#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/48/2204890.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204890_Fobs loop_ _publ_author_name 'Skovsgaard, Signe' 'Bond, Andrew D.' 'McKenzie, Christine J.' _publ_section_title ; Dipotassium hexakis({2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}nickel(II)) tetracyanonickelate(II) methanol hexasolvate dihydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m135 _journal_page_last m137 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.3214 _cell_length_b 24.8555 _cell_length_c 29.7089 _exptl_crystal_F_000 5016.00 _reflns_d_resolution_high 0.8501 _[local]_cod_data_source_file hb6126Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cm0447 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 823.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 98074.16 99073.77 2729.54 o 6 0 0 62499.96 65426.66 2362.61 o 8 0 0 23364.81 23867.61 1204.55 o 10 0 0 1206.91 963.56 723.70 o 12 0 0 713.97 2303.06 911.16 o 14 0 0 10508.46 11361.46 1292.53 o 16 0 0 4824.65 4423.52 3100.78 o 4 1 0 15348.05 15736.97 445.23 o 6 1 0 5255.44 4969.62 475.37 o 8 1 0 2623.35 3440.12 447.70 o 10 1 0 0.91 148.69 523.16 o 12 1 0 32.68 -231.65 588.04 o 14 1 0 1784.82 1231.69 733.39 o 16 1 0 16.89 757.56 844.59 o 4 2 0 12532.68 13168.58 399.15 o 6 2 0 24934.21 23176.95 753.81 o 8 2 0 146203.67 137272.03 3335.86 o 10 2 0 975.04 364.81 514.92 o 12 2 0 4186.31 3662.27 631.83 o 14 2 0 11139.56 11775.16 892.31 o 16 2 0 5050.46 4082.98 893.53 o 2 3 0 8940.39 6383.77 151.17 o 4 3 0 10349.25 11766.67 363.08 o 6 3 0 226.79 -191.32 319.77 o 8 3 0 45680.68 44282.16 1280.04 o 10 3 0 2317.17 2320.79 513.59 o 12 3 0 1238.66 1268.02 587.65 o 14 3 0 621.79 384.06 722.23 o 16 3 0 563.72 640.09 821.21 o 2 4 0 126545.71 126482.69 1600.21 o 4 4 0 31607.88 31395.10 598.78 o 6 4 0 9278.79 9082.97 546.84 o 8 4 0 294522.13 306983.25 7194.95 o 10 4 0 178.35 -470.83 470.83 o 12 4 0 1098.95 1380.81 739.52 o 14 4 0 3591.91 3057.03 658.43 o 16 4 0 2924.15 4237.15 963.65 o 2 5 0 48011.38 49663.32 788.65 o 4 5 0 8697.39 10101.83 287.24 o 6 5 0 3800.08 4563.65 573.26 o 8 5 0 101046.24 103303.18 2571.60 o 10 5 0 13210.50 14169.67 989.35 o 12 5 0 5.45 528.41 548.26 o 14 5 0 2066.12 3174.51 699.55 o 16 5 0 1153.32 1045.38 882.10 o 0 6 0 286831.56 255704.44 5708.13 o 2 6 0 17418.45 15540.18 328.59 o 4 6 0 10658.30 11593.16 307.74 o 6 6 0 10267.53 8424.95 403.30 o 8 6 0 138484.73 