#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204785.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204785_Fobs loop_ _publ_author_name 'Jian, Fangfang' 'Li, Chunlei' 'Sun, Pingping' 'Xiao, Hailian' _publ_section_title ; Diazidobis(2,2'-bipyridine)zinc(II) monohydrate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1811 _journal_page_last m1812 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.740 _cell_angle_beta 86.980 _cell_angle_gamma 69.580 _cell_length_a 8.3030 _cell_length_b 10.3340 _cell_length_c 13.2510 _exptl_crystal_F_000 492.00 _reflns_d_resolution_high 0.8417 _[local]_cod_data_source_file rz6014Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' RZ6014 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1382.82 1289.71 17.63 o 2 0 0 2007.18 2044.16 31.45 o 3 0 0 18.16 19.15 7.15 o 4 0 0 108.21 115.89 12.20 o 5 0 0 924.75 940.04 30.12 o 6 0 0 0.62 -6.02 14.89 o 7 0 0 793.32 822.58 35.56 o 8 0 0 3.36 -13.08 18.51 o 9 0 0 110.84 81.99 24.49 o -8 1 0 123.62 109.52 21.89 o -7 1 0 52.72 65.73 17.44 o -6 1 0 1117.41 1060.67 37.27 o -5 1 0 11.77 18.61 13.13 o -4 1 0 1512.61 1573.50 42.56 o -3 1 0 38.89 55.94 9.01 o -2 1 0 706.06 739.22 18.02 o -1 1 0 2701.22 2808.40 31.89 o 0 1 0 883.48 838.10 9.66 o 1 1 0 4102.91 4132.20 31.59 o 2 1 0 1149.46 1236.86 24.10 o 3 1 0 100.57 102.76 9.60 o 4 1 0 919.02 855.20 24.20 o 5 1 0 623.21 665.01 24.64 o 6 1 0 1113.21 1121.95 35.02 o 7 1 0 2.71 7.10 18.22 o 8 1 0 196.29 175.35 22.34 o 9 1 0 60.50 71.90 18.81 o -8 2 0 7.44 22.58 19.94 o -7 2 0 227.28 219.38 22.73 o -6 2 0 29.81 26.06 14.69 o -5 2 0 696.86 680.68 28.56 o -4 2 0 121.59 110.35 12.49 o -3 2 0 346.18 364.27 17.14 o -2 2 0 1776.17 1769.77 36.44 o -1 2 0 15.93 17.49 6.22 o 0 2 0 9287.35 8291.42 53.05 o 1 2 0 1716.22 1742.09 25.96 o 2 2 0 112.51 126.08 7.35 o 3 2 0 151.49 188.87 11.61 o 4 2 0 103.30 110.30 10.33 o 5 2 0 780.03 752.64 25.67 o 6 2 0 230.58 229.28 18.66 o 7 2 0 538.47 474.13 28.46 o 8 2 0 162.58 143.90 20.57 o 9 2 0 0.30 12.15 22.92 o -8 3 0 39.90 72.05 23.66 o -7 3 0 9.31 29.98 21.99 o -6 3 0 218.48 182.45 23.31 o -5 3 0 638.98 623.87 29.83 o -4 3 0 87.61 86.01 14.01 o -3 3 0 523.69 471.00 21.06 o -2 3 0 0.05 7.15 6.86 o -1 3 0 352.18 320.09 14.16 o 0 3 0 1257.71 1265.80 20.53 o 1 3 0 18252.51 15935.84 93.75 o 2 3 0 1820.08 1744.25 33.01 o 3 3 0 96.16 85.81 8.03 o 4 3 0 1479.57 1479.21 37.96 o 5 3 0 783.77 836.88 27.04 o 6 3 0 