#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/47/2204765.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2204765_Fobs
loop_
_publ_author_name
'Song, Cheng'
'Li, Yi-Zhi'
'Chen, Ya-Qing'
'Xiao, Shou-Jun'
'You, Xiao-Zeng'
_publ_section_title
;
 Poly[[terachlorogold(III)potassium(I)(<i>Au{---</i>K})]-\m-4,4'-bipyridine]
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1741
_journal_page_last               m1743
_journal_volume                  60
_journal_year                    2004
_space_group_IT_number           72
_symmetry_space_group_name_Hall  '-I 2 2c'
_symmetry_space_group_name_H-M   'I b a m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   12.9000
_cell_length_b                   7.8312
_cell_length_c                   14.7220
_exptl_crystal_F_000             992.00
_reflns_d_resolution_high        0.7828
_[local]_cod_data_source_file    ob6430Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     Ibam
_shelx_refln_list_code           4
_shelx_f_calc_maximum            547.38
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'x, -y, -z+1/2'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z+1'
'-x+1/2, y+1/2, -z+1'
'-x, -y, -z'
'x, y, -z'
'-x, y, z-1/2'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 87123.55 78056.96 724.22 o
4 0 0 55291.77 53079.42 1301.33 o
6 0 0 35406.30 33736.05 1554.80 o
8 0 0 54000.69 51894.65 86.00 o
10 0 0 32914.91 35414.19 1574.04 o
12 0 0 47734.65 44549.50 840.77 o
14 0 0 27011.24 26350.17 1975.75 o
16 0 0 3328.09 4150.67 1191.56 o
1 1 0 82431.20 108998.21 12312.88 o
3 1 0 89385.90 83443.19 309.68 o
5 1 0 118810.95 110355.59 214.22 o
7 1 0 105218.27 95364.89 988.90 o
9 1 0 26143.97 25906.59 1279.83 o
11 1 0 30503.94 32653.28 857.17 o
13 1 0 36062.53 32356.40 855.31 o
15 1 0 10667.63 9501.95 1674.75 o
0 2 0 145538.03 153430.64 429.75 o
2 2 0 51356.22 51455.54 198.26 o
4 2 0 141403.22 168719.11 14615.64 o
6 2 0 68678.98 62649.21 311.59 o
8 2 0 65098.78 62703.75 229.91 o
10 2 0 28033.83 30541.87 378.38 o
12 2 0 10027.11 13410.25 274.07 o
14 2 0 11741.24 12027.65 1518.59 o
16 2 0 13692.41 12818.63 422.08 o
1 3 0 50436.31 47689.47 159.97 o
3 3 0 108235.34 125249.65 4952.15 o
5 3 0 55472.29 52220.15 349.60 o
7 3 0 27967.34 27993.62 120.59 o
9 3 0 49713.94 46412.16 212.58 o
11 3 0 27463.92 29634.84 651.73 o
13 3 0 12940.94 12866.24 262.54 o
15 3 0 12273.37 11855.65 991.27 o
0 4 0 71848.73 69502.59 452.05 o
