#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/44/2204486.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204486_Fobs loop_ _publ_author_name 'Gao, Shan' 'Liu, Ji-Wei' 'Huo, Li-Hua' 'Zhao, Hui' _publ_section_title ; (N-Hydroxy-N-phenylbenzamidato-\k^2^O,O')[3-methoxysalicylaldehyde (2,4-dichlorophenoxyacetyl)hydrazonato-\k^3^O,N,O']oxovanadium(V) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1722 _journal_page_last m1724 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.302 _cell_angle_gamma 90.000 _cell_length_a 26.2898 _cell_length_b 14.4455 _cell_length_c 15.5682 _exptl_crystal_F_000 2640.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file cv6400Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' V in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 729.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 98867.30 108984.27 768.31 o 6 0 0 11672.54 11494.70 160.26 o 8 0 0 152731.67 167298.05 923.97 o 10 0 0 11834.33 11471.36 35.94 o 12 0 0 52707.07 57650.07 81.10 o 14 0 0 28828.31 26298.89 308.46 o 16 0 0 6621.10 6242.21 43.96 o 18 0 0 4231.66 3860.91 40.74 o 20 0 0 17643.07 17460.04 130.50 o 22 0 0 4238.77 4010.28 34.84 o 24 0 0 281.94 317.48 32.83 o 26 0 0 32.51 7.93 34.00 o 28 0 0 658.33 725.69 36.86 o 30 0 0 160.56 297.93 75.90 o 32 0 0 120.90 -0.08 51.99 o 5 1 0 97304.80 106897.88 602.10 o 7 1 0 82471.44 91283.50 410.15 o 9 1 0 12999.41 11791.98 104.53 o 11 1 0 93900.54 104457.95 776.66 o 13 1 0 13549.75 14235.84 79.08 o 15 1 0 40.73 4.38 13.78 o 17 1 0 2741.26 2472.09 19.05 o 19 1 0 1615.56 1601.30 20.12 o 21 1 0 4056.61 4189.85 25.65 o 23 1 0 2326.00 1940.98 39.29 o 25 1 0 5029.51 5056.91 36.50 o 27 1 0 82.23 54.70 28.39 o 29 1 0 34.44 25.01 31.80 o 31 1 0 1135.53 1195.40 30.14 o 2 2 0 11.05 16.67 4.64 o 4 2 0 33177.72 35642.68 118.15 o 6 2 0 709.68 557.13 7.97 o 8 2 0 3998.25 4596.80 34.09 o 10 2 0 1075.61 1142.84 16.64 o 12 2 0 3959.21 3676.81 49.73 o 14 2 0 10932.38 9909.40 34.07 o 16 2 0 898.10 1120.78 30.06 o 18 2 0 525.93 528.27 17.04 o 20 2 0 379.69 353.87 19.30 o 22 2 0 103.87 110.25 24.21 o 24 2 0 170.42 174.79 24.18 o 26 2 0 0.83 -2.43 24.67 o 28 2 0 498.94 634.30 25.27 o 30 2 0 2.35 11.96 31.83 o 32 2 0 42.04 74.64 40.17 o 1 3 0 84126.29 90695.86 481.57 o 3 3 0 96339.38 102529.47 287.36 o 5 3 0 25973.73 26006.40 151.91 o 7 3 0 9682.33 9963.05 33.32 o 9 3 0 5563.04 4955.31 45.56 o 11 