#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/45/2204596.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204596_Fobs loop_ _publ_author_name 'Wang, Jun-Wen' 'Song, Hai-Bin' 'Xu, Feng-Bo' 'Li, Qing-Shan' 'Zhang, Zheng-Zhi' _publ_section_title ; 1,2-Bis(3,5-dimethylpyrazol-1-yl)-anti-[2.2]paracyclonaphthane ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2047 _journal_page_last o2049 _journal_volume 60 _journal_year 2004 _space_group_IT_number 73 _symmetry_space_group_name_Hall '-I 2b 2c' _symmetry_space_group_name_H-M 'I b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.6732 _cell_length_b 16.6735 _cell_length_c 39.2666 _exptl_crystal_F_000 4224.00 _reflns_d_resolution_high 0.7981 _[local]_cod_data_source_file ya6218Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030808A in Ibca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1034.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-x+1/2, y+1, -z+1' 'x+1, -y+1, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'x+1/2, -y, z' '-x, y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1069179.13 1415129.75 34316.89 o 4 0 0 6997.22 7113.68 156.98 o 6 0 0 153920.47 163040.19 2810.79 o 8 0 0 56191.02 52084.67 953.74 o 10 0 0 1621.13 1526.73 98.15 o 12 0 0 21226.03 23182.54 496.19 o 14 0 0 476.52 771.78 184.91 o 16 0 0 5389.88 5631.11 362.00 o 18 0 0 418.93 506.47 176.86 o 20 0 0 117.70 184.89 176.86 o 2 2 0 20721.68 22693.29 521.84 o 4 2 0 3202.72 3954.19 81.03 o 6 2 0 12796.15 12368.25 185.93 o 8 2 0 1346.66 978.41 49.80 o 10 2 0 16764.78 17607.38 270.92 o 12 2 0 13474.85 14233.04 299.86 o 14 2 0 4814.08 4951.18 188.62 o 16 2 0 5324.47 5306.77 255.78 o 18 2 0 179.36 212.75 122.12 o 20 2 0 11.62 -52.25 125.05 o 0 4 0 4932.03 5608.84 271.54 o 2 4 0 4650.30 5395.03 101.15 o 4 4 0 1866.34 1754.48 52.16 o 6 4 0 921.27 988.09 76.60 o 8 4 0 4261.60 4412.03 134.22 o 10 4 0 1368.11 1438.22 90.73 o 12 4 0 1430.04 1394.98 102.73 o 14 4 0 1457.27 1211.50 112.09 o 16 4 0 845.91 816.42 133.50 o 18 4 0 343.62 562.45 136.07 o 20 4 0 2.57 -66.32 132.64 o 0 6 0 139999.13 153999.45 2316.69 o 2 6 0 14642.64 13931.10 307.72 o 4 6 0 723.70 867.22 50.06 o 6 6 0 922.45 662.69 39.92 o 8 6 0 153.55 8.04 73.90 o 10 6 0 6656.37 8001.62 208.78 o 12 6 0 132.57 92.70 75.41 o 14 6 0 4635.39 5052.33 188.09 o 16 6 0 385.97 371.77 99.16 o 18 6 0 663.75 704.62 141.78 o 20 6 0 84.29 -95.61 133.49 o 0 8 0 53685.45 51528.27 956.10 o 2 8 0 1272.74 914.86 63.14 o 4 8 0 3391.19 3915.35 108.00 o 6 8 0 105.73 41.24 43.87 o 8 8 0 5363.96 6015.85 188.20 o 10 8 0 24367.98 26907.24 518.42 o 12 8 0 2750.18 3339.80 141.32 o 14 8 0 154.75 102.51 89.73 o 16 8 0 49.56 -37.50 92.10 o 18 8 0 24.09 -156.76 213.03 o 0 10 0 1122.78 1289.53 90.48 o 2 10 0 16560.24 18166.05 276.11 o 4 10 0 987.76 1338.03 82.18 o 6 10 0 6049.40 7457.64 220.10 o 8 10 0 22712.35 26026.79 509.84 o 10 10 0 2848.14 2780.02 155.68 o 12 10 0 392.66 240.28 104.05 o 14 10 0 16.65 -9.65 88.74 o 16 10 0 36.58 55.86 89.04 o 18 10 0 638.00 569.49 133.44 o 0 12 0 19750.49 21964.55 424.45 o 2 12 0 13301.83 14101.67 242.57 o 4 12 0 1123.29 1335.19 92.47 o 6 12 0 152.91 175.55 101.25 o 8 12 0 2601.69 2998.04 171.09 o 10 12 0 301.76 