2 4 0 80793.20 75913.15 1959.63 o
4 4 0 60211.86 54817.79 127.68 o
6 4 0 7275.31 6931.75 170.25 o
8 4 0 21086.12 20660.90 243.06 o
10 4 0 35415.54 36386.48 1044.44 o
12 4 0 16871.88 17490.02 265.04 o
14 4 0 11385.20 11974.47 229.71 o
1 5 0 29604.20 30674.98 159.20 o
3 5 0 32874.55 32651.95 785.93 o
5 5 0 31748.25 31805.21 585.90 o
7 5 0 20856.04 21080.60 966.93 o
9 5 0 33021.67 32801.38 716.81 o
11 5 0 10685.19 10224.63 152.20 o
13 5 0 7543.32 7157.64 1266.19 o
0 6 0 14613.81 14744.51 284.37 o
2 6 0 17911.41 16500.43 233.34 o
4 6 0 26651.48 28106.07 339.24 o
6 6 0 32161.64 28194.60 750.01 o
8 6 0 15617.22 18999.36 870.28 o
10 6 0 3378.26 3621.34 716.04 o
12 6 0 6067.44 6830.34 1424.17 o
1 7 0 22294.78 21761.54 453.45 o
3 7 0 5161.31 5144.85 255.18 o
5 7 0 11972.90 14860.50 388.82 o
7 7 0 10621.39 10634.53 1343.16 o
9 7 0 9188.55 8653.67 373.07 o
11 7 0 5129.94 5069.26 1323.21 o
0 8 0 17294.70 17247.24 780.71 o
2 8 0 10413.26 8905.26 452.64 o
4 8 0 4632.92 4711.11 461.69 o
6 8 0 5417.74 5167.66 452.53 o
8 8 0 3250.68 3175.39 776.17 o
1 9 0 3653.30 3721.00 445.64 o
3 9 0 3004.02 3211.10 511.03 o
5 9 0 5747.06 5500.59 990.86 o
7 9 0 3908.75 4001.06 635.40 o
0 10 0 1022.25 1647.59 1213.06 o
2 1 1 19.37 311.70 376.89 o
4 1 1 17951.33 19718.09 109.81 o
6 1 1 492.27 624.76 337.76 o
8 1 1 8944.92 12698.75 393.29 o
10 1 1 1088.14 1519.95 287.96 o
12 1 1 648.77 555.70 106.47 o
14 1 1 0.12 126.23 196.52 o
16 1 1 443.20 550.13 264.92 o
1 2 1 2130.50 2008.74 68.77 o
3 2 1 699.85 854.46 187.44 o
5 2 1 6741.10 6296.25 196.73 o
7 2 1 2688.40 2721.23 109.93 o
9 2 1 853.48 696.61 138.63 o
11 2 1 3218.65 3077.94 126.64 o
13 2 1 119.93 515.32 717.25 o
15 2 1 1036.58 1020.39 342.96 o
2 3 1 20219.89 20438.04 76.68 o
4 3 1 1146.55 1323.86 310.42 o
6 3 1 95.67 224.94 99.15 o
8 3 1 978.24 867.99 75.55 o
10 3 1 1228.31 1289.23 124.81 o
12 3 1 58.00 128.57 132.52 o
14 3 1 2050.42 2359.25 599.02 o
1 4 1 2274.98 2225.19 82.02 o
3 4 1 275.75 511.81 170.50 o
5 4 1 40.20 89.30 51.40 o
7 4 1 135.98 286.25 175.84 o
9 4 1 7.17 148.55 173.80 o
11 4 1 70.19 324.18 357.04 o
13 4 1 34.96 181.02 167.75 o
15 4 1 134.01 186.37 220.46 o
2 5 1 5771.00 5408.78 67.01 o
4 5 1 210.62 370.05 285.81 o
6 5 1 449.09 504.69 170.77 o
8 5 1 88.06 298.20 345.96 o
10 5 1 2222.42 2231.54 284.27 o
12 5 1 520.50 595.19 377.10 o
14 5 1 1380.59 1609.70 586.54 o
1 6 1 840.42 1039.26 127.89 o
3 6 1 74.24 84.48 82.48 o
5 6 1 1593.18 1648.54 99.23 o
