#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/45/2204549.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204549_Fobs loop_ _publ_author_name 'Zhong, Yun' 'Zhang, Weiguang' 'Fan, Jun' 'Tan, Mingyu' 'Lai, Chian Sing' 'Tiekink, Edward R. T.' _publ_section_title ; Bis[\m-N,N-bis(2-hydroxyethyl)dithiocarbamato]-1:2\k^3^S,S':S';2:1\k^3^S,S':S'-bis{[N,N-bis(2-hydroxyethyl)dithiocarbamato-\k^2^S,S']cadmium(II)} ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1633 _journal_page_last m1635 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.956 _cell_angle_gamma 90.000 _cell_length_a 8.1588 _cell_length_b 8.3040 _cell_length_c 25.0084 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7110 _[local]_cod_data_source_file ng6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_f_calc_maximum 258.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3871.25 4336.24 127.78 o 2 0 0 5763.61 6141.54 183.52 o 3 0 0 39940.39 30650.07 866.86 o 4 0 0 9292.05 9343.11 201.31 o 5 0 0 5729.12 5825.63 135.94 o 6 0 0 438.52 463.41 27.72 o 7 0 0 10509.19 10301.36 193.07 o 8 0 0 1436.11 1466.60 63.52 o 9 0 0 553.45 573.75 53.04 o 10 0 0 1943.35 1872.98 109.87 o 11 0 0 555.37 578.35 56.77 o 1 1 0 4590.87 4950.04 58.97 o 2 1 0 278.83 306.23 13.60 o 3 1 0 11782.15 11430.83 197.50 o 4 1 0 7076.02 7521.77 118.18 o 5 1 0 794.13 753.90 23.06 o 6 1 0 502.95 512.62 23.51 o 7 1 0 1764.26 1800.04 39.32 o 8 1 0 108.48 124.61 10.73 o 9 1 0 32.74 39.29 9.21 o 10 1 0 11.22 43.26 12.67 o 11 1 0 2.11 44.48 24.37 o 0 2 0 9390.89 9890.05 203.97 o 1 2 0 1642.83 1794.14 38.84 o 2 2 0 13504.90 13129.89 185.69 o 3 2 0 7949.92 8429.65 128.73 o 4 2 0 12412.58 12111.00 183.40 o 5 2 0 17288.05 15479.55 409.97 o 6 2 0 2454.12 2319.29 50.75 o 7 2 0 3211.22 2999.34 74.28 o 8 2 0 68.99 82.30 12.67 o 9 2 0 1498.04 1416.42 81.78 o 10 2 0 259.34 335.88 35.50 o 11 2 0 532.05 562.79 69.17 o 1 3 0 4676.23 4917.24 78.35 o 2 3 0 2656.00 2752.76 49.09 o 3 3 0 3223.61 3408.70 70.26 o 4 3 0 1736.50 1788.01 37.46 o 5 3 0 4562.31 4603.62 70.45 o 6 3 0 7752.44 7453.64 121.50 o 7 3 0 88.93 91.66 20.84 o 8 3 0 5907.55 5757.57 158.87 o 9 3 0 709.74 706.03 27.87 o 10 3 0 778.37 789.67 44.64 o 11 3 0 1478.84 1511.10 103.84 o 0 4 0 6243.23 6371.09 142.83 o 1 4 0 13630.57 13834.55 205.53 o 2 4 0 16787.50 16198.76 277.75 o 3 4 0 862.20 977.67 25.96 o 4 4 0 319.62 345.25 19.37 o 5 4 0 1122.70 1173.16 38.39 o 6 4 0 6.26 37.55 18.59 o 7 4 0 67.46 52.26 18.34 o 8 4 0 248.94 302.77 