#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/46/2204699.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204699_Fobs loop_ _publ_author_name 'Grice, I. Darren' 'Jenkins, Ian D.' 'Busfield, W. Ken' 'Byriel, Karl A.' 'Kennard, Colin H. L.' _publ_section_title ; tert-Butyl diphenylphosphinate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2384 _journal_page_last o2385 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5300 _cell_length_b 17.1180 _cell_length_c 15.2850 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8425 _[local]_cod_data_source_file hg60973sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 195RQ12 {C16 H19 O2 P} pbca z=8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 348.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 81697.22 81620.80 418.49 o 4 0 0 51.89 59.46 25.54 o 6 0 0 179.47 190.08 31.74 o 8 0 0 1613.42 1541.62 63.94 o 10 0 0 1380.78 1177.41 67.93 o 12 0 0 0.47 -108.33 108.33 o 2 1 0 6815.98 6663.62 64.08 o 4 1 0 28.26 51.07 55.81 o 6 1 0 2.18 19.70 68.94 o 8 1 0 807.54 783.45 51.84 o 10 1 0 1068.72 1048.57 68.64 o 12 1 0 287.26 164.17 118.57 o 0 2 0 18247.59 17510.68 146.22 o 2 2 0 28348.27 27098.52 246.81 o 4 2 0 1.32 -29.91 59.45 o 6 2 0 459.45 505.14 36.86 o 8 2 0 1468.21 1482.52 62.11 o 10 2 0 433.39 291.91 54.37 o 12 2 0 182.29 99.23 113.09 o 2 3 0 2803.96 2689.28 42.30 o 4 3 0 0.29 78.06 47.42 o 6 3 0 647.89 769.58 41.98 o 8 3 0 2.93 28.82 84.26 o 10 3 0 13.25 132.77 85.35 o 12 3 0 53.77 33.56 100.31 o 0 4 0 121602.10 124990.48 594.96 o 2 4 0 396.87 368.41 27.38 o 4 4 0 2873.80 2894.93 55.73 o 6 4 0 735.40 838.28 44.54 o 8 4 0 355.12 395.17 46.34 o 10 4 0 273.71 185.34 49.62 o 12 4 0 20.00 113.07 94.47 o 2 5 0 14735.41 14243.94 137.78 o 4 5 0 758.45 830.85 38.35 o 6 5 0 302.24 220.39 34.30 o 8 5 0 79.23 76.97 93.38 o 10 5 0 23.04 101.77 87.18 o 12 5 0 0.10 69.30 93.74 o 0 6 0 1773.95 1738.40 38.08 o 2 6 0 21149.91 21282.76 207.86 o 4 6 0 25.76 77.69 58.00 o 6 6 0 523.49 479.95 40.51 o 8 6 0 2814.92 2818.63 87.42 o 10 6 0 834.48 817.25 64.97 o 12 6 0 250.25 361.90 54.36 o 2 7 0 10.81 -25.17 53.98 o 4 7 0 3390.16 3172.02 64.87 o 6 7 0 467.55 493.77 42.70 o 8 7 0 146.78 91.93 101.78 o 10 7 0 6.17 -104.32 104.32 o 12 7 0 58.90 0.00 102.50 o 0 8 0 3472.74 3721.84 63.45 o 2 8 0 2711.34 2612.45 58.97 o 4 8 0 3593.24 3412.48 71.46 o 6 8 0 1203.63 1312.64 55.52 o 8 8 0 215.93 105.07 113.46 o 10 8 0 98.86 20.43 101.04 o 12 8 0 39.85 -124.38 126.94 o 2 9 0 