#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204390.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204390_Fobs loop_ _publ_author_name 'Liu, Qing-Xiang' 'Song, Hai-Bin' _publ_section_title ; Bis[N-(9-anthrylmethyl)propylamino]methane ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1762 _journal_page_last o1763 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.6944 _cell_length_b 12.0314 _cell_length_c 23.6936 _exptl_crystal_F_000 2192.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file su61372sup2.hkl _[local]_cod_data_source_block 2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 020317C in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 555.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 48782.65 51552.88 403.53 o 6 0 0 49404.41 46710.55 403.53 o 10 0 0 3026.71 3376.98 130.17 o 12 0 0 2428.19 2272.40 122.73 o 14 0 0 452.07 416.54 79.96 o 16 0 0 3497.25 2692.66 145.05 o 18 0 0 2694.76 2612.70 211.99 o 20 0 0 92.08 197.11 119.01 o 22 0 0 3.55 -55.79 122.73 o 24 0 0 97.97 14.88 137.61 o 2 1 0 3377.56 3164.00 40.70 o 4 1 0 17797.47 14375.39 701.06 o 6 1 0 4263.42 3689.42 71.65 o 8 1 0 3285.11 3436.28 79.54 o 10 1 0 670.59 700.05 57.19 o 12 1 0 436.24 457.22 81.82 o 14 1 0 72.67 98.87 53.48 o 16 1 0 971.07 1025.77 153.41 o 18 1 0 126.24 86.85 74.11 o 20 1 0 4.46 -52.62 52.62 o 22 1 0 23.43 -0.32 86.75 o 24 1 0 10.96 -97.20 97.20 o 0 2 0 256.86 278.68 21.67 o 2 2 0 113.82 115.24 17.96 o 4 2 0 125.43 128.95 24.50 o 6 2 0 63.47 69.24 22.79 o 8 2 0 38.38 43.41 22.20 o 10 2 0 4.24 -22.31 22.31 o 12 2 0 5.77 -5.45 24.50 o 14 2 0 4.70 21.14 33.15 o 16 2 0 1.03 29.16 61.42 o 18 2 0 2.57 40.59 68.22 o 20 2 0 0.01 27.93 99.49 o 22 2 0 0.66 20.38 59.33 o 24 2 0 0.00 331.00 150.63 o 2 3 0 8104.19 7406.59 92.06 o 4 3 0 0.03 26.69 25.11 o 6 3 0 107.38 92.95 26.11 o 8 3 0 415.61 455.23 40.41 o 10 3 0 4478.51 3907.56 198.85 o 12 3 0 6.28 11.50 29.33 o 14 3 0 100.35 125.28 35.76 o 16 3 0 2337.46 2054.76 165.50 o 18 3 0 1582.79 1231.05 97.34 o 20 3 0 26.76 -65.51 91.12 o 22 3 0 58.35 118.80 77.03 o 24 3 0 27.11 181.64 79.37 o 0 4 0 7626.27 7627.96 165.50 o 2 4 0 1264.21 1733.73 173.30 o 4 4 0 646.39 664.63 40.46 o 6 4 0 4327.26 3686.69 115.52 o 8 4 0 21789.48 20627.55 316.17 o 10 4 0 4103.51 3707.40 203.51 o 12 4 0 44.78 69.23 33.82 o 14 4 0 15.28 -27.05 32.58 o 16 4 0 15.67 -5.24 60.88 o 18 4 0 199.58 190.02 68.30 o 20 4 0 