#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204676.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204676_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Kemmitt, Tim' _publ_section_title ; Poly[sodium(I)-\m~3~-bis(ethylenedioxy)borato] ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1943 _journal_page_last m1944 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.271 _cell_angle_gamma 90.000 _cell_length_a 7.9902 _cell_length_b 14.6754 _cell_length_c 5.7065 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.7993 _[local]_cod_data_source_file er6002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' heglna in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 81.18 129.77 9.86 o 6 0 0 64.16 194.24 19.44 o 0 2 0 699.09 1186.52 56.40 o 4 2 0 28.68 75.47 7.11 o 8 2 0 70.13 170.70 22.18 o 5 3 0 763.02 1164.48 66.66 o 7 3 0 8.19 4.69 25.67 o 9 3 0 1.64 5.21 14.87 o 0 4 0 6892.87 11077.42 521.12 o 2 4 0 158.05 205.71 20.26 o 4 4 0 210.08 328.11 24.50 o 6 4 0 12.62 15.83 9.52 o 8 4 0 40.53 41.71 12.80 o 3 5 0 832.05 1084.81 59.96 o 7 5 0 728.68 689.63 39.56 o 9 5 0 71.03 86.65 21.76 o 0 6 0 643.70 811.45 40.38 o 2 6 0 249.23 240.71 11.51 o 4 6 0 229.95 247.69 17.34 o 8 6 0 52.25 50.65 12.48 o 1 7 0 760.32 657.87 33.95 o 3 7 0 78.70 75.84 7.94 o 5 7 0 12.24 21.72 9.44 o 7 7 0 687.51 674.92 31.42 o 0 8 0 6479.37 5547.68 262.68 o 2 8 0 16.17 23.74 6.48 o 4 8 0 228.94 264.84 14.20 o 6 8 0 9.06 17.46 9.37 o 8 8 0 147.28 154.56 15.41 o 1 9 0 1162.21 1013.74 35.96 o 3 9 0 377.76 443.75 43.29 o 5 9 0 753.28 761.61 30.29 o 7 9 0 33.06 27.65 11.74 o 0 10 0 34.64 39.97 9.99 o 2 10 0 8.09 13.14 8.35 o 4 10 0 528.71 557.25 20.61 o 6 10 0 44.38 52.09 12.15 o 8 10 0 26.99 39.29 18.48 o 1 11 0 183.34 176.75 10.02 o 3 11 0 514.27 484.02 31.42 o 5 11 0 110.82 107.39 12.04 o 7 11 0 56.36 45.68 17.38 o 0 12 0 2318.48 2083.53 101.71 o 2 12 0 0.16 3.45 6.72 o 4 12 0 41.02 34.07 10.40 o 6 12 0 26.69 27.43 12.97 o 1 13 0 208.40 193.83 23.82 o 3 13 0 46.30 37.91 7.60 o 5 13 0 33.10 18.63 11.05 o 0 14 0 1.69 -6.98 9.58 o 2 14 0 39.33 46.18 7.97 o 4 14 0 5.03 -5.48 10.40 o 6 14 0 228.72 274.60 19.40 o 1 15 0 19.99 12.01 8.18 o 3 15 0 57.99 48.93 13.35 o 5 15 0 125.24 152.90 19.44 o 0 