312.65 319.79 20.87 o 7 3 0 859.32 855.05 34.19 o 8 3 0 388.54 348.94 29.39 o 9 3 0 287.42 256.07 26.35 o -7 4 0 132.24 166.39 25.91 o -6 4 0 38.44 30.27 21.40 o -5 4 0 147.61 153.31 18.51 o -4 4 0 957.59 963.79 34.43 o -3 4 0 0.39 -7.45 13.62 o -2 4 0 466.59 553.14 22.14 o -1 4 0 128.13 121.08 11.56 o 0 4 0 131.01 129.38 10.60 o 1 4 0 3653.15 3702.54 53.19 o 2 4 0 5021.72 5052.50 62.60 o 3 4 0 2478.51 2387.66 45.60 o 4 4 0 26.43 43.10 9.75 o 5 4 0 556.96 558.28 23.36 o 6 4 0 1525.12 1512.67 40.26 o 7 4 0 19.69 22.78 14.60 o 8 4 0 238.71 209.83 23.27 o 9 4 0 3.52 2.35 22.63 o -7 5 0 64.61 101.54 19.30 o -6 5 0 5.33 2.40 21.36 o -5 5 0 104.50 85.52 19.25 o -4 5 0 2.73 24.88 17.05 o -3 5 0 641.33 630.33 28.02 o -2 5 0 5.81 21.16 9.65 o -1 5 0 1763.56 1845.20 48.10 o 0 5 0 1756.48 1765.16 35.68 o 1 5 0 546.05 578.56 21.21 o 2 5 0 6524.91 6659.84 80.03 o 3 5 0 786.90 890.27 25.47 o 4 5 0 464.16 487.01 21.31 o 5 5 0 939.82 922.40 30.47 o 6 5 0 4.28 36.10 10.09 o 7 5 0 552.68 571.26 29.63 o 8 5 0 381.49 425.49 27.77 o 9 5 0 297.57 252.79 29.49 o -6 6 0 55.68 97.86 21.01 o -5 6 0 92.71 94.58 20.52 o -4 6 0 585.13 609.61 31.98 o -3 6 0 95.28 61.52 17.05 o -2 6 0 353.39 367.21 24.59 o -1 6 0 25.30 35.22 12.54 o 0 6 0 271.16 258.86 12.90 o 1 6 0 699.63 694.20 25.32 o 2 6 0 796.65 814.50 27.43 o 3 6 0 2122.69 2082.51 51.28 o 4 6 0 3.74 -4.95 12.69 o 5 6 0 283.17 252.89 19.10 o 6 6 0 251.04 271.60 20.33 o 7 6 0 0.63 22.14 14.99 o 8 6 0 510.98 532.76 32.96 o 9 6 0 0.24 7.30 18.37 o -5 7 0 45.15 39.14 30.37 o -4 7 0 20.46 36.88 22.34 o -3 7 0 518.81 502.15 30.66 o -2 7 0 149.12 167.42 18.32 o -1 7 0 21.64 11.46 16.16 o 0 7 0 487.72 484.68 17.63 o 1 7 0 108.94 102.61 15.23 o 2 7 0 1241.41 1249.89 35.71 o 3 7 0 1.96 -11.95 13.62 o 4 7 0 321.33 311.52 20.72 o 5 7 0 44.36 51.23 14.06 o 6 7 0 1.33 15.67 17.78 o 7 7 0 305.03 305.39 24.78 o 8 7 0 184.12 198.37 23.85 o 9 7 0 280.37 264.10 27.67 o -4 8 0 32.53 46.78 18.76 o -3 8 0 45.43 71.22 19.94 o -2 8 0 36.16 51.72 17.83 o -1 8 0 78.27 80.03 18.02 o 0 8 0 316.65 307.07 16.92 o 1 8 0 162.43 157.57 17.83 o 2 8 0 55.73 60.59 13.86 o 3 8 0 625.19 593.30 28.60 o 4 8 0 207.10 196.56 19.45 o 5 8 0 63.71 48.05 15.18 o 6 8 0 418.98 470.36 27.77 o 7 8 0 245.51 172.61 22.97 o 8 8 0 404.72 440.83 31.64 o 9 8 0 70.96 44.87 28.07 o -3 9 0 59.20 33.31 21.11 o -2 9 0 248.75 242.26 25.67 o -1 9 0 38.55 46.78 15.72 o 0 9 0 39.33 44.90 11.80 o 1 9 0 