136522.98 2675.77 o 10 6 0 317.15 218.77 434.20 o 12 6 0 3792.31 3400.56 679.84 o 14 6 0 1729.23 1955.27 735.81 o 16 6 0 2298.26 808.18 985.71 o 2 7 0 3892.31 3331.58 179.20 o 4 7 0 7495.59 6568.49 276.53 o 6 7 0 49947.06 42382.48 814.51 o 8 7 0 6355.98 5994.40 373.57 o 10 7 0 9590.85 10220.51 481.68 o 12 7 0 1277.29 1408.19 481.40 o 14 7 0 6400.67 6427.52 669.25 o 16 7 0 5851.89 3910.59 909.37 o 0 8 0 16684.02 15734.49 471.85 o 2 8 0 46608.07 45684.51 708.69 o 4 8 0 4300.89 3335.88 324.52 o 6 8 0 96.13 -148.58 229.73 o 8 8 0 2734.93 2407.11 323.17 o 10 8 0 3249.05 3263.86 405.69 o 12 8 0 462.86 536.41 438.38 o 14 8 0 4282.33 3735.44 767.57 o 16 8 0 5222.98 4199.06 1083.99 o 2 9 0 91093.15 90278.20 1267.93 o 4 9 0 444.68 830.68 188.30 o 6 9 0 36532.26 36716.68 735.18 o 8 9 0 7340.00 7372.64 397.07 o 10 9 0 1502.82 1619.74 410.31 o 12 9 0 1523.41 1713.47 461.10 o 14 9 0 2609.10 3473.46 752.58 o 16 9 0 13472.98 11099.84 1638.85 o 0 10 0 142580.50 146089.02 3315.45 o 2 10 0 22726.31 21375.68 433.21 o 4 10 0 1177.48 1314.80 215.50 o 6 10 0 48.19 252.58 256.42 o 8 10 0 4523.59 5887.15 387.58 o 10 10 0 5139.41 4837.01 511.18 o 12 10 0 10.41 395.67 548.07 o 14 10 0 1761.32 1618.59 878.61 o 2 11 0 142590.69 133682.16 2326.47 o 4 11 0 10517.49 8721.52 349.17 o 6 11 0 78873.50 71965.32 1278.56 o 8 11 0 3166.12 3061.08 523.41 o 10 11 0 972.77 491.94 410.42 o 12 11 0 1279.99 725.88 552.39 o 14 11 0 6309.32 5409.27 1069.60 o 0 12 0 18199.91 15209.83 505.04 o 2 12 0 19486.62 18138.93 486.07 o 4 12 0 2760.32 4045.82 256.05 o 6 12 0 109.48 143.05 264.89 o 8 12 0 297.40 131.30 375.50 o 10 12 0 26.04 -143.79 459.97 o 12 12 0 19.17 406.44 574.62 o 14 12 0 19.41 30.21 766.81 o 2 13 0 85709.74 78118.79 1531.75 o 4 13 0 27422.12 27935.05 620.26 o 6 13 0 61969.80 59464.43 1094.68 o 8 13 0 5648.69 5709.46 449.85 o 10 13 0 4897.65 5367.41 559.00 o 12 13 0 2401.85 1791.02 683.51 o 14 13 0 10209.19 10294.41 1120.05 o 0 14 0 1364.65 2324.45 360.08 o 2 14 0 3280.98 3541.64 343.95 o 4 14 0 5655.17 6299.88 298.93 o 6 14 0 1763.56 1909.42 358.97 o 8 14 0 2651.93 2610.82 471.47 o 10 14 0 933.74 1314.77 517.73 o 12 14 0 657.82 703.62 681.01 o 14 14 0 19.44 48.77 808.32 o 2 15 0 88788.98 85826.42 1684.48 o 4 15 0 55381.77 51366.38 1078.66 o 6 15 0 29302.16 29338.49 855.63 o 8 15 0 87.65 38.36 513.66 o 10 15 0 5671.40 4819.23 769.95 o 12 15 0 2419.24 3090.23 729.15 o 14 15 0 5117.88 4967.35 873.32 o 0 16 0 361.74 1384.65 396.95 