#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/47/2204770.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204770_Fobs loop_ _publ_author_name 'Gao, Shan' 'Gu, Chang-Sheng' 'Huo, Li-Hua' 'Liu, Ji-Wei' 'Zhao, Jing-Gui' _publ_section_title ; catena-Poly[[aqua(2,2'-bipyridine-\k^2^N,N')zinc(II)]-\m-4-carboxylatophenoxyacetato-\k^3^O,O':O''] ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1906 _journal_page_last m1908 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.555 _cell_angle_gamma 90.000 _cell_length_a 14.2344 _cell_length_b 13.2098 _cell_length_c 19.5220 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file ob6435Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' g in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 703.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 57679.17 64780.72 1100.98 o 6 0 0 7101.10 6524.17 94.88 o 8 0 0 12269.87 11424.60 251.59 o 10 0 0 12621.14 11990.80 183.21 o 12 0 0 4822.42 5142.23 312.31 o 14 0 0 247.98 301.69 179.21 o 16 0 0 677.91 852.12 210.05 o 3 1 0 16026.75 16724.26 138.58 o 5 1 0 2.70 -5.78 24.73 o 7 1 0 35.54 389.14 50.32 o 9 1 0 701.36 679.12 36.72 o 11 1 0 499.77 507.92 48.88 o 13 1 0 700.72 554.79 112.35 o 15 1 0 198.15 193.26 132.17 o 17 1 0 98.00 492.53 222.78 o 0 2 0 84550.90 93362.84 59.13 o 2 2 0 14567.01 14379.25 262.26 o 4 2 0 11096.72 10963.47 118.46 o 6 2 0 10563.13 10458.01 173.13 o 8 2 0 14808.42 14696.34 295.22 o 10 2 0 5879.52 5489.50 57.45 o 12 2 0 1445.39 1285.64 39.44 o 14 2 0 772.54 669.34 113.69 o 16 2 0 1550.31 1855.29 277.76 o 1 3 0 14201.21 14645.48 157.19 o 3 3 0 4650.64 4885.40 71.62 o 5 3 0 1721.07 1807.61 58.66 o 7 3 0 214.56 113.74 40.04 o 9 3 0 581.65 539.24 62.80 o 11 3 0 4619.90 4514.49 48.24 o 13 3 0 5064.65 4784.39 48.80 o 15 3 0 783.60 687.01 134.50 o 17 3 0 82.70 0.99 151.28 o 0 4 0 14660.78 14327.84 138.19 o 2 4 0 43.55 68.39 37.02 o 4 4 0 468.54 462.59 27.87 o 6 4 0 3671.72 3852.06 41.51 o 8 4 0 12492.12 12938.69 167.65 o 10 4 0 2479.60 2427.61 127.24 o 12 4 0 346.36 297.35 42.07 o 14 4 0 21.12 30.48 39.86 o 16 4 0 1.44 18.55 133.88 o 1 5 0 11880.06 13118.53 185.32 o 3 5 0 2531.00 2537.46 47.96 o 5 5 0 1684.73 1547.03 35.04 o 7 5 0 4487.01 5024.57 63.38 o 9 5 0 5341.91 5478.52 55.95 o 11 5 0 1690.71 1697.22 66.73 o 13 5 0 1537.00 1580.95 49.06 o 15 5 0 603.08 660.07 48.88 o 17 5 0 233.66 -39.96 221.10 o 0 6 0 