3 0 944.24 1491.16 11.85 o 13 3 0 2347.47 2033.90 18.14 o 15 3 0 1303.53 1357.19 16.68 o 17 3 0 431.11 365.19 26.11 o 19 3 0 231.32 222.55 22.03 o 21 3 0 22.56 38.17 20.79 o 23 3 0 735.82 878.09 25.19 o 25 3 0 934.40 986.78 25.13 o 27 3 0 480.57 532.85 29.78 o 29 3 0 882.75 971.69 63.10 o 31 3 0 299.16 355.79 31.16 o 0 4 0 4466.62 3512.39 63.27 o 2 4 0 7975.68 8375.35 32.11 o 4 4 0 16.59 23.40 7.99 o 6 4 0 8720.52 9251.20 108.67 o 8 4 0 358.47 389.58 10.80 o 10 4 0 1154.64 1379.50 13.24 o 12 4 0 826.99 918.27 16.15 o 14 4 0 6527.91 6062.21 55.23 o 16 4 0 929.45 932.70 34.35 o 18 4 0 295.64 375.77 17.71 o 20 4 0 2.77 0.54 19.47 o 22 4 0 1090.98 894.32 26.07 o 24 4 0 785.44 713.25 33.36 o 26 4 0 753.21 720.55 28.93 o 28 4 0 594.47 622.94 44.96 o 30 4 0 403.87 436.23 31.77 o 1 5 0 6986.87 6924.61 46.68 o 3 5 0 446.02 430.64 8.85 o 5 5 0 28199.37 29829.40 210.72 o 7 5 0 3.56 24.09 9.91 o 9 5 0 9073.52 9477.00 26.82 o 11 5 0 1331.48 1108.48 20.97 o 13 5 0 30.76 107.12 46.79 o 15 5 0 74.64 73.32 15.06 o 17 5 0 1961.46 1965.52 19.51 o 19 5 0 2783.99 3015.93 66.11 o 21 5 0 2344.22 2167.74 43.75 o 23 5 0 327.34 320.30 22.31 o 25 5 0 18.29 21.90 23.55 o 27 5 0 1.80 32.01 30.80 o 29 5 0 179.10 189.45 38.39 o 31 5 0 165.56 153.09 30.46 o 0 6 0 1311.26 1578.06 16.62 o 2 6 0 9257.91 9280.23 21.81 o 4 6 0 727.08 821.13 12.69 o 6 6 0 2997.22 3165.23 14.19 o 8 6 0 5961.53 6686.74 60.34 o 10 6 0 579.95 563.83 14.87 o 12 6 0 7043.68 7308.16 20.65 o 14 6 0 334.30 301.19 17.11 o 16 6 0 15848.99 15911.40 99.11 o 18 6 0 106.90 156.11 26.54 o 20 6 0 611.61 519.76 47.24 o 22 6 0 1290.55 1219.37 23.11 o 24 6 0 105.86 115.48 23.15 o 26 6 0 2.07 32.44 28.66 o 28 6 0 28.55 31.39 30.76 o 30 6 0 239.14 296.74 64.09 o 1 7 0 11269.86 11380.93 40.53 o 3 7 0 16260.09 17118.17 111.41 o 5 7 0 25751.13 27382.87 180.65 o 7 7 0 2995.53 3102.03 39.57 o 9 7 0 662.29 677.37 19.78 o 11 7 0 441.82 466.78 21.04 o 13 7 0 81.54 89.93 19.76 o 15 7 0 1057.11 1173.74 60.03 o 17 7 0 171.17 97.37 20.72 o 19 7 0 843.30 768.89 27.12 o 21 7 0 123.45 157.01 60.53 o 23 7 0 469.84 544.04 176.23 o 25 7 0 36.37 22.79 54.24 o 27 7 0 2.49 59.91 36.47 o 29 7 0 58.79 131.82 32.97 o 0 8 0 363.33 153.11 29.52 o 2 8 0 904.46 935.15 14.44 o 4 8 0 462.47 522.55 14.49 o 6 8 0 2550.21 2306.98 20.88 o 8 8 0 7462.74 7787.63 92.05 o 10 8 0 321.19 310.20 22.86 o 12 8 0 1508.02 1615.78 24.57 o 14 8 0 1688.54 1618.38 