#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/47/2204740.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204740_Fobs loop_ _publ_author_name 'Comerlato, Nadia M.' 'Ferreira, Glaucio B.' 'Howie, R. Alan' 'Wardell, James L.' _publ_section_title ; Bis(tetraphenylarsonium) tris(2-thioxo-1,3-dithiole-4,5-dithiolato)stannate(IV) acetone solvate at 120K ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1781 _journal_page_last m1783 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.080 _cell_angle_beta 99.966 _cell_angle_gamma 101.187 _cell_length_a 11.2238 _cell_length_b 14.7826 _cell_length_c 19.9333 _exptl_crystal_F_000 1540.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file lh6303Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ph4As]2 [Sn(dmit)3] at 120 K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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10317.48 211.93 o 5 1 0 22165.90 21796.10 361.96 o 6 1 0 32452.23 33398.77 723.74 o 7 1 0 28803.87 29782.89 580.36 o 8 1 0 2488.60 2710.10 253.10 o 9 1 0 11137.79 11724.18 287.58 o 10 1 0 2992.96 3507.06 609.92 o 11 1 0 3.30 -254.13 381.20 o 12 1 0 794.60 889.47 457.44 o 13 1 0 1525.57 613.47 386.04 o -14 2 0 151.88 310.41 469.40 o -13 2 0 266.82 304.96 508.27 o -12 2 0 3491.19 3354.58 559.10 o -11 2 0 11339.42 11842.68 1016.54 o -10 2 0 8.32 -254.13 254.13 o -9 2 0 2367.90 2643.00 457.44 o -8 2 0 2137.47 2111.00 122.21 o -7 2 0 20.44 20.10 37.36 o -6 2 0 2580.12 2414.56 80.84 o -5 2 0 1820.49 1859.79 63.36 o -4 2 0 17313.71 17277.88 304.28 o -3 2 0 2692.63 2501.56 69.17 o -2 2 0 4138.87 3912.54 77.12 o -1 2 0 1217.81 1220.19 99.04 o 1 2 0 562.03 629.63 38.12 o 2 2 0 103597.50 98214.60 1989.98 o 3 2 0 13506.65 13531.74 258.96 o 4 2 0 4161.87 3925.72 141.96 o 5 2 0 1674.08 1681.25 76.40 o 6 2 0 18731.41 19157.11 417.24 o 7 2 0 5019.02 5067.89 177.43 o 8 2 0 5438.36 5511.02 236.90 o 9 2 0 7631.53 7380.88 256.42 o 10 2 0 207.87 185.16 69.96 o 11 2 0 5993.38 5845.10 686.16 o 12 2 0 2140.24 1906.01 559.10 o 13 2 0 2294.51 2149.32 485.19 o -14 3 0 2.72 -268.05 372.26 o -13 3 0 1796.33 2008.64 395.34 o -12 3 0 104.29 41.86 368.50 o -11 3 0 1012.45 864.06 381.20 o -10 3 0 2.82 25.41 279.55 o -9 3 0 1175.73 1074.02 118.23 o -8 3 0 13.82 46.68 41.39 o -7 3 0 103.24 45.19 69.18 o -6 3 0 18739.79 19144.04 441.64 o -5 3 0 4431.66 4595.52 110.97 o -4 3 0 12795.66 12977.28 240.93 o -3 3 