2997.28 3279.87 183.06 o 2 6 0 642.93 672.88 48.68 o 4 6 0 340.34 398.16 62.15 o 6 6 0 11.17 -15.07 34.90 o 8 6 0 2.90 41.50 22.32 o 10 6 0 283.82 440.30 66.71 o 12 6 0 130.54 158.54 56.80 o 14 6 0 246.64 170.23 55.06 o 16 6 0 89.74 124.30 93.21 o 1 7 0 138.86 323.50 45.41 o 3 7 0 223.76 355.78 91.20 o 5 7 0 2502.83 2395.25 44.41 o 7 7 0 304.48 347.92 45.10 o 9 7 0 129.80 127.77 44.04 o 11 7 0 121.08 91.80 72.96 o 13 7 0 1040.89 1222.32 64.12 o 15 7 0 622.97 591.57 96.08 o 2 8 0 12155.42 12120.36 344.45 o 4 8 0 7825.72 7941.11 77.55 o 6 8 0 3923.70 3987.22 108.27 o 8 8 0 10229.08 10400.44 292.16 o 10 8 0 952.14 946.42 25.21 o 12 8 0 69.09 235.83 119.87 o 14 8 0 842.50 889.99 67.26 o 1 9 0 828.11 1212.12 98.99 o 3 9 0 2793.22 2953.12 91.93 o 5 9 0 3234.81 3291.60 52.14 o 7 9 0 29.85 62.08 49.90 o 9 9 0 61.31 78.59 44.55 o 11 9 0 3.49 10.08 30.68 o 13 9 0 916.36 1048.58 69.88 o 15 9 0 721.04 639.27 131.87 o 0 10 0 7563.35 7393.55 147.94 o 2 10 0 6281.00 6072.43 229.54 o 4 10 0 2057.48 1958.64 67.61 o 6 10 0 2808.72 2838.15 60.10 o 8 10 0 15179.58 15778.46 359.66 o 10 10 0 1711.95 1715.20 79.44 o 12 10 0 202.19 337.29 84.93 o 14 10 0 1393.95 1383.02 91.76 o 3 11 0 943.24 777.50 134.99 o 5 11 0 23.18 -14.29 51.66 o 7 11 0 242.19 378.91 76.50 o 9 11 0 437.76 341.20 69.89 o 11 11 0 65.06 199.39 71.12 o 13 11 0 298.24 281.36 72.95 o 2 12 0 3192.54 3379.52 153.03 o 4 12 0 2396.42 2209.72 359.87 o 6 12 0 758.33 770.50 54.76 o 8 12 0 2322.98 2492.38 92.70 o 10 12 0 1822.42 1958.73 106.87 o 12 12 0 888.24 949.26 91.67 o 1 13 0 0.17 10.18 179.94 o 3 13 0 418.47 393.94 124.76 o 5 13 0 386.65 398.43 50.88 o 7 13 0 216.40 183.77 60.37 o 9 13 0 95.29 144.08 45.43 o 11 13 0 181.95 235.36 144.43 o 2 14 0 1634.21 1578.41 194.05 o 4 14 0 816.42 684.90 87.44 o 6 14 0 142.12 73.19 75.59 o 8 14 0 423.78 454.17 71.06 o 10 14 0 134.58 128.85 86.62 o 1 15 0 97.02 186.19 201.32 o 3 15 0 89.37 69.68 80.00 o 5 15 0 191.97 51.94 93.61 o 7 15 0 4.00 80.29 79.06 o 0 16 0 14.09 -228.81 228.81 o 2 16 0 10.56 117.39 201.03 o 4 16 0 9.34 102.61 90.93 o 6 16 0 0.18 -84.15 84.15 o 1 17 0 1.92 -179.21 237.54 o -17 1 1 1342.17 1539.38 349.11 o -15 1 1 2276.79 1935.57 127.27 o -13 1 1 2104.33 1910.66 229.20 o -11 1 1 4802.49 4639.94 122.89 o -9 1 1 18166.62 17469.43 117.70 o -7 1 1 41623.32 43894.14 196.77 o -5 1 1 966.11 891.41 24.30 o -3 1 1 53317.47 62405.98 471.52 o 3 1 1 