18.50 o 16 8 0 881.11 881.84 25.27 o 18 8 0 0.04 -22.03 22.03 o 20 8 0 0.96 -6.96 23.99 o 22 8 0 1822.09 1798.69 55.75 o 24 8 0 51.73 77.08 32.58 o 26 8 0 87.37 117.37 29.93 o 28 8 0 991.51 989.50 33.67 o 1 9 0 70.06 77.31 16.75 o 3 9 0 22278.48 23014.77 30.61 o 5 9 0 1714.61 1887.95 36.94 o 7 9 0 2167.86 2296.50 29.17 o 9 9 0 2888.10 2823.44 19.77 o 11 9 0 3376.51 3356.43 39.30 o 13 9 0 312.24 283.04 14.36 o 15 9 0 115.13 140.02 16.41 o 17 9 0 5075.39 4916.19 51.45 o 19 9 0 41.99 73.66 23.25 o 21 9 0 80.19 85.57 25.63 o 23 9 0 176.24 133.55 42.70 o 25 9 0 719.24 774.76 48.44 o 27 9 0 247.92 311.24 30.78 o 0 10 0 12643.37 12532.55 122.91 o 2 10 0 1437.65 1409.43 27.05 o 4 10 0 465.31 434.68 28.72 o 6 10 0 5712.67 5578.16 44.22 o 8 10 0 1371.67 1351.93 27.87 o 10 10 0 1239.36 1241.22 24.63 o 12 10 0 1101.43 867.71 23.12 o 14 10 0 4339.26 4316.29 44.38 o 16 10 0 174.37 172.90 19.77 o 18 10 0 1462.85 1365.67 27.68 o 20 10 0 281.16 297.77 25.99 o 22 10 0 1096.14 1195.31 32.75 o 24 10 0 175.82 87.12 28.93 o 26 10 0 471.93 412.57 37.74 o 1 11 0 1.04 34.30 19.55 o 3 11 0 2193.34 2046.73 30.16 o 5 11 0 1868.45 1942.55 19.24 o 7 11 0 19.49 -11.98 17.21 o 9 11 0 981.06 1034.36 23.43 o 11 11 0 5037.25 5152.45 67.62 o 13 11 0 1282.49 1206.78 21.04 o 15 11 0 32.40 47.42 28.30 o 17 11 0 787.93 750.81 27.63 o 19 11 0 3370.86 3350.47 30.37 o 21 11 0 1023.20 1053.07 24.16 o 23 11 0 10.15 40.58 26.71 o 25 11 0 990.58 958.47 41.16 o 0 12 0 2184.59 2224.09 43.37 o 2 12 0 2.13 -4.03 18.83 o 4 12 0 2.03 5.04 56.44 o 6 12 0 3524.01 3598.50 29.69 o 8 12 0 1406.72 1474.18 27.29 o 10 12 0 146.02 200.43 17.38 o 12 12 0 1.67 24.64 20.25 o 14 12 0 2087.33 2147.84 52.38 o 16 12 0 334.80 340.34 22.37 o 18 12 0 109.85 83.97 36.77 o 20 12 0 979.13 981.20 42.28 o 22 12 0 2144.94 2149.70 58.18 o 24 12 0 241.20 184.49 33.11 o 1 13 0 55.29 85.60 27.71 o 3 13 0 684.72 821.71 27.39 o 5 13 0 1501.92 1581.62 31.63 o 7 13 0 1025.44 1018.73 36.65 o 9 13 0 1088.49 1025.78 27.09 o 11 13 0 799.99 967.57 36.83 o 13 13 0 75.50 78.46 19.40 o 15 13 0 195.17 223.73 20.92 o 17 13 0 791.52 727.72 23.75 o 19 13 0 340.29 377.11 32.72 o 21 13 0 112.53 82.74 30.54 o 23 13 0 210.74 231.42 30.08 o 0 14 0 416.14 571.62 45.45 o 2 14 0 412.00 460.62 26.00 o 4 14 0 5.66 -23.47 23.58 o 6 14 0 1025.02 1175.74 47.74 o 8 14 0 186.29 235.50 24.60 o 10 14 0 113.75 106.78 22.49 o 12 14 0 114.37 108.91 