107.54 83.29 125.52 o 22 4 0 35.61 45.31 69.10 o 2 5 0 668.92 784.80 41.14 o 4 5 0 43.89 29.66 30.25 o 6 5 0 297.79 272.99 36.90 o 8 5 0 20.48 -3.50 28.17 o 10 5 0 42.14 8.00 31.27 o 12 5 0 228.93 219.96 40.48 o 14 5 0 137.64 102.97 41.28 o 16 5 0 261.51 163.70 75.31 o 18 5 0 8.49 -51.54 53.24 o 20 5 0 0.64 -18.37 58.41 o 22 5 0 10.70 47.55 113.43 o 0 6 0 32.05 41.83 42.72 o 2 6 0 23.31 8.85 31.48 o 4 6 0 9.91 -20.65 29.95 o 6 6 0 85.54 101.09 36.27 o 8 6 0 100.62 66.61 35.94 o 10 6 0 4.17 19.22 35.40 o 12 6 0 67.98 27.21 37.42 o 14 6 0 0.33 -38.25 38.25 o 16 6 0 24.46 18.29 56.50 o 18 6 0 2.20 -13.02 57.86 o 20 6 0 0.72 23.21 88.33 o 22 6 0 3.42 58.40 71.00 o 2 7 0 5648.52 5422.93 104.81 o 4 7 0 503.76 585.54 53.49 o 6 7 0 14.73 -1.86 38.77 o 8 7 0 0.76 8.61 37.87 o 10 7 0 167.75 200.86 45.32 o 12 7 0 910.64 838.94 64.37 o 14 7 0 656.76 494.89 59.99 o 16 7 0 355.37 328.80 67.25 o 18 7 0 5.66 -11.16 57.86 o 20 7 0 75.39 99.49 92.05 o 0 8 0 3904.38 3638.01 141.33 o 2 8 0 1413.23 1360.98 71.15 o 4 8 0 227.07 194.49 52.04 o 6 8 0 320.08 244.87 49.87 o 8 8 0 971.44 1044.97 62.47 o 10 8 0 4147.32 3730.01 104.25 o 12 8 0 313.44 209.78 46.01 o 14 8 0 326.60 307.52 48.01 o 16 8 0 125.57 78.93 54.46 o 18 8 0 103.16 23.42 95.77 o 20 8 0 22.35 -15.67 96.70 o 2 9 0 173.92 132.79 54.91 o 4 9 0 47.58 90.56 52.31 o 6 9 0 13.49 33.08 48.37 o 8 9 0 78.27 45.61 46.63 o 10 9 0 320.14 369.57 62.35 o 12 9 0 60.20 40.90 37.33 o 14 9 0 27.77 22.80 43.28 o 16 9 0 34.59 101.76 57.19 o 18 9 0 1.67 35.48 136.68 o 0 10 0 4.69 42.77 102.28 o 2 10 0 13.80 -22.14 54.01 o 4 10 0 83.05 77.33 55.88 o 6 10 0 569.88 570.09 93.61 o 8 10 0 81.80 48.15 47.38 o 10 10 0 8.11 37.68 39.14 o 12 10 0 0.07 -5.50 39.87 o 14 10 0 71.02 28.31 52.95 o 16 10 0 25.05 11.96 82.75 o 2 11 0 17.23 -57.45 57.45 o 4 11 0 134.36 144.86 53.27 o 6 11 0 2155.44 2215.56 213.21 o 8 11 0 711.59 785.32 70.11 o 10 11 0 46.97 21.61 39.85 o 12 11 0 27.16 68.84 41.21 o 14 11 0 38.56 90.55 137.61 o 0 12 0 182.45 9.30 89.26 o 2 12 0 318.32 428.30 83.30 o 4 12 0 25.27 87.92 62.75 o 6 12 0 125.83 201.91 52.96 o 8 12 0 0.20 -10.57 42.92 o 10 12 0 6.25 -40.70 40.70 o 12 12 0 6.06 -10.37 39.56 o 2 13 0 6.91 12.42 71.59 o 4 13 0 27.45 80.63 58.41 o 6 13 0 14.48 -56.36 56.36 o 8 13 0 8.66 -14.92 51.93 o 10 13 0 3.66 38.71 60.57 o 0 14 0 22.27 24.17 83.68 o 2 14 0 30.43 13.22 65.39 o 4 14 0 3.43 -11.81 93.91 o 1 1 1 1157.42 