#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/43/2204386.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204386_Fobs loop_ _publ_author_name 'Teo, Yin Yin' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; Bis[1,3-bis(diphenylphosphino)propane-\k^2^P,P']silver(I) hemi[cyclopentyldiphenylbis(trifluoroacetato-\kO)stannate(IV)] hemi[triphenylbis(trifluoroacetato-\kO)stannate(IV)] ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1478 _journal_page_last m1480 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.372 _cell_angle_beta 93.985 _cell_angle_gamma 105.418 _cell_length_a 10.6019 _cell_length_b 18.0331 _cell_length_c 18.3529 _exptl_crystal_F_000 1530.00 _reflns_d_resolution_high 0.7990 _[local]_cod_data_source_file sj6007Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [(Ph2CH2CH2CH2Ph2)2Ag]2 [Ph3Sn(O2CCF3)2][Ph2CpSn(O2CCF3)2] co-crystal' _shelx_refln_list_code 4 _shelx_f_calc_maximum 268.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 41600.10 40465.98 1135.16 o 3 0 0 1373.23 1177.25 25.04 o 4 0 0 3541.17 3958.57 73.09 o 5 0 0 7823.32 8603.17 152.39 o 6 0 0 5988.10 6408.84 117.76 o 7 0 0 4987.17 5216.60 99.92 o 8 0 0 1595.48 1613.27 42.04 o 9 0 0 843.14 841.70 31.40 o 10 0 0 911.89 929.83 35.85 o 11 0 0 1027.75 1057.25 40.38 o 12 0 0 273.08 248.89 33.75 o -12 1 0 60.97 57.33 24.99 o -11 1 0 47.09 62.11 23.27 o -10 1 0 606.59 690.41 31.04 o -9 1 0 3794.86 3753.17 79.88 o -8 1 0 148.66 161.13 20.67 o -7 1 0 4395.46 4876.62 94.37 o -6 1 0 4169.06 4257.23 91.58 o -5 1 0 3909.49 4276.90 134.09 o -4 1 0 17120.57 16872.41 288.91 o -3 1 0 223.35 524.17 24.65 o -2 1 0 213.06 126.64 10.84 o -1 1 0 1000.13 953.26 30.75 o 2 1 0 31399.30 31735.39 891.49 o 3 1 0 5267.21 4888.84 86.77 o 4 1 0 5148.40 5255.83 94.56 o 5 1 0 3464.61 3885.75 73.58 o 6 1 0 91.57 37.31 11.77 o 7 1 0 1139.47 1158.76 51.69 o 8 1 0 36.13 10.34 16.44 o 9 1 0 2901.28 2790.24 110.40 o 10 1 0 4.33 29.27 20.69 o 11 1 0 4.66 8.88 24.83 o 12 1 0 174.20 196.20 33.05 o -12 2 0 125.36 148.99 53.09 o -11 2 0 545.29 639.25 31.98 o -10 2 0 100.00 36.49 20.67 o -9 2 0 623.27 604.76 27.20 o -8 2 0 639.23 652.30 30.55 o -7 2 0 3102.93 2813.75 60.31 o -6 2 0 1247.11 1248.98 32.13 o -5 2 0 5230.95 5320.69 98.04 o -4 2 0 4098.92 3872.60 80.64 o -3 2 0 7435.62 7376.02 215.36 o -2 2 0 7059.42 6490.21 188.00 o -1 2 0 1457.21 1417.02 44.29 o 1 2 0 4973.52 4407.22 127.18 o 2 2 0 12282.84 12158.83 344.43 o 3 2 0 11377.57 10453.05 179.56 o 4 2 0 20.31 31.52 8.17 o 5 2 0 22439.59 22642.32 386.36 o 6 2 0 930.93 966.52 27.19 o 7 2 0 5201.21 5093.41 97.80 o 8 2 0 1009.75 1067.58 33.44 o 9 2 0 14.51 14.23 18.36 o 10 2 0 1734.98 1565.90 46.73 o 11 2 0 888.82 1030.35 56.95 o 12 