181.99 147.97 20.38 o 2 9 0 775.49 733.39 35.22 o 3 9 0 33.95 37.37 15.87 o 4 9 0 224.59 223.30 21.75 o 5 9 0 222.55 228.89 23.46 o 6 9 0 104.54 110.94 20.42 o 7 9 0 290.10 284.72 28.16 o 8 9 0 100.34 119.02 21.26 o -2 10 0 2.66 2.69 21.16 o -1 10 0 212.66 151.79 28.07 o 0 10 0 46.17 59.41 12.34 o 1 10 0 253.79 228.35 24.69 o 2 10 0 341.38 320.48 26.30 o 3 10 0 8.13 12.83 20.38 o 4 10 0 230.30 241.62 25.37 o 5 10 0 3.59 11.12 19.49 o 6 10 0 280.65 289.48 25.86 o 7 10 0 57.82 64.90 18.02 o 8 10 0 32.17 40.60 25.27 o 0 11 0 23.46 20.33 17.74 o 1 11 0 18.44 -22.04 22.04 o 2 11 0 98.77 145.33 19.69 o 3 11 0 99.55 146.79 23.31 o 4 11 0 0.16 -7.00 17.58 o 5 11 0 108.41 83.12 22.82 o 6 11 0 2.55 -15.04 24.54 o 7 11 0 27.28 21.94 25.42 o 2 12 0 48.30 37.42 20.67 o 3 12 0 0.04 11.07 24.10 o 4 12 0 33.37 57.06 19.20 o 5 12 0 6.88 20.52 19.30 o -4 -12 1 5.09 -18.56 25.03 o -3 -12 1 44.50 39.23 26.84 o -6 -11 1 17.69 36.78 19.40 o -5 -11 1 5.71 -2.45 18.66 o -4 -11 1 102.48 96.05 22.48 o -3 -11 1 17.23 14.94 20.18 o -2 -11 1 130.73 128.97 22.04 o -1 -11 1 9.34 18.07 20.18 o 0 -11 1 78.09 88.82 16.10 o -7 -10 1 31.02 32.91 25.71 o -6 -10 1 146.92 164.23 23.61 o -5 -10 1 344.77 322.78 28.21 o -4 -10 1 4.12 2.20 20.23 o -3 -10 1 169.32 206.36 22.38 o -2 -10 1 1.96 22.09 22.73 o -1 -10 1 136.05 146.84 24.64 o 0 -10 1 199.00 189.37 22.19 o 1 -10 1 4.56 12.69 24.69 o 2 -10 1 206.80 218.94 27.53 o -8 -9 1 39.01 25.47 25.47 o -7 -9 1 59.91 72.59 21.01 o -6 -9 1 328.28 310.83 27.14 o -5 -9 1 3.38 -3.87 18.86 o -4 -9 1 220.36 251.66 21.01 o -3 -9 1 8.50 19.05 17.24 o -2 -9 1 771.08 782.32 36.98 o -1 -9 1 828.00 795.05 36.44 o 0 -9 1 0.48 -9.61 12.22 o 1 -9 1 133.19 145.13 21.85 o 2 -9 1 4.79 22.53 14.45 o 3 -9 1 67.12 77.93 22.24 o -9 -8 1 36.68 80.08 18.76 o -8 -8 1 110.86 101.63 22.53 o -7 -8 1 93.76 76.80 18.42 o -6 -8 1 79.90 83.95 16.95 o -5 -8 1 148.56 147.82 18.86 o -4 -8 1 128.59 137.29 16.36 o -3 -8 1 243.24 242.36 21.11 o -2 -8 1 10.52 4.95 16.51 o -1 -8 1 1.29 13.67 16.36 o 0 -8 1 3.31 1.72 11.34 o 1 -8 1 203.79 207.53 23.85 o 2 -8 1 201.21 186.71 21.65 o 3 -8 1 96.14 118.97 23.56 o 4 -8 1 30.37 18.37 25.03 o -9 -7 1 35.62 38.25 24.59 o -8 -7 1 226.95 259.21 23.76 o -7 -7 1 162.83 145.57 21.85 o -6 -7 1 340.97 354.37 25.86 o -5 -7 1 172.94 170.45 17.63 o -4 -7 1 391.18 389.93 23.17 o -3 -7 1 394.22 388.76 22.82 o -2 -7 1 191.46 182.21 15.82 o -1 -7 1 579.44 581.74 26.25 o 0 -7 1 