16 0 15.11 23.00 11.91 o 2 16 0 9.22 18.68 7.69 o 4 16 0 46.39 53.25 10.58 o 1 17 0 101.02 87.43 10.89 o 3 17 0 129.07 132.14 12.27 o 0 18 0 36.44 30.53 14.65 o -9 1 1 0.87 -9.26 17.93 o -7 1 1 247.99 239.38 14.36 o -5 1 1 2752.72 2697.50 91.81 o -3 1 1 462.41 437.06 16.41 o -1 1 1 257.73 258.05 24.43 o 1 1 1 56.21 66.83 4.72 o 3 1 1 455.66 567.46 15.76 o 5 1 1 536.24 568.77 19.43 o 7 1 1 12.37 23.98 16.08 o 9 1 1 110.70 149.43 18.73 o -8 2 1 202.98 180.69 21.90 o -4 2 1 1020.67 1029.20 45.55 o -2 2 1 4615.91 4349.07 122.12 o 0 2 1 8368.52 7763.57 364.80 o 2 2 1 1321.66 1192.94 34.32 o 4 2 1 107.23 92.51 5.58 o 6 2 1 35.45 48.17 8.02 o 8 2 1 231.14 255.43 25.05 o -9 3 1 5.60 -1.69 12.32 o -7 3 1 0.08 -8.81 9.45 o -5 3 1 2469.64 2498.84 132.92 o -3 3 1 150.37 111.31 6.60 o 1 3 1 5238.39 5323.84 127.96 o 3 3 1 1264.68 1340.16 30.41 o 5 3 1 107.66 121.86 7.30 o 7 3 1 14.50 22.69 10.91 o 9 3 1 49.01 36.14 24.78 o -8 4 1 123.57 135.72 19.10 o -6 4 1 377.85 372.21 40.72 o -4 4 1 213.41 192.51 13.79 o -2 4 1 589.24 674.02 37.64 o 2 4 1 4917.38 5381.81 132.49 o 4 4 1 2606.79 2907.85 152.90 o 6 4 1 1142.68 1081.62 41.90 o 8 4 1 116.14 143.16 15.97 o -9 5 1 4.75 14.80 13.79 o -7 5 1 197.21 206.41 13.02 o -5 5 1 439.67 418.06 28.54 o -3 5 1 9.04 9.50 5.77 o -1 5 1 666.52 762.31 37.92 o 1 5 1 6562.44 6611.81 229.57 o 3 5 1 2902.43 3226.82 71.33 o 5 5 1 25.35 29.95 8.50 o 7 5 1 43.37 50.50 13.21 o -8 6 1 16.70 14.16 11.68 o -6 6 1 253.28 226.81 13.20 o -4 6 1 549.66 603.40 20.81 o -2 6 1 3.47 -7.62 8.70 o 0 6 1 194.31 224.46 8.75 o 2 6 1 1158.87 1245.05 36.51 o 4 6 1 103.83 113.75 6.40 o 6 6 1 0.57 -2.19 8.33 o 8 6 1 5.48 28.36 15.47 o -9 7 1 91.83 102.68 15.30 o -7 7 1 39.98 31.06 10.46 o -5 7 1 402.94 380.22 26.76 o -3 7 1 128.15 145.27 23.54 o -1 7 1 0.94 -3.73 5.25 o 1 7 1 1593.68 1606.23 102.94 o 3 7 1 50.27 43.03 5.31 o 5 7 1 6.87 0.74 7.43 o 7 7 1 12.15 14.88 11.89 o -8 8 1 175.95 171.68 14.70 o -6 8 1 76.45 74.73 13.35 o -4 8 1 102.57 104.35 9.84 o -2 8 1 154.28 141.59 7.68 o 0 8 1 1008.85 886.93 34.03 o 2 8 1 638.24 693.61 21.93 o 4 8 1 607.65 666.95 30.40 o 6 8 1 179.32 188.76 11.80 o 8 8 1 77.76 70.28 16.45 o -7 9 1 0.68 -9.95 10.50 o -5 9 1 1167.02 1112.58 40.89 o -3 9 1 447.10 416.89 