2 0 527.22 484.63 39.41 o -13 3 0 100.35 88.31 58.51 o -12 3 0 42.21 33.73 49.84 o -11 3 0 1050.07 1032.25 49.99 o -10 3 0 420.35 423.10 26.46 o -9 3 0 3544.07 3447.58 75.53 o -8 3 0 366.92 353.08 21.03 o -7 3 0 1341.49 1737.16 42.22 o -6 3 0 8572.44 8830.49 158.69 o -5 3 0 163.27 209.34 33.86 o -4 3 0 10048.99 10247.65 178.81 o -3 3 0 4423.25 4890.89 146.69 o -2 3 0 3369.03 2828.35 86.68 o -1 3 0 1616.00 1527.54 48.35 o 0 3 0 2244.58 1726.24 52.01 o 1 3 0 364.82 514.82 18.56 o 2 3 0 72214.02 63330.24 1436.08 o 3 3 0 7916.36 8830.96 232.63 o 4 3 0 644.38 1016.07 23.90 o 5 3 0 2309.44 2390.44 48.47 o 6 3 0 357.65 399.71 17.43 o 7 3 0 342.27 411.79 21.44 o 8 3 0 362.87 366.59 39.48 o 9 3 0 1853.95 1906.48 49.77 o 10 3 0 207.93 196.45 31.08 o 11 3 0 98.72 104.83 39.14 o 12 3 0 78.26 65.63 37.38 o -13 4 0 20.59 43.21 55.26 o -12 4 0 106.43 185.42 52.82 o -11 4 0 23.39 -18.56 37.38 o -10 4 0 14.69 -25.19 25.19 o -9 4 0 1.13 -16.71 18.11 o -8 4 0 1392.41 1288.71 46.13 o -7 4 0 2124.16 2155.79 51.32 o -6 4 0 798.14 812.38 32.56 o -5 4 0 140.75 134.08 12.77 o -4 4 0 1005.72 1011.77 42.66 o -3 4 0 2107.02 1835.54 62.44 o -2 4 0 6604.10 8304.76 240.14 o -1 4 0 8375.49 8893.54 254.23 o 0 4 0 15851.41 14409.23 407.69 o 1 4 0 4453.21 4356.59 86.92 o 2 4 0 3199.48 3062.01 51.18 o 3 4 0 5804.46 5552.00 97.45 o 4 4 0 531.87 621.96 17.70 o 5 4 0 3786.12 3239.92 62.73 o 6 4 0 2.33 -1.83 11.60 o 7 4 0 6435.30 5807.34 174.55 o 8 4 0 199.01 199.36 33.87 o 9 4 0 5.71 -20.39 20.93 o 10 4 0 1322.19 1169.11 47.77 o 11 4 0 632.63 556.44 68.33 o -13 5 0 0.26 -9.35 52.28 o -12 5 0 635.02 591.76 59.73 o -11 5 0 1943.77 2085.03 99.28 o -10 5 0 220.57 213.87 39.82 o -9 5 0 7493.29 7424.32 214.54 o -8 5 0 1307.50 1338.76 60.08 o -7 5 0 204.81 202.44 17.63 o -6 5 0 8835.78 8908.93 139.92 o -5 5 0 52.41 101.52 11.05 o -4 5 0 5729.78 5901.62 129.94 o -3 5 0 772.34 577.95 49.91 o -2 5 0 10929.96 12940.59 268.69 o -1 5 0 95.75 106.64 8.86 o 0 5 0 2.31 -4.51 4.51 o 1 5 0 10840.72 9925.15 188.02 o 2 5 0 4377.42 4598.10 68.04 o 3 5 0 19930.17 19878.90 330.24 o 4 5 0 802.13 932.83 18.96 o 5 5 0 63.29 71.18 11.83 o 6 5 0 350.35 334.98 17.00 o 7 5 0 1226.57 1298.02 34.81 o 8 5 0 724.39 734.64 33.89 o 9 5 0 665.43 687.39 35.77 o 10 5 0 7.42 -32.15 39.14 o 11 5 0 147.12 190.18 30.82 o -13 6 0 132.34 149.67 50.52 o -12 6 0 5.40 -15.98 39.82 o -11 6 0 827.11 798.04 62.03 o -10 6 0 786.43 727.47 59.19 o -9 6 0 7.81 -25.33 29.39 o -8 6 0 1527.38 1591.19 52.37 o -7 6 0 244.69 224.70 19.28 o -6 6 0 527.61 604.76 30.61 o -5 6 0 1806.13 1753.52 40.30 o -4 6 0 3158.55 3788.51 127.18 o -3 6 0 1570.97 1843.29 46.42 o -2 6 0 10150.04 10255.08 214.53 o -1 6 0 144.21 175.99 10.63 o 0 6 0 2416.34 