163.59 105.11 o 12 12 0 186.94 186.24 90.75 o 14 12 0 588.61 592.79 133.44 o 16 12 0 117.51 30.08 195.65 o 0 14 0 410.52 578.83 305.49 o 2 14 0 3768.03 4154.95 145.54 o 4 14 0 1800.73 1661.81 179.43 o 6 14 0 3826.17 4128.72 248.39 o 8 14 0 183.12 -123.42 127.03 o 10 14 0 13.97 -50.21 209.01 o 12 14 0 569.17 716.89 129.18 o 14 14 0 169.26 122.98 152.91 o 0 16 0 4899.67 5437.67 277.52 o 2 16 0 4655.94 4766.25 190.49 o 4 16 0 1057.23 971.63 233.16 o 6 16 0 290.80 194.19 164.80 o 8 16 0 72.72 16.08 160.78 o 10 16 0 44.13 -135.87 135.87 o 12 16 0 119.86 -44.02 155.84 o 0 18 0 624.12 545.33 147.16 o 2 18 0 125.99 150.55 139.59 o 4 18 0 230.58 111.02 245.19 o 6 18 0 535.48 291.39 253.24 o 8 18 0 35.47 -160.78 160.78 o 10 18 0 595.77 279.52 361.77 o 2 20 0 8.44 -139.76 139.76 o 4 20 0 1.77 -176.85 176.85 o 2 1 1 7755.66 6101.45 101.16 o 4 1 1 115092.98 101968.44 946.01 o 6 1 1 63211.78 57682.43 515.83 o 8 1 1 3846.00 3786.55 64.68 o 10 1 1 603.23 658.08 39.70 o 12 1 1 3303.84 3560.53 77.65 o 14 1 1 2864.59 2788.18 128.58 o 16 1 1 115.27 158.28 73.63 o 18 1 1 1174.43 1184.29 109.50 o 20 1 1 13.10 62.80 87.37 o 1 2 1 6852.84 5278.49 149.08 o 3 2 1 23713.12 19656.70 265.49 o 5 2 1 16782.88 14221.48 169.44 o 7 2 1 2010.95 1641.86 39.08 o 9 2 1 3312.14 3458.66 62.41 o 11 2 1 3804.48 3791.46 72.64 o 13 2 1 11409.11 10829.28 182.67 o 15 2 1 3814.67 4324.52 157.74 o 17 2 1 344.95 541.61 90.23 o 19 2 1 40.05 -10.07 81.34 o 2 3 1 15921.16 13861.91 370.97 o 4 3 1 18934.40 16349.94 237.10 o 6 3 1 6291.97 6372.51 96.33 o 8 3 1 2693.42 3102.93 63.11 o 10 3 1 9081.40 8394.00 109.00 o 12 3 1 3756.49 4414.99 107.78 o 14 3 1 3548.05 3870.46 112.89 o 16 3 1 1143.02 1142.51 103.02 o 18 3 1 4003.29 4385.03 174.82 o 20 3 1 66.40 -19.91 88.29 o 1 4 1 127199.16 114297.31 959.44 o 3 4 1 13275.12 12408.88 234.74 o 5 4 1 1585.23 1824.74 45.82 o 7 4 1 785.97 739.02 49.56 o 9 4 1 1790.95 1896.87 68.12 o 11 4 1 1140.90 1180.55 63.52 o 13 4 1 2560.62 2552.81 92.19 o 15 4 1 4283.47 4504.36 123.00 o 17 4 1 523.30 619.91 95.30 o 19 4 1 603.67 764.97 103.01 o 2 5 1 11453.99 10411.21 162.45 o 4 5 1 1614.98 1866.26 40.45 o 6 5 1 8131.11 7969.53 122.98 o 8 5 1 11294.41 11464.35 188.21 o 10 5 1 555.60 608.74 53.43 o 12 5 1 2790.52 2916.59 94.11 o 14 5 1 928.34 987.77 83.14 o 16 5 1 901.22 1052.39 102.45 o 18 5 1 410.58 405.08 92.87 o 20 5 1 488.75 461.87 105.35 o 1 6 1 65354.76 60827.39 487.35 o 3 6 1 8387.42 8498.56 106.96 o 5 6 1 7477.61 7196.35 95.14 o 7 6 1 1097.90 1076.27 42.29 o 9 6 1 4073.03 4254.23 109.19 o 11 6 1 285.79 312.00 52.81 o 13 6 1 4046.59 4479.06 122.27 o 15 6 1 188.24 247.51 64.00 o 17 6 1 464.73 436.93 90.57 o 19 6 1 0.19 -88.29 88.29 o 2 7 1 1460.09 1389.98 46.59 o 4 7 1 529.47 548.50 36.93 o 6 7 1 1635.76 1620.40 44.52 o 8 7 1 2581.47 2452.67 84.19 o 10 7 1 333.02 375.72 59.56 o 12 7 1 4337.81 4468.68 120.05 o 14 7 1 131.69 202.57 63.85 o 16 7 1 551.11 504.13 72.69 o 18 7 1 5.78 -87.24 87.24 o 1 8 1 5524.68 5610.37 111.75 o 3 8 1 3202.63 3666.55 74.24 o 5 8 1 11836.87 11910.10 147.24 o 7 8 1 2653.03 2543.21 67.36 o 9 8 1 1090.13 1281.87 73.91 o 11 8 1 18.79 -5.67 50.07 o 13 8 1 219.48 204.42 65.05 o 15 8 1 1595.30 1889.17 96.20 o 17 8 1 602.26 