1054.01 997.93 43.10 o 4 9 0 937.06 890.63 45.28 o 6 9 0 660.01 628.16 47.81 o 8 9 0 100.28 128.77 96.67 o 10 9 0 153.16 198.08 46.69 o 12 9 0 76.98 76.97 104.32 o 0 10 0 431.49 386.85 33.94 o 2 10 0 2301.61 2402.93 63.28 o 4 10 0 61.89 68.94 32.10 o 6 10 0 178.86 208.67 45.97 o 8 10 0 26.37 19.33 86.81 o 10 10 0 31.78 88.27 87.18 o 2 11 0 328.44 285.34 37.58 o 4 11 0 970.37 896.37 53.67 o 6 11 0 30.10 8.39 90.46 o 8 11 0 47.94 112.71 93.38 o 10 11 0 50.20 -34.65 95.93 o 0 12 0 3561.39 3591.78 80.92 o 2 12 0 1162.30 1096.70 55.15 o 4 12 0 788.55 833.01 51.47 o 6 12 0 176.88 81.35 102.51 o 8 12 0 91.13 119.28 95.21 o 10 12 0 54.07 48.51 101.04 o 2 13 0 17.27 39.39 76.96 o 4 13 0 664.56 692.36 51.83 o 6 13 0 208.30 106.16 94.12 o 8 13 0 3.17 22.98 94.83 o 10 13 0 58.62 126.94 96.66 o 0 14 0 61.85 56.17 76.60 o 2 14 0 53.41 -43.04 87.54 o 4 14 0 225.42 198.46 41.59 o 6 14 0 517.41 508.31 52.55 o 8 14 0 146.63 182.39 117.46 o 2 15 0 157.85 94.12 99.59 o 4 15 0 30.56 118.55 68.57 o 6 15 0 9.61 99.58 74.04 o 8 15 0 2.54 0.00 94.83 o 0 16 0 94.11 103.60 37.57 o 2 16 0 6.95 11.67 38.66 o 4 16 0 7.97 -95.93 95.93 o 6 16 0 21.04 94.47 97.39 o 8 16 0 20.99 150.28 93.74 o 2 17 0 0.00 -33.19 78.79 o 4 17 0 26.10 57.27 92.28 o 6 17 0 87.74 -63.11 120.37 o 0 18 0 173.97 111.99 89.38 o 2 18 0 164.34 71.50 109.07 o 4 18 0 180.56 61.65 127.31 o 6 18 0 126.08 148.10 108.70 o 2 19 0 0.67 76.96 88.63 o 4 19 0 1.02 -66.02 107.97 o 0 20 0 84.51 77.70 95.20 o 2 20 0 104.57 165.24 101.04 o 1 1 1 926.26 914.77 21.64 o 2 1 1 1185.60 1154.55 28.58 o 3 1 1 1539.01 1482.32 37.36 o 4 1 1 1429.51 1471.78 39.88 o 5 1 1 2055.39 2095.49 52.71 o 6 1 1 14.08 -14.95 62.74 o 7 1 1 305.18 321.10 39.41 o 8 1 1 15.43 -28.09 79.52 o 9 1 1 152.39 -45.60 100.32 o 10 1 1 95.98 112.72 82.80 o 11 1 1 7.27 -99.21 99.21 o 12 1 1 11.47 66.02 107.60 o 13 1 1 3.79 -98.12 106.87 o 0 2 1 951.14 888.82 21.27 o 1 2 1 13054.42 13661.85 131.76 o 2 2 1 22454.85 23783.34 236.20 o 3 2 1 5397.60 5138.16 57.31 o 4 2 1 48.27 84.63 59.82 o 5 2 1 440.65 413.56 34.68 o 6 2 1 283.33 191.57 34.30 o 7 2 1 485.69 448.54 42.70 o 8 2 1 261.33 175.49 45.97 o 9 2 1 1878.57 1779.23 72.35 o 10 2 1 304.35 252.47 51.08 o 11 2 1 429.67 491.12 53.27 o 12 2 1 3.40 88.63 106.14 o 13 2 1 64.32 86.45 101.04 o 1 3 1 124.39 109.84 21.89 o 2 3 1 505.61 509.21 29.22 o 3 3 1 1496.81 1484.96 37.33 o 4 3 1 0.17 46.69 51.43 o 5 3 1 7195.86 7708.38 91.49 o 6 3 1 312.66 355.05 34.67 o 7 3 1 1519.95 1699.55 61.76 o 8 