0 41050.01 39524.40 679.32 o -2 3 0 43830.22 42754.74 565.48 o -1 3 0 21416.21 21103.57 313.35 o 0 3 0 4494.61 4522.75 132.97 o 1 3 0 1716.23 1625.88 72.36 o 2 3 0 1118.05 996.66 63.53 o 3 3 0 7966.49 8018.69 186.17 o 4 3 0 194.79 241.26 58.75 o 5 3 0 2706.96 3114.47 101.11 o 6 3 0 3253.07 3359.13 113.47 o 7 3 0 7703.76 8292.69 330.13 o 8 3 0 13657.90 14012.53 486.97 o 9 3 0 9794.30 10416.79 344.06 o 10 3 0 57.38 -4.04 65.74 o 11 3 0 0.88 127.07 355.79 o 12 3 0 79.55 279.55 457.44 o 13 3 0 1594.12 1676.61 825.94 o -14 4 0 440.41 254.13 508.27 o -13 4 0 17.62 0.00 432.03 o -12 4 0 18.90 -37.27 404.03 o -11 4 0 3877.70 3573.42 457.44 o -10 4 0 1295.12 1192.78 98.22 o -9 4 0 5292.29 4957.31 165.02 o -8 4 0 1905.38 1912.11 106.32 o -7 4 0 700.88 692.84 71.53 o -6 4 0 72.43 66.05 43.05 o -5 4 0 2883.67 3026.42 89.21 o -4 4 0 21943.78 23189.80 451.81 o -3 4 0 28178.64 28272.73 433.26 o -2 4 0 12716.37 12118.29 200.11 o -1 4 0 477.12 348.99 37.68 o 0 4 0 24802.49 24312.18 520.59 o 1 4 0 6817.34 6935.63 214.85 o 2 4 0 1522.31 1436.12 81.86 o 3 4 0 20041.92 20472.93 374.31 o 4 4 0 1130.06 1133.16 109.86 o 5 4 0 4115.77 4190.35 149.64 o 6 4 0 19.12 -18.90 62.94 o 7 4 0 2747.79 2811.32 176.94 o 8 4 0 553.68 614.56 94.66 o 9 4 0 144.29 114.02 127.16 o 10 4 0 547.37 415.98 138.45 o 11 4 0 207.67 252.98 165.19 o 12 4 0 38.11 101.65 432.03 o -14 5 0 3683.80 3939.09 787.82 o -13 5 0 464.22 482.86 508.27 o -12 5 0 322.19 711.58 432.03 o -11 5 0 270.32 234.11 286.43 o -10 5 0 3330.50 3725.52 216.30 o -9 5 0 3626.84 3531.09 174.94 o -8 5 0 2788.98 2692.25 145.85 o -7 5 0 645.81 751.56 68.96 o -6 5 0 909.53 995.19 71.37 o -5 5 0 458.64 458.30 57.10 o -4 5 0 11084.76 11325.33 217.12 o -3 5 0 10010.94 10344.13 188.58 o -2 5 0 4022.06 4456.70 108.64 o -1 5 0 2573.24 2567.37 132.09 o 0 5 0 5.39 37.05 85.58 o 1 5 0 4459.61 4387.40 158.45 o 2 5 0 8648.02 8567.49 281.95 o 3 5 0 1300.83 1161.29 85.09 o 4 5 0 528.78 578.19 77.61 o 5 5 0 19710.14 20491.05 419.99 o 6 5 0 944.77 968.12 87.31 o 7 5 0 13.89 -65.35 68.16 o 8 5 0 2128.17 2063.43 127.56 o 9 5 0 144.82 130.50 140.82 o 10 5 0 987.56 889.47 406.62 o 11 5 0 59.83 -406.62 406.62 o 12 5 0 818.91 1219.85 559.10 o -14 6 0 375.50 50.83 533.68 o -13 6 0 1678.43 1728.12 559.10 o -12 6 0 2320.42 2185.56 559.10 o -11 6 0 1184.92 762.40 508.27 o -10 6 0 0.63 -47.65 76.82 o -9 6 0 9556.80 10060.61 289.13 o -8 6 0 384.81 422.64 90.47 o -7 6 