2291.41 41.90 o 1 6 0 2.09 40.17 5.80 o 2 6 0 35.92 47.75 5.44 o 3 6 0 6440.93 6280.20 92.87 o 4 6 0 1108.73 1106.22 30.03 o 5 6 0 3101.40 3140.29 61.65 o 6 6 0 815.23 907.80 26.75 o 7 6 0 1973.82 1998.78 93.52 o 8 6 0 2693.18 2491.84 70.72 o 9 6 0 77.12 96.57 24.17 o 10 6 0 1630.44 1598.59 58.08 o 11 6 0 40.61 59.88 28.89 o -13 7 0 232.51 218.74 59.32 o -12 7 0 1194.33 1210.33 81.40 o -11 7 0 218.42 247.05 44.43 o -10 7 0 767.23 915.74 61.63 o -9 7 0 3454.89 3306.06 125.42 o -8 7 0 597.20 614.24 47.27 o -7 7 0 325.21 399.56 36.71 o -6 7 0 11651.04 12604.47 194.02 o -5 7 0 1783.30 2146.11 58.11 o -4 7 0 9229.05 9861.62 210.92 o -3 7 0 277.40 157.58 13.79 o -2 7 0 10915.22 12121.01 253.35 o -1 7 0 3805.22 3890.75 69.94 o 0 7 0 2588.06 2659.54 48.75 o 1 7 0 14866.11 14347.06 244.28 o 2 7 0 5739.91 6423.63 131.96 o 3 7 0 10216.27 10535.05 153.36 o 4 7 0 987.35 1052.83 41.41 o 5 7 0 386.50 473.11 22.17 o 6 7 0 325.81 443.01 24.03 o 7 7 0 134.01 139.31 20.83 o 8 7 0 296.36 315.55 26.01 o 9 7 0 868.80 940.00 42.31 o 10 7 0 107.97 53.51 27.25 o 11 7 0 24.05 99.67 34.54 o -13 8 0 635.12 582.82 65.28 o -12 8 0 14.07 38.20 47.68 o -11 8 0 77.30 42.12 42.39 o -10 8 0 892.07 1011.63 64.47 o -9 8 0 1375.25 1362.30 70.70 o -8 8 0 3345.86 3521.96 127.86 o -7 8 0 533.39 564.37 40.36 o -6 8 0 220.95 278.01 18.32 o -5 8 0 27.85 -8.50 14.96 o -4 8 0 7924.15 8300.02 179.83 o -3 8 0 5676.00 5442.97 120.32 o -2 8 0 27.23 24.75 8.28 o -1 8 0 57.78 39.42 7.72 o 0 8 0 158.06 260.25 10.25 o 1 8 0 1467.09 1642.38 32.26 o 2 8 0 1276.80 1703.26 38.97 o 3 8 0 12893.31 12818.29 220.42 o 4 8 0 368.35 352.59 15.87 o 5 8 0 4311.57 4151.02 98.26 o 6 8 0 162.59 174.86 20.11 o 7 8 0 2.53 20.58 19.24 o 8 8 0 1793.58 1766.96 56.59 o 9 8 0 20.07 -14.41 22.59 o 10 8 0 1223.60 1244.44 52.18 o -13 9 0 686.59 633.47 67.04 o -12 9 0 643.84 696.45 67.86 o -11 9 0 108.39 54.72 39.14 o -10 9 0 126.89 117.16 37.52 o -9 9 0 257.08 293.91 42.80 o -8 9 0 330.59 314.77 38.06 o -7 9 0 61.23 58.44 15.87 o -6 9 0 2194.74 2185.37 137.00 o -5 9 0 192.10 372.75 27.97 o -4 9 0 9983.79 9883.50 175.28 o -3 9 0 8949.25 9281.76 163.85 o -2 9 0 711.59 620.59 25.89 o -1 9 0 2677.22 3086.28 58.01 o 0 9 0 1699.97 1972.90 38.80 o 1 9 0 12024.54 11918.04 204.34 o 2 9 0 190.31 166.84 10.80 o 3 9 0 4342.01 4344.18 79.11 o 4 9 0 2118.07 2054.99 55.74 o 5 9 0 571.75 549.46 24.71 o 6 9 0 4840.41 4921.76 117.47 o 7 9 0 70.17 108.06 22.11 o 8 9 0 181.41 193.07 25.51 o 9 9 0 698.01 784.54 47.41 o 10 9 0 240.00 183.14 30.35 o -12 10 0 96.86 103.75 44.97 o -11 10 0 34.58 4.20 42.26 o -10 10 0 265.99 248.81 41.99 o -9 10 0 489.78 472.29 46.05 o -8 10 0 4273.14 4403.56 154.41 o -7 10 0 492.48 623.10 26.33 o -6 10 0 2260.09 