3 1 16.24 14.59 89.73 o 9 3 1 13.11 62.74 86.45 o 10 3 1 36.17 97.76 94.47 o 11 3 1 98.07 0.00 97.76 o 12 3 1 10.89 111.61 101.04 o 13 3 1 0.01 -99.58 117.08 o 0 4 1 6093.99 5616.58 59.08 o 1 4 1 21512.54 21320.52 207.75 o 2 4 1 5701.49 5520.61 59.56 o 3 4 1 4538.06 4325.58 56.71 o 4 4 1 1.29 15.68 51.06 o 5 4 1 1997.51 2047.34 54.15 o 6 4 1 58.84 43.77 70.04 o 7 4 1 1174.68 1146.88 56.25 o 8 4 1 101.02 59.82 86.45 o 9 4 1 741.13 844.99 57.67 o 10 4 1 3.23 -54.35 88.63 o 11 4 1 229.70 111.63 123.67 o 12 4 1 2.59 8.02 47.05 o 13 4 1 31.82 138.97 101.77 o 1 5 1 1870.51 1772.58 39.20 o 2 5 1 1574.18 1527.29 38.80 o 3 5 1 362.05 327.77 26.64 o 4 5 1 151.09 129.52 29.55 o 5 5 1 125.46 97.04 31.37 o 6 5 1 40.97 -17.14 62.38 o 7 5 1 6.41 -13.50 82.43 o 8 5 1 20.10 107.97 89.37 o 9 5 1 24.76 57.63 99.21 o 10 5 1 0.03 120.73 97.02 o 11 5 1 38.41 113.80 87.18 o 12 5 1 0.00 -126.20 126.20 o 13 5 1 9.49 76.96 104.32 o 0 6 1 5974.26 6304.92 66.11 o 1 6 1 5373.71 5773.42 65.64 o 2 6 1 30.35 -18.60 55.08 o 3 6 1 149.44 146.30 25.54 o 4 6 1 1029.59 1036.05 42.01 o 5 6 1 264.74 222.94 35.03 o 6 6 1 234.34 253.21 37.58 o 7 6 1 291.30 389.31 42.32 o 8 6 1 1.42 16.05 88.63 o 9 6 1 54.30 76.60 87.18 o 10 6 1 3.04 9.48 81.70 o 11 6 1 51.18 95.57 102.50 o 12 6 1 2.35 -47.42 109.42 o 13 6 1 79.87 75.51 52.89 o 1 7 1 422.40 466.50 30.30 o 2 7 1 223.52 227.32 28.10 o 3 7 1 3584.99 3502.26 64.18 o 4 7 1 1318.20 1410.17 49.70 o 5 7 1 1629.82 1639.28 54.46 o 6 7 1 55.86 136.06 73.68 o 7 7 1 359.08 342.63 46.34 o 8 7 1 18.87 -95.93 95.93 o 9 7 1 81.97 -8.75 91.56 o 10 7 1 59.68 78.79 94.47 o 11 7 1 0.91 -110.88 110.88 o 12 7 1 8.43 12.04 111.61 o 0 8 1 28.76 0.00 51.07 o 1 8 1 13332.28 14381.22 147.82 o 2 8 1 1558.31 1387.10 46.07 o 3 8 1 1450.56 1476.96 48.61 o 4 8 1 489.15 576.67 39.05 o 5 8 1 239.30 202.13 36.85 o 6 8 1 114.89 131.33 94.48 o 7 8 1 1156.71 1201.05 61.35 o 8 8 1 14.10 -118.18 118.18 o 9 8 1 458.41 467.79 51.45 o 10 8 1 0.21 -109.06 109.06 o 11 8 1 50.16 56.54 110.16 o 12 8 1 0.13 -37.57 107.97 o 1 9 1 0.25 5.11 52.16 o 2 9 1 1979.33 2118.32 57.05 o 3 9 1 548.28 511.01 35.77 o 4 9 1 0.25 30.27 60.91 o 5 9 1 284.35 311.59 38.31 o 6 9 1 2.51 59.09 77.33 o 7 9 1 349.82 374.36 54.00 o 8 9 1 97.44 147.74 89.74 o 9 9 1 35.64 57.63 84.99 o 10 9 1 0.31 10.58 94.47 o 11 9 1 1.63 -11.67 106.51 o 12 9 1 4.60 180.19 90.82 o 0 10 1 67.60 124.75 27.72 o 1 10 1 605.16 594.64 38.69 o 2 10 1 158.75 218.53 31.37 o 3 10 1 3883.63 3666.88 78.05 o 4 10 