34.24 o 9 4 0 471.60 520.46 39.68 o 10 4 0 279.71 374.88 37.14 o 1 5 0 17507.60 17165.04 260.30 o 2 5 0 3621.98 3664.58 78.31 o 3 5 0 10509.56 10296.96 161.58 o 4 5 0 8864.89 8646.22 163.94 o 5 5 0 51.06 73.80 19.72 o 6 5 0 8306.44 8005.37 202.77 o 7 5 0 1084.40 985.78 52.67 o 8 5 0 875.17 825.76 49.40 o 9 5 0 689.46 766.90 64.72 o 10 5 0 460.61 472.38 36.48 o 0 6 0 5496.05 5829.19 141.17 o 1 6 0 634.67 716.91 24.32 o 2 6 0 1291.30 1263.50 33.92 o 3 6 0 252.26 275.42 24.06 o 4 6 0 1459.41 1462.19 46.03 o 5 6 0 408.74 463.22 36.17 o 6 6 0 5.18 15.24 14.73 o 7 6 0 7.02 36.70 14.47 o 8 6 0 1094.32 1147.55 60.68 o 9 6 0 298.61 387.48 32.92 o 1 7 0 2750.17 2653.64 77.02 o 2 7 0 1231.44 1188.98 34.16 o 3 7 0 1141.46 1010.30 36.95 o 4 7 0 884.25 860.35 38.22 o 5 7 0 761.60 725.02 65.35 o 6 7 0 2359.13 2297.39 88.24 o 7 7 0 322.49 305.05 35.30 o 8 7 0 2394.87 2269.62 92.87 o 9 7 0 449.33 446.05 30.82 o 0 8 0 29.11 64.19 13.21 o 1 8 0 1090.05 1058.14 39.14 o 2 8 0 2282.05 2275.49 63.57 o 3 8 0 280.57 330.79 32.92 o 4 8 0 493.25 446.35 34.84 o 5 8 0 2597.49 2475.42 103.82 o 6 8 0 81.75 104.01 20.45 o 7 8 0 521.70 537.74 42.12 o 8 8 0 177.27 262.84 28.62 o 1 9 0 333.21 383.23 34.92 o 2 9 0 21.32 37.31 7.89 o 3 9 0 63.17 83.06 16.76 o 4 9 0 141.58 195.16 30.57 o 5 9 0 93.99 132.85 18.96 o 6 9 0 40.70 77.11 14.04 o 7 9 0 2.62 20.05 8.14 o 0 10 0 2436.74 2455.28 125.37 o 1 10 0 3.61 52.59 12.61 o 2 10 0 1857.33 1818.04 120.86 o 3 10 0 1301.56 1336.94 93.57 o 4 10 0 580.22 586.35 37.87 o 5 10 0 683.55 682.76 40.73 o 1 11 0 362.10 383.03 37.41 o 2 11 0 385.86 407.34 57.63 o 3 11 0 8.74 74.40 24.86 o -11 1 1 177.38 189.10 26.85 o -10 1 1 3627.90 3659.31 122.36 o -9 1 1 1219.41 1232.02 44.36 o -8 1 1 1227.77 1244.31 50.07 o -7 1 1 11765.06 11087.95 145.83 o -6 1 1 2529.07 2538.52 47.36 o -5 1 1 16091.59 15299.22 229.63 o -4 1 1 7348.33 7448.17 116.88 o -3 1 1 45035.50 34086.57 1494.65 o -2 1 1 32531.25 25409.94 1587.26 o -1 1 1 81.93 84.10 8.00 o 0 1 1 34074.49 27308.34 791.47 o 1 1 1 7.88 0.25 3.40 o 2 1 1 16918.94 15679.36 927.60 o 3 1 1 15106.04 13896.20 308.45 o 4 1 1 8339.69 8498.29 132.02 o 5 1 1 4507.32 4771.48 82.70 o 6 1 1 6.29 13.35 7.00 o 7 1 1 8757.44 8361.15 212.57 o 8 1 1 54.85 78.58 8.47 o 9 1 1 706.05 746.68 34.39 o 10 1 1 692.28 722.34 44.88 o 11 1 1 806.92 882.22 49.60 o -11 2 1 659.08 734.71 67.79 o -10 2 1 144.31 164.45 24.67 o -9 2 1 276.58 281.51 15.85 o -8 2 1 188.01 217.87 23.61 o -7 2 1 755.45 785.38 31.51 o -6 2 1 2198.53 2144.19 47.94 o -5 2 1 734.67 788.88 24.29 o -4 2 1 15783.40 14778.83 220.48 o -3 2 1 619.81 828.03 17.73 o -2 2 1 1117.13 1237.98 25.11 o -1 2 1 28074.97 25304.49 619.51 o 0 2 1 39437.22 35029.78 571.93 o 1 2 1 11121.00 11343.88 165.61 o 2 2 1 6962.95 7126.38 94.60 o 3 2 1 6663.43 6556.67 102.78 o 4 2 1 3120.02 3151.36 57.47 o 5 2 1 1400.32 1482.19 35.52 o 6 2 1 1966.80 1931.36 44.83 o 7 2 1 7.13 21.18 13.26 o 8 2 1 1009.28 1031.64 39.69 o 9 2 1 295.33 329.88 26.39 o 10 2 1 906.27 961.86 39.81 o 11 2 1 124.64 219.46 42.94 o -11 3 1 28.72 89.26 23.99 o -10 3 1 209.31 247.39 18.91 o -9 3 1 1991.89 1871.19 60.35 o -8 3 1 1056.50 977.05 101.63 o -7 3 1 850.09 799.19 43.48 o -6 3 1 14.08 34.65 5.80 o -5 3 1 12292.88 11988.74 160.81 o -4 3 1 232.48 217.41 10.19 o -3 3 1 370.02 380.25 16.57 o -2 3 1 8593.46 8893.97 134.50 o -1 3 1 4561.34 5075.71 93.27 o 0 3 1 553.28 544.48 15.43 o 1 3 1 154.06 163.14 9.48 o 2 3 1 18772.99 18344.73 309.49 o 3 3 1 5.52 24.95 7.70 o 4 3 1 931.97 881.55 26.87 o 5 3 1 6351.21 6359.89 92.77 o 6 3 1 2444.53 2353.06 62.08 o 7 3 1 254.48 244.98 18.27 o 8 3 1 32.21 76.63 28.30 o 9 3 1 2178.77 2073.68 82.02 o 10 3 1 0.45 54.25 20.67 o 11 3 1 116.07 146.61 31.34 o -10 4 1 613.50 632.85 35.96 o -9 4 1 2672.43 2611.19 96.52 o -8 4 1 3411.67 3322.62 109.79 o -7 4 1 52.12 60.03 17.75 o -6 4 1 5753.73 5420.02 146.11 o -5 4 1 178.70 209.84 15.74 o -4 4 1 5056.31 5104.61 104.37 o -3 4 1 1878.62 1889.52 47.00 o -2 4 1 6478.28 6596.21 105.35 o -1 4 1 14587.05 14543.26 215.03 o 0 4 1 4261.83 4615.67 76.52 o 1 4 1 30744.85 28666.76 411.54 o 2 4 1 2009.65 1956.95 40.41 o 3 4 1 5791.67 5833.84 97.11 o 4 4 1 4930.92 4852.86 99.95 o 5 4 1 6431.64 6410.22 152.98 o 6 4 1 3193.27 3184.58 63.38 o 7 4 1 107.62 115.63 23.04 o 8 4 1 5822.46 5775.57 176.57 o 9 4 1 1461.13 1349.19 119.08 o 10 4 1 184.29 212.96 25.57 o -10 5 1 0.83 13.66 9.48 o -9 5 1 10.19 54.56 11.45 o -8 5 1 190.51 213.39 29.47 o -7 5 1 172.29 187.90 39.58 o -6 5 1 543.21 519.22 39.32 o -5 5 1 29.58 66.17 19.49 o -4 5 1 1239.47 1279.51 40.01 o -3 5 1 803.88 786.08 29.09 o -2 5 1 256.31 284.12 18.72 o -1 5 1 1654.88 1674.28 37.14 o 0 5 1 797.45 795.00 23.13 o 1 5 1 370.99 388.72 16.86 o 2 5 1 12.43 26.29 7.24 o 3 5 1 20.55 25.13 4.68 o 4 5 1 1822.43 1725.09 86.56 o 5 5 1 722.69 740.70 31.03 o 6 5 1 1014.10 1012.99 52.72 o 7 5 1 234.49 243.95 41.19 o 8 5 1 90.50 125.63 22.97 o 9 5 1 187.84 187.92 26.88 o 10 5 1 152.42 149.99 36.62 o -9 6 1 253.41 