1089.32 83.21 o 2 1 1 1258.02 1171.81 31.06 o 3 1 1 11672.63 10260.91 177.79 o 4 1 1 316.71 331.17 15.88 o 5 1 1 11236.30 9687.91 300.18 o 6 1 1 9.38 13.99 15.85 o 7 1 1 3211.74 2873.97 43.81 o 8 1 1 1983.86 1832.99 43.20 o 9 1 1 1195.27 1177.48 48.05 o 10 1 1 1185.19 1151.48 43.85 o 11 1 1 3.61 -17.70 17.88 o 12 1 1 54.30 55.33 20.34 o 13 1 1 164.34 166.73 25.91 o 14 1 1 11.59 -20.75 34.18 o 15 1 1 778.51 957.43 73.01 o 16 1 1 0.05 58.76 44.54 o 17 1 1 1367.67 1393.58 82.94 o 18 1 1 11.46 12.55 44.71 o 19 1 1 65.01 2.85 40.62 o 20 1 1 6.66 -31.65 41.48 o 21 1 1 10.87 27.47 53.74 o 22 1 1 0.74 -0.39 63.88 o 23 1 1 28.49 69.54 68.15 o 24 1 1 4.05 26.75 70.83 o 0 2 1 490.12 400.64 22.40 o 1 2 1 27815.62 27650.03 135.44 o 2 2 1 825.44 826.43 18.34 o 3 2 1 34831.56 32166.59 286.62 o 4 2 1 165.75 127.79 16.87 o 5 2 1 99.96 102.37 19.82 o 6 2 1 60.97 64.04 16.30 o 7 2 1 28.79 23.45 14.42 o 8 2 1 16.13 -10.64 14.12 o 9 2 1 494.89 454.79 31.46 o 10 2 1 221.98 244.11 21.06 o 11 2 1 508.79 562.83 38.21 o 12 2 1 0.71 -16.61 16.61 o 13 2 1 328.74 332.12 26.61 o 14 2 1 2.80 -25.78 25.78 o 15 2 1 97.28 145.65 43.06 o 16 2 1 562.32 544.34 59.51 o 17 2 1 550.08 566.35 62.21 o 18 2 1 182.66 231.37 55.56 o 19 2 1 48.66 61.82 48.75 o 20 2 1 9.88 -9.35 43.89 o 21 2 1 64.62 151.15 74.77 o 22 2 1 1.50 23.40 46.71 o 23 2 1 32.64 74.28 46.09 o 24 2 1 3.90 -22.87 56.90 o 1 3 1 1852.69 1774.14 33.16 o 2 3 1 1486.31 1412.85 32.27 o 3 3 1 2116.76 1824.66 32.27 o 4 3 1 308.79 362.13 23.46 o 5 3 1 375.12 438.00 23.79 o 6 3 1 1263.74 1244.50 26.55 o 7 3 1 620.54 580.20 22.39 o 8 3 1 732.80 746.40 26.94 o 9 3 1 1743.44 1601.61 74.08 o 10 3 1 82.50 60.61 19.12 o 11 3 1 721.01 659.59 32.65 o 12 3 1 66.43 46.26 21.52 o 13 3 1 114.70 89.85 24.16 o 14 3 1 9.90 -23.97 26.62 o 15 3 1 14.93 22.40 45.63 o 16 3 1 813.38 774.46 63.94 o 17 3 1 530.60 526.60 58.41 o 18 3 1 199.42 174.15 50.47 o 19 3 1 312.96 251.58 71.78 o 20 3 1 27.87 12.15 45.17 o 21 3 1 6.81 44.53 51.19 o 22 3 1 2.41 -1.71 50.98 o 23 3 1 10.08 54.62 52.13 o 24 3 1 0.01 102.31 54.61 o 0 4 1 6536.22 6426.19 76.19 o 1 4 1 253.04 312.52 24.53 o 2 4 1 4664.62 4474.39 89.74 o 3 4 1 2.81 13.48 19.24 o 4 4 1 244.55 244.33 23.29 o 5 4 1 23.59 25.15 18.35 o 6 4 1 130.17 132.32 21.62 o 7 4 1 672.57 640.33 25.48 o 8 4 1 1349.83 1284.21 53.61 o 9 4 1 205.69 233.45 24.11 o 10 4 1 213.89 252.32 25.30 o 11 4 1 41.96 26.37 20.54 o 12 4 1 63.11 