1 726.50 832.67 47.82 o 5 10 1 2797.27 2661.01 77.19 o 6 10 1 213.86 178.40 45.24 o 7 10 1 1574.82 1469.52 73.42 o 8 10 1 25.09 -48.88 86.45 o 9 10 1 253.03 193.36 51.44 o 10 10 1 15.23 10.94 86.45 o 11 10 1 223.71 223.99 58.00 o 1 11 1 2.80 -66.75 66.75 o 2 11 1 3.66 0.00 60.55 o 3 11 1 0.60 -20.43 65.29 o 4 11 1 58.26 27.72 33.56 o 5 11 1 946.06 833.14 58.05 o 6 11 1 176.77 132.79 48.88 o 7 11 1 517.59 517.81 57.66 o 8 11 1 107.84 -109.07 109.07 o 9 11 1 0.06 137.51 86.81 o 10 11 1 1.38 115.99 88.27 o 11 11 1 3.70 37.93 100.31 o 0 12 1 243.11 93.77 75.89 o 1 12 1 309.88 339.33 40.87 o 2 12 1 166.75 123.31 75.15 o 3 12 1 1331.12 1258.28 62.46 o 4 12 1 371.77 263.81 47.07 o 5 12 1 3260.52 3274.15 95.13 o 6 12 1 197.85 233.84 44.14 o 7 12 1 214.40 240.78 46.70 o 8 12 1 0.31 -54.35 93.01 o 9 12 1 66.84 -33.56 114.17 o 10 12 1 0.14 -123.65 123.65 o 11 12 1 56.38 171.07 102.86 o 1 13 1 0.06 -7.66 78.06 o 2 13 1 90.46 -47.79 91.20 o 3 13 1 2.31 32.46 67.48 o 4 13 1 77.64 101.77 80.62 o 5 13 1 9.09 45.23 72.95 o 6 13 1 11.95 -38.66 86.81 o 7 13 1 2.97 42.68 76.96 o 8 13 1 10.98 126.57 101.04 o 9 13 1 0.69 -70.40 90.82 o 10 13 1 14.26 -38.30 114.53 o 0 14 1 288.96 318.51 42.69 o 1 14 1 292.81 352.81 46.34 o 2 14 1 224.55 198.10 45.24 o 3 14 1 96.00 131.69 75.87 o 4 14 1 23.38 119.28 84.62 o 5 14 1 5.83 39.03 91.55 o 6 14 1 37.14 35.75 44.50 o 7 14 1 0.13 22.61 89.36 o 8 14 1 3.85 -85.35 114.90 o 9 14 1 1.25 -49.61 92.65 o 1 15 1 9.82 -55.44 81.70 o 2 15 1 2.09 -28.45 67.48 o 3 15 1 1.18 -9.48 72.95 o 4 15 1 4.68 39.76 62.74 o 5 15 1 320.77 256.48 52.54 o 6 15 1 140.26 22.25 106.52 o 7 15 1 122.57 121.11 109.43 o 8 15 1 6.15 -87.54 87.54 o 9 15 1 6.12 -13.13 89.36 o 0 16 1 16.32 86.08 68.21 o 1 16 1 0.43 100.67 72.58 o 2 16 1 10.13 40.85 85.72 o 3 16 1 397.15 396.61 47.80 o 4 16 1 77.83 138.61 94.84 o 5 16 1 828.38 844.93 64.24 o 6 16 1 105.08 83.17 87.91 o 7 16 1 114.22 89.01 52.53 o 8 16 1 0.77 41.22 91.92 o 1 17 1 4.65 43.41 74.04 o 2 17 1 2.08 44.13 79.88 o 3 17 1 18.04 44.50 84.62 o 4 17 1 0.03 68.94 79.52 o 5 17 1 0.57 12.04 89.36 o 6 17 1 4.86 12.77 98.85 o 7 17 1 2.97 109.42 96.66 o 0 18 1 58.98 89.73 96.30 o 1 18 1 50.26 58.73 94.84 o 2 18 1 35.36 107.24 90.10 o 3 18 1 145.58 167.44 98.49 o 4 18 1 20.99 74.04 42.68 o 5 18 1 131.26 -12.77 117.82 o 6 18 1 3.80 -98.48 98.48 o 1 19 1 3.21 -12.77 81.34 o 2 19 1 27.40 25.53 85.35 o 3 19 1 6.82 102.86 65.65 o 4 19 1 57.75 118.91 94.47 o 0 20 1 25.22 -103.23 103.23 o 1 20 1 