163.56 165.67 8.96 o 5 1 1 1096.93 1185.92 74.13 o 7 1 1 22071.81 22994.59 315.28 o 9 1 1 10779.16 11117.60 152.04 o 11 1 1 443.51 402.33 27.58 o 13 1 1 91.37 236.12 92.16 o 15 1 1 22.89 -16.24 265.22 o 17 1 1 336.85 392.85 229.47 o -16 2 1 33.81 187.02 147.21 o -14 2 1 88.64 107.60 30.19 o -12 2 1 5.40 54.71 29.15 o -10 2 1 2642.37 2789.10 59.44 o -8 2 1 7753.77 7756.08 92.45 o -6 2 1 11137.05 12393.87 176.20 o -4 2 1 1178.92 1223.03 58.79 o -2 2 1 14754.68 15799.55 184.74 o 0 2 1 43.43 58.49 26.15 o 2 2 1 150.90 184.11 16.78 o 4 2 1 10646.03 9860.53 90.39 o 6 2 1 754.43 657.95 28.56 o 8 2 1 4795.73 4881.09 42.47 o 10 2 1 6946.60 6986.29 117.55 o 12 2 1 941.23 928.95 47.69 o 14 2 1 125.50 109.13 20.01 o 16 2 1 9.97 -105.64 144.01 o -17 3 1 1461.25 1448.04 171.46 o -15 3 1 802.23 826.95 190.12 o -13 3 1 53.11 68.02 45.06 o -11 3 1 9594.87 9708.12 124.13 o -9 3 1 16495.84 16885.77 110.65 o -7 3 1 3350.88 3164.50 86.62 o -5 3 1 1747.52 1752.83 48.40 o -3 3 1 131.25 181.79 18.93 o -1 3 1 163.15 278.36 31.98 o 1 3 1 78833.78 85370.55 904.95 o 3 3 1 910.05 810.12 26.96 o 5 3 1 581.58 542.05 24.83 o 7 3 1 2577.59 2477.75 98.46 o 9 3 1 2.08 11.71 45.65 o 11 3 1 0.50 -0.05 36.90 o 13 3 1 38.55 70.06 32.93 o 15 3 1 34.31 57.69 49.80 o 17 3 1 19.84 69.30 199.07 o -16 4 1 1.36 142.10 130.60 o -14 4 1 115.97 83.17 42.59 o -12 4 1 57.40 68.63 53.18 o -10 4 1 37.39 -53.01 53.01 o -8 4 1 2917.77 3246.94 119.45 o -6 4 1 13400.24 14534.88 344.67 o -4 4 1 85.59 126.84 23.98 o -2 4 1 1248.63 1100.92 37.57 o 0 4 1 4981.38 4375.78 82.53 o 2 4 1 20413.75 20539.08 53.07 o 4 4 1 17851.65 17738.97 298.20 o 6 4 1 22539.81 23519.04 191.48 o 8 4 1 20188.51 20266.69 447.06 o 10 4 1 3987.14 3952.40 120.12 o 12 4 1 3373.24 3470.78 45.29 o 14 4 1 3611.41 3489.34 119.59 o 16 4 1 1668.75 1868.70 163.50 o -17 5 1 51.19 58.35 145.23 o -15 5 1 69.52 40.86 50.10 o -13 5 1 19.35 35.98 46.35 o -11 5 1 747.65 748.21 73.86 o -9 5 1 8.84 63.52 26.24 o -7 5 1 202.50 261.40 37.60 o -5 5 1 98.71 357.22 99.39 o -3 5 1 89.68 69.40 25.39 o -1 5 1 9286.89 9473.96 70.05 o 1 5 1 49588.43 57164.73 613.41 o 3 5 1 1952.86 2067.83 63.81 o 5 5 1 41.51 -30.72 32.13 o 7 5 1 97.70 105.55 19.00 o 9 5 1 958.43 958.78 67.65 o 11 5 1 415.26 564.42 58.81 o 13 5 1 30.20 48.91 55.14 o 15 5 1 79.22 94.31 44.11 o -16 6 1 11.13 132.57 59.56 o -14 6 1 28.07 5.09 50.94 o -12 6 1 904.53 894.01 50.87 o -10 6 1 291.14 441.40 58.74 o -8 6 1 1442.92 1430.52 36.68 o -6 6 1 12789.13 13118.39 235.10 o -4 6 1 12768.35 12945.69 216.61 o -2 6 1 12059.58 12028.00 65.90 o 0 6 1 10326.34 9604.93 176.86 o 2 6 1 14587.73 13620.85 69.41 o 4 6 1 8826.26 8404.23 73.65 o 6 6 1 6671.72 6788.97 78.92 o 8 6 1 9155.69 9358.60 120.89 o 10 6 1 5952.01 6581.87 75.05 o 12 6 1 3897.23 4073.27 78.97 o 14 6 1 1425.38 1494.20 88.77 o 16 6 1 978.74 1090.19 178.55 o -15 7 1 297.73 167.46 69.63 o -13 7 1 568.42 619.45 65.32 o -11 7 1 1071.50 1229.56 84.63 o -9 7 1 941.78 925.01 86.06 o -7 7 1 1016.13 1023.52 41.85 o -5 7 1 68.41 107.94 57.09 o -3 7 1 5193.58 5333.39 73.17 o -1 7 1 12508.74 13171.40 98.52 o 1 7 1 976.17 699.69 53.50 o 3 7 1 2271.65 2060.91 67.47 o 5 7 1 96.49 91.40 37.80 o 7 7 1 108.55 129.65 45.77 o 9 7 1 1411.36 1380.19 33.79 o 11 7 1 966.56 1095.02 83.96 o 13 7 1 32.50 133.82 105.52 o 15 7 1 23.72 35.70 61.72 o -14 8 1 0.36 -14.59 64.70 o -12 8 1 1687.81 1744.20 72.39 o -10 8 1 21.92 57.40 40.18 o -8 8 1 1185.91 1248.26 68.53 o -6 8 1 1992.82 2037.18 84.58 o -4 8 1 1820.64 1914.17 54.92 o -2 8 1 3333.28 3281.11 123.28 o 0 8 1 3177.00 2939.65 111.71 o 2 8 1 11028.13 11442.22 72.91 o 4 8 1 4932.87 4978.06 72.91 o 6 8 1 6103.19 6187.19 109.68 o 8 8 1 2932.34 3140.13 52.37 o 10 8 1 647.77 623.69 47.51 o 12 8 1 3241.50 3650.34 125.49 o 14 8 1 1049.99 1018.16 71.48 o -15 9 1 1127.94 1215.39 129.72 o -13 9 1 183.65 62.97 67.82 o -11 9 1 1263.01 1213.28 44.56 o -9 9 1 1831.83 1924.98 75.04 o -7 9 1 6014.11 6118.66 74.50 o -5 9 1 6570.84 6859.20 102.53 o -3 9 1 3638.31 3528.76 122.41 o -1 9 1 9930.36 9906.14 227.73 o 1 9 1 17081.93 16948.65 104.66 o 3 9 1 3283.11 3473.93 114.19 o 5 9 1 5451.79 5525.39 99.46 o 7 9 1 732.16 821.15 42.04 o 9 9 1 739.78 829.20 35.93 o 11 9 1 51.83 57.43 24.97 o 13 9 1 174.06 163.16 95.28 o 15 9 1 158.29 260.82 75.28 o -14 10 1 14.47 27.55 72.27 o -12 10 1 45.41 74.36 64.53 o -10 10 1 363.52 397.39 57.60 o -8 10 1 1546.63 1541.24 53.60 o -6 10 1 3078.73 3075.64 121.46 o -4 10 1 150.15 217.28 44.82 o -2 10 1 441.37 1844.75 140.81 o 0 10 1 520.84 705.06 133.68 o 2 10 1 3357.51 3457.37 97.90 o 4 10 1 485.57 546.27 48.76 o 6 10 1 160.00 142.56 51.11 o 8 10 1 1673.17 1775.19 59.74 o 10 10 1 1555.73 1470.39 88.88 o 12 10 1 15.65 19.05 81.92 o 14 10 1 7.71 139.06 77.88 o -13 11 1 681.47 633.18 70.65 o -11 11 1 3108.56 2688.13 145.65 