347.71 37.94 o -8 6 1 311.18 364.64 39.25 o -7 6 1 1016.64 1059.38 56.24 o -6 6 1 5328.39 5045.19 145.44 o -5 6 1 61.81 96.62 21.35 o -4 6 1 8249.94 8082.98 182.42 o -3 6 1 12620.87 12357.28 277.48 o -2 6 1 5537.62 5413.18 121.81 o -1 6 1 3458.53 3377.17 64.82 o 0 6 1 150.48 188.80 13.95 o 1 6 1 15078.89 14697.25 224.14 o 2 6 1 84.80 112.41 12.69 o 3 6 1 6527.73 6256.50 146.02 o 4 6 1 4266.33 4225.61 94.74 o 5 6 1 601.05 636.16 62.72 o 6 6 1 3514.14 3353.75 140.93 o 7 6 1 266.82 336.74 36.29 o 8 6 1 320.82 369.11 39.53 o 9 6 1 39.18 80.45 15.66 o -9 7 1 45.83 87.93 10.77 o -8 7 1 803.68 844.11 50.53 o -7 7 1 212.62 207.01 29.11 o -6 7 1 10.47 33.49 13.78 o -5 7 1 1434.39 1244.19 77.52 o -4 7 1 157.71 200.35 20.51 o -3 7 1 1143.14 1135.02 55.20 o -2 7 1 2778.87 2700.06 68.50 o -1 7 1 2899.46 2794.34 58.97 o 0 7 1 2798.66 2640.16 64.72 o 1 7 1 2857.77 2875.75 60.56 o 2 7 1 3619.44 3359.35 76.91 o 3 7 1 502.74 452.18 52.85 o 4 7 1 493.91 508.17 26.88 o 5 7 1 1395.85 1451.39 97.90 o 6 7 1 653.96 659.79 61.74 o 7 7 1 793.50 730.46 46.70 o 8 7 1 1120.08 1185.45 71.64 o 9 7 1 359.46 399.80 41.04 o -8 8 1 1551.22 1708.25 76.57 o -7 8 1 1.21 1.03 8.99 o -6 8 1 175.31 177.22 26.93 o -5 8 1 368.47 322.47 47.56 o -4 8 1 175.03 196.07 26.30 o -3 8 1 16.42 30.85 8.60 o -2 8 1 885.86 842.53 34.95 o -1 8 1 822.15 787.15 33.13 o 0 8 1 518.31 537.58 21.44 o 1 8 1 1738.83 1668.31 43.20 o 2 8 1 24.01 35.45 10.49 o 3 8 1 2039.81 1976.06 58.74 o 4 8 1 329.29 311.04 32.54 o 5 8 1 1421.11 1341.68 63.02 o 6 8 1 1171.41 1087.39 57.80 o 7 8 1 536.42 628.35 46.41 o 8 8 1 799.01 731.92 45.14 o -7 9 1 618.95 620.58 75.23 o -6 9 1 232.74 267.50 30.99 o -5 9 1 1884.70 1716.33 73.56 o -4 9 1 1103.67 1053.45 53.33 o -3 9 1 362.20 333.18 33.03 o -2 9 1 645.64 625.96 30.09 o -1 9 1 172.92 189.07 13.94 o 0 9 1 771.21 779.40 43.54 o 1 9 1 70.30 92.37 18.48 o 2 9 1 3275.68 3195.66 82.25 o 3 9 1 457.77 507.86 26.69 o 4 9 1 1050.01 1063.05 53.97 o 5 9 1 2626.25 2520.82 94.12 o 6 9 1 52.40 99.84 16.20 o 7 9 1 1109.29 1062.75 56.05 o -5 10 1 9.00 19.51 14.78 o -4 10 1 312.22 375.30 28.31 o -3 10 1 73.37 101.35 12.64 o -2 10 1 85.73 131.91 32.95 o -1 10 1 1.28 14.73 23.13 o 0 10 1 356.64 415.17 55.08 o 1 10 1 2.33 32.42 23.22 o 2 10 1 135.66 194.57 24.86 o 3 10 1 103.98 92.08 31.46 o 4 10 1 0.06 -3.30 8.08 o 5 10 1 16.93 43.55 9.07 o -3 11 1 1340.45 1204.62 90.24 o -2 11 1 341.65 383.34 55.91 o -1 11 1 282.60 306.65 48.28 o 0 11 1 3246.92 3215.35 110.30 o 1 