23.64 109.06 90.46 o 2 20 1 8.83 41.58 47.42 o 1 0 2 5065.31 5185.89 53.03 o 2 0 2 35562.30 36789.33 293.01 o 3 0 2 311.90 251.88 28.11 o 4 0 2 2158.91 2090.71 43.59 o 5 0 2 511.57 507.43 35.78 o 6 0 2 1358.01 1265.18 47.14 o 7 0 2 767.66 719.96 45.27 o 8 0 2 1794.01 1767.00 67.98 o 9 0 2 851.68 903.87 62.42 o 10 0 2 185.48 183.86 101.78 o 11 0 2 0.13 -47.42 47.42 o 12 0 2 0.37 66.38 93.74 o 13 0 2 0.66 -24.80 107.60 o 1 1 2 2305.29 2085.96 30.58 o 2 1 2 94.05 48.16 24.45 o 3 1 2 332.51 371.26 28.11 o 4 1 2 202.68 244.85 27.00 o 5 1 2 103.73 85.73 29.18 o 6 1 2 2073.19 2119.87 57.80 o 7 1 2 41.36 0.00 65.66 o 8 1 2 561.14 563.51 50.37 o 9 1 2 43.29 -61.65 97.76 o 10 1 2 460.11 522.53 52.91 o 11 1 2 194.38 128.41 108.71 o 12 1 2 14.44 -91.19 91.19 o 13 1 2 22.47 37.20 122.92 o 0 2 2 12679.50 11859.57 112.88 o 1 2 2 60.37 85.74 20.80 o 2 2 2 1664.92 1708.66 36.66 o 3 2 2 45.68 11.31 57.27 o 4 2 2 1850.36 1863.94 43.19 o 5 2 2 539.11 517.30 36.87 o 6 2 2 983.11 1097.92 47.12 o 7 2 2 249.63 242.63 39.40 o 8 2 2 606.43 782.90 51.83 o 9 2 2 245.15 253.56 50.35 o 10 2 2 226.92 257.20 48.16 o 11 2 2 40.43 79.52 101.40 o 12 2 2 47.97 126.21 48.88 o 13 2 2 1.26 74.77 109.79 o 1 3 2 5169.16 5184.56 51.90 o 2 3 2 20.61 -56.54 56.54 o 3 3 2 1665.06 1943.93 41.37 o 4 3 2 523.81 527.57 33.22 o 5 3 2 31.20 68.21 58.36 o 6 3 2 183.32 143.75 71.87 o 7 3 2 48.73 32.10 74.78 o 8 3 2 111.61 117.83 89.74 o 9 3 2 61.38 79.15 103.96 o 10 3 2 26.79 -44.87 85.72 o 11 3 2 48.61 100.67 84.26 o 12 3 2 113.49 182.02 49.61 o 13 3 2 29.38 75.50 92.28 o 0 4 2 806.03 738.45 28.88 o 1 4 2 2561.98 2554.43 42.60 o 2 4 2 854.67 799.67 32.53 o 3 4 2 1466.45 1614.38 39.51 o 4 4 2 130.91 147.76 29.19 o 5 4 2 2218.04 2350.86 57.45 o 6 4 2 126.09 222.17 33.93 o 7 4 2 95.78 86.09 84.63 o 8 4 2 99.50 15.32 103.96 o 9 4 2 244.52 97.41 112.37 o 10 4 2 0.96 109.79 86.81 o 11 4 2 4.58 122.92 83.16 o 12 4 2 21.73 -54.35 54.35 o 13 4 2 1.43 -123.28 123.28 o 1 5 2 3420.16 3244.47 49.25 o 2 5 2 4198.28 4247.38 57.76 o 3 5 2 4270.41 4269.85 65.06 o 4 5 2 88.89 113.09 27.72 o 5 5 2 1821.37 1998.82 56.68 o 6 5 2 62.68 116.36 67.48 o 7 5 2 193.55 194.82 41.23 o 8 5 2 329.55 379.46 52.18 o 9 5 2 58.29 -33.19 106.51 o 10 5 2 0.11 149.91 78.42 o 11 5 2 11.59 104.32 94.47 o 12 5 2 10.65 -35.02 115.99 o 13 5 2 18.80 -51.79 120.00 o 0 6 2 12829.06 12123.75 122.31 o 1 6 2 1744.71 1686.86 40.99 o 2 6 2 1727.01 1777.16 45.74 o 3 6 2 488.17 549.02 33.95 o 4 6 2 876.71 797.65 39.44 o 5 6 