o 2 16 0 2411.77 3086.45 316.29 o 4 16 0 11495.83 11254.17 458.86 o 6 16 0 2072.63 1895.80 415.94 o 8 16 0 353.89 613.10 464.53 o 10 16 0 547.01 802.04 541.18 o 12 16 0 143.58 -751.90 751.90 o 14 16 0 40.39 1659.94 1907.29 o 2 17 0 49109.44 44222.64 967.18 o 4 17 0 19775.65 20269.12 739.55 o 6 17 0 48031.08 46238.13 1187.32 o 8 17 0 7031.18 6719.48 553.01 o 10 17 0 2228.91 2451.26 587.70 o 12 17 0 1460.68 479.21 721.59 o 0 18 0 20227.56 20926.78 972.38 o 2 18 0 1961.02 2628.52 338.72 o 4 18 0 6889.24 6348.87 470.77 o 6 18 0 2444.75 2472.01 448.77 o 8 18 0 1953.18 2131.97 501.93 o 10 18 0 550.11 272.69 563.08 o 12 18 0 2.87 77.55 907.90 o 2 19 0 16084.04 16457.63 624.92 o 4 19 0 11469.88 11313.35 580.61 o 6 19 0 40642.36 39068.88 1395.41 o 8 19 0 381.50 262.46 524.32 o 10 19 0 429.83 -424.25 683.25 o 12 19 0 2014.82 1686.17 976.41 o 0 20 0 14336.54 12759.26 812.10 o 2 20 0 4055.63 4130.12 394.44 o 4 20 0 1414.27 2073.78 453.45 o 6 20 0 8989.28 9138.56 709.57 o 8 20 0 6566.54 6889.94 687.46 o 10 20 0 110.60 337.44 697.91 o 12 20 0 121.73 -398.21 954.69 o 2 21 0 4304.43 5873.32 422.75 o 4 21 0 4524.97 6594.37 607.02 o 6 21 0 16315.56 18258.43 919.30 o 8 21 0 50.61 -1176.45 1176.45 o 10 21 0 901.31 2815.07 808.13 o 0 22 0 178.39 378.01 479.54 o 2 22 0 4044.57 4365.33 462.63 o 4 22 0 14.43 492.31 547.35 o 6 22 0 7755.39 6806.87 931.50 o 8 22 0 10418.33 13963.22 1000.18 o 10 22 0 468.03 706.24 816.42 o 2 23 0 5694.20 5961.36 1511.25 o 4 23 0 995.64 1456.39 574.52 o 6 23 0 7538.06 7601.78 783.58 o 8 23 0 269.99 5315.71 3105.90 o 10 23 0 34.45 -334.43 892.29 o 0 24 0 13829.38 17925.53 2016.67 o 2 24 0 49.21 2226.84 1456.20 o 4 24 0 62.74 -358.10 753.76 o 6 24 0 3344.97 4427.32 761.05 o 8 24 0 13217.67 13922.92 1026.49 o 2 25 0 2144.27 2889.53 1411.17 o 4 25 0 3462.17 3836.74 1599.89 o 6 25 0 381.08 1772.55 943.94 o 8 25 0 31.62 1816.00 885.00 o 0 26 0 16547.46 20801.48 2138.20 o 2 26 0 517.22 -1137.37 1375.42 o 4 26 0 0.95 749.91 1638.50 o 6 26 0 2603.32 4157.72 1756.45 o 2 27 0 223.29 1148.09 1707.84 o 4 27 0 1851.21 -1444.77 1476.93 o 6 27 0 40.54 912.18 1730.00 o 0 28 0 12552.13 13258.10 2216.83 o 2 28 0 798.02 1002.97 1883.70 o 4 28 0 239.47 396.04 1835.80 o 2 29 0 17.54 202.31 1950.18 o 3 1 1 71916.10 73845.25 1018.05 o 4 1 1 290793.28 290641.19 3877.46 o 5 1 1 18794.92 19296.64 393.14 o 6 1 1 48783.18 45197.25 866.46 o 7 1 1 77910.97 76058.74 1365.56 o 8 1 1 3021.10 2896.85 308.18 o 9 1 1 