7 6 1 248.43 236.95 85.10 o
9 6 1 348.54 470.20 149.43 o
11 6 1 249.54 289.74 92.12 o
13 6 1 0.50 332.53 528.33 o
2 7 1 535.06 652.93 240.88 o
4 7 1 1065.27 1105.05 202.88 o
6 7 1 4.20 339.32 487.56 o
8 7 1 784.56 811.93 208.08 o
10 7 1 74.98 151.29 141.54 o
1 8 1 42.67 236.10 279.33 o
3 8 1 30.53 373.42 522.10 o
5 8 1 257.79 449.46 269.16 o
7 8 1 48.78 336.03 475.71 o
9 8 1 316.34 370.96 200.99 o
2 9 1 11.42 403.49 596.05 o
4 9 1 589.24 741.11 483.09 o
6 9 1 9.99 51.29 220.72 o
0 0 2 77104.43 73839.85 682.29 o
2 0 2 82987.01 96055.23 7662.99 o
4 0 2 3444.25 3840.77 235.65 o
6 0 2 58425.82 51894.84 285.61 o
8 0 2 14423.18 14725.54 851.84 o
10 0 2 13845.67 16032.62 716.68 o
12 0 2 41437.46 40018.33 939.96 o
14 0 2 17022.64 15320.09 303.04 o
1 1 2 110115.21 134751.50 7690.75 o
3 1 2 17969.01 17617.17 269.14 o
5 1 2 33302.87 29605.49 213.87 o
7 1 2 38653.34 39855.07 191.68 o
9 1 2 14484.34 17904.93 294.41 o
11 1 2 14176.86 16495.75 677.13 o
13 1 2 13963.56 13530.67 56.61 o
15 1 2 6762.48 6525.41 364.71 o
0 2 2 2495.08 2824.96 202.61 o
2 2 2 36278.15 33549.23 81.82 o
4 2 2 44835.95 44705.11 304.62 o
6 2 2 74032.26 77054.47 2836.77 o
8 2 2 28231.73 30769.64 336.69 o
10 2 2 14937.37 17902.84 132.76 o
12 2 2 6699.33 6060.99 361.68 o
14 2 2 5844.00 4954.25 338.76 o
16 2 2 9079.62 7844.83 1315.88 o
1 3 2 33670.20 30902.66 113.92 o
3 3 2 62219.68 59283.37 193.34 o
5 3 2 17707.17 19706.85 62.50 o
7 3 2 9119.07 9681.12 640.48 o
9 3 2 21344.34 18868.07 302.54 o
11 3 2 16070.93 18502.72 381.86 o
13 3 2 3629.12 3518.41 223.27 o
15 3 2 10679.29 10007.68 359.23 o
0 4 2 17084.82 18260.67 261.39 o
2 4 2 46891.66 43255.72 235.79 o
4 4 2 19011.02 20237.13 408.08 o
6 4 2 3590.16 3674.84 254.04 o
8 4 2 11537.74 15720.91 1173.05 o
10 4 2 30645.25 27032.06 265.83 o
12 4 2 9675.90 9623.66 610.88 o
14 4 2 6032.25 5531.13 582.34 o
1 5 2 13655.48 13384.46 137.26 o
3 5 2 27342.16 25874.81 331.56 o
5 5 2 13949.86 16500.83 400.38 o
7 5 2 12824.50 11189.67 539.90 o
9 5 2 8270.45 7593.38 339.92 o
11 5 2 7234.99 6677.44 543.99 o
13 5 2 2725.67 2705.66 188.27 o
0 6 2 6822.05 8105.88 877.07 o
2 6 2 6537.34 6404.48 391.29 o
4 6 2 10167.75 14323.02 325.93 o
6 6 2 21809.60 23506.92 110.79 o
8 6 2 12593.30 13660.59 256.13 o
10 6 2 4412.79 4054.44 309.44 o
12 6 2 2239.36 2185.64 230.54 o
1 7 2 13180.00 12300.13 357.27 o
3 7 2 5514.31 5585.63 274.42 o
5 7 2 5305.99 5078.15 272.43 o
7 7 2 8150.65 9200.47 643.60 o
9 7 2 866.11 1311.38 444.50 o
