#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204758.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204758_Fobs loop_ _publ_author_name 'Zhao, Jing-Gui' 'Zhang, Zhu-Yan' 'Huo, Li-Hua' 'Gao, Shan' _publ_section_title ; Hexaaquamagnesium(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1987 _journal_page_last m1988 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.211 _cell_angle_gamma 90.000 _cell_length_a 12.4856 _cell_length_b 12.9038 _cell_length_c 6.8131 _exptl_crystal_F_000 500.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file ng6065Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' z in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 119.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 404.05 352.56 2.50 o 3 0 0 303.35 341.04 4.93 o 4 0 0 7242.48 8165.32 51.65 o 5 0 0 6775.06 7751.33 32.62 o 6 0 0 503.71 747.26 8.60 o 7 0 0 3299.84 4073.55 73.48 o 8 0 0 742.41 802.52 4.12 o 9 0 0 267.17 280.04 3.84 o 10 0 0 194.10 208.30 3.22 o 11 0 0 1069.61 1076.64 10.59 o 12 0 0 4.33 1.84 1.42 o 13 0 0 62.89 65.91 2.81 o 14 0 0 4.27 3.14 1.29 o 15 0 0 2.75 1.77 1.68 o 16 0 0 0.09 -0.93 1.49 o 2 1 0 410.48 453.75 4.87 o 3 1 0 18.17 19.79 0.79 o 4 1 0 10.53 6.59 0.21 o 5 1 0 51.61 57.89 0.64 o 6 1 0 163.50 142.16 1.71 o 7 1 0 1546.23 1858.36 19.52 o 8 1 0 66.26 97.81 1.56 o 9 1 0 10.22 7.45 0.50 o 10 1 0 42.20 46.04 0.67 o 11 1 0 121.69 128.35 3.35 o 12 1 0 123.88 129.42 3.40 o 13 1 0 24.21 26.44 1.28 o 14 1 0 58.01 57.40 1.31 o 15 1 0 46.81 36.86 2.87 o 0 2 0 0.33 11.97 0.26 o 1 2 0 160.18 143.15 0.41 o 2 2 0 2931.94 2994.29 37.16 o 3 2 0 505.42 511.09 9.09 o 4 2 0 17.97 15.72 0.83 o 5 2 0 934.20 1087.14 12.61 o 6 2 0 2469.88 2900.68 23.17 o 7 2 0 1029.49 1138.40 11.27 o 8 2 0 11.81 12.67 0.49 o 9 2 0 145.01 163.14 1.40 o 10 2 0 28.95 23.39 0.84 o 11 2 0 25.63 32.88 1.58 o 12 2 0 98.81 102.11 1.40 o 13 2 0 148.35 143.65 6.24 o 14 2 0 19.05 20.20 1.50 o 15 2 0 4.38 5.22 1.15 o 1 3 0 738.97 862.14 4.98 o 2 3 0 556.78 520.74 3.43 o 3 3 0 4.52 5.01 0.27 o 4 3 0 1117.37 1228.95 12.39 o 5 3 0 913.24 1072.17 8.55 o 6 3 0 5.43 7.98 0.51 o 7 3 0 55.64 68.17 0.52 o 8 3 0 4.19 4.98 0.41 o 9 3 0 12.19 9.93 0.69 o 10 3 0 77.26 86.56 1.53 o 11 3 0 355.14 365.60 