36096.86 35212.52 787.89 o 10 1 1 8460.79 8115.45 430.29 o 11 1 1 22627.29 23887.35 685.75 o 12 1 1 4098.95 4235.63 459.36 o 13 1 1 1300.33 1388.62 454.74 o 14 1 1 11676.63 12364.48 652.32 o 15 1 1 61.10 -320.15 557.90 o 16 1 1 18.64 -623.11 623.11 o 3 2 1 6630.23 7138.71 198.82 o 4 2 1 678447.38 678335.38 8314.32 o 5 2 1 72.57 -33.77 187.26 o 6 2 1 160.38 279.96 224.80 o 7 2 1 20475.38 21342.89 540.43 o 8 2 1 26.70 101.57 287.01 o 9 2 1 10.93 178.19 310.27 o 10 2 1 2.65 -122.24 348.04 o 11 2 1 161.16 -434.91 434.91 o 12 2 1 339.82 522.35 430.35 o 13 2 1 687.12 810.97 472.79 o 14 2 1 547.30 672.57 505.43 o 15 2 1 1.84 932.80 568.57 o 16 2 1 0.06 -433.31 570.55 o 2 3 1 6215.11 5877.62 98.57 o 3 3 1 24191.33 26609.33 344.88 o 4 3 1 501600.19 502972.34 5948.13 o 5 3 1 1561.57 1032.65 224.66 o 6 3 1 11200.25 12113.21 411.27 o 7 3 1 88713.79 87568.16 1548.68 o 8 3 1 11892.99 12584.83 475.77 o 9 3 1 37843.68 36817.42 810.74 o 10 3 1 8225.76 8454.64 602.95 o 11 3 1 21320.83 22288.02 663.38 o 12 3 1 1715.17 1907.73 449.37 o 13 3 1 3559.52 3498.58 497.91 o 14 3 1 8338.35 8192.44 585.80 o 15 3 1 31.84 -540.57 540.57 o 16 3 1 258.03 482.96 556.12 o 1 4 1 19715.73 14650.61 151.16 o 2 4 1 8991.15 8851.97 157.96 o 3 4 1 27125.54 26030.06 313.84 o 4 4 1 59001.56 61173.02 773.84 o 5 4 1 18897.80 16997.09 346.07 o 6 4 1 13064.19 13220.89 362.97 o 7 4 1 14196.84 12344.71 395.87 o 8 4 1 4903.46 4616.08 335.71 o 9 4 1 2757.11 3486.81 387.19 o 10 4 1 6849.44 6275.29 422.03 o 11 4 1 1747.48 1737.52 392.92 o 12 4 1 3826.93 4145.25 713.49 o 13 4 1 230.37 164.83 429.05 o 14 4 1 621.72 1006.52 475.81 o 15 4 1 14.95 915.11 513.16 o 16 4 1 7.31 -252.24 546.87 o 1 5 1 4084.41 3604.72 72.20 o 2 5 1 8262.90 7702.97 124.79 o 3 5 1 338.38 28.70 88.97 o 4 5 1 4626.11 5165.47 157.03 o 5 5 1 2865.13 3279.45 169.19 o 6 5 1 19124.22 19228.02 373.42 o 7 5 1 21248.40 19809.18 475.23 o 8 5 1 318.32 1454.92 281.87 o 9 5 1 46953.77 46196.76 899.40 o 10 5 1 12018.97 13319.93 507.59 o 11 5 1 14483.52 15100.90 530.89 o 12 5 1 11371.06 11637.49 520.82 o 13 5 1 1697.58 973.45 428.36 o 14 5 1 6988.71 6534.83 508.05 o 15 5 1 526.89 310.83 514.80 o 16 5 1 670.33 862.58 633.58 o 0 6 1 150.14 271.65 123.75 o 1 6 1 32422.37 29762.07 358.83 o 2 6 1 29019.03 28731.29 338.07 o 3 6 1 2957.73 3022.08 110.05 o 4 6 1 2865.75 2590.96 135.73 o 5 6 1 13768.53 14390.52 266.06 o 6 6 1 12678.94 12549.99 263.36 o 7 6 1 826.79 1492.18 200.92 o 8 6 1 1444.00 