68.66 23.13 o 13 4 1 0.00 10.34 23.47 o 14 4 1 63.35 87.46 31.16 o 15 4 1 8.91 -22.97 36.78 o 16 4 1 0.00 -34.71 43.53 o 17 4 1 63.28 101.17 45.53 o 18 4 1 92.19 70.04 42.90 o 19 4 1 0.41 26.24 41.76 o 20 4 1 6.41 -15.64 41.54 o 21 4 1 2.83 -45.43 45.43 o 22 4 1 15.98 36.52 52.88 o 23 4 1 1.61 104.14 56.00 o 1 5 1 1175.57 1316.86 35.59 o 2 5 1 2368.55 2275.84 40.71 o 3 5 1 38.54 68.07 20.10 o 4 5 1 30.59 80.26 21.51 o 5 5 1 188.48 168.97 24.42 o 6 5 1 1162.80 1083.79 47.96 o 7 5 1 157.24 145.83 24.11 o 8 5 1 95.53 122.44 23.49 o 9 5 1 505.39 509.75 30.71 o 10 5 1 70.89 62.25 23.64 o 11 5 1 27.01 38.38 25.04 o 12 5 1 4.46 20.99 24.87 o 13 5 1 0.59 -18.56 23.75 o 14 5 1 0.08 -10.47 29.25 o 15 5 1 746.82 735.51 61.04 o 16 5 1 92.59 115.01 41.73 o 17 5 1 62.46 16.83 37.95 o 18 5 1 220.85 248.50 47.97 o 19 5 1 21.16 46.43 42.47 o 20 5 1 31.77 -5.56 43.45 o 21 5 1 13.83 -3.81 44.83 o 22 5 1 0.23 2.64 72.74 o 23 5 1 11.94 24.45 50.68 o 0 6 1 455.04 473.78 31.46 o 1 6 1 1649.45 1485.55 40.83 o 2 6 1 22.27 -13.28 21.89 o 3 6 1 774.61 783.23 34.27 o 4 6 1 0.29 10.15 22.50 o 5 6 1 584.66 497.88 35.90 o 6 6 1 126.59 145.55 27.57 o 7 6 1 1929.51 1828.06 43.86 o 8 6 1 57.92 66.27 25.27 o 9 6 1 950.10 849.50 36.61 o 10 6 1 33.41 56.11 26.44 o 11 6 1 604.80 637.66 37.91 o 12 6 1 27.31 14.31 25.79 o 13 6 1 787.70 879.72 47.96 o 14 6 1 1.35 -24.37 30.20 o 15 6 1 89.15 38.62 38.18 o 16 6 1 25.82 6.17 39.41 o 17 6 1 52.40 99.30 41.48 o 18 6 1 2.54 13.39 40.67 o 19 6 1 27.71 21.67 41.16 o 20 6 1 7.29 24.54 43.05 o 21 6 1 3.35 16.08 44.84 o 22 6 1 0.99 -3.99 52.61 o 1 7 1 153.64 211.98 30.36 o 2 7 1 85.99 87.48 26.66 o 3 7 1 653.66 825.10 39.26 o 4 7 1 75.76 100.95 29.10 o 5 7 1 87.45 35.16 28.51 o 6 7 1 99.46 135.21 29.88 o 7 7 1 5.52 34.19 28.37 o 8 7 1 132.80 173.83 29.97 o 9 7 1 28.76 48.07 28.47 o 10 7 1 38.97 49.56 28.36 o 11 7 1 275.15 226.17 32.57 o 12 7 1 3.99 20.77 27.43 o 13 7 1 398.58 369.40 36.43 o 14 7 1 0.48 -27.57 27.57 o 15 7 1 75.09 14.86 36.37 o 16 7 1 42.55 58.39 55.29 o 17 7 1 29.72 13.59 37.31 o 18 7 1 14.87 32.07 39.13 o 19 7 1 1.72 10.06 42.41 o 20 7 1 0.89 88.13 88.52 o 21 7 1 10.17 -32.58 51.27 o 0 8 1 881.38 1036.77 70.81 o 1 8 1 140.85 111.55 33.76 o 2 8 1 957.16 1022.57 44.35 o 3 8 1 8.15 66.29 33.43 o 4 8 1 137.80 139.98 35.23 o 5 8 1 39.30 17.49 30.93 o 6 8 1 6.06 3.51 30.19 o 7 8 1 94.11 93.86 32.94 o 8 8 1 51.12 69.10 30.94 o 9 8 1 111.41 