#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180970 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/50/2205008.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205008_Fobs loop_ _publ_author_name 'Mizuguchi, Jin' 'Hino, Kazuyuki' 'Sato, Kazuyuki' 'Takahashi, Hiroo' 'Suzuki, Shigeru' _publ_section_title ; N,N'-Di-3-pyridylperylene-3,4:9,10-bis(dicarboximide) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o434 _journal_page_last o436 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cod_data_source_file bt6588Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 1 0 -1 2827.40 71.33 2817.10 o 1 0 1 2532.22 63.85 2545.48 o 0 0 2 4200.93 106.33 4250.22 o 2 0 0 515.91 14.93 559.69 o 2 0 -2 1305.19 34.60 1356.54 o 1 0 -3 13811.24 377.15 15669.07 o 1 0 3 260.74 11.47 279.82 o 2 0 2 535.48 17.35 580.78 o 3 0 -1 591.46 22.96 594.09 o 0 0 4 70.66 8.96 96.17 o 3 0 1 969.24 33.03 983.63 o 2 0 -4 2019.80 53.37 2094.52 o 3 0 -3 1093.98 30.12 1116.04 o 1 0 -5 7186.44 178.58 7058.55 o 4 0 -2 1193.20 33.15 1237.36 o 4 0 0 2673.72 69.55 2637.28 o 0 1 1 875.75 24.68 816.22 o 1 1 0 3320.32 86.06 3475.67 o 1 1 -1 5602.38 146.25 5851.15 o 2 0 4 802.90 24.94 876.63 o 1 1 1 949.71 24.11 916.28 o 0 1 2 15033.87 384.95 15504.46 o 3 0 3 1089.66 30.93 1105.59 o 1 1 -2 1326.13 34.43 1343.97 o 1 0 5 15.02 12.56 18.00 o 2 1 -1 1890.43 51.71 2060.27 o 2 1 0 0.53 11.76 3.89 o 3 0 -5 716.88 22.00 697.76 o 1 1 2 3354.69 84.99 3300.35 o 4 0 -4 397.47 15.77 397.02 o 2 1 -2 4197.29 108.44 4356.59 o 2 1 1 166.15 15.99 184.10 o 1 1 -3 2303.30 61.61 2361.35 o 0 1 3 30444.45 818.37 33829.06 o 4 0 2 485.11 18.74 517.53 o 2 0 -6 2586.19 65.32 2472.58 o 2 1 -3 1222.70 32.37 1276.09 o 0 0 6 88.41 13.71 69.39 o 1 1 3 6103.35 158.78 6140.05 o 2 1 2 1530.55 42.19 1512.00 o 5 0 -1 22.30 9.68 18.21 o 3 1 -1 2273.94 59.98 2340.15 o 3 1 0 414.00 17.64 437.03 o 3 1 -2 2592.41 68.91 2754.39 o 1 1 -4 93.72 15.24 96.43 o 5 0 -3 1253.42 34.24 1237.95 o 0 1 4 4939.28 122.97 4758.80 o 3 1 1 20.63 16.09 24.00 o 2 1 -4 4260.36 116.16 4414.53 o 3 1 -3 662.49 19.00 671.61 o 2 1 3 31.97 17.01 31.54 o 5 0 1 1118.67 31.47 1086.33 o 1 1 4 1530.06 39.77 1506.35 o 3 1 2 334.55 18.21 345.88 o 1 0 -7 334.40 13.90 354.78 o 3 1 -4 208.33 8.39 206.26 o 4 0 -6 334.43 17.14 311.52 o 3 0 5 1791.18 47.70 1785.44 o 1 1 -5 453.07 19.69 421.48 o 4 1 -1 528.92 19.35 546.60 o 4 1 -2 8.42 11.34 13.21 o 0 1 5 2623.70 67.48 2604.92 o 4 1 0 18.74 18.51 17.68 o 2 0 6 23.13 11.80 17.48 o 2 1 -5 720.56 26.05 725.61 o 5 0 -5 1681.38 41.98 1491.53 o 4 0 4 59.24 14.47 71.89 o 2 1 4 0.46 14.26 1.93 o 3 0 -7 672.73 22.44 670.32 o 4 1 -3 1435.39 41.77 1462.86 o 3 1 3 140.29 16.75 158.01 o 4 1 1 131.41 17.36 136.16 o 6 0 -2 970.27 29.31 1006.68 o 1 1 5 268.48 19.51 287.04 o 3 1 -5 94.06 18.53 86.46 o 1 0 7 2138.92 56.81 2153.16 o 4 1 -4 1169.76 36.06 1165.40 o 6 0 0 203.02 11.10 217.44 o 5 0 3 1023.21 30.77 1036.22 o 4 1 2 2.09 16.42 3.81 o 1 1 -6 8.00 16.35 13.99 o 6 0 -4 292.30 16.12 313.66 o 2 1 -6 307.85 20.10 317.16 o 0 1 6 401.26 17.00 381.37 o 3 1 4 54.20 18.88 