6.12 o 12 3 0 48.83 55.40 2.32 o 13 3 0 10.06 6.81 0.70 o 14 3 0 0.53 1.29 0.78 o 15 3 0 8.03 11.51 1.06 o 0 4 0 14243.58 14418.22 77.22 o 1 4 0 8797.99 9346.64 37.83 o 2 4 0 2160.10 2211.23 20.84 o 3 4 0 1617.02 1714.75 15.80 o 4 4 0 221.11 240.94 2.46 o 5 4 0 173.01 211.38 3.06 o 6 4 0 1434.60 1544.76 13.34 o 7 4 0 359.97 420.94 5.98 o 8 4 0 28.34 31.41 0.56 o 9 4 0 10.05 12.26 0.67 o 10 4 0 4.35 4.75 0.55 o 11 4 0 12.55 8.05 0.55 o 12 4 0 438.46 425.80 6.29 o 13 4 0 5.33 1.86 0.65 o 14 4 0 4.05 3.57 1.20 o 15 4 0 0.15 1.69 0.74 o 1 5 0 2076.28 2300.92 10.47 o 2 5 0 76.84 87.48 1.46 o 3 5 0 1045.02 988.88 8.79 o 4 5 0 343.13 328.21 3.33 o 5 5 0 46.76 48.24 0.45 o 6 5 0 53.52 56.36 0.90 o 7 5 0 3.54 4.01 0.43 o 8 5 0 24.74 23.02 0.57 o 9 5 0 5.61 6.49 0.53 o 10 5 0 51.40 50.46 2.27 o 11 5 0 9.58 9.13 1.03 o 12 5 0 20.49 18.85 2.20 o 13 5 0 0.44 0.30 0.75 o 14 5 0 9.53 12.17 0.92 o 15 5 0 4.03 4.00 1.18 o 0 6 0 277.15 335.51 1.06 o 1 6 0 1305.79 1355.85 4.42 o 2 6 0 3.59 6.24 0.38 o 3 6 0 180.13 222.26 2.51 o 4 6 0 66.03 64.69 1.02 o 5 6 0 339.41 349.09 3.34 o 6 6 0 617.04 616.34 6.93 o 7 6 0 20.08 17.40 0.72 o 8 6 0 84.00 85.01 1.38 o 9 6 0 222.56 231.27 4.73 o 10 6 0 185.25 181.66 3.74 o 11 6 0 38.42 43.50 1.31 o 12 6 0 165.27 167.57 6.57 o 13 6 0 102.81 115.87 5.65 o 14 6 0 42.31 42.54 1.18 o 1 7 0 52.43 52.92 0.67 o 2 7 0 292.49 304.76 2.37 o 3 7 0 81.47 88.17 1.13 o 4 7 0 79.46 75.37 0.76 o 5 7 0 101.05 98.80 0.79 o 6 7 0 294.67 266.60 2.94 o 7 7 0 38.59 42.66 0.86 o 8 7 0 43.44 46.68 0.97 o 9 7 0 27.19 27.54 1.34 o 10 7 0 16.36 19.10 0.71 o 11 7 0 5.69 6.93 0.75 o 12 7 0 0.14 0.78 0.64 o 13 7 0 12.56 8.85 1.50 o 14 7 0 8.38 5.94 1.78 o 0 8 0 2344.14 2581.04 14.01 o 1 8 0 902.04 956.92 7.34 o 2 8 0 697.32 667.36 6.11 o 3 8 0 413.79 403.70 2.93 o 4 8 0 28.02 23.75 0.58 o 5 8 0 542.90 528.50 4.16 o 6 8 0 130.45 103.18 0.99 o 7 8 0 1076.95 1118.11 12.93 o 8 8 0 26.81 24.95 1.06 o 9 8 0 28.85 25.94 1.23 o 10 8 0 21.22 24.60 1.42 o 11 8 0 199.86 214.80 3.86 o 12 8 0 9.61 11.50 1.12 o 13 8 0 240.71 256.87 4.21 o 14 8 0 35.04 4.89 3.12 o 1 9 0 370.87 349.80 1.38 o 2 9 0 6.69 5.37 0.73 o 3 9 0 90.75 84.19 1.33 o 4 9 0 58.87 58.56 1.32 o 5 9 0 243.97 230.68 1.71 o 6 9 0 91.99 85.11 0.66 