11 7 2 4054.34 3817.01 358.73 o
0 8 2 12163.81 10579.09 906.85 o
2 8 2 4748.50 4591.44 130.39 o
4 8 2 1424.45 1532.48 224.45 o
6 8 2 3461.21 3279.18 380.82 o
8 8 2 2665.58 2918.15 317.11 o
1 9 2 2321.65 2363.59 440.48 o
3 9 2 3081.14 3179.95 1061.16 o
5 9 2 2921.67 2800.77 272.60 o
2 1 3 3155.60 2902.30 82.76 o
4 1 3 14547.92 16480.77 79.09 o
6 1 3 420.51 574.97 239.16 o
8 1 3 13584.96 12625.57 327.46 o
10 1 3 184.68 500.60 597.85 o
12 1 3 736.86 642.91 155.12 o
14 1 3 0.26 22.62 130.34 o
16 1 3 147.22 271.42 230.41 o
1 2 3 25777.92 28551.43 93.95 o
3 2 3 808.29 772.99 85.23 o
5 2 3 2620.53 2998.19 117.83 o
7 2 3 13.47 287.21 306.62 o
9 2 3 483.02 484.76 71.06 o
11 2 3 705.64 625.96 159.98 o
13 2 3 41.92 369.92 698.91 o
15 2 3 946.13 1289.04 116.33 o
2 3 3 2207.71 2260.93 246.28 o
4 3 3 1436.16 1759.98 182.47 o
6 3 3 124.31 412.36 367.39 o
8 3 3 505.66 601.90 223.15 o
10 3 3 4537.02 3975.48 129.17 o
12 3 3 160.88 322.62 255.61 o
14 3 3 1669.65 1912.01 280.70 o
1 4 3 1008.22 1282.59 262.38 o
3 4 3 261.80 404.13 209.47 o
5 4 3 349.61 364.36 112.27 o
7 4 3 581.92 656.73 98.37 o
9 4 3 14.63 54.39 74.20 o
11 4 3 1411.97 1589.87 205.13 o
13 4 3 0.51 271.45 509.43 o
2 5 3 10965.95 10163.94 274.54 o
4 5 3 5.56 42.30 106.00 o
6 5 3 243.11 548.47 289.01 o
8 5 3 450.74 691.22 448.75 o
10 5 3 463.09 397.15 91.78 o
12 5 3 356.35 621.39 599.65 o
14 5 3 1263.75 1341.00 508.94 o
1 6 3 52.80 236.57 188.35 o
3 6 3 24.88 289.49 274.27 o
5 6 3 1620.96 1520.83 62.25 o
7 6 3 559.07 698.37 149.57 o
9 6 3 457.24 540.91 222.65 o
11 6 3 768.29 981.00 592.17 o
2 7 3 337.85 301.24 122.22 o
4 7 3 1183.87 1135.28 298.26 o
6 7 3 2.54 15.43 113.56 o
8 7 3 498.44 578.88 143.07 o
10 7 3 117.32 195.57 106.01 o
1 8 3 6.47 210.02 236.35 o
3 8 3 40.54 98.41 172.69 o
5 8 3 237.15 205.34 65.47 o
7 8 3 128.37 227.26 155.48 o
9 8 3 253.08 501.45 354.08 o
2 9 3 9.45 189.66 277.11 o
4 9 3 602.30 659.35 262.56 o
6 9 3 11.84 175.27 232.34 o
0 0 4 299629.69 288035.66 10411.18 o
2 0 4 103012.02 93362.82 416.01 o
4 0 4 45673.48 42645.32 165.64 o
6 0 4 55289.89 53697.61 259.48 o
8 0 4 33283.96 29884.87 1040.99 o
10 0 4 17606.91 18351.41 1229.42 o
12 0 4 47620.99 45902.45 441.78 o
14 0 4 23268.23 21340.63 355.32 o
16 0 4 4334.97 4609.41 413.73 o
1 1 4 113092.20 118491.16 4168.28 o
3 1 4 40452.63 37852.36 313.57 o
5 1 4 80263.65 77466.84 2833.99 o
7 1 4 64017.08 62799.81 300.86 o
9 1 4 38332.75 38361.44 647.01 o