508.18 77.69 o 19 8 1 28.93 -109.78 109.78 o 2 9 1 4741.03 4893.98 82.60 o 4 9 1 1202.78 1509.35 56.96 o 6 9 1 3641.09 3844.77 76.66 o 8 9 1 982.46 1229.84 78.00 o 10 9 1 435.02 374.66 67.16 o 12 9 1 1185.89 1165.93 72.91 o 14 9 1 838.65 785.15 71.41 o 16 9 1 429.52 395.06 68.12 o 18 9 1 7.17 122.85 85.49 o 1 10 1 557.87 596.77 46.77 o 3 10 1 11831.34 11052.32 150.40 o 5 10 1 485.28 610.35 47.98 o 7 10 1 427.52 546.76 71.45 o 9 10 1 506.29 247.58 69.50 o 11 10 1 198.18 191.36 62.42 o 13 10 1 1691.29 1684.14 85.70 o 15 10 1 642.95 604.55 75.05 o 17 10 1 42.17 31.51 77.40 o 2 11 1 5606.04 5430.29 106.84 o 4 11 1 1595.03 1767.45 66.70 o 6 11 1 196.38 268.62 70.32 o 8 11 1 26.99 -10.72 68.67 o 10 11 1 251.51 83.15 73.24 o 12 11 1 229.47 255.38 66.81 o 14 11 1 308.21 237.02 68.77 o 16 11 1 227.19 121.70 68.64 o 1 12 1 3008.81 3349.41 81.30 o 3 12 1 5216.02 5961.10 111.93 o 5 12 1 2512.79 2822.80 91.93 o 7 12 1 3102.32 3538.15 124.26 o 9 12 1 799.77 829.69 87.51 o 11 12 1 289.45 178.56 79.72 o 13 12 1 1146.90 1132.82 83.58 o 15 12 1 111.75 82.05 97.23 o 17 12 1 715.82 869.12 112.35 o 2 13 1 9532.90 9696.44 145.55 o 4 13 1 2273.44 2404.50 81.53 o 6 13 1 3190.93 3805.02 127.28 o 8 13 1 159.77 53.07 75.60 o 10 13 1 1313.88 1139.25 97.88 o 12 13 1 810.23 884.86 93.73 o 14 13 1 115.64 140.78 77.04 o 16 13 1 209.85 83.58 118.04 o 1 14 1 3822.72 3793.11 98.88 o 3 14 1 4052.87 4392.57 114.81 o 5 14 1 675.23 844.14 96.77 o 7 14 1 194.18 153.97 85.46 o 9 14 1 574.51 408.58 107.86 o 11 14 1 210.88 -17.33 152.00 o 13 14 1 161.39 151.91 80.26 o 15 14 1 53.00 -77.74 81.22 o 2 15 1 4842.01 5368.90 146.98 o 4 15 1 5874.35 5903.06 199.15 o 6 15 1 268.77 176.23 120.68 o 8 15 1 1633.37 1732.56 135.48 o 10 15 1 614.15 373.45 112.59 o 12 15 1 156.41 -66.78 99.31 o 14 15 1 78.78 -83.57 136.66 o 1 16 1 99.18 112.65 63.26 o 3 16 1 987.12 888.68 138.09 o 5 16 1 1238.18 1098.54 143.90 o 7 16 1 795.82 533.49 225.12 o 9 16 1 471.44 190.32 190.30 o 11 16 1 305.13 -59.59 154.33 o 13 16 1 173.28 27.86 122.12 o 2 17 1 509.25 410.61 117.20 o 4 17 1 762.55 628.90 116.59 o 6 17 1 313.27 81.06 211.18 o 8 17 1 476.97 278.57 225.11 o 10 17 1 28.68 -75.45 111.91 o 12 17 1 762.90 736.59 261.09 o 1 18 1 920.68 926.46 97.96 o 3 18 1 4001.68 4406.77 186.02 o 5 18 1 409.52 25.79 160.13 o 7 18 1 7.59 -113.69 113.69 o 9 18 1 8.78 -119.37 119.37 o 2 19 1 51.13 -96.37 96.37 o 4 19 1 581.62 548.73 164.77 o 6 19 1 0.17 -116.42 116.42 o 8 19 1 19.54 -122.11 122.11 o 1 20 1 13.94 -70.53 98.58 o 3 20 1 45.76 -132.27 132.27 o 5 20 1 429.55 144.78 228.59 o 0 0 2 3.86 0.00 8.04 o 2 0 2 15810.88 13394.45 1125.09 o 4 0 2 144967.42 149189.61 1820.58 o 6 0 2 9835.12 10262.72 162.32 o 8 0 2 81779.65 90217.96 1126.44 o 10 0 2 233.89 259.99 50.97 o 12 0 2 2014.67 2477.04 77.13 o 14 0 2 1011.71 919.00 130.39 o 16 0 2 35.31 16.51 132.64 o 18 0 2 127.03 57.96 107.55 o 20 0 2 1079.75 1413.12 167.63 o 1 1 2 158.01 74.59 16.25 o 3 1 2 19925.72 19250.60 192.66 o 5 1 2 162200.38 171242.27 1476.27 o 7 1 2 32997.63 37374.89 346.97 o 9 1 2 466.44 449.01 33.93 o 11 1 2 367.29 357.18 37.13 o 13 1 2 1591.78 1704.62 73.64 o 15 1 2 3002.50 3189.94 138.60 o 17 1 2 53.41 31.24 77.32 o 19 1 2 123.84 136.36 