0 12046.00 12067.24 296.76 o -6 6 0 57.26 93.03 56.40 o -5 6 0 5151.03 5034.75 157.28 o -4 6 0 624.03 765.51 60.07 o -3 6 0 39847.57 38896.10 702.17 o -2 6 0 272.53 341.37 69.02 o -1 6 0 12.78 -3.76 38.64 o 0 6 0 18919.24 20221.59 474.85 o 1 6 0 3032.74 2839.02 136.24 o 2 6 0 2612.54 2390.06 127.23 o 3 6 0 15090.92 15372.84 318.76 o 4 6 0 14.68 68.30 68.94 o 5 6 0 4242.28 4444.98 180.66 o 6 6 0 178.07 -7.61 88.71 o 7 6 0 3579.20 3449.79 181.42 o 8 6 0 918.73 999.23 116.67 o 9 6 0 2141.00 2050.06 199.66 o 10 6 0 1494.14 1320.88 444.74 o 11 6 0 2328.36 2267.81 293.11 o 12 6 0 266.35 279.55 711.58 o -14 7 0 187.28 914.88 711.58 o -13 7 0 743.65 203.31 432.03 o -12 7 0 1630.19 1626.46 559.10 o -11 7 0 497.36 584.62 101.32 o -10 7 0 1023.37 1044.64 96.84 o -9 7 0 423.46 313.48 69.35 o -8 7 0 11325.46 11291.60 271.57 o -7 7 0 6592.80 6812.30 182.85 o -6 7 0 8859.23 8850.48 203.75 o -5 7 0 1429.29 1599.16 78.03 o -4 7 0 636.04 547.79 56.88 o -3 7 0 30070.68 30306.18 643.68 o -2 7 0 5189.47 5326.48 183.92 o -1 7 0 5041.75 5633.72 157.12 o 0 7 0 4116.05 4209.24 164.45 o 1 7 0 1412.58 1264.11 95.56 o 2 7 0 3910.78 3810.47 197.90 o 3 7 0 112.49 189.01 74.37 o 4 7 0 3503.54 3715.32 157.13 o 5 7 0 1511.02 1515.04 117.36 o 6 7 0 11944.01 12534.16 369.90 o 7 7 0 7387.33 6999.97 377.27 o 8 7 0 439.04 566.87 148.49 o 9 7 0 775.65 691.11 196.13 o 10 7 0 3.28 6.84 292.25 o 11 7 0 673.34 594.35 257.84 o -14 8 0 7.41 -50.83 533.68 o -13 8 0 1047.31 1219.85 533.68 o -12 8 0 2731.45 2871.72 584.51 o -11 8 0 5967.79 6421.94 384.79 o -10 8 0 9700.23 9679.87 650.02 o -9 8 0 139.31 97.03 88.56 o -8 8 0 200.50 104.94 63.62 o -7 8 0 67.65 37.38 69.37 o -6 8 0 3.46 -73.17 73.17 o -5 8 0 3645.13 3850.33 136.13 o -4 8 0 2627.54 2619.46 113.18 o -3 8 0 3750.91 3581.55 161.72 o -2 8 0 24.49 125.03 85.19 o -1 8 0 56537.02 57080.77 985.49 o 0 8 0 669.38 884.64 75.66 o 1 8 0 90.62 57.44 63.76 o 2 8 0 3734.49 4003.45 182.17 o 3 8 0 1179.20 1102.08 108.67 o 4 8 0 3206.12 3281.66 158.51 o 5 8 0 552.12 544.95 104.40 o 6 8 0 3766.17 4241.85 283.42 o 7 8 0 2221.28 1822.97 171.19 o 8 8 0 3427.68 3306.32 281.95 o 9 8 0 3269.14 3409.29 365.44 o 10 8 0 203.68 -54.89 199.35 o 11 8 0 866.27 1036.66 261.38 o -13 9 0 1728.23 1423.15 559.10 o -12 9 0 211.02 377.25 266.84 o -11 9 0 811.14 595.67 241.43 o -10 9 0 241.02 115.55 160.06 o -9 9 0 283.05 159.69 111.10 o -8 9 0 22.36 -34.93 76.08 o -7 9 0 3969.15 