2 109.83 201.01 32.83 o 6 6 2 241.60 266.34 37.58 o 7 6 2 0.90 21.52 89.00 o 8 6 2 280.93 313.41 55.82 o 9 6 2 141.06 60.19 109.80 o 10 6 2 180.95 144.46 104.33 o 11 6 2 82.33 160.50 92.65 o 12 6 2 84.43 118.92 107.97 o 1 7 2 1943.58 2028.19 49.41 o 2 7 2 75.45 100.32 51.07 o 3 7 2 367.44 403.63 33.58 o 4 7 2 149.24 159.06 31.01 o 5 7 2 17.82 122.92 68.21 o 6 7 2 170.91 156.51 83.18 o 7 7 2 195.36 271.06 45.97 o 8 7 2 218.06 186.79 107.26 o 9 7 2 92.89 107.24 102.50 o 10 7 2 0.05 -79.52 99.58 o 11 7 2 1.47 99.21 78.79 o 12 7 2 44.78 85.35 99.94 o 0 8 2 4209.06 3691.17 64.98 o 1 8 2 317.61 339.75 31.02 o 2 8 2 3938.90 3835.85 70.44 o 3 8 2 2438.90 2454.96 60.02 o 4 8 2 399.20 421.13 36.13 o 5 8 2 533.35 469.73 41.24 o 6 8 2 779.99 772.09 50.38 o 7 8 2 308.61 339.32 51.45 o 8 8 2 217.77 260.48 55.45 o 9 8 2 55.48 139.34 89.73 o 10 8 2 150.88 195.16 51.07 o 11 8 2 12.80 125.11 91.55 o 12 8 2 73.22 0.00 115.27 o 1 9 2 216.95 235.70 29.19 o 2 9 2 1365.74 1426.58 48.23 o 3 9 2 30.70 -45.60 63.47 o 4 9 2 13.53 31.00 67.48 o 5 9 2 33.78 -70.76 70.76 o 6 9 2 176.03 176.21 40.86 o 7 9 2 48.70 16.78 97.76 o 8 9 2 132.64 93.39 93.39 o 9 9 2 0.09 0.00 92.28 o 10 9 2 188.60 117.83 117.10 o 11 9 2 37.52 -115.99 115.99 o 12 9 2 70.80 13.13 106.15 o 0 10 2 2.08 10.94 64.20 o 1 10 2 292.71 309.79 32.84 o 2 10 2 5.62 24.44 62.74 o 3 10 2 473.22 480.64 39.78 o 4 10 2 1.65 6.57 59.82 o 5 10 2 409.26 360.16 44.52 o 6 10 2 25.92 -15.68 92.28 o 7 10 2 24.48 116.72 96.30 o 8 10 2 129.99 0.00 110.53 o 9 10 2 19.71 -90.46 90.46 o 10 10 2 18.63 -33.56 96.66 o 11 10 2 9.89 158.67 99.94 o 1 11 2 64.48 75.14 33.19 o 2 11 2 0.76 -53.62 71.13 o 3 11 2 124.68 132.79 34.29 o 4 11 2 18.87 7.30 76.23 o 5 11 2 4.04 -15.68 83.53 o 6 11 2 461.37 368.19 54.74 o 7 11 2 90.99 57.27 101.77 o 8 11 2 23.24 10.21 88.64 o 9 11 2 2.43 -74.77 93.74 o 10 11 2 34.29 -70.03 106.87 o 11 11 2 3.04 12.77 103.95 o 0 12 2 788.08 818.83 46.00 o 1 12 2 19.96 136.42 68.57 o 2 12 2 919.37 1012.06 52.94 o 3 12 2 117.20 0.00 90.10 o 4 12 2 40.29 79.15 86.08 o 5 12 2 50.77 85.36 92.65 o 6 12 2 143.82 81.71 93.02 o 7 12 2 71.07 30.28 94.48 o 8 12 2 76.70 43.77 87.91 o 9 12 2 0.20 33.56 97.39 o 10 12 2 52.09 -48.88 91.56 o 1 13 2 78.53 -55.08 83.53 o 2 13 2 49.14 152.84 83.90 o 3 13 2 470.11 464.17 50.36 o 4 13 2 15.10 25.90 90.46 o 5 13 2 97.33 0.00 80.98 o 6 13 2 175.10 -19.33 102.87 o 7 13 2 1.03 43.04 86.08 o 8 13 2 31.02 139.34 102.50 o 9 13 2 2.81 0.00 95.93 o 10 13 2 44.07 -12.77 