83.35 o 0 2 2 16716.31 13536.31 242.32 o 2 2 2 77.87 92.15 16.19 o 4 2 2 58989.31 57601.70 590.88 o 6 2 2 39830.97 42578.39 413.48 o 8 2 2 4193.71 4963.64 73.09 o 10 2 2 11493.87 11153.87 135.61 o 12 2 2 1351.40 1561.66 69.82 o 14 2 2 1581.38 1643.05 79.73 o 16 2 2 19.34 47.98 77.15 o 18 2 2 83.68 210.30 85.36 o 20 2 2 360.58 421.48 97.06 o 1 3 2 20463.83 19790.16 173.31 o 3 3 2 835.66 748.02 31.89 o 5 3 2 18722.35 17464.63 215.25 o 7 3 2 27.95 -22.01 29.53 o 9 3 2 1323.05 1447.90 48.25 o 11 3 2 508.03 373.93 51.77 o 13 3 2 2689.24 2762.86 94.47 o 15 3 2 208.37 245.20 69.68 o 17 3 2 909.98 803.12 97.93 o 19 3 2 3.97 -23.42 107.91 o 0 4 2 138151.06 143543.20 1622.17 o 2 4 2 62280.50 59864.66 732.24 o 4 4 2 61.51 65.44 30.54 o 6 4 2 713.64 815.66 33.51 o 8 4 2 1819.34 2419.39 58.53 o 10 4 2 2.03 -19.72 34.91 o 12 4 2 1989.49 2280.92 84.63 o 14 4 2 3033.87 3172.39 104.95 o 16 4 2 1522.59 1442.12 110.28 o 18 4 2 224.72 315.76 90.23 o 20 4 2 149.64 81.65 91.39 o 1 5 2 156281.20 167131.80 1275.06 o 3 5 2 20261.51 18720.18 214.51 o 5 5 2 0.00 -3.67 18.20 o 7 5 2 14146.49 14266.26 183.29 o 9 5 2 2145.16 1954.95 76.51 o 11 5 2 110.73 154.85 49.51 o 13 5 2 192.27 227.14 59.94 o 15 5 2 46.40 122.07 60.17 o 17 5 2 269.09 245.45 88.29 o 19 5 2 100.17 124.93 93.99 o 0 6 2 7362.15 8623.57 236.04 o 2 6 2 41788.92 44486.32 524.12 o 4 6 2 662.34 788.56 35.04 o 6 6 2 184.07 118.07 23.23 o 8 6 2 3.08 -28.81 29.91 o 10 6 2 3884.07 4219.27 113.31 o 12 6 2 23.30 -6.97 55.38 o 14 6 2 4884.77 4830.91 130.21 o 16 6 2 3530.78 3680.46 120.16 o 18 6 2 171.77 51.22 87.05 o 1 7 2 31549.40 36393.94 307.98 o 3 7 2 34.49 66.98 33.90 o 5 7 2 14043.67 14066.72 161.33 o 7 7 2 72.31 80.16 32.60 o 9 7 2 353.71 520.94 54.24 o 11 7 2 718.61 847.05 65.33 o 13 7 2 1011.28 1269.50 79.89 o 15 7 2 13.51 53.11 92.93 o 17 7 2 51.93 -66.40 73.43 o 19 7 2 119.34 -94.39 94.39 o 0 8 2 77864.66 88369.91 949.75 o 2 8 2 4398.64 5136.57 83.61 o 4 8 2 2092.31 2705.54 63.91 o 6 8 2 2.90 27.41 30.86 o 8 8 2 0.07 6.12 51.64 o 10 8 2 63.11 133.75 52.28 o 12 8 2 8740.84 9758.19 175.42 o 14 8 2 89.25 80.08 63.85 o 16 8 2 2172.25 2670.67 112.26 o 18 8 2 4.68 -100.04 100.04 o 1 9 2 584.31 596.77 40.61 o 3 9 2 1109.50 1297.54 54.59 o 5 9 2 1903.41 1888.53 60.50 o 7 9 2 400.80 568.45 67.00 o 9 9 2 39.98 -16.47 58.48 o 11 9 2 132.48 210.17 60.31 o 13 9 2 1148.40 1428.86 77.97 o 15 9 2 11.69 30.33 62.04 o 17 9 2 133.20 108.17 76.72 o 0 10 2 325.40 334.35 52.86 o 2 10 2 11164.33 11197.82 139.19 o 4 10 2 2.55 56.26 42.22 o 6 10 2 3606.00 4057.58 97.24 o 8 10 2 48.62 44.64 62.80 o 10 10 2 0.26 -63.17 63.17 o 12 10 2 5663.14 6450.39 149.74 o 14 10 2 918.15 1071.27 80.24 o 16 10 2 127.16 127.63 73.78 o 18 10 2 35.56 50.53 79.08 o 1 11 2 543.41 526.45 48.13 o 3 11 2 730.07 718.36 55.29 o 5 11 2 77.66 150.76 45.44 o 7 11 2 627.52 813.23 81.84 o 9 11 2 90.61 122.85 73.08 o 11 11 2 49.39 -64.84 64.84 o 13 11 2 2891.06 3248.02 109.54 o 15 11 2 181.98 18.70 70.51 o 17 11 2 9.01 10.81 88.49 o 0 12 2 1440.04 2078.51 106.54 o 2 12 2 1400.52 1683.58 65.75 o 4 12 2 1900.85 2230.18 75.03 o 6 12 2 32.95 132.69 68.11 o 8 12 2 9229.36 9806.50 201.36 o 10 12 2 5379.18 6079.61 160.64 o 12 12 2 50.52 -64.41 72.68 