30.11 o -1 9 1 33.39 24.08 5.88 o 1 9 1 1204.33 1158.33 34.46 o 3 9 1 213.19 216.50 13.26 o 5 9 1 399.56 429.31 19.19 o 7 9 1 30.35 41.11 13.34 o -8 10 1 21.62 20.46 19.30 o -6 10 1 991.23 970.33 37.22 o -4 10 1 878.74 843.65 31.75 o -2 10 1 1398.54 1267.38 44.81 o 0 10 1 194.50 161.64 13.89 o 2 10 1 919.32 916.72 47.09 o 4 10 1 186.59 192.03 10.68 o 6 10 1 192.71 205.47 15.78 o -7 11 1 0.62 9.76 12.22 o -5 11 1 1362.52 1333.28 48.54 o -3 11 1 448.76 456.93 36.48 o -1 11 1 0.00 2.53 6.19 o 1 11 1 132.77 118.13 8.91 o 3 11 1 254.57 281.14 15.12 o 5 11 1 167.97 183.35 12.22 o 7 11 1 20.87 31.83 26.28 o -6 12 1 40.27 60.59 12.41 o -4 12 1 250.50 272.75 22.38 o -2 12 1 227.03 216.96 11.76 o 0 12 1 33.96 30.52 7.02 o 2 12 1 380.28 378.13 16.64 o 4 12 1 126.88 130.83 11.38 o 6 12 1 89.15 100.41 14.70 o -7 13 1 53.10 68.44 21.49 o -5 13 1 83.98 89.79 11.81 o -3 13 1 131.91 146.24 12.18 o -1 13 1 240.12 218.48 26.35 o 1 13 1 36.91 27.83 7.88 o 3 13 1 451.70 434.44 50.78 o 5 13 1 353.77 388.52 27.86 o -6 14 1 88.29 98.68 14.85 o -4 14 1 11.42 5.72 8.70 o -2 14 1 1104.29 1041.86 40.38 o 0 14 1 4.12 10.02 7.09 o 2 14 1 0.50 -5.00 6.92 o 4 14 1 49.40 62.83 16.02 o -5 15 1 66.32 62.97 16.84 o -3 15 1 112.47 111.85 10.25 o -1 15 1 174.75 161.38 11.18 o 1 15 1 494.89 436.55 19.26 o 3 15 1 31.55 36.57 13.07 o 5 15 1 161.24 187.40 23.54 o -4 16 1 4.49 3.98 9.73 o -2 16 1 16.99 10.28 8.32 o 0 16 1 379.55 363.94 19.57 o 2 16 1 218.04 238.56 14.26 o 4 16 1 259.73 330.85 28.34 o -3 17 1 1.42 12.50 9.49 o -1 17 1 0.53 2.27 8.74 o 1 17 1 153.33 174.97 22.31 o 3 17 1 130.57 169.46 21.49 o 0 18 1 36.28 48.87 17.11 o -8 0 2 1261.15 1107.67 58.04 o -6 0 2 16.64 26.28 11.09 o -4 0 2 3638.37 3109.16 195.13 o -2 0 2 1.46 2.34 4.24 o 0 0 2 1292.15 1075.73 36.72 o 2 0 2 624.73 502.23 21.65 o 4 0 2 4164.68 3985.36 112.80 o 6 0 2 844.96 786.72 25.89 o 8 0 2 38.87 38.69 13.69 o -9 1 2 128.60 129.54 14.81 o -7 1 2 417.63 405.24 18.49 o -5 1 2 42.13 46.51 10.80 o -3 1 2 1709.33 1708.07 60.73 o -1 1 2 2758.50 2558.98 85.39 o 1 1 2 204.01 237.24 5.85 o 3 1 2 2389.67 2237.88 45.23 o 5 1 2 1518.90 1333.55 31.19 o 7 1 2 14.92 12.56 7.38 o -8 2 2 0.10 -10.62 10.62 o -6 2 2 116.78 100.13 8.66 o -4 2 2 755.83 797.66 38.34 o -2 