2113.81 53.81 o -5 10 0 1398.29 1739.04 41.74 o -4 10 0 2608.22 2628.76 54.75 o -3 10 0 5222.11 6076.93 111.02 o -2 10 0 172.61 195.85 22.28 o -1 10 0 28.53 28.51 11.92 o 0 10 0 1567.39 1483.14 31.56 o 1 10 0 1404.30 1502.86 31.61 o 2 10 0 3426.44 3435.57 63.90 o 3 10 0 3477.16 3349.76 79.01 o 4 10 0 5.77 1.67 14.15 o 5 10 0 2507.19 2613.53 67.57 o 6 10 0 201.92 252.15 22.62 o 7 10 0 2.65 0.34 21.15 o 8 10 0 1038.71 1104.05 44.46 o 9 10 0 5.45 2.45 35.69 o -12 11 0 35.67 40.63 42.80 o -11 11 0 88.75 37.65 38.60 o -10 11 0 2.86 6.09 35.35 o -9 11 0 13.11 -1.76 34.40 o -8 11 0 2992.72 2722.43 108.22 o -7 11 0 1256.32 1221.64 36.86 o -6 11 0 1642.27 1850.82 45.26 o -5 11 0 1023.01 1231.45 33.36 o -4 11 0 1687.38 1814.20 42.15 o -3 11 0 1409.13 1169.38 30.02 o -2 11 0 31.67 41.93 11.55 o -1 11 0 6887.06 7037.26 132.36 o 0 11 0 2057.21 2183.01 46.24 o 1 11 0 7797.42 7743.28 136.12 o 2 11 0 1410.44 1338.46 37.50 o 3 11 0 2568.53 2424.13 60.81 o 4 11 0 1528.32 1442.57 42.31 o 5 11 0 28.09 32.80 16.89 o 6 11 0 4219.22 4370.47 107.60 o 7 11 0 51.05 34.55 22.30 o 8 11 0 459.71 514.68 32.88 o 9 11 0 71.96 95.36 29.50 o -12 12 0 17.22 -24.11 41.45 o -11 12 0 346.39 314.10 48.62 o -10 12 0 1531.76 1496.52 80.59 o -9 12 0 496.64 604.35 50.25 o -8 12 0 1287.65 1141.52 65.01 o -7 12 0 254.94 295.41 36.65 o -6 12 0 4671.05 4957.36 97.86 o -5 12 0 217.82 310.76 18.50 o -4 12 0 1679.29 1534.10 38.19 o -3 12 0 3040.96 2749.90 56.86 o -2 12 0 299.95 265.53 15.67 o -1 12 0 1893.23 1909.69 40.80 o 0 12 0 6.15 -8.44 15.11 o 1 12 0 204.62 175.68 15.43 o 2 12 0 616.50 631.43 24.26 o 3 12 0 2117.78 1955.05 52.33 o 4 12 0 735.76 646.99 60.75 o 5 12 0 970.50 1083.85 53.70 o 6 12 0 721.51 786.21 34.76 o 7 12 0 2.91 8.10 22.75 o 8 12 0 454.23 537.52 36.00 o -12 13 0 184.00 118.78 47.81 o -11 13 0 187.35 185.83 45.78 o -10 13 0 227.82 270.21 48.76 o -9 13 0 277.32 297.16 41.99 o -8 13 0 285.59 314.91 42.53 o -7 13 0 250.99 149.63 19.61 o -6 13 0 3784.76 3890.45 80.81 o -5 13 0 2258.48 2358.46 58.01 o -4 13 0 1.90 6.29 14.02 o -3 13 0 2288.70 2293.05 50.12 o -2 13 0 664.04 683.90 22.76 o -1 13 0 4246.59 4390.47 83.00 o 0 13 0 534.36 524.07 23.88 o 1 13 0 870.65 1008.83 32.80 o 2 13 0 384.16 391.42 20.54 o 3 13 0 220.65 237.85 19.31 o 4 13 0 2589.81 2582.08 67.95 o 5 13 0 159.75 146.18 21.51 o 6 13 0 1340.24 1369.26 47.88 o 7 13 0 59.96 26.26 24.58 o 8 13 0 330.28 404.63 34.93 o -12 14 0 0.81 26.14 48.22 o -11 14 0 747.32 749.41 65.15 o -10 14 0 528.13 468.10 53.09 o -9 14 0 106.35 176.48 39.14 o -8 14 0 182.49 146.12 26.01 o -7 14 0 728.73 918.01 32.74 o -6 14 0 174.86 120.50 17.46 o -5 14 0 3461.27 3033.01 65.75 o -4 14 0 58.95 49.35 15.54 o -3 14 0 2465.33 2438.13 53.35 