o 14 12 2 299.73 152.77 77.10 o 16 12 2 1033.93 1399.93 104.95 o 1 13 2 2139.71 2227.19 73.54 o 3 13 2 2405.56 2617.50 83.77 o 5 13 2 156.39 328.78 76.40 o 7 13 2 1351.08 1342.76 95.18 o 9 13 2 1228.24 1340.01 111.44 o 11 13 2 2602.50 2943.16 123.85 o 13 13 2 205.34 124.97 76.64 o 15 13 2 144.46 108.38 76.93 o 0 14 2 788.49 994.79 138.93 o 2 14 2 1550.57 1705.28 83.47 o 4 14 2 2915.90 3254.52 134.72 o 6 14 2 4710.81 4482.78 154.16 o 8 14 2 73.80 -79.31 79.31 o 10 14 2 907.73 777.10 108.26 o 12 14 2 301.65 124.17 103.11 o 14 14 2 9.29 -68.13 85.21 o 1 15 2 2747.08 2906.94 90.82 o 3 15 2 221.38 230.77 71.17 o 5 15 2 34.84 -9.18 131.11 o 7 15 2 17.01 -106.75 106.75 o 9 15 2 8.16 -87.11 87.11 o 11 15 2 230.43 -113.69 143.88 o 13 15 2 139.53 -58.88 100.95 o 0 16 2 39.98 1.91 88.76 o 2 16 2 13.07 -21.35 71.90 o 4 16 2 1521.98 1344.71 125.26 o 6 16 2 3489.75 3383.13 179.92 o 8 16 2 2223.09 2313.63 186.86 o 10 16 2 126.64 117.52 111.89 o 12 16 2 991.25 1155.82 162.46 o 1 17 2 36.88 -63.83 63.83 o 3 17 2 790.29 486.54 135.77 o 5 17 2 250.61 -32.97 111.39 o 7 17 2 38.54 124.60 113.69 o 9 17 2 176.32 -50.39 202.24 o 11 17 2 13.14 -116.42 116.42 o 0 18 2 85.22 -32.07 93.23 o 2 18 2 62.71 4.68 95.72 o 4 18 2 190.81 18.05 102.64 o 6 18 2 187.88 -24.12 113.69 o 8 18 2 3.55 -13.40 118.96 o 10 18 2 26.32 35.71 122.11 o 1 19 2 113.68 -5.87 96.54 o 3 19 2 3.62 -100.17 100.17 o 5 19 2 96.87 -104.51 120.58 o 7 19 2 114.35 4.02 125.06 o 0 20 2 1076.97 1648.14 313.55 o 2 20 2 340.79 75.76 109.61 o 4 20 2 134.71 -77.25 161.28 o 2 1 3 41921.43 35017.24 837.50 o 4 1 3 9687.53 7394.55 96.75 o 6 1 3 6744.54 5900.49 89.88 o 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65.36 o 6 8 26 6513.78 6652.23 164.74 o 8 8 26 11.49 -45.04 68.31 o 10 8 26 108.23 1.85 81.29 o 12 8 26 723.41 773.90 101.14 o 14 8 26 0.65 48.72 107.89 o 1 9 26 6633.22 6815.56 132.70 o 3 9 26 411.36 433.83 60.08 o 5 9 26 136.58 170.71 72.42 o 7 9 26 525.59 416.76 75.79 o 9 9 26 5.29 0.14 70.47 o 11 9 26 600.73 585.64 105.59 o 13 9 26 318.23 366.45 160.13 o 15 9 26 612.70 553.46 133.44 o 0 10 26 3684.51 3579.88 141.46 o 2 10 26 962.45 944.32 68.92 o 4 10 26 12.69 -47.43 66.13 o 6 10 26 5780.94 5632.12 157.91 o 8 10 26 91.59 56.24 71.14 o 10 10 26 33.88 -0.88 127.63 o 12 10 26 206.04 68.16 120.67 o 14 10 26 999.52 909.94 131.13 o 1 11 26 2641.71 2619.14 90.39 o 3 11 26 170.75 149.40 61.86 o 5 11 26 1244.42 1246.28 93.89 o 7 11 26 31.57 15.46 71.32 o 9 11 26 620.25 415.37 98.49 o 11 11 26 13.96 -89.83 89.83 o 13 11 26 953.09 859.37 178.70 o 0 12 26 553.03 687.83 91.70 o 2 12 26 97.36 147.96 57.81 o 4 12 26 1725.87 1980.75 119.28 o 6 12 26 100.27 25.14 70.31 o 8 12 26 837.54 898.22 110.08 o 10 12 26 164.78 -44.11 110.23 o 12 12 26 20.04 30.55 113.26 o 1 13 26 1023.17 1112.25 72.35 o 3 13 26 316.96 448.07 85.00 o 5 13 26 2098.56 2204.28 115.16 o 7 13 26 1193.41 1130.27 148.54 o 9 13 26 316.93 122.40 174.05 o 11 13 26 984.61 1136.56 226.28 o 0 14 26 448.69 627.37 98.63 o 2 14 26 21.40 149.70 70.36 o 4 14 26 1446.63 1504.12 121.34 o 6 14 26 481.45 410.24 185.66 o 8 14 26 0.53 8.29 87.34 o 10 14 26 1038.46 1049.40 155.56 o 1 15 26 7.22 136.64 107.25 o 3 15 26 609.18 689.57 136.05 o 