98.48 o 0 14 2 905.83 875.41 56.58 o 1 14 2 403.05 432.75 47.07 o 2 14 2 231.37 279.46 43.41 o 3 14 2 198.68 71.14 82.45 o 4 14 2 133.41 153.94 44.50 o 5 14 2 209.12 202.47 42.32 o 6 14 2 74.88 124.39 87.91 o 7 14 2 20.83 -11.31 92.28 o 8 14 2 254.08 159.79 109.45 o 9 14 2 0.68 12.40 97.39 o 1 15 2 0.98 0.00 82.80 o 2 15 2 29.91 104.69 73.32 o 3 15 2 1.95 -57.63 81.70 o 4 15 2 0.02 59.82 77.33 o 5 15 2 0.33 -52.89 78.42 o 6 15 2 136.77 166.34 95.94 o 7 15 2 0.81 60.91 88.63 o 8 15 2 0.01 -117.08 117.08 o 9 15 2 30.98 -121.83 121.83 o 0 16 2 11.85 58.00 58.00 o 1 16 2 210.14 152.49 91.57 o 2 16 2 12.59 103.22 65.29 o 3 16 2 52.93 72.59 80.98 o 4 16 2 19.98 -86.08 86.08 o 5 16 2 0.00 45.23 76.96 o 6 16 2 27.27 -82.80 95.57 o 7 16 2 2.19 -92.65 92.65 o 8 16 2 25.78 -110.16 110.16 o 1 17 2 34.36 -76.96 88.64 o 2 17 2 0.66 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o 3 3 16 0.17 -35.38 84.26 o 4 3 16 6.22 98.12 86.81 o 5 3 16 3.10 -25.53 119.64 o 6 3 16 28.24 -114.90 114.90 o 0 4 16 1.08 -22.98 72.22 o 1 4 16 7.35 68.94 79.52 o 2 4 16 1.10 11.67 95.56 o 3 4 16 0.03 35.75 90.09 o 4 4 16 31.30 49.97 89.73 o 5 4 16 0.40 25.90 91.55 o 1 5 16 0.72 -93.74 93.74 o 2 5 16 2.81 83.16 66.38 o 3 5 16 0.71 60.91 71.86 o 4 5 16 0.73 113.80 95.56 o 5 5 16 12.81 52.52 94.84 o 0 6 16 1.73 23.71 84.26 o 1 6 16 35.77 -24.07 95.57 o 2 6 16 33.39 22.61 44.14 o 3 6 16 35.80 161.22 81.34 o 4 6 16 115.61 143.36 47.42 o 5 6 16 141.63 120.38 116.00 o 1 7 16 8.67 -11.31 44.50 o 2 7 16 3.45 -12.40 100.31 o 3 7 16 1.60 -38.30 105.78 o 4 7 16 0.55 -124.01 124.01 o 0 8 16 80.68 138.25 80.25 o 1 8 16 15.57 50.34 66.75 o 2 8 16 44.48 -64.20 83.89 o 3 8 16 53.65 130.58 94.11 o 1 9 16 2.96 156.11 84.26 o 1 1 17 7.65 12.04 73.68 o 2 1 17 0.36 -36.84 97.75 o 3 1 17 2.47 -62.74 98.12 o 4 1 17 0.03 -26.26 76.23 o 0 2 17 115.39 84.99 94.84 o 1 2 17 18.45 -98.85 98.85 o 2 2 17 94.64 68.58 47.79 o 3 2 17 56.63 -88.27 91.92 o 4 2 17 16.48 -6.20 43.77 o 1 3 17 5.56 49.24 88.63 o 2 3 17 4.05 -37.57 89.36 o 3 3 17 2.44 51.06 67.48 o 4 3 17 7.95 52.89 77.33 o 0 4 17 185.61 174.74 49.25 o 1 4 17 16.18 -49.97 87.91 o 2 4 17 68.35 0.00 93.02 o 3 4 17 53.88 141.89 94.11 o 1 5 17 1.41 37.93 79.15 o 2 5 17 2.15 64.20 69.30 o 3 5 17 3.37 78.79 78.79 o 0 6 17 6.56 38.66 97.02 o 1 6 17 47.07 -64.56 90.46 o 2 6 17 0.25 78.79 90.82 o 0 0 18 61.87 13.13 96.66 o 1 0 18 47.11 -111.98 111.98 o 1 1 18 0.11 0.00 101.76 o 0 2 18 6.66 -26.26 94.83 o 1 2 18 44.85 26.26 67.48 o