1386.47 246.81 o 9 6 1 697.47 910.26 253.92 o 10 6 1 209.28 321.70 339.07 o 11 6 1 816.92 459.41 325.95 o 12 6 1 42773.69 42283.52 1084.97 o 13 6 1 72.66 512.42 403.37 o 14 6 1 697.10 758.67 443.67 o 15 6 1 238.75 -404.33 477.54 o 16 6 1 87.00 -639.58 639.58 o 1 7 1 37514.23 39266.77 447.35 o 2 7 1 81.57 138.80 93.90 o 3 7 1 23935.69 27525.09 334.22 o 4 7 1 7327.71 7117.88 173.29 o 5 7 1 258.51 -13.33 152.28 o 6 7 1 24547.99 25030.19 398.57 o 7 7 1 10689.45 11401.35 288.25 o 8 7 1 150.61 53.42 206.57 o 9 7 1 34463.82 35022.95 611.81 o 10 7 1 15273.30 14635.66 435.70 o 11 7 1 4518.45 4724.50 325.01 o 12 7 1 18146.69 17926.23 606.40 o 13 7 1 1159.59 718.38 365.86 o 14 7 1 4156.00 4153.17 445.91 o 15 7 1 172.76 -463.63 549.31 o 16 7 1 1893.88 673.82 646.83 o 0 8 1 489.58 355.26 153.60 o 1 8 1 5956.24 6047.53 123.71 o 2 8 1 15472.07 14272.12 209.73 o 3 8 1 10274.87 11366.58 210.66 o 4 8 1 6659.70 6220.81 192.82 o 5 8 1 8318.18 7754.95 249.98 o 6 8 1 17433.22 17852.39 323.46 o 7 8 1 6665.33 6326.22 245.61 o 8 8 1 0.45 -70.50 215.07 o 9 8 1 3028.31 3201.74 261.15 o 10 8 1 1827.96 1559.00 276.53 o 11 8 1 313.46 343.65 288.79 o 12 8 1 33333.18 32912.45 681.06 o 13 8 1 1020.50 1140.09 391.08 o 14 8 1 1195.68 912.80 513.71 o 15 8 1 874.59 391.93 561.82 o 16 8 1 108.79 -225.89 640.49 o 1 9 1 5541.74 4344.99 116.61 o 2 9 1 4458.60 4619.00 117.73 o 3 9 1 2604.15 1838.67 161.71 o 4 9 1 7604.28 7897.35 192.57 o 5 9 1 27943.95 27678.41 412.50 o 6 9 1 10692.27 10830.59 251.90 o 7 9 1 6518.71 5976.45 265.18 o 8 9 1 2675.29 2743.45 243.51 o 9 9 1 20964.90 18535.91 411.70 o 10 9 1 1829.95 2056.92 278.87 o 11 9 1 1132.38 979.10 296.68 o 12 9 1 291.46 -158.72 314.97 o 13 9 1 4550.43 3964.41 513.45 o 14 9 1 2646.61 2513.43 544.25 o 15 9 1 182.50 -578.29 578.29 o 16 9 1 292.37 474.06 944.80 o 0 10 1 1409.93 1599.17 189.37 o 1 10 1 1902.57 1840.81 113.23 o 2 10 1 27697.97 25965.19 344.41 o 3 10 1 1183.45 699.85 117.55 o 4 10 1 12831.91 13020.69 255.45 o 5 10 1 1734.82 1027.10 187.42 o 6 10 1 11574.32 10517.72 253.70 o 7 10 1 3472.40 3647.50 217.87 o 8 10 1 169.69 120.03 227.30 o 9 10 1 808.04 1247.34 262.78 o 10 10 1 8348.65 8635.59 342.01 o 11 10 1 218.59 -172.84 297.04 o 12 10 1 11141.21 11547.56 515.33 o 13 10 1 1720.54 1960.44 548.30 o 14 10 1 1390.57 1718.02 541.94 o 15 10 1 1833.06 1847.96 596.30 o 1 11 1 267.14 433.03 157.47 o 2 11 1 55.11 402.26 112.20 o 3 11 1 1029.42 1147.02 135.37 o 4 11 1 8346.37 