11 1 4 22708.38 21054.95 330.91 o
13 1 4 27097.37 26138.29 92.85 o
15 1 4 7146.12 6786.13 190.22 o
0 2 4 51440.66 48561.16 178.18 o
2 2 4 56367.45 53795.50 58.08 o
4 2 4 107245.92 98107.70 857.16 o
6 2 4 67009.38 60541.70 438.82 o
8 2 4 45583.55 41132.74 213.27 o
10 2 4 17461.34 16676.18 153.95 o
12 2 4 11384.31 12566.84 384.53 o
14 2 4 10085.36 13291.77 802.32 o
1 3 4 43032.21 43308.61 241.69 o
3 3 4 73682.92 68134.41 90.29 o
5 3 4 46074.74 43450.45 387.38 o
7 3 4 20779.74 21058.52 496.64 o
9 3 4 46488.78 44330.78 511.71 o
11 3 4 21721.01 20593.91 735.06 o
13 3 4 10257.24 9547.75 589.85 o
15 3 4 9911.17 9413.57 653.56 o
0 4 4 65835.52 62120.09 133.37 o
2 4 4 61801.77 57321.25 156.24 o
4 4 4 47519.13 43741.95 129.42 o
6 4 4 4800.38 4995.34 471.05 o
8 4 4 18413.04 19125.16 200.18 o
10 4 4 29136.67 30538.52 152.84 o
12 4 4 14044.53 17018.67 596.11 o
14 4 4 9097.50 8774.14 471.33 o
1 5 4 19039.60 21035.83 95.19 o
3 5 4 30228.32 32504.97 72.06 o
5 5 4 27856.69 30661.90 449.71 o
7 5 4 19365.64 18497.96 411.39 o
9 5 4 22239.45 24693.27 375.84 o
11 5 4 9544.24 8588.89 183.73 o
13 5 4 6653.23 6343.40 156.11 o
0 6 4 20288.12 20924.69 548.54 o
2 6 4 12271.15 13617.01 1045.93 o
4 6 4 20808.25 23742.62 369.55 o
6 6 4 21967.32 21768.31 209.19 o
8 6 4 14945.26 15424.94 257.34 o
10 6 4 4163.41 4129.54 166.51 o
12 6 4 4090.71 4079.51 389.88 o
1 7 4 15154.27 15140.84 330.15 o
3 7 4 6203.50 5963.09 394.18 o
5 7 4 10022.41 10364.74 375.24 o
7 7 4 10793.65 11234.23 555.99 o
9 7 4 4724.63 4829.42 328.08 o
11 7 4 4970.37 4613.54 475.88 o
0 8 4 18633.95 21367.00 472.35 o
2 8 4 7244.16 6734.57 471.76 o
4 8 4 3819.37 3919.49 179.34 o
6 8 4 3771.70 3438.15 149.71 o
8 8 4 3224.79 3062.80 132.96 o
1 9 4 2614.60 2610.51 333.96 o
3 9 4 3167.61 3274.87 591.44 o
5 9 4 4512.23 4305.33 258.94 o
2 1 5 56.76 312.10 330.66 o
4 1 5 11162.65 11981.04 127.51 o
6 1 5 307.10 384.99 90.67 o
8 1 5 5134.38 4925.56 112.46 o
10 1 5 1076.40 1067.80 131.39 o
12 1 5 470.08 555.34 303.93 o
14 1 5 1.92 133.66 204.31 o
1 2 5 900.08 915.96 89.48 o
3 2 5 466.29 757.81 401.71 o
5 2 5 3373.30 3085.71 149.13 o
7 2 5 2193.49 2318.96 376.27 o
9 2 5 577.80 626.41 120.84 o
11 2 5 3062.55 3330.50 130.80 o
13 2 5 125.22 423.92 361.28 o
15 2 5 767.56 970.99 739.48 o
2 3 5 13460.54 14339.78 474.19 o
4 3 5 313.18 314.83 70.88 o
6 3 5 54.00 309.45 319.77 o
8 3 5 1172.79 1498.47 167.11 o
10 3 5 352.51 501.91 245.79 o
12 3 5 45.38 551.23 1067.31 o
14 3 5 1494.34 1787.02 334.06 o