11 1 285.39 276.91 32.09 o 2 11 1 292.51 260.56 43.68 o 3 11 1 1167.70 1075.23 84.79 o -11 0 2 132.86 123.48 29.05 o -10 0 2 8132.31 7894.26 295.92 o -9 0 2 121.70 149.31 31.23 o -8 0 2 1190.18 1151.30 39.07 o -7 0 2 13867.70 13351.13 241.91 o -6 0 2 340.18 336.02 26.85 o -5 0 2 27701.98 25672.55 534.57 o -4 0 2 146.70 158.50 11.85 o -3 0 2 26614.88 24720.22 600.62 o -2 0 2 16979.82 16843.68 332.73 o -1 0 2 25828.41 22346.10 993.43 o 0 0 2 41274.32 10917.21 317.79 o 1 0 2 947.73 1109.33 40.93 o 2 0 2 3661.23 3999.51 127.67 o 3 0 2 32305.74 26445.69 754.40 o 4 0 2 9117.47 9465.52 290.69 o 5 0 2 1213.97 1408.69 45.59 o 6 0 2 2268.31 2420.47 70.71 o 7 0 2 1910.14 2021.79 65.06 o 8 0 2 811.00 810.16 54.36 o 9 0 2 548.23 482.42 32.89 o 10 0 2 453.76 463.94 58.61 o 11 0 2 238.52 259.93 43.45 o -11 1 2 99.48 90.53 23.88 o -10 1 2 592.60 640.28 40.81 o -9 1 2 38.92 66.03 14.87 o -8 1 2 36.16 61.29 9.38 o -7 1 2 5681.17 5367.94 111.65 o -6 1 2 780.85 762.89 20.26 o -5 1 2 7.69 20.42 5.84 o -4 1 2 19992.32 19010.11 309.46 o -3 1 2 2512.73 2718.37 47.51 o -2 1 2 1552.66 1738.64 31.64 o -1 1 2 9472.27 10289.36 175.13 o 0 1 2 244.84 270.72 7.83 o 1 1 2 4093.22 4462.96 92.43 o 2 1 2 1935.81 2184.72 43.93 o 3 1 2 9532.52 9642.78 167.69 o 4 1 2 4352.87 4386.48 85.05 o 5 1 2 1686.54 1759.91 44.14 o 6 1 2 1729.72 1705.11 66.80 o 7 1 2 245.44 246.01 17.74 o 8 1 2 407.81 420.29 24.57 o 9 1 2 149.77 175.86 19.74 o 10 1 2 161.56 191.67 27.18 o 11 1 2 40.34 74.45 16.59 o -11 2 2 455.27 561.93 56.37 o -10 2 2 1215.28 1191.59 87.08 o -9 2 2 1170.10 1172.39 39.46 o -8 2 2 1348.92 1333.08 39.56 o -7 2 2 2471.78 2367.11 53.97 o -6 2 2 401.33 408.71 18.64 o -5 2 2 5626.09 5469.90 93.28 o -4 2 2 1272.42 1409.34 31.72 o -3 2 2 2233.31 2354.66 36.78 o -2 2 2 17957.12 17386.06 251.13 o -1 2 2 4608.81 5064.19 77.41 o 0 2 2 3966.20 4272.38 66.23 o 1 2 2 48335.89 36003.98 1089.69 o 2 2 2 34119.89 28321.72 765.86 o 3 2 2 467.47 540.89 15.72 o 4 2 2 11032.32 10580.85 226.84 o 5 2 2 2126.46 2059.37 44.28 o 6 2 2 267.99 293.68 24.42 o 7 2 2 2895.57 2771.82 71.84 o 8 2 2 0.61 23.04 10.64 o 9 2 2 2066.10 1933.57 76.30 o 10 2 2 226.97 260.77 26.70 o 11 2 2 126.49 189.49 38.58 o -11 3 2 1416.94 1580.79 107.92 o -10 3 2 8.88 51.43 23.31 o -9 3 2 1033.78 1017.23 41.62 o -8 3 2 4020.21 4031.48 96.63 o -7 3 2 404.74 422.23 34.38 o -6 3 2 591.11 570.73 17.40 o -5 3 2 177.72 227.54 10.64 o -4 3 2 5241.75 5479.71 91.24 o -3 3 2 315.01 357.93 15.74 o -2 3 2 13170.47 