3875.32 145.17 o -6 9 0 17605.76 18460.14 421.06 o -5 9 0 167.48 143.06 67.96 o -4 9 0 26942.93 27309.59 794.62 o -3 9 0 1682.60 1773.36 138.90 o -2 9 0 237.55 47.19 110.04 o -1 9 0 4007.52 4250.21 149.11 o 0 9 0 470.58 507.74 53.70 o 1 9 0 759.25 690.86 102.10 o 2 9 0 6279.84 6048.92 240.75 o 3 9 0 12980.22 13655.63 457.26 o 4 9 0 6790.90 7059.56 294.72 o 5 9 0 11270.81 11689.97 390.08 o 6 9 0 1449.41 1629.55 238.43 o 7 9 0 1264.76 1517.55 297.79 o 8 9 0 3462.35 3351.68 286.76 o 9 9 0 2919.13 2736.56 354.04 o 10 9 0 76.52 270.47 234.70 o -13 10 0 2.21 228.72 457.44 o -12 10 0 996.77 819.89 229.45 o -11 10 0 410.14 313.43 227.30 o -10 10 0 16.98 -202.14 202.14 o -9 10 0 4018.67 4047.73 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2546.78 205.65 o 0 11 0 35.88 107.36 51.99 o 1 11 0 302.21 423.09 100.87 o 2 11 0 15609.82 15694.25 678.98 o 3 11 0 1025.28 1238.80 151.52 o 4 11 0 451.70 286.69 128.89 o 5 11 0 8216.71 8442.80 460.11 o 6 11 0 269.20 364.78 186.21 o 7 11 0 2133.03 1936.77 250.39 o 8 11 0 3675.70 2679.91 376.09 o 9 11 0 30.37 53.82 303.91 o -12 12 0 3483.05 2864.92 406.62 o -11 12 0 450.55 483.83 225.43 o -10 12 0 1448.71 1419.61 243.97 o -9 12 0 2.72 -176.00 176.00 o -8 12 0 137.13 38.03 134.28 o -7 12 0 4013.07 4087.28 239.09 o -6 12 0 952.22 1297.77 173.80 o -5 12 0 0.65 -68.15 101.68 o -4 12 0 2855.11 2827.52 246.62 o -3 12 0 1791.51 1806.92 212.76 o -2 12 0 199.14 84.96 213.59 o -1 12 0 7.02 143.95 189.53 o 0 12 0 1552.17 1363.43 190.74 o 1 12 0 481.78 570.45 158.97 o 2 12 0 17102.06 18283.81 674.27 o 3 12 0 818.39 737.90 151.80 o 4 12 0 2915.18 3090.11 364.45 o 5 12 0 1525.65 991.89 239.78 o 6 12 0 100.76 429.49 222.23 o 7 12 0 285.54 328.75 224.67 o 8 12 0 976.39 875.79 347.32 o -12 13 0 762.01 527.75 262.44 o -11 13 0 33.45 145.47 260.10 o -10 13 0 575.25 744.61 241.93 o -9 13 0 585.26 862.21 213.94 o -8 13 0 212.59 240.86 147.20 o -7 13 0 1211.20 1270.89 239.65 o -6 13 0 9497.89 10177.96 465.18 o -5 13 0 106.97 211.55 185.45 o -4 13 0 108.78 64.74 190.97 o -3 13 0 127.22 259.43 213.40 o -2 13 0 200.65 254.13 215.64 o -1 13 0 925.06 954.33 249.66 o 0 13 0 1787.30 1785.54 229.18 o 1 13 0 26.82 95.15 129.02 o 2 13 0 1964.62 1997.72 267.01 o 3 13 0 3334.09 3474.94 329.13 o 4 13 0 2348.49 2082.18 261.50 o 5 13 0 695.91 365.07 273.35 o 6 13 0 483.26 219.17 237.63 o 7 13 0 765.33 974.89 321.97 o -11 14 0 12.18 212.33 274.64 o -10 14 0 