5 15 26 484.22 508.99 88.44 o 7 15 26 126.89 114.21 101.17 o 9 15 26 547.42 539.67 164.47 o 0 16 26 48.41 100.72 177.22 o 2 16 26 20.58 83.59 86.50 o 4 16 26 193.44 389.62 91.67 o 6 16 26 6.89 5.77 94.83 o 1 17 26 250.95 397.78 146.20 o 3 17 26 90.37 129.22 85.84 o 2 1 27 227.53 134.65 41.61 o 4 1 27 655.19 622.41 51.63 o 6 1 27 1004.48 1051.54 82.90 o 8 1 27 820.60 762.52 61.11 o 10 1 27 240.23 92.08 58.59 o 12 1 27 671.66 616.20 86.31 o 14 1 27 17.26 -69.09 88.10 o 16 1 27 107.87 160.38 168.82 o 1 2 27 156.13 58.66 36.96 o 3 2 27 2581.68 2254.49 132.58 o 5 2 27 814.92 821.45 59.93 o 7 2 27 14955.83 15223.93 396.95 o 9 2 27 4124.04 4063.77 133.33 o 11 2 27 419.69 276.68 62.82 o 13 2 27 491.11 436.39 77.96 o 15 2 27 16.31 186.42 91.06 o 17 2 27 32.26 -5.59 130.37 o 2 3 27 3847.24 3838.47 94.49 o 4 3 27 2125.80 2047.66 73.46 o 6 3 27 4370.46 4260.66 103.69 o 8 3 27 868.97 854.05 58.24 o 10 3 27 1812.97 1747.44 95.08 o 12 3 27 2150.06 2121.85 85.23 o 14 3 27 125.54 17.13 164.76 o 16 3 27 369.09 360.71 188.22 o 1 4 27 971.93 1096.55 60.70 o 3 4 27 2104.89 2085.52 74.40 o 5 4 27 1397.60 1409.31 68.93 o 7 4 27 16745.35 16658.25 439.67 o 9 4 27 9149.26 8926.08 251.37 o 11 4 27 582.65 537.76 81.49 o 13 4 27 927.14 954.36 133.45 o 15 4 27 26.23 178.33 106.22 o 17 4 27 409.29 60.54 405.98 o 2 5 27 907.24 1014.93 61.55 o 4 5 27 1782.63 2080.67 82.31 o 6 5 27 1240.11 1113.33 71.12 o 8 5 27 2085.44 2095.16 103.31 o 10 5 27 1872.43 1954.84 97.33 o 12 5 27 1209.14 1224.82 103.45 o 14 5 27 238.86 125.13 127.78 o 16 5 27 3.97 -105.68 115.59 o 1 6 27 1377.49 1582.90 72.41 o 3 6 27 3834.67 3765.37 98.66 o 5 6 27 1499.61 1548.92 78.33 o 7 6 27 2800.79 2976.10 116.23 o 9 6 27 31.19 5.51 62.67 o 11 6 27 42.94 -49.66 76.43 o 13 6 27 273.48 158.80 82.49 o 15 6 27 248.47 292.21 119.76 o 2 7 27 10601.03 9944.88 271.82 o 4 7 27 12668.83 11791.83 328.36 o 6 7 27 1942.31 1924.02 85.60 o 8 7 27 2296.07 2285.35 149.73 o 10 7 27 1323.16 1438.44 94.97 o 12 7 27 588.43 568.96 186.82 o 14 7 27 142.94 239.71 90.39 o 1 8 27 1174.76 1271.57 80.06 o 3 8 27 1295.24 1268.69 73.95 o 5 8 27 2076.80 2055.86 102.14 o 7 8 27 1587.61 1476.89 96.77 o 9 8 27 2043.61 2031.73 105.52 o 11 8 27 389.49 365.78 141.56 o 13 8 27 332.69 153.60 155.24 o 15 8 27 153.44 83.83 135.05 o 2 9 27 3054.89 2817.65 94.98 o 4 9 27 7674.23 7595.83 158.83 o 6 9 27 21.40 71.36 70.26 o 8 9 27 2720.92 2648.79 118.52 o 10 9 27 1364.07 1332.62 188.00 o 12 9 27 980.94 857.64 110.69 o 14 9 27 243.87 214.10 107.36 o 1 10 27 313.73 269.39 57.83 o 3 10 27 1353.60 1351.59 82.29 o 5 10 27 1838.67 1784.81 100.17 o 7 10 27 897.78 903.08 83.73 o 9 10 27 921.80 845.75 107.54 o 11 10 27 109.81 37.73 101.71 o 13 10 27 37.87 35.72 124.22 o 2 11 27 537.22 571.84 63.90 o 4 11 27 638.85 761.64 83.84 o 6 11 27 29.58 -4.27 67.56 o 8 11 27 308.42 200.63 88.46 o 10 11 27 123.50 19.29 136.92 o 12 11 27 117.93 23.54 190.29 o 1 12 27 468.43 522.98 65.31 o 3 12 27 2228.08 2563.28 183.96 o 5 12 27 1353.34 1544.15 101.65 o 7 12 27 408.11 324.17 75.32 o 9 12 27 659.51 555.03 156.65 o 11 12 27 163.64 167.09 176.62 o 2 13 27 585.94 613.47 75.19 o 4 13 27 1216.76 1386.23 112.89 o 6 13 27 386.17 323.64 117.16 o 8 13 27 474.55 