o 7 9 0 221.33 207.92 3.89 o 8 9 0 149.10 151.01 3.88 o 9 9 0 7.58 10.56 1.73 o 10 9 0 16.49 18.96 1.10 o 11 9 0 104.84 121.13 2.00 o 12 9 0 27.74 26.62 1.01 o 13 9 0 0.61 1.12 0.88 o 0 10 0 1542.55 1483.22 33.95 o 1 10 0 8.26 8.75 0.73 o 2 10 0 58.77 56.39 0.71 o 3 10 0 0.01 0.98 0.80 o 4 10 0 0.58 0.90 0.61 o 5 10 0 0.00 1.23 0.68 o 6 10 0 75.26 71.70 1.69 o 7 10 0 71.98 75.57 0.83 o 8 10 0 57.09 49.31 2.07 o 9 10 0 0.00 0.86 0.72 o 10 10 0 17.12 19.32 2.35 o 11 10 0 160.03 183.01 1.90 o 12 10 0 3.01 3.19 1.70 o 1 11 0 748.26 747.14 5.31 o 2 11 0 249.36 250.04 1.54 o 3 11 0 8.66 8.28 0.79 o 4 11 0 33.54 33.44 0.84 o 5 11 0 52.40 53.46 0.80 o 6 11 0 49.03 47.52 0.74 o 7 11 0 15.58 12.49 0.80 o 8 11 0 0.01 2.16 1.42 o 9 11 0 68.48 73.96 1.23 o 10 11 0 0.06 1.39 0.82 o 11 11 0 0.03 0.37 0.87 o 12 11 0 45.44 55.75 2.05 o 0 12 0 475.64 451.76 2.88 o 1 12 0 343.86 360.97 3.32 o 2 12 0 100.19 97.36 0.95 o 3 12 0 20.10 20.71 1.03 o 4 12 0 61.47 74.41 1.21 o 5 12 0 36.48 44.12 0.84 o 6 12 0 297.29 309.95 2.72 o 7 12 0 1.05 1.63 0.70 o 8 12 0 0.93 1.75 0.85 o 9 12 0 44.60 50.55 2.95 o 10 12 0 5.85 7.05 1.41 o 11 12 0 9.25 14.58 2.80 o 1 13 0 9.00 11.47 1.40 o 2 13 0 10.77 12.36 1.21 o 3 13 0 40.24 37.53 0.91 o 4 13 0 2.14 4.70 1.30 o 5 13 0 30.76 28.78 0.93 o 6 13 0 14.85 17.68 0.83 o 7 13 0 60.83 62.18 2.54 o 8 13 0 61.33 64.17 1.17 o 9 13 0 43.81 52.63 2.17 o 10 13 0 66.48 65.32 2.88 o 0 14 0 94.66 101.51 2.71 o 1 14 0 304.19 322.99 1.51 o 2 14 0 69.61 81.45 1.20 o 3 14 0 42.72 45.40 1.02 o 4 14 0 224.01 227.00 2.82 o 5 14 0 64.72 70.60 1.84 o 6 14 0 78.35 86.65 2.11 o 7 14 0 15.29 14.75 1.09 o 8 14 0 30.96 31.80 1.38 o 1 15 0 55.27 54.67 1.15 o 2 15 0 8.10 11.42 1.04 o 3 15 0 34.54 34.67 1.27 o 4 15 0 28.56 30.57 1.31 o 5 15 0 5.80 7.99 1.36 o 6 15 0 3.51 6.51 1.25 o 7 15 0 0.00 1.09 0.82 o 0 16 0 43.81 42.19 1.73 o 1 16 0 0.12 1.42 1.11 o 2 16 0 103.86 112.51 2.76 o 3 16 0 63.09 66.99 2.18 o 4 16 0 6.58 6.60 1.07 o -16 1 1 1.59 0.74 1.16 o -15 1 1 11.49 7.42 2.03 o -14 1 1 57.39 62.25 3.69 o -13 1 1 63.31 52.22 0.92 o -12 1 1 238.95 242.58 6.19 o -11 1 1 13.55 18.00 0.65 o -10 1 1 103.87 96.45 1.14 o -9 1 1 12.86 19.07 0.63 o -8 1 1 279.58 275.53 2.59 o -7 1 1 690.57 686.22 8.24 o -6 