o -9 11 1 3607.36 3403.60 117.58 o -7 11 1 6608.81 6993.48 131.92 o -5 11 1 2041.92 2126.53 78.77 o -3 11 1 2286.02 2318.81 140.52 o 1 11 1 3464.19 3509.87 107.80 o 3 11 1 1190.80 1187.36 138.93 o 5 11 1 1749.27 1897.59 80.24 o 7 11 1 246.50 283.98 47.98 o 9 11 1 120.95 164.14 59.72 o 11 11 1 62.12 147.85 76.02 o 13 11 1 485.44 395.55 133.11 o -12 12 1 4.13 51.19 111.56 o -10 12 1 7.51 14.33 42.44 o -8 12 1 180.37 179.51 46.95 o -6 12 1 56.56 128.86 47.07 o -4 12 1 419.73 337.75 46.68 o -2 12 1 436.60 499.97 215.21 o 2 12 1 252.98 234.05 160.44 o 4 12 1 231.49 414.25 52.25 o 6 12 1 866.27 1014.81 57.91 o 8 12 1 196.95 264.67 45.91 o 10 12 1 204.20 254.42 51.78 o 12 12 1 408.52 354.31 82.66 o -11 13 1 511.49 510.62 115.11 o -9 13 1 1012.84 1212.92 153.48 o -7 13 1 4031.81 3933.35 175.46 o -5 13 1 1292.26 1177.62 293.03 o -3 13 1 1764.81 1197.44 170.92 o 1 13 1 587.76 890.96 165.25 o 3 13 1 1498.18 1264.97 79.41 o 5 13 1 1127.71 999.00 57.35 o 7 13 1 177.84 220.21 65.33 o 9 13 1 145.22 166.45 75.73 o 11 13 1 3.67 33.60 140.60 o -10 14 1 29.47 119.49 63.06 o -8 14 1 9.33 -101.55 101.55 o -6 14 1 203.03 291.78 94.39 o -4 14 1 219.24 281.85 118.41 o -2 14 1 882.86 1460.73 199.28 o 2 14 1 972.66 1007.05 224.30 o 4 14 1 586.80 631.90 73.66 o 6 14 1 2155.59 2123.11 142.76 o 8 14 1 1045.94 1124.67 169.02 o 10 14 1 208.52 201.19 152.81 o -7 15 1 595.73 667.04 260.89 o -5 15 1 92.19 -182.26 182.26 o -3 15 1 21.17 246.70 183.28 o -1 15 1 3.19 -209.61 209.61 o 1 15 1 106.38 361.93 610.94 o 3 15 1 58.20 200.99 78.91 o 5 15 1 10.58 17.04 123.88 o 7 15 1 21.63 -41.63 76.82 o -6 16 1 185.90 261.10 177.03 o -4 16 1 124.74 494.43 188.66 o -2 16 1 613.43 490.35 215.87 o 0 16 1 609.15 512.93 157.08 o 2 16 1 832.80 694.53 151.64 o 4 16 1 1122.42 1024.63 83.23 o 6 16 1 838.28 829.91 181.91 o -1 17 1 133.79 458.21 239.72 o 1 17 1 4.68 127.42 244.96 o -18 0 2 972.27 1488.66 241.90 o -16 0 2 856.13 1263.63 200.45 o -14 0 2 1539.67 1636.45 165.83 o -12 0 2 1310.42 1529.76 35.65 o -10 0 2 1970.34 1792.36 104.80 o -8 0 2 525.04 668.26 18.82 o -6 0 2 2794.80 3333.16 80.51 o -4 0 2 91396.88 103481.72 894.87 o -2 0 2 4514.65 4715.39 20.82 o 2 0 2 9145.31 8906.41 169.10 o 4 0 2 8738.91 8585.13 240.08 o 6 0 2 12588.98 11979.38 289.03 o 8 0 2 1213.81 1261.97 119.88 o 10 0 2 186.48 165.65 33.39 o 12 0 2 3291.89 3228.77 106.86 o 14 0 2 6815.00 7520.54 203.65 o 16 0 2 