2 2 5068.19 4797.65 134.10 o 0 2 2 43.92 50.50 5.69 o 2 2 2 0.33 -3.69 3.69 o 4 2 2 10.05 9.80 5.00 o 6 2 2 647.70 594.09 16.33 o 8 2 2 2.21 17.74 11.35 o -9 3 2 8.64 -0.42 11.87 o -7 3 2 967.41 891.29 33.68 o -5 3 2 0.03 -3.82 6.52 o -3 3 2 986.43 1025.54 30.68 o -1 3 2 1781.45 1953.35 68.71 o 1 3 2 1347.43 1371.52 33.93 o 3 3 2 1099.89 1150.48 26.43 o 5 3 2 5.38 9.63 5.63 o 7 3 2 0.01 16.50 10.62 o -8 4 2 284.06 257.85 15.68 o -6 4 2 69.57 75.81 8.13 o -4 4 2 559.94 583.76 18.67 o -2 4 2 0.01 3.74 3.65 o 0 4 2 285.55 258.16 9.02 o 2 4 2 699.71 751.75 19.79 o 4 4 2 475.53 468.97 12.72 o 6 4 2 135.11 143.84 9.19 o 8 4 2 2.75 17.58 17.47 o -9 5 2 49.21 36.51 13.03 o -7 5 2 0.12 -4.93 9.00 o -5 5 2 481.81 476.00 29.05 o -3 5 2 1153.66 1127.72 33.11 o -1 5 2 5613.35 5729.64 137.83 o 1 5 2 34.98 40.58 5.19 o 3 5 2 152.87 155.47 8.00 o 5 5 2 482.02 450.39 12.95 o 7 5 2 44.80 35.72 11.23 o -8 6 2 5.54 -0.65 10.64 o -6 6 2 153.88 164.88 11.71 o -4 6 2 2079.52 2021.36 58.31 o -2 6 2 6387.60 6402.56 246.26 o 0 6 2 24.36 23.75 5.07 o 2 6 2 187.22 173.67 8.79 o 4 6 2 119.69 136.73 7.14 o 6 6 2 1390.52 1328.22 40.88 o 8 6 2 2.53 -1.95 16.93 o -9 7 2 38.42 38.98 12.32 o -7 7 2 18.43 16.77 9.01 o -5 7 2 26.28 28.36 7.57 o -3 7 2 1260.70 1141.91 39.24 o -1 7 2 2741.43 2474.13 78.64 o 1 7 2 512.29 581.04 23.02 o 3 7 2 120.14 113.61 7.02 o 5 7 2 545.68 476.57 17.71 o 7 7 2 3.14 -0.09 11.40 o -8 8 2 119.08 117.50 12.66 o -6 8 2 149.93 132.79 11.22 o -4 8 2 196.65 210.58 10.79 o -2 8 2 20.05 20.06 6.21 o 0 8 2 1.61 0.42 5.60 o 2 8 2 45.64 52.59 7.07 o 4 8 2 816.14 762.15 36.97 o 6 8 2 44.21 41.31 10.32 o -7 9 2 33.39 37.46 10.45 o -5 9 2 226.55 234.79 13.38 o -3 9 2 48.16 53.05 6.61 o -1 9 2 467.65 425.74 15.20 o 1 9 2 91.83 77.20 7.48 o 3 9 2 154.07 179.25 10.42 o 5 9 2 169.04 167.53 10.98 o 7 9 2 19.31 22.04 26.15 o -8 10 2 27.74 23.72 12.48 o -6 10 2 18.48 18.92 10.24 o -4 10 2 152.72 139.96 10.52 o -2 10 2 0.02 3.94 6.89 o 0 10 2 156.83 144.23 8.28 o 2 10 2 326.37 359.05 23.41 o 4 10 2 105.09 108.36 10.95 o 6 10 2 29.75 30.28 13.53 o -7 11 2 429.12 480.29 28.34 o -5 11 2 45.45 41.19 9.86 o -3 11 2 67.21 56.69 7.92 o -1 11 2 32.87 30.89 7.11 o 1 11 2 177.68 179.42 29.09 o 3 11 2 489.95 474.85 29.98 o 