 o 9 7 0 13117.42 13281.69 309.19 o 10 7 0 6563.19 7217.52 240.35 o 11 7 0 1068.55 1122.67 119.58 o 12 7 0 226.67 212.42 148.30 o 13 7 0 356.02 310.76 160.89 o 14 7 0 1273.45 1333.91 324.14 o 15 7 0 2007.64 1946.39 409.89 o 0 8 0 361.43 364.65 28.72 o 1 8 0 2191.35 2140.32 62.55 o 2 8 0 14784.58 14894.90 311.94 o 3 8 0 7594.14 7770.99 161.67 o 4 8 0 20465.22 21181.32 378.42 o 5 8 0 1631.78 1548.30 62.55 o 6 8 0 77.90 72.38 35.40 o 7 8 0 2206.73 2137.96 72.38 o 8 8 0 10355.52 10667.37 257.66 o 9 8 0 4920.81 4723.57 188.42 o 10 8 0 6519.24 6461.86 243.89 o 11 8 0 879.78 974.37 119.98 o 12 8 0 66.85 94.80 160.89 o 13 8 0 404.91 265.13 173.08 o 14 8 0 439.78 409.10 228.55 o 15 8 0 1602.02 1752.46 417.36 o 1 9 0 7714.81 7763.13 147.51 o 2 9 0 7519.47 7570.77 152.23 o 3 9 0 13473.29 13243.14 232.87 o 4 9 0 775.29 883.51 44.06 o 5 9 0 6614.24 6566.11 158.13 o 6 9 0 5095.33 5179.48 121.55 o 7 9 0 6090.20 6356.44 153.41 o 8 9 0 1382.25 1405.90 56.65 o 9 9 0 5594.79 5695.19 211.24 o 10 9 0 3836.02 3821.57 180.16 o 11 9 0 1407.77 1431.47 149.09 o 12 9 0 22.41 103.46 151.84 o 13 9 0 176.34 348.13 304.86 o 14 9 0 603.17 689.97 344.98 o 15 9 0 1111.33 1099.46 329.25 o 0 10 0 776.01 844.96 51.14 o 1 10 0 1678.31 1624.61 46.42 o 2 10 0 8069.98 8026.29 164.43 o 3 10 0 2060.53 2186.34 75.13 o 4 10 0 6680.71 6511.82 121.94 o 5 10 0 5756.58 5902.49 108.57 o 6 10 0 741.67 760.77 53.50 o 7 10 0 6099.27 6465.80 151.05 o 8 10 0 7247.97 7506.65 175.05 o 9 10 0 1916.56 1824.05 147.51 o 10 10 0 6237.22 6317.89 260.02 o 11 10 0 1798.98 1634.84 152.63 o 12 10 0 125.38 190.78 166.39 o 13 10 0 35.65 27.93 335.94 o 14 10 0 156.82 228.15 364.65 o 1 11 0 2625.40 2643.44 68.84 o 2 11 0 2572.78 2645.80 57.83 o 3 11 0 9242.50 9549.02 210.06 o 4 11 0 2403.43 2496.32 68.05 o 5 11 0 2162.34 2245.35 62.55 o 6 11 0 15223.15 15819.71 302.50 o 7 11 0 2482.04 2490.42 86.15 o 8 11 0 2149.10 2066.76 91.65 o 9 11 0 3721.01 3930.93 124.30 o 10 11 0 2518.59 2428.66 168.76 o 11 11 0 1587.37 1513.29 221.47 o 12 11 0 31.41 0.00 223.43 o 13 11 0 18.24 -83.00 274.18 o 14 11 0 258.62 206.91 311.94 o 0 12 0 259.11 285.98 38.16 o 1 12 0 2523.05 2567.12 84.57 o 2 12 0 2442.36 2366.11 77.10 o 3 12 0 689.69 707.67 46.02 o 4 12 0 524.41 653.39 42.48 o 5 12 0 11586.33 11557.17 207.31 o 6 12 0 1439.50 1405.11 70.02 o 7 12 0 12893.50 12953.23 278.50 o 8 12 0 1929.34 1871.65 98.74 o 9 12 0 123.69 160.49 54.68 o 10 12 0 1674.79 1634.05 217.93 o 11 12 0 2389.57 2397.58 232.48 o 12 12 0 493.22 510.99 376.45 o 13 12 0 11.46 -30.68 409.10 o 14 12 0 51.87 22.03 440.18 o 1 13 0 116.01 122.73 41.70 o 2 13 0 397.29 334.36 