1790.85 1295.05 296.10 o -9 14 0 73.40 14.92 174.85 o -8 14 0 689.45 541.31 354.04 o -7 14 0 9.32 -268.37 304.96 o -6 14 0 497.02 377.15 174.25 o -5 14 0 2254.35 2090.39 242.77 o -4 14 0 978.63 1106.64 296.10 o -3 14 0 507.83 438.23 368.06 o -2 14 0 9.36 48.08 332.08 o -1 14 0 8729.74 10927.79 1067.37 o 0 14 0 215.86 419.32 269.55 o 1 14 0 1945.90 1691.42 340.01 o 2 14 0 559.37 317.67 775.11 o 3 14 0 1628.28 1883.38 292.43 o 4 14 0 173.85 283.24 187.60 o 5 14 0 1399.98 1199.13 312.59 o 6 14 0 1749.95 1395.99 289.68 o 7 14 0 351.28 -127.07 482.86 o -11 15 0 641.20 762.40 508.27 o -10 15 0 219.01 -127.07 482.86 o -9 15 0 211.53 254.13 355.79 o -8 15 0 1418.94 736.99 285.84 o -7 15 0 31.02 311.97 260.10 o -6 15 0 1918.38 2091.49 358.05 o -5 15 0 889.88 571.80 269.55 o -4 15 0 7228.58 6771.01 600.19 o -3 15 0 1475.29 1423.01 332.08 o -2 15 0 590.46 763.94 296.10 o -1 15 0 646.01 405.80 278.10 o 0 15 0 67.45 -140.62 368.50 o 1 15 0 2214.34 1827.79 484.19 o 2 15 0 81.66 -212.99 212.99 o 3 15 0 914.59 938.91 286.91 o 4 15 0 1934.81 1975.78 289.45 o 5 15 0 4417.51 4274.42 574.20 o -10 16 0 2319.56 2922.55 660.75 o -9 16 0 1650.77 1143.61 635.34 o -8 16 0 530.91 898.40 329.18 o -7 16 0 42.36 231.03 292.85 o -5 16 0 308.08 243.24 311.02 o -4 16 0 10.07 20.79 292.85 o -3 16 0 236.87 508.27 508.27 o -2 16 0 869.91 1196.91 368.06 o -1 16 0 278.15 -100.93 314.09 o 0 16 0 100.45 225.73 303.91 o 1 16 0 5993.79 6901.28 745.59 o 2 16 0 1.41 -323.46 323.46 o 3 16 0 483.80 134.08 533.68 o 4 16 0 3.82 -465.13 762.40 o -9 17 0 280.59 609.92 660.75 o -8 17 0 1725.02 2230.29 567.50 o -6 17 0 1055.57 1136.98 412.14 o -4 17 0 1106.75 1101.54 520.20 o -3 17 0 216.61 496.47 499.32 o -2 17 0 1184.94 1325.49 736.99 o -1 17 0 215.98 432.03 571.80 o 0 17 0 1678.11 2033.08 889.47 o 1 17 0 484.91 304.96 431.28 o 2 17 0 748.88 707.79 422.01 o 3 17 0 805.13 1219.85 940.30 o -7 18 0 29.20 -76.24 609.92 o -6 18 0 37.65 159.41 592.19 o -5 18 0 2472.45 2338.62 502.20 o -4 18 0 11.34 -386.04 386.04 o -3 18 0 510.58 70.16 408.64 o -2 18 0 17.10 -458.22 582.16 o -1 18 0 4657.20 4649.43 687.48 o 0 18 0 157.64 1025.49 636.23 o 1 18 0 149.17 -609.92 609.92 o 3 -19 1 706.30 254.13 660.75 o -1 -18 1 2153.57 1266.66 682.15 o 0 -18 1 11.32 426.62 422.01 o 1 -18 1 19.68 316.14 673.46 o 2 -18 1 209.37 -37.57 412.14 o 3 -18 1 596.65 970.90 437.80 o 4 -18 1 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