1 1 573.36 512.10 6.80 o -5 1 1 12.27 10.58 0.24 o -4 1 1 120.73 100.41 1.41 o -3 1 1 43.37 39.86 1.21 o -2 1 1 358.48 313.62 2.40 o -1 1 1 3753.73 3441.19 22.17 o 0 1 1 70.15 71.61 0.40 o 1 1 1 3725.32 3376.32 42.27 o 2 1 1 1250.48 1225.85 1.42 o 3 1 1 60.50 65.65 0.51 o 4 1 1 567.59 508.92 3.68 o 5 1 1 2723.55 2807.28 24.25 o 6 1 1 4400.26 4832.04 39.32 o 7 1 1 439.76 384.63 2.55 o 8 1 1 35.00 38.29 0.61 o 9 1 1 431.33 427.40 6.61 o 10 1 1 60.15 70.16 1.96 o 11 1 1 169.88 171.72 4.54 o 12 1 1 387.60 334.53 4.77 o 13 1 1 102.22 111.05 2.04 o 14 1 1 18.25 21.77 2.21 o 15 1 1 3.63 5.29 1.05 o -16 2 1 22.79 14.85 2.27 o -15 2 1 15.71 10.34 1.52 o -14 2 1 7.18 9.12 0.86 o -13 2 1 28.87 21.65 0.83 o -12 2 1 303.03 283.58 4.77 o -11 2 1 326.69 292.35 1.90 o -10 2 1 0.27 1.63 0.67 o -9 2 1 0.01 0.52 0.49 o -8 2 1 16.08 19.34 0.40 o -7 2 1 2391.53 2572.67 25.48 o -6 2 1 458.43 558.13 5.00 o -5 2 1 21.45 18.12 1.49 o -4 2 1 242.22 224.43 0.74 o -3 2 1 2.68 4.46 1.11 o -2 2 1 218.82 187.34 3.02 o -1 2 1 3759.80 3344.33 37.47 o 0 2 1 5185.74 4738.42 14.60 o 1 2 1 3011.06 2987.72 28.92 o 2 2 1 336.25 336.58 3.41 o 3 2 1 3835.02 3958.83 73.67 o 4 2 1 27.72 24.35 0.40 o 5 2 1 48.93 46.21 1.17 o 6 2 1 4.86 0.95 0.76 o 7 2 1 166.60 160.03 2.36 o 8 2 1 40.42 35.22 0.92 o 9 2 1 180.32 174.29 2.76 o 10 2 1 463.42 457.19 8.23 o 11 2 1 283.43 272.50 5.88 o 12 2 1 16.65 15.63 0.87 o 13 2 1 55.25 53.96 1.90 o 14 2 1 5.14 5.23 0.81 o 15 2 1 19.58 28.65 3.81 o -15 3 1 1.88 1.36 0.80 o -14 3 1 5.09 7.78 0.90 o -13 3 1 30.81 31.64 1.89 o -12 3 1 28.16 23.25 1.83 o -11 3 1 69.60 67.29 1.01 o -10 3 1 301.17 288.69 4.87 o -9 3 1 16.26 18.13 0.78 o -8 3 1 503.78 485.01 5.68 o -7 3 1 52.97 54.81 1.06 o -6 3 1 458.86 405.30 4.33 o -5 3 1 41.12 23.17 0.64 o -4 3 1 3275.54 3414.89 25.32 o -3 3 1 1773.63 1724.89 11.81 o -2 3 1 1183.65 1232.81 16.80 o -1 3 1 659.33 595.14 3.55 o 0 3 1 9767.39 8791.52 32.34 o 1 3 1 328.32 282.67 4.07 o 2 3 1 887.28 789.63 2.38 o 3 3 1 537.17 544.55 4.34 o 4 3 1 174.72 153.90 1.79 o 5 3 1 646.01 615.25 3.53 o 6 3 1 20.72 23.80 0.50 o 7 3 1 44.12 51.55 0.52 o 8 3 1 302.62 291.09 2.32 o 9 3 1 100.83 97.03 1.17 o 10 3 1 234.44 222.51 3.88 o 11 3 1 159.82 158.66 3.44 o 12 3 1 22.54 29.86 