1893.24 2233.86 216.30 o -17 1 2 2.42 -148.91 148.91 o -15 1 2 7.73 78.23 128.42 o -13 1 2 163.33 151.38 31.18 o -11 1 2 989.34 1005.15 58.75 o -9 1 2 1523.35 1471.60 32.80 o -7 1 2 113.58 91.79 26.58 o -5 1 2 831.84 848.04 21.56 o -3 1 2 39026.82 44114.88 403.92 o 1 1 2 7142.56 6858.51 65.85 o 3 1 2 2361.04 2383.19 19.12 o 5 1 2 3320.22 3193.64 85.58 o 7 1 2 2313.94 2147.80 23.06 o 9 1 2 186.76 202.23 60.09 o 11 1 2 73.27 79.61 28.31 o 13 1 2 142.20 120.37 92.60 o 15 1 2 122.72 72.43 281.69 o 17 1 2 13.24 208.12 209.99 o -18 2 2 896.52 1004.52 189.03 o -16 2 2 271.40 390.12 132.28 o -14 2 2 1649.13 1641.82 43.65 o -12 2 2 4706.58 4638.40 190.58 o -10 2 2 1831.46 1744.60 65.82 o -8 2 2 482.44 416.89 68.66 o -6 2 2 14757.11 15849.05 129.66 o -4 2 2 65.41 113.96 21.88 o -2 2 2 850.01 681.71 23.89 o 0 2 2 4384.89 4117.93 43.93 o 2 2 2 5245.24 5245.94 57.37 o 4 2 2 1851.50 1839.26 69.94 o 6 2 2 17508.40 18031.17 120.67 o 8 2 2 1997.42 1936.23 38.03 o 10 2 2 292.20 314.55 52.93 o 12 2 2 1141.49 1104.14 74.16 o 14 2 2 3240.09 2831.79 116.32 o 16 2 2 1077.13 984.30 146.75 o -17 3 2 328.99 503.03 140.14 o -15 3 2 582.39 656.31 74.01 o -13 3 2 423.52 445.79 38.80 o -11 3 2 744.58 789.24 62.83 o -9 3 2 6556.72 6486.60 104.15 o -7 3 2 8405.68 8341.31 139.26 o -5 3 2 17447.46 17878.94 247.94 o -3 3 2 5846.22 5741.03 80.90 o -1 3 2 17012.53 16655.93 55.08 o 1 3 2 111032.66 126734.17 433.02 o 3 3 2 37412.07 38812.39 460.46 o 5 3 2 15940.44 15772.60 230.39 o 7 3 2 3693.26 3422.98 42.77 o 9 3 2 3619.00 3396.35 87.34 o 11 3 2 3256.77 3192.05 51.74 o 13 3 2 2510.44 2545.29 160.09 o 15 3 2 418.94 698.08 104.41 o 17 3 2 269.46 416.58 163.92 o -16 4 2 20.97 -96.43 264.81 o -14 4 2 105.06 142.00 44.00 o -12 4 2 1882.93 1881.95 143.27 o -10 4 2 1003.87 1157.87 40.98 o -8 4 2 9.86 82.59 37.87 o -6 4 2 1096.96 1150.26 60.65 o -4 4 2 5241.50 5629.13 91.22 o -2 4 2 56.11 56.44 14.08 o 0 4 2 15852.59 16712.08 495.01 o 2 4 2 423.43 474.88 34.55 o 4 4 2 23.32 27.82 24.47 o 6 4 2 6265.11 6434.19 126.09 o 8 4 2 41.29 -2.64 40.99 o 10 4 2 117.94 109.65 55.04 o 12 4 2 40.67 39.98 56.09 o 14 4 2 210.68 180.42 46.98 o 16 4 2 119.08 305.36 111.01 o -17 5 2 415.78 327.68 139.18 o -15 5 2 1865.69 1629.28 53.59 o -13 5 2 2693.10 2653.17 112.85 o -11 5 2 701.02 749.49 69.48 o -9 5 2 6119.94 6236.51 79.32 o -7 5 2 22045.33 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