216.52 160.13 o 10 13 27 29.00 -51.76 114.52 o 1 14 27 25.14 124.08 60.30 o 3 14 27 85.05 140.29 101.00 o 5 14 27 234.56 237.36 124.18 o 7 14 27 153.77 44.72 98.64 o 9 14 27 185.53 157.23 262.32 o 2 15 27 11.04 4.12 93.66 o 4 15 27 35.14 29.81 78.22 o 6 15 27 250.42 371.12 105.23 o 8 15 27 200.56 137.08 105.11 o 1 16 27 72.90 213.41 113.30 o 3 16 27 257.95 442.87 139.95 o 5 16 27 2.77 57.18 160.84 o 2 17 27 28.20 -11.30 85.69 o 0 0 28 1503.87 1339.49 112.02 o 2 0 28 6525.10 5929.32 145.06 o 4 0 28 9828.95 9250.79 225.30 o 6 0 28 39361.66 38094.20 632.37 o 8 0 28 558.45 726.87 93.83 o 10 0 28 794.29 821.26 239.05 o 12 0 28 3073.54 2954.75 225.17 o 14 0 28 1236.91 1372.29 232.49 o 16 0 28 298.77 257.25 176.86 o 1 1 28 2127.92 1853.18 61.00 o 3 1 28 207.50 162.11 49.28 o 5 1 28 5300.94 5325.08 120.20 o 7 1 28 164.60 275.39 54.66 o 9 1 28 208.37 169.67 52.60 o 11 1 28 1464.95 1384.98 86.30 o 13 1 28 2135.40 2132.24 130.05 o 15 1 28 589.90 397.68 162.82 o 17 1 28 93.05 78.09 118.97 o 0 2 28 6582.83 6048.31 146.22 o 2 2 28 4916.36 4345.07 90.42 o 4 2 28 4833.97 4634.62 102.71 o 6 2 28 13264.28 13425.26 194.45 o 8 2 28 1707.38 1855.81 77.30 o 10 2 28 3303.84 3187.65 107.26 o 12 2 28 225.19 53.17 77.90 o 14 2 28 189.77 96.71 98.05 o 16 2 28 2.62 149.99 80.90 o 1 3 28 232.34 231.32 39.59 o 3 3 28 1764.34 1733.39 68.78 o 5 3 28 752.14 589.84 59.54 o 7 3 28 1920.94 2016.23 79.97 o 9 3 28 564.23 632.66 69.11 o 11 3 28 503.86 513.08 61.44 o 13 3 28 64.83 -13.31 111.46 o 15 3 28 17.61 -10.72 132.64 o 0 4 28 9907.93 9571.35 203.31 o 2 4 28 4844.95 4755.01 105.27 o 4 4 28 4.23 14.79 60.77 o 6 4 28 2060.74 1679.86 80.27 o 8 4 28 5381.99 5203.92 117.17 o 10 4 28 1524.38 1551.90 84.27 o 12 4 28 16.48 -30.26 61.36 o 14 4 28 147.64 117.81 241.29 o 16 4 28 273.31 362.71 117.76 o 1 5 28 6133.02 6315.07 124.44 o 3 5 28 801.48 733.86 59.93 o 5 5 28 25.46 34.98 49.56 o 7 5 28 348.03 376.70 58.94 o 9 5 28 23.80 -36.67 61.21 o 11 5 28 210.22 262.75 70.06 o 13 5 28 218.20 66.03 92.33 o 15 5 28 379.73 137.03 236.77 o 0 6 28 41852.45 41752.88 612.39 o 2 6 28 13600.97 13909.52 201.36 o 4 6 28 2583.20 2417.20 108.58 o 6 6 28 14985.20 14531.83 226.39 o 8 6 28 8358.03 8163.52 186.91 o 10 6 28 1199.91 1248.84 88.01 o 12 6 28 240.83 150.23 165.93 o 14 6 28 176.36 -0.34 170.61 o 16 6 28 72.22 145.43 273.32 o 1 7 28 190.22 340.03 60.76 o 3 7 28 1951.94 2162.39 84.67 o 5 7 28 302.37 257.22 62.51 o 7 7 28 5796.51 5706.73 155.94 o 9 7 28 39.58 18.49 68.03 o 11 7 28 37.15 -72.70 87.71 o 13 7 28 57.45 -19.23 88.36 o 15 7 28 291.11 226.43 209.02 o 0 8 28 523.07 647.61 89.36 o 2 8 28 1573.49 1620.03 77.71 o 4 8 28 5735.08 5873.25 138.26 o 6 8 28 9155.46 8943.27 199.25 o 8 8 28 1397.79 1027.46 138.93 o 10 8 28 515.18 590.09 124.16 o 12 8 28 112.18 41.55 109.58 o 14 8 28 34.46 -93.86 93.86 o 1 9 28 206.41 241.60 59.33 o 3 9 28 475.41 657.95 64.67 o 5 9 28 20.81 76.06 75.01 o 7 9 28 30.14 91.84 72.69 o 9 9 28 3195.54 3283.77 172.36 o 11 9 28 16.58 -85.66 143.88 o 13 9 28 41.15 -98.64 98.64 o 0 10 28 948.11 849.00 93.38 o 2 10 28 3219.68 3168.73 101.72 o 4 10 28 1642.35 1583.85 97.34 o 6 10 28 1497.72 1613.08 114.67 o 8 10 28 360.75 589.85 114.46 o 10 10 28 1089.00 1104.75 