5 11 2 12.79 17.99 12.11 o -6 12 2 1.50 -6.09 10.72 o -4 12 2 201.97 227.61 13.54 o -2 12 2 176.03 177.97 10.93 o 0 12 2 103.34 83.09 13.00 o 2 12 2 244.03 240.23 18.62 o 4 12 2 240.39 244.28 23.48 o 6 12 2 23.83 29.29 19.16 o -5 13 2 11.27 9.75 13.14 o -3 13 2 43.19 45.45 9.72 o -1 13 2 140.42 150.44 14.10 o 1 13 2 9.42 15.33 11.50 o 3 13 2 126.62 119.50 15.33 o 5 13 2 89.49 88.05 21.76 o -6 14 2 26.46 13.14 13.83 o -4 14 2 72.25 86.92 14.24 o -2 14 2 630.03 668.00 38.05 o 0 14 2 8.17 5.48 12.05 o 2 14 2 1.01 -12.32 12.32 o 4 14 2 8.39 10.59 10.93 o -5 15 2 0.51 5.75 15.06 o -3 15 2 329.81 305.66 21.22 o -1 15 2 185.10 186.99 17.80 o 1 15 2 62.86 66.80 14.10 o 3 15 2 64.57 62.97 14.92 o -4 16 2 0.19 -1.64 13.96 o -2 16 2 163.29 155.50 17.11 o 0 16 2 2.96 -6.30 12.87 o 2 16 2 107.53 113.61 17.11 o -1 17 2 108.48 134.28 18.48 o 1 17 2 0.49 11.64 15.88 o -9 1 3 158.16 170.84 16.01 o -7 1 3 79.82 78.65 13.76 o -5 1 3 132.36 165.51 12.93 o -3 1 3 11.65 13.53 4.06 o -1 1 3 1952.08 1973.73 54.68 o 1 1 3 830.39 826.24 19.12 o 3 1 3 112.65 128.42 6.44 o 5 1 3 212.17 179.48 8.09 o 7 1 3 28.17 28.26 9.09 o -8 2 3 1.15 -0.65 10.64 o -6 2 3 101.27 101.12 13.63 o -4 2 3 634.78 693.79 27.89 o -2 2 3 1211.25 1194.79 44.96 o 0 2 3 3656.63 3582.47 86.81 o 2 2 3 97.82 91.33 5.13 o 4 2 3 332.67 314.16 10.13 o 6 2 3 22.78 14.16 6.92 o -9 3 3 85.22 100.03 13.74 o -7 3 3 703.31 642.65 21.87 o -5 3 3 34.98 37.95 7.22 o -3 3 3 125.55 120.81 7.09 o -1 3 3 662.68 648.76 24.31 o 1 3 3 1649.51 1611.29 40.05 o 3 3 3 2.26 9.14 4.95 o 5 3 3 23.56 18.06 6.27 o 7 3 3 570.65 543.56 20.81 o -8 4 3 308.90 304.45 16.99 o -6 4 3 1238.76 1204.18 36.42 o -4 4 3 59.68 49.45 10.40 o -2 4 3 207.98 238.87 9.07 o 0 4 3 2174.45 2276.30 55.87 o 2 4 3 77.20 70.28 5.07 o 4 4 3 829.10 757.28 18.95 o 6 4 3 104.50 114.74 8.09 o -9 5 3 7.04 -2.46 17.66 o -7 5 3 1320.16 1305.66 47.23 o -5 5 3 54.96 56.20 10.75 o -3 5 3 38.91 39.41 7.98 o -1 5 3 0.74 -0.25 5.36 o 1 5 3 836.77 786.49 20.85 o 3 5 3 39.04 35.77 5.93 o 5 5 3 80.28 82.75 8.02 o 7 5 3 523.60 530.40 28.75 o -8 6 3 111.23 135.52 18.07 o -6 6 3 71.31 63.42 10.52 o -4 6 3 92.26 72.76 9.41 o -2 6 3 231.48 196.76 11.09 o 0 6 3 525.62 528.02 28.86 o 2 6 3 79.26 89.85 7.39 o 4 6 3 77.54 