#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:07:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180966 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/46/2204668.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204668_Fobs loop_ _publ_author_name 'Therrien, Bruno' 'S\"uss-Fink, Georg' _publ_section_title ; Di-\m-chloro-bis[chloro(\h^6^-1,2,4-trimethylbenzene)ruthenium(II)]--dichloromethane (3/2) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1766 _journal_page_last m1768 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.105 _cell_angle_beta 90.644 _cell_angle_gamma 105.358 _cell_length_a 9.9388 _cell_length_b 12.3703 _cell_length_c 14.4034 _exptl_crystal_F_000 948.00 _reflns_d_resolution_high 0.8155 _cod_data_source_file dn6170Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title DN6170 _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2449.43 2016.34 105.05 o 2 0 0 13008.22 10242.74 892.32 o 3 0 0 871.73 943.94 49.39 o 4 0 0 2674.62 2801.92 76.75 o 5 0 0 12850.40 10883.81 676.68 o 6 0 0 337.20 195.37 45.92 o 7 0 0 463.72 395.70 68.33 o 8 0 0 498.92 512.41 58.19 o 9 0 0 2457.70 2431.04 154.67 o 10 0 0 0.02 -33.71 75.02 o 11 0 0 1829.95 2142.19 102.33 o -11 1 0 449.48 441.08 104.10 o -10 1 0 14.14 -74.09 81.01 o -9 1 0 161.67 122.42 73.91 o -8 1 0 4647.19 5190.54 282.57 o -7 1 0 0.10 42.11 48.72 o -6 1 0 35858.87 37463.57 918.60 o -5 1 0 407.98 381.84 40.66 o -4 1 0 646.57 670.73 48.02 o -3 1 0 1968.98 1812.00 137.81 o -2 1 0 5.38 56.60 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