21.48 o 14 14 0 1483.36 1669.42 37.45 o 16 14 0 1539.63 1378.57 67.54 o 18 14 0 362.97 378.79 71.19 o 20 14 0 732.89 639.13 33.24 o 1 15 0 0.74 5.45 20.25 o 3 15 0 1150.24 1238.35 33.98 o 5 15 0 1558.55 1515.41 104.08 o 7 15 0 63.89 123.66 31.04 o 9 15 0 1070.84 1091.34 38.46 o 11 15 0 441.38 476.72 34.27 o 13 15 0 12.98 54.71 38.32 o 15 15 0 251.41 227.70 22.67 o 17 15 0 887.62 698.65 65.67 o 19 15 0 344.27 256.65 41.52 o 0 16 0 632.15 672.32 42.20 o 2 16 0 569.54 508.28 32.06 o 4 16 0 108.10 148.78 61.39 o 6 16 0 1.93 -3.15 24.06 o 8 16 0 308.51 287.12 24.96 o 10 16 0 0.35 33.42 36.30 o 12 16 0 2.19 28.58 21.87 o 14 16 0 188.40 204.56 34.49 o 16 16 0 343.43 277.06 65.39 o 1 17 0 33.52 21.15 19.62 o 3 17 0 147.91 194.13 31.96 o 5 17 0 71.37 97.31 43.36 o 7 17 0 7.43 30.37 26.12 o 9 17 0 420.90 358.59 53.26 o 11 17 0 141.41 83.56 33.67 o 13 17 0 0.56 -2.82 23.30 o 0 18 0 576.74 648.28 41.70 o 2 18 0 140.83 152.65 44.89 o 4 18 0 63.83 43.38 33.17 o 6 18 0 219.43 311.59 41.97 o 8 18 0 107.89 109.85 29.90 o -33 1 1 53.58 6.95 30.18 o -31 1 1 29.17 59.25 30.87 o -29 1 1 85.06 101.70 26.59 o -27 1 1 130.25 115.45 27.97 o -25 1 1 56.66 64.64 24.01 o -23 1 1 4631.29 4510.41 46.28 o -21 1 1 2679.58 2790.48 22.36 o -19 1 1 548.09 547.66 18.27 o -17 1 1 3842.30 3752.49 23.71 o -15 1 1 2063.82 1811.73 16.97 o -13 1 1 2174.23 2061.73 19.57 o -11 1 1 7344.94 7219.07 48.01 o -9 1 1 4714.78 4766.67 18.46 o -7 1 1 38757.64 43359.77 178.60 o -5 1 1 292.69 307.53 9.57 o 3 1 1 4009.74 4050.40 39.03 o 5 1 1 29680.23 30317.20 118.11 o 7 1 1 28124.02 31436.84 314.95 o 9 1 1 2149.94 1985.44 20.10 o 11 1 1 1114.72 1092.69 18.02 o 13 1 1 40327.04 43391.71 285.51 o 15 1 1 2460.27 2284.69 36.88 o 17 1 1 1123.94 1048.07 20.82 o 19 1 1 105.39 87.47 20.04 o 21 1 1 6262.94 6103.61 32.59 o 23 1 1 13.48 -6.91 28.90 o 25 1 1 635.13 587.30 28.83 o 27 1 1 1169.58 1161.58 26.40 o 29 1 1 247.69 335.87 34.87 o 31 1 1 0.27 -41.50 41.50 o -32 2 1 655.33 692.96 29.84 o -30 2 1 1.20 47.72 27.09 o -28 2 1 273.02 273.17 29.86 o -26 2 1 1627.71 1596.72 40.80 o -24 2 1 469.86 540.52 21.67 o -22 2 1 5034.25 4863.88 48.89 o -20 2 1 152.66 134.28 28.69 o -18 2 1 650.53 579.06 16.68 o -16 2 1 82.39 59.55 13.78 o -14 2 1 575.66 629.03 22.50 o -12 2 1 13394.82 13958.94 94.87 o -10 2 1 1518.60 1435.63 22.73 o -8 2 1 13519.31 14083.82 53.73 o -6 2 1 22140.61 23825.83 145.55 o -4 2 1 2012.20 