170.87 33.15 o 10 8 1 1057.04 1074.16 56.27 o 11 8 1 8.55 67.92 30.61 o 12 8 1 358.08 323.66 35.16 o 13 8 1 20.24 -21.59 25.43 o 14 8 1 4.77 26.68 28.76 o 15 8 1 48.47 -3.95 35.90 o 16 8 1 1.72 27.50 35.19 o 17 8 1 37.09 21.45 38.61 o 18 8 1 0.78 -34.18 43.21 o 19 8 1 0.09 66.65 53.14 o 20 8 1 0.06 73.77 56.10 o 1 9 1 425.78 562.71 47.69 o 2 9 1 49.21 68.67 38.23 o 3 9 1 579.78 653.81 48.11 o 4 9 1 7.84 -4.84 35.49 o 5 9 1 32.82 -8.74 33.30 o 6 9 1 36.69 62.28 33.63 o 7 9 1 92.00 114.56 34.06 o 8 9 1 31.25 14.87 32.88 o 9 9 1 668.51 722.37 46.03 o 10 9 1 835.06 856.51 44.72 o 11 9 1 309.74 345.70 36.02 o 12 9 1 399.06 318.34 34.99 o 13 9 1 77.21 34.97 26.91 o 14 9 1 6.96 -27.33 27.33 o 15 9 1 47.51 62.15 37.05 o 16 9 1 14.25 -10.42 51.53 o 17 9 1 0.05 92.13 68.44 o 18 9 1 1.23 -36.28 36.28 o 19 9 1 0.06 1.71 52.61 o 0 10 1 2.01 -22.50 54.39 o 1 10 1 4.77 -41.11 41.11 o 2 10 1 1.97 -39.05 39.05 o 3 10 1 0.30 -34.35 35.27 o 4 10 1 3.40 -23.48 36.71 o 5 10 1 1014.27 1077.81 52.26 o 6 10 1 19.93 6.98 32.32 o 7 10 1 1476.12 1392.97 51.06 o 8 10 1 86.72 65.63 30.78 o 9 10 1 454.42 419.57 38.46 o 10 10 1 0.59 -1.16 27.48 o 11 10 1 230.26 168.84 32.20 o 12 10 1 11.57 3.13 26.69 o 13 10 1 0.83 -3.81 26.40 o 14 10 1 1.13 2.59 34.87 o 15 10 1 125.63 152.02 65.76 o 16 10 1 5.92 52.62 35.80 o 17 10 1 27.93 33.65 47.78 o 1 11 1 8.16 -36.22 36.22 o 2 11 1 0.04 -38.65 38.65 o 3 11 1 0.77 -39.30 39.30 o 4 11 1 29.46 -2.66 38.39 o 5 11 1 7.60 33.53 37.11 o 6 11 1 19.98 29.82 36.04 o 7 11 1 107.17 117.64 34.14 o 8 11 1 10.62 26.69 31.04 o 9 11 1 15.26 -12.75 29.14 o 10 11 1 25.68 11.30 28.69 o 11 11 1 1.09 14.80 31.34 o 12 11 1 9.50 -11.26 27.21 o 13 11 1 14.96 34.80 27.76 o 14 11 1 1.00 19.33 62.55 o 15 11 1 13.32 5.39 72.20 o 0 12 1 6.10 -57.45 57.45 o 1 12 1 38.20 -6.22 44.26 o 2 12 1 0.02 -38.25 41.53 o 3 12 1 24.21 -26.46 36.16 o 4 12 1 50.88 -43.96 46.98 o 5 12 1 1.38 -0.71 43.17 o 6 12 1 175.10 164.43 40.12 o 7 12 1 16.67 35.32 35.93 o 8 12 1 42.65 2.77 34.35 o 9 12 1 0.26 24.98 42.88 o 10 12 1 47.40 42.39 30.50 o 11 12 1 3.43 12.99 35.49 o 12 12 1 13.31 18.92 28.83 o 13 12 1 0.17 -19.99 43.66 o 1 13 1 6.39 -42.70 42.70 o 2 13 1 3.09 -21.11 42.84 o 3 13 1 118.09 131.28 45.91 o 4 13 1 32.44 66.33 52.52 o 5 13 1 189.68 193.25 51.22 o 6 13 1 18.82 42.01 38.82 o 7 13 1 52.95 -18.05 57.03 o 8 13 1 0.91 23.14 54.59 o 9 13 1 4.14 -10.44 55.86 o 10 13 1 0.97 16.94 