147.17 o 12 10 28 68.03 -19.83 168.24 o 1 11 28 1044.67 1062.45 73.67 o 3 11 28 551.84 591.21 81.93 o 5 11 28 175.41 57.64 110.00 o 7 11 28 29.59 -77.56 77.56 o 9 11 28 13.85 -47.62 145.04 o 11 11 28 1172.58 1013.21 251.82 o 13 11 28 101.31 -47.33 160.84 o 0 12 28 3055.73 3084.90 140.54 o 2 12 28 274.42 346.99 62.42 o 4 12 28 22.95 -7.43 70.43 o 6 12 28 199.30 150.18 81.16 o 8 12 28 83.19 -63.93 161.15 o 10 12 28 100.40 7.17 105.48 o 12 12 28 35.59 137.26 113.26 o 1 13 28 2195.74 2359.47 94.52 o 3 13 28 72.67 75.61 81.52 o 5 13 28 317.06 196.42 79.24 o 7 13 28 53.75 -90.10 95.63 o 9 13 28 52.84 19.03 95.77 o 11 13 28 144.30 63.57 214.29 o 0 14 28 1096.71 1245.10 107.91 o 2 14 28 199.84 193.73 96.39 o 4 14 28 219.69 149.56 98.23 o 6 14 28 191.81 -25.63 90.85 o 8 14 28 40.85 31.56 113.83 o 1 15 28 574.43 761.46 76.70 o 3 15 28 21.50 -6.02 93.45 o 5 15 28 441.35 422.05 129.83 o 7 15 28 234.29 203.49 156.68 o 0 16 28 218.55 430.09 188.53 o 2 16 28 3.65 23.27 104.42 o 4 16 28 193.76 440.65 155.48 o 6 16 28 65.51 190.06 102.87 o 1 17 28 81.60 155.08 148.04 o 2 1 29 1379.10 1143.20 57.87 o 4 1 29 1891.77 1979.37 78.90 o 6 1 29 645.98 640.76 63.56 o 8 1 29 1029.74 1029.64 69.96 o 10 1 29 32.99 -90.50 90.50 o 12 1 29 383.01 273.33 87.74 o 14 1 29 184.87 140.86 135.71 o 16 1 29 103.79 141.17 144.70 o 1 2 29 1735.63 1624.75 59.34 o 3 2 29 3004.42 2911.90 89.76 o 5 2 29 5245.02 5318.28 121.19 o 7 2 29 6558.87 6500.12 129.32 o 9 2 29 2448.18 2163.47 80.99 o 11 2 29 936.74 893.39 100.22 o 13 2 29 731.78 768.08 121.04 o 15 2 29 32.89 187.71 113.26 o 2 3 29 2025.14 1677.13 68.34 o 4 3 29 4459.92 4492.90 105.66 o 6 3 29 229.89 116.98 52.03 o 8 3 29 3769.60 3547.93 98.42 o 10 3 29 1505.96 1479.01 85.57 o 12 3 29 2122.34 2192.13 137.25 o 14 3 29 373.84 117.03 190.30 o 16 3 29 163.53 331.89 118.97 o 1 4 29 1816.30 1799.80 73.26 o 3 4 29 3918.66 3573.83 101.00 o 5 4 29 962.25 960.70 67.95 o 7 4 29 5057.86 4918.54 113.91 o 9 4 29 3564.49 3572.89 123.31 o 11 4 29 1181.40 1244.33 81.68 o 13 4 29 316.25 45.56 165.93 o 15 4 29 34.96 167.61 111.99 o 2 5 29 3917.15 3509.91 96.46 o 4 5 29 858.37 854.88 67.13 o 6 5 29 26.85 6.68 55.96 o 8 5 29 2081.38 1995.01 102.73 o 10 5 29 1320.77 1302.44 90.17 o 12 5 29 1779.23 1818.92 117.05 o 14 5 29 100.51 132.83 172.84 o 16 5 29 16.05 157.01 129.19 o 1 6 29 960.69 1193.78 69.70 o 3 6 29 342.58 356.06 51.67 o 5 6 29 32.06 68.55 58.12 o 7 6 29 230.14 233.40 85.24 o 9 6 29 547.51 482.78 75.58 o 11 6 29 22.47 -81.98 81.98 o 13 6 29 99.86 134.35 131.28 o 15 6 29 385.20 112.28 263.45 o 2 7 29 7939.40 8409.50 153.09 o 4 7 29 5470.68 5387.73 129.91 o 6 7 29 178.84 262.07 63.34 o 8 7 29 1723.63 1692.50 99.82 o 10 7 29 552.01 551.91 80.21 o 12 7 29 363.20 125.90 106.75 o 14 7 29 62.17 45.52 113.05 o 1 8 29 1085.94 1049.97 71.08 o 3 8 29 4495.05 4411.00 113.90 o 5 8 29 3019.42 3171.73 151.51 o 7 8 29 2385.44 2467.41 115.42 o 9 8 29 776.49 767.91 83.63 o 11 8 29 884.28 752.66 120.68 o 13 8 29 403.59 248.36 184.00 o 2 9 29 3585.87 3437.49 102.98 o 4 9 29 4640.78 4825.35 129.97 o 6 9 29 814.46 694.62 90.37 o 8 9 29 938.53 1085.52 116.59 o 10 9 29 697.09 735.38 110.24 o 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