9357.02 252.78 o 5 11 1 2015.25 2730.88 171.22 o 6 11 1 4641.21 5721.80 216.07 o 7 11 1 5386.87 6202.30 259.50 o 8 11 1 1174.31 1212.44 242.14 o 9 11 1 13993.48 14326.75 466.71 o 10 11 1 79.05 256.59 281.06 o 11 11 1 4302.50 4716.33 396.76 o 12 11 1 4424.14 4299.85 465.63 o 13 11 1 2717.86 2109.69 502.84 o 14 11 1 943.38 264.02 529.61 o 15 11 1 14.60 -300.41 609.47 o 0 12 1 10373.69 10532.95 500.55 o 1 12 1 672.30 706.54 134.98 o 2 12 1 29366.55 27326.88 446.47 o 3 12 1 5833.62 5537.23 170.65 o 4 12 1 12093.19 12133.86 276.64 o 5 12 1 11101.67 12250.38 293.05 o 6 12 1 27592.40 26710.58 432.39 o 7 12 1 10079.23 11458.55 294.14 o 8 12 1 0.75 -95.12 245.16 o 9 12 1 60.66 191.08 272.23 o 10 12 1 743.50 717.61 338.73 o 11 12 1 120.39 -350.11 350.11 o 12 12 1 17686.34 17644.49 695.35 o 13 12 1 1372.56 1930.00 513.20 o 14 12 1 60.24 -527.77 527.77 o 15 12 1 2330.36 739.21 1063.31 o 1 13 1 706.32 801.57 137.38 o 2 13 1 163.58 299.89 145.25 o 3 13 1 11797.28 12038.28 258.01 o 4 13 1 559.15 389.20 160.98 o 5 13 1 1890.23 1057.32 211.36 o 6 13 1 29.77 170.07 187.56 o 7 13 1 4494.88 4504.36 257.18 o 8 13 1 1787.99 1530.18 297.61 o 9 13 1 7269.62 7329.59 482.23 o 10 13 1 61.97 -353.22 353.22 o 11 13 1 7769.13 7502.90 450.63 o 12 13 1 471.94 350.93 445.33 o 13 13 1 1234.76 1916.88 520.84 o 14 13 1 67.67 -550.26 550.26 o 15 13 1 3.90 -888.30 888.30 o 0 14 1 4913.05 5547.47 367.11 o 1 14 1 262.38 156.58 145.60 o 2 14 1 15555.60 14679.86 357.27 o 3 14 1 32110.29 31964.21 513.73 o 4 14 1 7047.48 7051.58 226.17 o 5 14 1 12052.49 12032.09 301.68 o 6 14 1 23791.70 23919.43 497.65 o 7 14 1 9366.17 7543.44 357.59 o 8 14 1 15.26 -206.93 305.57 o 9 14 1 1267.42 1972.99 388.37 o 10 14 1 2574.60 2324.60 499.77 o 11 14 1 1275.02 1393.03 399.61 o 12 14 1 3011.60 2598.09 468.81 o 13 14 1 2218.28 1343.10 528.66 o 14 14 1 137.84 -391.20 566.83 o 1 15 1 162.06 227.22 153.20 o 2 15 1 419.03 914.60 168.33 o 3 15 1 710.72 827.76 191.26 o 4 15 1 13782.89 12523.75 293.60 o 5 15 1 489.24 437.83 201.24 o 6 15 1 9.44 424.91 267.51 o 7 15 1 3646.27 4023.19 327.13 o 8 15 1 227.00 64.16 309.74 o 9 15 1 2643.07 2811.85 359.95 o 10 15 1 64.00 -359.95 370.51 o 11 15 1 770.50 -71.15 396.59 o 12 15 1 1284.73 1932.67 525.60 o 13 15 1 2170.64 1581.58 545.68 o 14 15 1 67.97 421.84 596.73 o 0 16 1 39.30 -8.02 369.73 o 1 16 1 3356.50 3876.00 200.49 o 2 16 1 16127.72 15836.48 336.25 o 3 16 1 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