1 4 5 2463.00 2532.61 232.24 o
3 4 5 155.47 327.42 171.85 o
5 4 5 14.12 226.68 172.73 o
7 4 5 271.33 346.74 128.25 o
9 4 5 3.81 280.33 343.77 o
11 4 5 1.90 226.88 422.82 o
13 4 5 49.69 374.23 508.58 o
2 5 5 2887.43 2813.56 182.74 o
4 5 5 119.34 189.77 102.33 o
6 5 5 349.84 516.85 326.37 o
8 5 5 213.66 241.05 72.95 o
10 5 5 1949.36 2318.85 153.86 o
12 5 5 378.23 677.05 679.54 o
1 6 5 987.34 1312.72 165.51 o
3 6 5 49.38 101.34 88.25 o
5 6 5 920.16 1130.29 194.30 o
7 6 5 106.06 152.69 91.06 o
9 6 5 242.34 501.48 262.49 o
11 6 5 152.09 159.36 96.24 o
2 7 5 413.80 391.06 145.47 o
4 7 5 813.11 964.00 430.36 o
6 7 5 4.24 252.60 324.71 o
8 7 5 549.18 883.96 594.80 o
10 7 5 54.64 82.32 63.45 o
1 8 5 37.55 171.14 212.16 o
3 8 5 22.17 93.79 69.91 o
5 8 5 202.46 342.91 171.35 o
7 8 5 26.30 280.99 318.11 o
2 9 5 14.60 223.61 302.83 o
4 9 5 370.16 479.00 249.49 o
0 0 6 136125.17 123615.89 559.78 o
2 0 6 26065.88 26140.29 339.99 o
4 0 6 3232.84 3711.42 355.55 o
6 0 6 21647.00 20450.78 406.48 o
8 0 6 16974.88 20652.77 636.32 o
10 0 6 17215.84 19495.83 711.97 o
12 0 6 20057.56 20457.92 352.60 o
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3 1 6 29450.44 28360.49 90.44 o
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11 1 6 12127.44 13966.23 244.47 o
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15 1 6 6650.86 5940.42 628.86 o
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2 2 6 15391.15 14799.70 246.67 o
4 2 6 27242.95 29199.33 126.96 o
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8 2 6 23397.47 22620.63 184.71 o
10 2 6 15233.31 18279.70 186.66 o
12 2 6 3086.80 3340.84 465.67 o
14 2 6 4148.69 4038.43 706.02 o
1 3 6 18165.50 20319.39 95.46 o
3 3 6 43798.10 42360.98 201.38 o
5 3 6 12314.61 11790.38 1135.63 o
7 3 6 8012.88 9948.31 719.96 o
9 3 6 11521.18 12468.53 393.78 o
11 3 6 11676.01 11657.73 356.55 o
13 3 6 2958.80 3282.91 384.13 o
0 4 6 10162.03 9409.37 242.22 o
2 4 6 29617.36 26971.65 114.24 o
4 4 6 14195.13 13640.93 606.79 o
6 4 6 3346.60 3765.48 661.30 o
8 4 6 7549.29 7156.27 223.31 o
10 4 6 20167.47 19105.03 563.44 o
12 4 6 6814.12 6108.36 328.72 o
14 4 6 4544.25 4050.52 353.41 o
1 5 6 12387.02 12564.68 132.66 o
3 5 6 14887.37 17728.34 173.43 o
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9 5 6 8951.48 12604.57 865.06 o
11 5 6 4482.74 4445.70 556.23 o
13 5 6 1889.23 2010.56 196.73 o
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