o -2 14 0 568.64 488.54 21.01 o -1 14 0 858.01 782.36 43.07 o 0 14 0 622.09 611.70 25.81 o 1 14 0 90.51 69.68 15.61 o 2 14 0 90.43 68.97 15.41 o 3 14 0 787.74 722.28 29.78 o 4 14 0 663.89 675.87 31.03 o 5 14 0 487.10 578.71 31.36 o 6 14 0 60.69 35.87 23.11 o 7 14 0 11.09 -9.43 24.99 o -11 15 0 195.50 205.47 49.57 o -10 15 0 599.93 692.12 64.34 o -9 15 0 252.75 199.24 45.64 o -8 15 0 433.62 455.61 26.71 o -7 15 0 922.02 971.26 34.27 o -6 15 0 678.07 538.26 25.89 o -5 15 0 24.97 -0.96 17.15 o -4 15 0 36.57 -14.86 14.86 o -3 15 0 3.92 -2.52 13.99 o -2 15 0 1900.54 1962.41 78.08 o -1 15 0 2720.05 2963.29 76.19 o 0 15 0 1.57 2.61 15.58 o 1 15 0 167.41 185.33 19.24 o 2 15 0 525.18 448.92 24.57 o 3 15 0 0.27 12.60 19.19 o 4 15 0 2449.26 2517.81 69.33 o 5 15 0 116.78 150.09 28.17 o 6 15 0 877.20 756.05 37.10 o 7 15 0 70.45 37.24 47.41 o -11 16 0 1456.69 1517.38 94.68 o -10 16 0 479.34 456.45 56.07 o -9 16 0 1.24 12.05 42.66 o -8 16 0 5.86 9.32 20.02 o -7 16 0 6.65 -4.37 19.18 o -6 16 0 175.17 172.90 20.78 o -5 16 0 483.11 418.34 33.67 o -4 16 0 857.93 1026.26 33.16 o -3 16 0 3978.93 3846.85 116.82 o -2 16 0 13.28 20.53 19.41 o -1 16 0 122.85 103.45 20.59 o 0 16 0 982.13 1055.03 37.92 o 1 16 0 62.42 24.60 18.74 o 2 16 0 957.25 916.13 60.41 o 3 16 0 450.38 508.69 28.72 o 4 16 0 430.06 506.42 41.78 o 5 16 0 52.52 85.19 34.13 o 6 16 0 21.66 -0.12 26.81 o -11 17 0 133.66 164.02 53.50 o -10 17 0 57.26 -5.01 49.84 o -9 17 0 3.84 -37.65 43.07 o -8 17 0 91.29 91.45 23.24 o -7 17 0 303.77 293.76 24.39 o -6 17 0 222.10 135.02 21.86 o -5 17 0 96.82 96.53 19.07 o -4 17 0 1.02 -22.25 34.54 o -3 17 0 506.24 518.94 30.68 o -2 17 0 217.68 182.03 22.02 o -1 17 0 453.78 442.54 34.34 o 0 17 0 21.42 14.00 18.88 o 1 17 0 435.76 368.82 34.40 o 2 17 0 263.78 226.61 23.60 o 3 17 0 6.62 -8.14 20.52 o 4 17 0 463.86 458.48 30.68 o 5 17 0 17.14 -26.34 26.34 o -10 18 0 254.82 276.58 60.00 o -9 18 0 56.76 9.75 49.57 o -8 18 0 199.31 293.49 27.58 o -7 18 0 387.73 434.18 35.23 o -6 18 0 1234.62 1363.32 43.52 o -5 18 0 443.25 491.16 46.86 o -4 18 0 282.53 354.50 28.05 o -3 18 0 1098.47 1088.57 62.10 o -2 18 0 67.91 59.77 20.99 o -1 18 0 8.50 -7.13 20.54 o 0 18 0 936.28 998.35 39.51 o 1 18 0 5.14 -26.41 28.04 o 2 18 0 722.56 796.45 36.34 o 3 18 0 107.94 87.47 24.66 o 4 18 0 44.33 57.02 25.10 o -9 19 0 14.70 35.35 54.04 o -8 19 0 418.39 564.17 34.22 o -7 19 0 17.16 -12.14 35.28 o -6 19 0 4.12 5.27 24.32 o -5 19 0 30.60 -21.66 21.66 o -4 19 0 146.34 128.57 24.18 o -3 19 0 7.68 -19.97 19.97 o -2 19 0 853.24 836.45 37.81 o -1 19 0 118.02 56.90 22.76 o 0 19 0 38.36 49.07 22.06 o 1 19 0 1.23 -8.44 21.73 o 2 19 0 348.99 350.29 30.60 o 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