2072.60 19.38 o -2 2 1 1505.99 1410.03 4.04 o 0 2 1 28056.85 29229.03 176.99 o 2 2 1 2927.91 2750.75 20.37 o 4 2 1 14990.14 15657.42 102.13 o 6 2 1 20523.66 21641.03 168.84 o 8 2 1 1172.25 1239.87 13.28 o 10 2 1 27110.25 27408.44 103.66 o 12 2 1 1295.00 1355.18 23.15 o 14 2 1 3716.60 3804.72 39.55 o 16 2 1 2898.90 2989.43 25.49 o 18 2 1 225.70 242.35 22.51 o 20 2 1 796.92 825.49 27.87 o 22 2 1 1066.41 1000.58 29.58 o 24 2 1 1410.41 1478.95 38.26 o 26 2 1 835.79 689.99 26.57 o 28 2 1 416.46 429.27 33.87 o 30 2 1 553.57 559.71 31.89 o -31 3 1 226.19 237.17 29.03 o -29 3 1 79.79 80.40 32.02 o -27 3 1 35.35 28.54 23.76 o -25 3 1 7.77 20.81 24.94 o -23 3 1 15.23 5.10 21.23 o -21 3 1 3640.92 3885.93 41.90 o -19 3 1 5035.84 5216.72 43.06 o -17 3 1 46.54 44.68 20.97 o -15 3 1 1752.06 1378.64 14.31 o -13 3 1 1425.58 1329.16 14.09 o -11 3 1 1907.61 2047.52 28.80 o -9 3 1 204.81 178.77 10.03 o -7 3 1 121.47 93.29 9.81 o -5 3 1 2.78 38.00 12.65 o -3 3 1 59407.13 67470.95 193.96 o -1 3 1 124661.05 133727.39 693.86 o 1 3 1 100988.64 111599.95 488.21 o 3 3 1 11729.38 11290.08 63.75 o 5 3 1 20.89 46.22 11.08 o 7 3 1 4127.41 3795.65 24.49 o 9 3 1 14048.61 13947.35 69.06 o 11 3 1 5.55 18.11 12.48 o 13 3 1 26854.24 27001.11 120.31 o 15 3 1 235.59 229.64 29.59 o 17 3 1 231.98 187.34 21.18 o 19 3 1 68.47 68.11 19.38 o 21 3 1 6095.56 6114.45 47.33 o 23 3 1 671.79 644.47 26.74 o 25 3 1 0.93 -27.27 27.27 o 27 3 1 474.63 604.32 45.78 o 29 3 1 47.67 82.98 28.76 o 31 3 1 208.49 189.67 32.46 o -32 4 1 200.08 324.91 32.96 o -30 4 1 522.34 565.34 30.97 o -28 4 1 748.31 687.05 29.68 o -26 4 1 2965.85 3021.45 32.02 o -24 4 1 72.21 53.02 22.73 o -22 4 1 3146.14 3261.82 23.63 o -20 4 1 1294.58 1363.84 30.81 o -18 4 1 3379.16 3290.64 23.16 o -16 4 1 1101.35 1108.48 16.53 o -14 4 1 1836.83 2092.04 31.87 o -12 4 1 1723.21 1541.74 14.93 o -10 4 1 5275.05 5078.51 22.47 o -8 4 1 10827.99 10642.39 72.32 o -6 4 1 2321.53 2275.25 29.33 o -4 4 1 6767.87 6446.72 39.55 o -2 4 1 48.01 35.42 11.32 o 0 4 1 22476.32 23552.36 164.13 o 2 4 1 49914.16 52220.75 300.28 o 4 4 1 308.59 536.46 8.46 o 6 4 1 1875.01 1844.14 10.74 o 8 4 1 7713.53 8363.38 75.41 o 10 4 1 12511.39 12321.49 85.84 o 12 4 1 109.32 183.08 17.24 o 14 4 1 616.18 634.53 15.02 o 16 4 1 4166.79 3708.93 48.49 o 18 4 1 3461.50 3556.28 57.85 o 20 4 1 1133.51 1267.49 25.49 o 22 4 1 995.94 776.19 31.03 o 24 4 1 1519.34 1608.03 33.19 o 