13326.44 195.71 o -1 3 2 16570.00 16808.51 260.56 o 0 3 2 2664.56 2892.31 49.44 o 1 3 2 16928.29 16613.18 241.66 o 2 3 2 39.30 72.22 7.90 o 3 3 2 17187.80 16373.98 345.22 o 4 3 2 49.66 61.79 8.76 o 5 3 2 4146.02 4268.53 76.64 o 6 3 2 9384.47 9087.76 174.39 o 7 3 2 85.71 94.80 13.64 o 8 3 2 4061.17 3892.11 120.51 o 9 3 2 2633.40 2497.81 92.39 o 10 3 2 551.87 610.27 41.91 o -10 4 2 50.01 55.75 13.42 o -9 4 2 392.15 454.29 41.21 o -8 4 2 1275.43 1284.73 60.51 o -7 4 2 383.85 402.22 46.87 o -6 4 2 3.17 -13.14 13.14 o -5 4 2 3335.87 3352.68 106.20 o -4 4 2 18.70 29.64 14.44 o -3 4 2 10087.68 10374.22 184.83 o -2 4 2 255.79 239.91 11.73 o -1 4 2 2184.17 2213.94 49.28 o 0 4 2 1238.66 1278.86 28.79 o 1 4 2 5572.49 6017.08 97.21 o 2 4 2 730.76 694.58 22.35 o 3 4 2 751.30 783.59 28.46 o 4 4 2 93.11 80.07 22.99 o 5 4 2 0.55 1.75 8.70 o 6 4 2 3743.63 3718.55 71.98 o 7 4 2 79.97 81.16 20.02 o 8 4 2 1.05 20.57 19.66 o 9 4 2 11.16 39.04 9.85 o 10 4 2 110.30 135.87 18.58 o -10 5 2 148.23 164.25 14.99 o -9 5 2 3147.77 3115.99 110.16 o -8 5 2 188.80 232.01 32.43 o -7 5 2 2223.69 2109.47 81.30 o -6 5 2 8841.38 8381.97 246.32 o -5 5 2 1414.09 1294.77 56.80 o -4 5 2 12804.61 12543.77 288.57 o -3 5 2 7871.66 8018.89 128.61 o -2 5 2 12503.62 12718.21 193.58 o -1 5 2 3669.17 3828.38 68.19 o 0 5 2 114.47 146.83 11.25 o 1 5 2 12589.81 12313.35 187.91 o 2 5 2 94.48 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215.34 28.23 o 0 8 23 49.49 67.99 14.38 o 1 8 23 349.61 403.15 42.04 o 2 8 23 69.72 95.96 23.82 o 3 8 23 4.90 19.11 33.61 o -8 0 24 186.09 233.12 45.29 o -7 0 24 3279.15 3179.32 170.72 o -6 0 24 88.20 109.13 30.60 o -5 0 24 253.01 273.93 48.68 o -4 0 24 2376.66 2298.34 126.29 o -3 0 24 1270.51 1208.84 51.96 o -2 0 24 1724.54 1496.39 62.51 o -1 0 24 397.11 405.94 22.07 o 0 0 24 1948.13 1898.46 46.44 o 1 0 24 1304.19 1206.33 71.73 o 2 0 24 1349.39 1204.57 77.84 o 3 0 24 8967.94 9090.44 322.67 o 4 0 24 1648.64 1582.63 99.19 o 5 0 24 706.57 694.93 62.86 o 6 0 24 1055.68 930.86 75.83 o 7 0 24 70.24 87.71 21.87 o -8 1 24 122.90 149.31 19.75 o -7 1 24 84.42 105.75 24.97 o -6 1 24 103.79 94.55 19.73 o -5 1 24 1032.33 1035.20 57.48 o -4 1 24 1192.95 1168.54 65.50 o -3 1 24 2106.83 2056.89 70.80 o -2 1 24 565.58 582.89 29.84 o -1 1 24 1284.81 1211.22 25.80 o 0 1 24 776.91 842.70 34.42 o 1 1 24 136.49 150.18 12.60 o 2 1 24 25.79 38.72 10.26 o 3 1 24 459.83 466.62 31.33 o 4 1 24 643.86 641.15 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