0.14 12.11 10.05 o 1 -7 1 414.11 455.37 25.71 o 2 -7 1 110.47 125.39 18.07 o 3 -7 1 287.75 302.75 25.86 o 4 -7 1 210.87 217.18 23.85 o 5 -7 1 0.05 10.53 19.00 o -9 -6 1 81.92 68.92 23.41 o -8 -6 1 98.09 87.19 20.18 o -7 -6 1 75.60 74.70 18.27 o -6 -6 1 272.53 246.57 21.75 o -5 -6 1 476.35 472.47 24.54 o -4 -6 1 560.89 548.63 24.49 o -3 -6 1 32.41 28.11 10.73 o -2 -6 1 357.69 356.87 18.91 o -1 -6 1 94.22 89.05 13.67 o 0 -6 1 446.71 451.57 40.46 o 1 -6 1 358.49 348.25 21.11 o 2 -6 1 594.18 506.17 29.05 o 3 -6 1 840.71 815.97 34.68 o 4 -6 1 38.12 24.59 21.26 o 5 -6 1 94.62 123.48 21.40 o 6 -6 1 0.32 8.08 19.20 o -9 -5 1 109.34 72.20 21.31 o -8 -5 1 189.89 195.04 23.85 o -7 -5 1 12.62 1.76 16.41 o -6 -5 1 1314.00 1292.70 39.09 o -5 -5 1 299.28 318.62 19.54 o -4 -5 1 4.49 -12.59 12.59 o -3 -5 1 763.52 701.84 23.46 o -2 -5 1 19.38 13.57 11.46 o -1 -5 1 1488.58 1498.71 40.36 o 0 -5 1 228.36 229.16 10.91 o 1 -5 1 1317.76 1364.45 34.92 o 2 -5 1 16.84 18.86 12.44 o 3 -5 1 112.21 91.74 15.72 o 4 -5 1 662.04 625.97 31.05 o 5 -5 1 90.60 75.09 19.84 o 6 -5 1 46.22 53.19 17.88 o -9 -4 1 243.94 197.69 26.65 o -8 -4 1 155.17 144.00 21.45 o -7 -4 1 822.36 824.64 35.22 o -6 -4 1 1.12 -2.89 14.06 o -5 -4 1 274.97 307.65 18.71 o -4 -4 1 1184.42 1278.00 37.57 o -3 -4 1 41.37 50.45 8.91 o -2 -4 1 6431.84 6657.30 73.03 o -1 -4 1 2281.06 2517.65 45.70 o 0 -4 1 3458.36 3506.18 44.74 o 1 -4 1 168.99 152.97 13.37 o 2 -4 1 122.09 111.97 12.93 o 3 -4 1 380.83 385.48 20.62 o 4 -4 1 28.34 47.07 13.42 o 5 -4 1 472.69 472.37 27.87 o 6 -4 1 19.08 -2.11 20.47 o 7 -4 1 302.96 302.41 30.37 o -9 -3 1 0.99 -4.75 21.55 o -8 -3 1 554.80 572.29 33.31 o -7 -3 1 132.85 161.88 17.39 o -6 -3 1 1040.11 1042.75 34.09 o -5 -3 1 468.36 515.91 21.75 o -4 -3 1 10.31 7.54 9.89 o -3 -3 1 1479.64 1435.52 33.89 o -2 -3 1 1320.02 1326.98 29.78 o -1 -3 1 1182.30 1147.08 27.33 o 0 -3 1 776.76 805.08 15.35 o 1 -3 1 231.89 204.49 12.93 o 2 -3 1 5.72 15.53 9.75 o 3 -3 1 2.24 -12.15 12.15 o 4 -3 1 1730.56 1798.57 52.46 o 5 -3 1 137.25 130.24 17.44 o 6 -3 1 145.95 154.73 21.70 o 7 -3 1 67.45 37.08 25.76 o 8 -3 1 2.20 24.39 21.55 o -9 -2 1 305.62 304.90 29.93 o -8 -2 1 0.52 0.00 18.81 o -7 -2 1 70.09 77.44 15.77 o -6 -2 1 279.66 273.90 20.42 o -5 -2 1 26.18 32.23 8.82 o -4 -2 1 1410.41 1335.60 35.61 o -3 -2 1 3092.64 3261.52 48.05 o -2 -2 1 8078.10 7814.66 63.43 o -1 -2 1 3446.92 3325.44 37.37 o 0 -2 1 228.66 216.67 6.15 o 1 -2 1 