55.86 o 3 13 0 922.21 929.53 75.53 o 4 13 0 2507.23 2479.01 74.74 o 5 13 0 501.39 453.55 42.09 o 6 13 0 20865.21 21425.21 413.04 o 7 13 0 729.87 892.16 84.18 o 8 13 0 2439.53 2529.36 136.50 o 9 13 0 535.97 565.66 150.27 o 10 13 0 482.95 534.98 226.19 o 11 13 0 620.89 707.28 372.52 o 12 13 0 278.73 239.56 289.13 o 13 13 0 130.46 210.06 311.15 o 0 14 0 800.36 758.41 95.59 o 1 14 0 1150.64 1193.87 81.82 o 2 14 0 761.71 725.37 90.87 o 3 14 0 618.36 573.53 61.76 o 4 14 0 275.15 197.86 59.01 o 5 14 0 9606.73 9743.74 207.70 o 6 14 0 1087.42 1173.42 90.08 o 7 14 0 8626.49 8970.77 277.32 o 8 14 0 577.86 559.76 89.69 o 9 14 0 6.32 74.35 304.07 o 10 14 0 215.78 277.72 248.61 o 11 14 0 1818.38 1613.60 411.46 o 12 14 0 712.05 658.89 437.03 o 1 15 0 1459.73 1552.23 108.96 o 2 15 0 1224.88 1266.25 101.88 o 3 15 0 15.05 14.95 81.82 o 4 15 0 1422.63 1229.28 99.13 o 5 15 0 448.57 450.01 38.55 o 6 15 0 11897.49 12375.37 269.46 o 7 15 0 815.27 744.25 158.92 o 8 15 0 1120.04 1386.62 341.44 o 9 15 0 184.88 203.37 351.28 o 10 15 0 1057.26 959.82 400.06 o 11 15 0 714.07 670.69 328.07 o 12 15 0 477.63 1053.44 453.55 o 0 16 0 1906.99 2191.85 191.57 o 1 16 0 1591.61 1467.66 119.98 o 2 16 0 2616.93 2690.64 152.63 o 3 16 0 543.71 701.38 107.00 o 4 16 0 306.02 287.95 84.18 o 5 16 0 4954.15 4613.03 193.93 o 6 16 0 441.95 267.49 136.89 o 7 16 0 3972.18 3591.06 241.92 o 8 16 0 939.46 1008.99 353.24 o 9 16 0 658.07 703.34 382.35 o 10 16 0 1141.64 1292.61 446.87 o 11 16 0 1543.73 1385.44 341.05 o 1 17 0 2547.07 2732.73 199.44 o 2 17 0 2402.86 2441.64 171.51 o 3 17 0 2299.64 2343.69 164.03 o 4 17 0 168.16 147.12 96.38 o 5 17 0 494.53 468.90 161.28 o 6 17 0 2858.53 2625.73 241.53 o 7 17 0 794.19 857.54 273.78 o 8 17 0 252.87 271.03 385.50 o 9 17 0 1406.37 1348.07 454.34 o 10 17 0 1508.65 1569.15 524.36 o 0 18 0 909.65 1036.53 247.43 o 1 18 0 1213.01 1318.96 177.80 o 2 18 0 2311.94 2338.97 219.89 o 3 18 0 1791.27 1747.74 197.86 o 4 18 0 1613.91 1423.99 173.08 o 5 18 0 1146.36 744.25 278.11 o 6 18 0 71.82 33.83 364.26 o 7 18 0 912.47 823.71 397.70 o 8 18 0 1198.73 1269.40 351.28 o 9 18 0 678.85 428.38 467.32 o 1 19 0 444.74 400.45 178.59 o 2 19 0 3081.65 3030.51 238.77 o 3 19 0 1751.50 1786.68 217.53 o 4 19 0 442.79 630.96 265.92 o 5 19 0 389.50 367.80 273.39 o 6 19 0 266.10 274.96 295.42 o 7 19 0 422.47 525.15 425.23 o 8 19 0 133.92 20.06 325.71 o 0 20 0 30.46 18.88 268.67 o 1 20 0 679.04 662.43 198.65 o 2 20 0 322.13 351.67 188.82 o 3 20 0 2725.39 2656.81 360.33 o 4 20 0 1126.86 937.40 393.37 o 5 20 0 186.94 111.72 403.20 o 6 20 0 13.22 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