26 4 1 116.65 105.51 25.23 o 28 4 1 405.60 345.26 34.29 o 30 4 1 69.90 174.09 29.17 o -31 5 1 2.90 33.78 36.67 o -29 5 1 1268.50 1347.16 40.11 o -27 5 1 164.41 180.59 25.41 o -25 5 1 745.31 720.07 24.51 o -23 5 1 879.16 798.68 24.07 o -21 5 1 1233.44 1399.02 42.93 o -19 5 1 722.02 701.65 20.42 o -17 5 1 12.18 74.39 41.93 o -15 5 1 4587.51 4590.94 48.68 o -13 5 1 47.92 154.40 18.39 o -11 5 1 3437.63 3699.36 61.97 o -9 5 1 4241.49 4590.61 32.21 o -7 5 1 229.50 73.74 9.73 o -5 5 1 6445.84 6969.82 79.68 o -3 5 1 28238.29 30913.72 183.98 o -1 5 1 16174.40 14279.59 69.18 o 1 5 1 15965.32 16676.30 21.95 o 3 5 1 590.85 711.95 20.10 o 5 5 1 3486.84 4007.96 66.20 o 7 5 1 3453.72 3006.85 41.55 o 9 5 1 7224.74 7527.61 70.24 o 11 5 1 181.09 238.36 16.45 o 13 5 1 27560.52 27898.45 83.67 o 15 5 1 1924.68 2116.67 17.58 o 17 5 1 417.02 394.43 47.56 o 19 5 1 1269.22 1304.63 40.64 o 21 5 1 3374.61 3686.05 71.65 o 23 5 1 201.74 197.53 32.33 o 25 5 1 961.84 922.11 73.02 o 27 5 1 754.82 888.99 36.12 o 29 5 1 556.64 607.01 34.51 o -30 6 1 133.91 216.26 28.19 o -28 6 1 383.06 405.56 45.07 o -26 6 1 2631.09 2894.82 49.04 o -24 6 1 2861.68 2737.40 28.32 o -22 6 1 961.85 986.95 33.36 o -20 6 1 140.71 141.82 20.87 o -18 6 1 8556.25 8201.99 76.68 o -16 6 1 1774.06 1828.52 35.15 o -14 6 1 1337.22 1369.27 17.19 o -12 6 1 4796.62 4500.63 48.78 o -10 6 1 627.21 402.17 14.15 o -8 6 1 548.63 575.60 16.28 o -6 6 1 16.73 53.61 12.18 o -4 6 1 57965.58 62564.76 459.79 o -2 6 1 5644.57 4929.64 14.20 o 0 6 1 23.31 -4.43 10.49 o 2 6 1 36408.09 38074.79 147.82 o 4 6 1 73232.81 82088.65 748.16 o 6 6 1 2514.96 2872.55 16.48 o 8 6 1 2776.69 2726.40 32.77 o 10 6 1 16614.10 15613.08 110.39 o 12 6 1 924.41 917.68 27.16 o 14 6 1 1097.90 1164.74 22.20 o 16 6 1 5027.61 4784.48 118.42 o 18 6 1 7759.22 7937.14 71.70 o 20 6 1 276.35 387.84 67.68 o 22 6 1 205.49 235.08 26.46 o 24 6 1 2424.55 2457.92 63.99 o 26 6 1 383.62 377.82 28.11 o 28 6 1 0.02 14.26 45.00 o 30 6 1 597.62 608.76 65.24 o -29 7 1 1708.52 1746.36 46.28 o -27 7 1 22.84 112.80 44.83 o -25 7 1 40.92 112.52 31.91 o -23 7 1 2490.85 2557.72 63.17 o -21 7 1 4009.32 4252.21 52.66 o -19 7 1 2.20 11.23 28.37 o -17 7 1 1369.65 1537.37 89.01 o -15 7 1 11108.49 10702.28 32.67 o -13 7 1 4099.39 4104.12 44.27 o -11 7 1 1445.56 1672.67 14.14 o -9 7 1 1256.01 1261.22 21.74 o -7 7 1 32291.00 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