44.02 o 0 14 1 0.05 -3.72 74.38 o 1 14 1 64.87 30.61 40.10 o 2 14 1 0.77 -13.93 40.78 o 3 14 1 50.76 58.51 44.79 o 4 14 1 1.97 36.29 92.60 o 5 14 1 2.80 24.28 41.80 o 2 0 2 64.43 58.49 8.47 o 3 0 2 0.96 -5.11 10.27 o 4 0 2 1816.62 1396.37 33.71 o 5 0 2 0.20 -23.38 33.47 o 6 0 2 72.28 60.79 25.01 o 7 0 2 158.33 192.86 29.48 o 8 0 2 2208.22 2318.90 166.43 o 9 0 2 221.26 223.52 34.35 o 10 0 2 406.76 357.14 38.81 o 11 0 2 2.95 21.76 38.12 o 12 0 2 1198.79 1045.58 102.28 o 13 0 2 137.72 98.95 43.15 o 14 0 2 457.37 391.29 60.44 o 15 0 2 43.11 116.36 80.89 o 16 0 2 977.88 979.82 131.10 o 17 0 2 590.57 533.21 82.86 o 18 0 2 629.57 639.69 139.47 o 19 0 2 18.94 -65.71 65.71 o 20 0 2 5.27 -4.46 77.72 o 21 0 2 14.69 -74.95 74.95 o 22 0 2 14.53 7.44 84.15 o 23 0 2 10.36 12.79 89.80 o 24 0 2 15.36 31.70 97.64 o 1 1 2 270.30 295.78 16.91 o 2 1 2 4989.20 4701.44 135.54 o 3 1 2 1919.94 1757.89 39.92 o 4 1 2 7659.42 6680.73 157.62 o 5 1 2 1490.34 1431.28 27.66 o 6 1 2 1536.39 1399.05 36.14 o 7 1 2 1284.05 1096.80 28.98 o 8 1 2 146.91 213.45 21.62 o 9 1 2 1252.45 1124.53 34.45 o 10 1 2 4.08 -21.52 21.52 o 11 1 2 6.70 -25.37 25.37 o 12 1 2 78.38 85.78 19.01 o 13 1 2 113.37 96.11 21.79 o 14 1 2 15.10 12.35 35.46 o 15 1 2 190.23 203.55 45.20 o 16 1 2 141.12 156.85 49.41 o 17 1 2 300.17 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1629.93 1573.27 27.06 o 6 3 2 6571.35 5952.93 80.25 o 7 3 2 1513.13 1638.73 29.79 o 8 3 2 2971.33 2639.44 69.02 o 9 3 2 94.45 98.59 18.60 o 10 3 2 28.46 18.15 17.73 o 11 3 2 66.77 89.86 21.32 o 12 3 2 148.10 146.96 23.41 o 13 3 2 71.76 53.21 23.54 o 14 3 2 142.26 160.07 32.69 o 15 3 2 5.06 22.73 30.55 o 16 3 2 637.68 779.81 64.19 o 17 3 2 133.45 125.98 47.47 o 18 3 2 20.57 30.12 43.19 o 19 3 2 47.00 0.48 41.83 o 20 3 2 75.35 52.44 46.76 o 21 3 2 0.04 56.59 50.01 o 22 3 2 4.87 51.03 52.06 o 23 3 2 0.11 68.00 56.10 o 24 3 2 13.31 94.07 56.31 o 0 4 2 75.88 103.38 32.70 o 1 4 2 1.99 17.01 20.75 o 2 4 2 1697.80 1624.75 35.60 o 3 4 2 17.78 16.00 18.01 o 4 4 2 1725.42 1825.92 35.21 o 5 4 2 190.78 192.87 18.81 o 6 4 2 1599.25 1241.95 28.26 o 7 4 2 0.72 -13.94 16.00 o 8 4 2 4050.51 3890.24 82.61 o 9 4 2 148.74 158.06 21.57 o 10 4 2 662.34 706.38 31.74 o 11 4 2 3.43 -0.07 20.20 o 12 4 2 54.50 4.83 23.37 o 13 4 2 0.52 5.29 23.68 o 14 4 2 1.03 39.40 32.25 o 15 4 2 23.91 6.25 32.59 o 16 4 2 652.87 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