73.15 7.31 o 6 6 3 75.20 71.37 16.56 o -7 7 3 202.76 207.79 19.30 o -5 7 3 2.38 13.10 9.08 o -3 7 3 423.45 412.77 18.47 o -1 7 3 1196.00 1128.35 41.57 o 1 7 3 51.25 49.54 13.48 o 3 7 3 205.73 209.48 9.00 o 5 7 3 62.29 59.64 8.35 o -8 8 3 0.91 -14.24 14.24 o -6 8 3 544.25 533.27 24.03 o -4 8 3 232.70 243.17 14.17 o -2 8 3 47.49 58.89 9.74 o 0 8 3 195.71 195.35 11.28 o 2 8 3 41.28 32.79 8.52 o 4 8 3 892.30 811.64 23.08 o 6 8 3 15.08 17.35 13.18 o -7 9 3 158.86 146.88 18.34 o -5 9 3 11.04 8.27 9.47 o -3 9 3 481.13 471.45 20.82 o -1 9 3 469.10 442.50 37.51 o 1 9 3 631.02 589.94 24.09 o 3 9 3 104.46 102.04 8.44 o 5 9 3 1.81 5.40 11.18 o -8 10 3 49.77 30.80 17.52 o -6 10 3 161.55 172.61 18.21 o -4 10 3 34.13 30.66 9.53 o -2 10 3 1012.03 984.12 37.88 o 0 10 3 1874.75 1726.88 63.05 o 2 10 3 298.87 302.91 15.46 o 4 10 3 64.49 45.41 11.01 o -7 11 3 63.73 68.99 18.07 o -5 11 3 0.32 11.77 13.55 o -3 11 3 6.36 11.57 15.67 o -1 11 3 1139.76 1070.25 42.57 o 1 11 3 690.85 688.42 29.84 o 5 11 3 7.32 18.96 12.61 o -6 12 3 37.67 34.22 14.51 o -4 12 3 18.15 19.44 12.73 o -2 12 3 0.45 8.08 12.46 o 0 12 3 283.14 260.36 19.16 o 2 12 3 4.57 -0.82 11.64 o 4 12 3 6.50 1.41 11.34 o -5 13 3 0.07 17.80 14.37 o -3 13 3 219.79 204.64 17.11 o -1 13 3 55.53 57.77 13.41 o 1 13 3 4.80 -11.77 11.77 o 3 13 3 44.99 57.90 14.10 o -4 14 3 75.96 96.64 15.33 o -2 14 3 223.76 189.04 19.03 o 0 14 3 157.35 152.49 17.38 o 2 14 3 36.99 41.34 14.24 o -3 15 3 377.29 423.39 27.65 o -1 15 3 1.89 -12.87 13.41 o 1 15 3 113.92 94.04 16.15 o -2 16 3 0.03 -14.51 14.51 o 0 16 3 94.95 96.91 16.97 o 0 0 4 41.88 57.22 11.91 o 2 0 4 657.79 624.24 24.97 o 4 0 4 1018.10 892.53 35.15 o 6 0 4 0.18 8.81 11.26 o -7 1 4 74.10 107.04 19.30 o -3 1 4 647.22 604.89 34.36 o -1 1 4 12.46 25.08 8.07 o 1 1 4 506.66 460.13 13.47 o 3 1 4 356.96 336.35 11.54 o 5 1 4 328.57 288.96 11.75 o -8 2 4 10.81 -7.25 20.12 o -6 2 4 135.01 94.59 17.25 o -4 2 4 8.25 10.40 11.77 o -2 2 4 37.12 57.24 8.62 o 0 2 4 11.31 8.04 5.85 o 2 2 4 1475.57 1427.27 36.88 o 4 2 4 4.88 5.01 6.57 o 6 2 4 28.79 25.18 8.59 o -7 3 4 113.59 81.72 20.53 o -5 3 4 11.73 9.99 15.19 o -3 3 4 579.98 513.46 30.11 o -1 3 4 33.19 28.83 8.35 o 1 3 4 175.06 166.53 9.24 o 3 3 4 130.17 110.85 7.49 o 5 3 4 