1.16 o 13 3 1 50.09 50.47 2.06 o 14 3 1 1.61 2.16 0.75 o 15 3 1 0.37 0.34 1.03 o -15 4 1 31.33 33.74 1.55 o -14 4 1 23.78 21.80 1.66 o -13 4 1 12.76 10.21 0.82 o -12 4 1 15.95 20.67 1.05 o -11 4 1 119.10 115.53 1.62 o -10 4 1 1.47 2.73 0.57 o -9 4 1 173.90 171.54 2.84 o -8 4 1 37.20 33.23 1.04 o -7 4 1 2.03 2.50 0.29 o -6 4 1 1018.33 995.34 12.66 o -5 4 1 804.06 805.74 8.35 o -4 4 1 19.28 21.84 0.48 o -3 4 1 205.44 205.08 1.49 o -2 4 1 127.99 122.61 1.47 o -1 4 1 2982.86 3044.86 8.90 o 0 4 1 74.77 69.71 2.78 o 1 4 1 2748.47 2679.96 15.31 o 2 4 1 5988.64 5922.41 73.92 o 3 4 1 2764.23 2793.82 32.30 o 4 4 1 64.54 44.70 0.61 o 5 4 1 267.13 256.41 4.01 o 6 4 1 577.07 570.01 5.79 o 7 4 1 101.87 99.02 1.38 o 8 4 1 53.58 57.45 0.57 o 9 4 1 191.29 193.40 0.85 o 10 4 1 153.89 141.42 1.58 o 11 4 1 32.16 38.86 1.12 o 12 4 1 10.03 8.85 0.81 o 13 4 1 3.24 3.57 0.76 o 14 4 1 1.83 3.37 0.99 o 15 4 1 0.18 0.86 0.96 o -15 5 1 2.66 1.26 1.74 o -14 5 1 4.38 3.66 1.31 o -13 5 1 267.89 264.59 3.53 o -12 5 1 276.74 270.61 3.77 o -11 5 1 0.02 0.31 0.48 o -10 5 1 178.53 158.57 5.08 o -9 5 1 7.28 4.88 0.48 o -8 5 1 1057.26 992.00 12.50 o -7 5 1 897.85 819.35 9.83 o -6 5 1 200.88 175.23 2.71 o -5 5 1 587.25 520.58 2.05 o -4 5 1 1023.43 957.07 9.61 o -3 5 1 1370.37 1225.76 18.87 o -2 5 1 137.79 142.10 0.91 o -1 5 1 43.76 58.87 1.20 o 0 5 1 1639.28 1543.65 11.12 o 1 5 1 118.87 134.67 0.74 o 2 5 1 227.91 252.73 2.76 o 3 5 1 701.52 646.42 6.17 o 4 5 1 492.47 441.49 4.25 o 5 5 1 110.94 101.13 2.24 o 6 5 1 51.78 35.32 1.54 o 7 5 1 683.27 600.99 8.24 o 8 5 1 87.06 93.98 2.10 o 9 5 1 1672.80 1594.55 18.33 o 10 5 1 0.64 1.32 0.71 o 11 5 1 299.12 277.10 6.51 o 12 5 1 98.72 97.69 3.15 o 13 5 1 1.31 2.58 1.06 o 14 5 1 0.09 1.50 1.13 o -15 6 1 2.72 3.42 1.20 o -14 6 1 7.28 4.59 1.11 o -13 6 1 1.43 -0.05 0.66 o -12 6 1 21.75 16.96 1.26 o -11 6 1 875.26 860.99 7.99 o -10 6 1 0.06 -0.15 0.64 o -9 6 1 576.39 541.77 9.99 o -8 6 1 234.09 212.68 1.76 o -7 6 1 835.68 814.87 7.01 o -6 6 1 125.81 129.89 1.16 o -5 6 1 48.07 47.32 0.79 o -4 6 1 422.40 387.50 1.90 o -3 6 1 1447.69 1403.53 18.40 o -2 6 1 329.28 287.15 2.45 o -1 6 1 402.18 408.92 3.53 o 0 6 1 4590.28 4847.35 10.92 o 1 6 1 40.60 36.02 0.73 o 2 6 1 197.71 184.23 1.62 o 3 