1226.31 1312.44 28.16 o 2 -2 1 408.08 429.36 15.87 o 3 -2 1 55.46 48.93 8.47 o 4 -2 1 1044.24 1042.06 30.96 o 5 -2 1 871.82 875.48 33.16 o 6 -2 1 272.62 254.90 22.92 o 7 -2 1 26.33 14.94 20.38 o 8 -2 1 50.26 35.27 20.38 o -9 -1 1 22.30 36.98 20.03 o -8 -1 1 148.28 152.33 21.99 o -7 -1 1 344.01 351.19 23.71 o -6 -1 1 60.01 -1.47 19.74 o -5 -1 1 4.81 4.70 12.15 o -4 -1 1 24.48 20.18 7.84 o -3 -1 1 1234.68 1236.22 30.12 o -2 -1 1 2317.09 2421.75 33.94 o -1 -1 1 156.70 142.78 5.83 o 0 -1 1 5465.83 5169.68 70.04 o 1 -1 1 1064.28 1090.16 21.40 o 2 -1 1 1393.09 1478.68 30.51 o 3 -1 1 35.78 9.21 8.72 o 4 -1 1 1643.55 1630.66 43.74 o 5 -1 1 1746.46 1717.46 50.30 o 6 -1 1 315.45 330.57 22.19 o 7 -1 1 170.60 194.01 21.06 o 8 -1 1 11.76 25.86 17.14 o -9 0 1 100.11 108.69 22.48 o -8 0 1 267.43 230.31 26.50 o -7 0 1 57.17 43.59 16.90 o -6 0 1 1098.22 1059.30 35.32 o -5 0 1 149.52 141.55 14.55 o -4 0 1 4375.89 4520.22 67.59 o -3 0 1 4669.96 4756.46 58.97 o -2 0 1 2512.30 2609.34 36.10 o -1 0 1 3203.72 3241.29 29.83 o 0 0 1 761.69 811.28 20.20 o 1 0 1 8388.01 8160.12 46.58 o 2 0 1 8.07 9.06 7.35 o 3 0 1 201.66 180.00 12.00 o 4 0 1 1130.34 1072.43 27.92 o 5 0 1 182.44 183.04 16.56 o 6 0 1 703.75 655.51 28.07 o 7 0 1 3.05 20.42 15.04 o 8 0 1 24.49 22.19 18.32 o 9 0 1 6.88 -24.20 24.20 o -8 1 1 45.72 43.98 17.88 o -7 1 1 194.12 194.11 21.80 o -6 1 1 1.77 -1.62 15.23 o -5 1 1 634.69 604.62 25.81 o -4 1 1 39.29 36.88 9.94 o -3 1 1 1713.81 1701.64 38.40 o -2 1 1 2925.07 2890.98 41.73 o -1 1 1 1725.60 1715.94 25.86 o 0 1 1 10627.02 9394.05 98.40 o 1 1 1 4339.07 4200.14 33.50 o 2 1 1 887.23 971.92 21.50 o 3 1 1 1218.25 1210.41 29.83 o 4 1 1 3.64 25.96 7.69 o 5 1 1 1179.39 1148.50 31.98 o 6 1 1 139.63 162.37 16.80 o 7 1 1 613.11 634.10 30.56 o 8 1 1 2.43 8.47 20.62 o 9 1 1 52.37 51.92 20.18 o -8 2 1 68.89 58.73 20.47 o -7 2 1 91.27 69.55 19.10 o -6 2 1 304.50 304.46 23.61 o -5 2 1 82.22 80.72 13.13 o -4 2 1 926.55 996.12 30.07 o -3 2 1 915.95 947.63 25.76 o -2 2 1 415.06 404.14 15.92 o -1 2 1 1583.77 1588.83 29.68 o 0 2 1 61.16 69.84 6.49 o 1 2 1 6282.37 5909.36 47.46 o 2 2 1 164.13 180.54 9.40 o 3 2 1 66.78 65.00 7.54 o 4 2 1 37.68 49.13 9.06 o 5 2 1 0.81 13.62 10.78 o 6 2 1 1379.08 1355.00 38.45 o 7 2 1 73.21 59.61 15.28 o 8 2 1 85.92 45.26 19.69 o 9 2 1 141.01 142.53 23.36 o -8 3 1 29.70 27.09 21.70 o -7 3 1 485.77 426.57 31.84 o -6 3 1 304.69 258.72 24.20 o -5 3 1 450.17 476.34 26.50 o -4 3 1 329.28 347.86 20.62 o -3 3 1 1540.90 1635.71 44.18 o -2 3 1 1228.50 1172.15 33.89 o -1 3 1 19.34 20.91 7.54 o 0 3 1 767.21 793.16 33.77 o 1 3 1 21330.89 19330.93 103.10 o 2 3 1 2652.78 2597.74 39.92 o 3 3 1 168.61 156.25 10.97 o 4 3 1 0.21 11.02 8.13 o 5 3 1 407.78 387.29 19.69 o 6 3 1 26.09 25.23 15.33 o 7 3 1 490.84 491.57 27.43 o 8 3 1 138.52 148.12 19.30 o 9 3 1 16.53 -14.16 23.12 o -7 4 1 39.34 45.45 22.38 o -6 4 1 13.70 10.82 20.42 o -5 4 1 17.33 19.69 14.30 o -4 4 1 220.42 222.91 18.66 o -3 4 1 578.44 594.18 24.69 o -2 4 1 51.40 55.05 11.02 o -1 4 1 23.68 -11.41 11.41 o 0 4 1 582.69 598.77 18.44 o 1 4 1 4387.02 4437.20 57.99 o 2 4 1 4844.74 4999.01 61.76 o 3 4 1 45.26 50.35 9.40 o 4 4 1 425.54 397.13 17.78 o 5 4 1 505.42 551.23 23.31 o 6 4 1 995.02 1003.51 33.99 o 7 4 1 1950.24 1898.49 50.55 o 8 4 1 110.54 114.17 19.79 o 9 4 1 139.19 124.70 22.92 o -7 5 1 89.30 55.40 23.90 o -6 5 1 141.63 128.13 23.95 o -5 5 1 100.50 121.32 19.30 o -4 5 1 614.86 579.34 31.69 o -3 5 1 9.89 -12.98 16.41 o -2 5 1 831.61 854.76 29.44 o -1 5 1 111.15 89.19 12.98 o 0 5 1 4051.34 3979.46 46.01 o 1 5 1 3315.61 3373.34 57.85 o 2 5 1 240.04 241.67 15.28 o 3 5 1 396.47 404.48 17.83 o 4 5 1 53.25 35.46 11.46 o 5 5 1 286.59 262.63 17.73 o 6 5 1 1037.13 990.09 33.89 o 7 5 1 98.41 113.39 18.37 o 8 5 1 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156.93 23.31 o -6 -8 3 298.57 330.42 26.65 o -5 -8 3 685.32 658.98 33.55 o -4 -8 3 5.50 -13.91 16.31 o -3 -8 3 63.16 54.12 14.60 o -2 -8 3 9.97 12.39 15.18 o -1 -8 3 520.70 500.04 29.54 o 0 -8 3 310.56 296.44 18.12 o 1 -8 3 250.16 249.12 23.95 o 2 -8 3 268.56 292.32 27.87 o 3 -8 3 26.41 31.84 22.58 o 4 -8 3 36.84 35.41 24.25 o -9 -7 3 48.68 21.21 22.82 o -8 -7 3 0.51 32.91 16.02 o -7 -7 3 188.73 213.07 19.74 o -6 -7 3 505.92 495.83 28.56 o -5 -7 3 9.51 42.12 13.42 o -4 -7 3 924.38 957.28 33.94 o -3 -7 3 3.67 -15.87 15.87 o -2 -7 3 129.26 150.91 16.85 o -1 -7 3 181.92 148.71 18.81 o 0 -7 3 142.48 154.40 13.47 o 1 -7 3 555.73 534.82 29.88 o 2 -7 3 12.82 19.49 17.58 o 3 -7 3 323.91 307.16 28.60 o 4 -7 3 109.59 129.11 20.67 o 5 -7 3 67.23 78.12 24.44 o -9 -6 3 1.78 7.69 21.26 o -8 -6 3 114.11 122.65 21.55 o -7 -6 3 384.52 396.25 26.60 o -6 -6 3 47.98 51.97 16.36 o -5 -6 3 1509.46 1534.46 42.07 o -4 -6 3 65.84 67.54 12.59 o -3 -6 3 10.28 11.95 10.53 o -2 -6 3 44.45 11.71 12.98 o -1 -6 3 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