156.49 136.56 9.14 o -8 4 4 46.32 43.94 18.89 o -6 4 4 175.92 158.65 19.99 o -4 4 4 290.91 306.80 15.51 o -2 4 4 358.68 395.35 27.38 o 0 4 4 12.61 26.35 6.48 o 2 4 4 51.55 54.92 6.49 o 4 4 4 175.80 172.48 9.34 o 6 4 4 36.04 35.99 9.10 o -7 5 4 1.80 -2.37 11.51 o -5 5 4 751.96 709.06 42.98 o -3 5 4 0.03 5.56 7.48 o -1 5 4 463.51 486.90 20.31 o 1 5 4 1065.31 1041.61 31.88 o 3 5 4 256.64 249.73 10.08 o 5 5 4 125.10 119.55 12.11 o -8 6 4 165.69 179.78 55.92 o -6 6 4 152.06 187.14 14.20 o -4 6 4 0.53 -6.54 10.09 o -2 6 4 405.92 403.13 25.87 o 0 6 4 75.19 76.71 10.49 o 2 6 4 2893.22 2621.16 66.28 o 4 6 4 4.03 -7.07 7.07 o -7 7 4 1.13 8.26 12.98 o -5 7 4 726.94 789.32 95.00 o -3 7 4 4.69 1.79 10.40 o -1 7 4 6.16 2.19 7.87 o 1 7 4 543.35 569.44 41.07 o 3 7 4 279.21 265.22 10.75 o 5 7 4 20.45 9.60 8.15 o -8 8 4 42.64 60.91 18.07 o -6 8 4 144.89 153.04 22.72 o -4 8 4 595.88 649.00 38.19 o -2 8 4 85.97 80.96 10.17 o 0 8 4 90.59 105.17 9.97 o 2 8 4 36.44 40.49 7.83 o 4 8 4 157.76 128.89 11.38 o -7 9 4 18.67 36.27 16.97 o -5 9 4 125.75 134.73 13.05 o -3 9 4 172.85 192.69 36.00 o -1 9 4 665.60 629.44 25.77 o 1 9 4 65.51 61.50 9.46 o 3 9 4 14.15 12.67 8.24 o 5 9 4 2.21 8.92 12.91 o -6 10 4 3.29 25.73 15.60 o -4 10 4 49.31 21.89 10.89 o -2 10 4 264.41 269.47 15.84 o 0 10 4 58.85 74.07 10.38 o 2 10 4 32.34 30.65 9.30 o 4 10 4 0.01 12.18 15.74 o -5 11 4 109.92 107.32 17.66 o -3 11 4 112.47 145.00 12.49 o -1 11 4 18.23 13.98 11.16 o 1 11 4 17.06 26.71 10.40 o 3 11 4 42.07 52.92 10.89 o -6 12 4 62.71 68.03 17.25 o -4 12 4 188.19 209.98 20.26 o -2 12 4 93.32 108.27 13.71 o 0 12 4 20.84 12.67 11.08 o 2 12 4 2.35 11.09 13.28 o -5 13 4 173.20 179.59 21.08 o -3 13 4 9.01 23.13 13.28 o -1 13 4 0.53 14.24 14.10 o 1 13 4 43.75 37.51 14.24 o -4 14 4 0.28 -5.89 15.60 o -2 14 4 4.77 -0.55 16.15 o 0 14 4 1.10 -9.72 14.37 o -1 15 4 0.05 -9.99 16.56 o -7 1 5 7.63 10.78 12.29 o -5 1 5 3.80 1.93 9.93 o -3 1 5 116.89 138.12 12.32 o -1 1 5 55.11 74.32 10.78 o 1 1 5 6.98 7.70 5.50 o 3 1 5 349.70 412.71 23.87 o 5 1 5 11.45 28.31 10.13 o -8 2 5 146.19 141.13 21.35 o -6 2 5 25.13 55.18 12.19 o -4 2 5 25.30 24.86 10.88 o -2 2 5 17.48 13.30 7.56 o 0 2 5 8.21 8.45 6.70 o 2 2 5 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