6 1 277.61 254.88 0.97 o 4 6 1 72.35 66.33 0.56 o 5 6 1 230.86 223.26 2.62 o 6 6 1 12.50 9.66 1.32 o 7 6 1 409.93 410.03 4.75 o 8 6 1 1124.66 1046.01 21.39 o 9 6 1 11.93 10.78 0.96 o 10 6 1 5.76 5.77 0.75 o 11 6 1 87.10 85.21 1.70 o 12 6 1 0.09 1.11 0.80 o 13 6 1 73.34 75.54 3.17 o 14 6 1 1.03 1.15 0.86 o -14 7 1 82.57 77.93 1.84 o -13 7 1 17.90 21.19 1.81 o -12 7 1 184.52 191.04 1.54 o -11 7 1 272.38 276.17 5.55 o -10 7 1 530.13 521.75 5.66 o -9 7 1 205.37 184.85 3.01 o -8 7 1 509.68 486.03 5.85 o -7 7 1 309.64 289.23 2.89 o -6 7 1 1436.98 1370.97 4.58 o -5 7 1 260.96 237.34 2.19 o -4 7 1 67.99 56.68 1.37 o -3 7 1 501.09 455.37 2.68 o -2 7 1 539.17 496.01 5.38 o -1 7 1 4416.60 4409.70 27.81 o 0 7 1 93.91 84.62 1.47 o 1 7 1 2189.72 2142.01 10.96 o 2 7 1 84.40 73.68 0.75 o 3 7 1 102.71 99.47 0.81 o 4 7 1 58.58 58.18 1.10 o 5 7 1 195.40 178.00 3.30 o 6 7 1 519.98 489.75 7.08 o 7 7 1 91.44 94.31 1.64 o 8 7 1 20.73 22.13 1.23 o 9 7 1 183.78 175.90 3.04 o 10 7 1 191.67 193.16 2.88 o 11 7 1 6.53 5.99 0.85 o 12 7 1 0.42 0.69 0.72 o 13 7 1 6.05 3.41 1.28 o 14 7 1 1.58 2.11 1.57 o -14 8 1 0.22 1.88 1.18 o -13 8 1 21.78 21.28 2.46 o -12 8 1 19.08 14.30 1.58 o -11 8 1 5.44 3.37 1.19 o -10 8 1 3.19 2.16 0.90 o -9 8 1 21.14 18.66 0.62 o -8 8 1 1.87 3.31 0.97 o -7 8 1 38.21 33.11 0.89 o -6 8 1 131.01 116.88 0.96 o -5 8 1 155.38 128.52 1.18 o -4 8 1 4.20 2.47 0.48 o -3 8 1 796.04 750.13 1.59 o -2 8 1 852.47 780.28 2.37 o -1 8 1 1387.96 1269.99 6.55 o 0 8 1 379.92 342.35 5.06 o 1 8 1 67.28 61.18 0.99 o 2 8 1 1.92 1.47 0.59 o 3 8 1 222.91 201.31 2.27 o 4 8 1 472.81 445.61 2.52 o 5 8 1 54.74 52.12 1.02 o 6 8 1 57.86 56.56 1.11 o 7 8 1 0.03 0.94 0.65 o 8 8 1 200.82 192.21 1.43 o 9 8 1 2.65 2.59 0.66 o 10 8 1 39.27 42.10 1.20 o 11 8 1 35.60 31.32 1.19 o 12 8 1 26.61 27.01 1.72 o 13 8 1 1.67 2.60 0.85 o -13 9 1 26.28 27.29 1.45 o -12 9 1 77.89 76.21 2.20 o -11 9 1 23.96 21.78 2.01 o -10 9 1 0.97 3.01 0.95 o -9 9 1 73.82 71.35 4.28 o -8 9 1 67.53 65.56 1.07 o -7 9 1 147.36 129.33 1.12 o -6 9 1 146.80 140.51 0.67 o -5 9 1 231.98 211.91 1.70 o -4 9 1 312.05 281.13 1.90 o -3 9 1 49.31 50.77 1.04 o -2 9 1 143.87 116.39 0.99 o -1 9 1 686.36 641.61 5.79 o 0 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