67.91 o 2 1 5 365.27 13.72 401.23 o 2 0 -8 1883.41 48.30 1738.61 o 5 1 -1 32.35 18.89 54.55 o 5 1 -2 376.80 17.02 382.30 o 4 1 -5 1182.39 31.82 1229.09 o 5 1 0 438.88 37.94 479.04 o 5 1 -3 1450.15 41.68 1408.79 o 3 1 -6 253.84 7.41 263.05 o 0 0 8 1434.56 38.67 1432.84 o 4 1 3 1004.36 26.22 1031.25 o 1 1 6 2156.03 56.33 2004.38 o 5 1 1 430.58 20.72 433.99 o 6 0 2 3553.38 88.39 3346.23 o 5 1 -4 51.20 19.01 58.26 o 5 0 -7 111.28 15.53 96.25 o 1 1 -7 376.19 34.67 358.29 o 4 0 -8 294.61 15.54 276.84 o 2 1 -7 262.41 20.18 250.51 o 4 1 -6 914.82 24.50 930.99 o 6 0 -6 2845.83 67.91 2450.90 o 3 1 5 7.17 19.38 11.89 o 5 1 2 69.22 35.53 97.96 o 0 1 7 1063.07 29.77 984.72 o 2 1 6 33.22 37.67 24.56 o 7 0 -3 38.46 14.44 38.96 o 7 0 -1 116.17 10.76 132.86 o 5 1 -5 70.81 9.52 66.09 o 4 1 4 276.41 9.55 278.20 o 4 0 6 339.89 17.82 360.49 o 3 1 -7 780.60 27.84 749.00 o 3 0 7 370.39 18.29 373.30 o 1 0 -9 1674.37 45.36 1656.35 o 6 1 -2 450.68 19.43 448.36 o 6 1 -1 1049.83 31.39 999.76 o 5 0 5 467.86 20.33 463.20 o 1 1 7 5094.02 124.43 4707.53 o 6 1 -3 596.88 20.27 559.04 o 2 0 8 6.33 15.75 25.35 o 3 0 -9 38.80 14.37 38.48 o 6 1 0 1403.91 39.41 1323.99 o 5 1 3 395.87 11.31 422.22 o 7 0 -5 379.53 18.13 373.53 o 7 0 1 14447.72 340.63 13075.67 o 5 1 -6 2.12 21.35 4.22 o 4 1 -7 393.94 11.88 430.04 o 6 1 -4 768.61 23.62 767.17 o 3 1 6 18.58 9.91 21.02 o 6 1 1 3566.69 92.15 3512.69 o 1 1 -8 53.29 17.29 66.16 o 2 1 -8 40.35 20.69 40.98 o 4 1 5 9.86 16.80 12.34 o 6 0 4 10685.40 255.52 9913.72 o 2 1 7 20.18 11.65 11.74 o 1 0 9 7706.53 186.15 7194.69 o 0 1 8 140.48 16.31 106.93 o 6 1 -5 2820.15 71.42 2741.13 o 3 1 -8 496.64 25.54 433.46 o 5 1 4 447.34 16.82 477.04 o 6 1 2 866.95 28.85 772.13 o 5 1 -7 40.01 22.56 49.22 o 6 0 -8 13392.99 314.78 12078.72 o 1 1 8 813.55 33.14 783.60 o 5 0 -9 7.13 14.37 0.05 o 4 1 -8 124.36 22.27 129.95 o 2 0 -10 5.65 16.12 7.88 o 8 0 -2 59.35 17.50 75.07 o 6 1 -6 1107.67 29.37 1018.19 o 0 2 0 175.83 13.74 163.88 o 7 1 -2 1904.35 50.67 1791.98 o 0 2 1 10.81 14.15 13.29 o 7 0 -7 2115.98 55.66 2007.56 o 7 1 -3 192.78 16.57 178.24 o 7 1 -1 565.40 39.82 550.69 o 8 0 -4 307.88 15.64 308.19 o 7 0 3 156.94 18.97 112.42 o 1 2 0 9.25 13.35 15.92 o 1 2 -1 80.48 21.26 82.41 o 4 1 6 266.17 11.99 262.32 o 3 1 7 21.50 22.96 35.56 o 1 2 1 205.41 8.53 206.82 o 6 1 3 11.19 20.75 23.94 o 0 0 10 403.80 21.91 360.69 o 8 0 0 10.28 9.41 8.69 o 0 2 2 312.82 13.48 333.05 o 7 1 -4 339.78 17.70 350.20 o 1 2 -2 15.55 9.00 14.00 o 7 1 0 4.70 19.53 0.00 o 2 1 -9 385.41 24.55 365.96 o 1 1 -9 534.76 23.90 555.67 o 4 0 -10 92.88 14.20 68.62 o 2 2 -1 436.49 22.75 446.73 o 2 2 0 225.70 21.25 244.33 o 5 1 5 889.79 28.45 922.64 o 1 2 2 170.90 17.86 144.18 o 2 1 8 189.02 15.55 192.85 o 3 1 -9 112.60 22.09 105.62 o 2 2 -2 1595.48 47.23 1667.86 o 5 1 -8 121.48 7.47 140.86 o 2 2 1 377.67 15.17 389.34 o 1 2 -3 413.36 15.02 417.03 o 0 1 9 455.72 21.87 409.17 o 0 2 3 230.52 12.29 223.41 o 6 1 -7 2.05 21.01 6.18 o 7 1 -5 759.09 24.97 767.00 o 7 1 1 89.58 20.99 73.54 o 4 0 8 4.97 14.98 3.05 o 2 2 -3 24.54 20.44 6.76 o 5 0 7 561.95 23.70 595.32 o 1 2 3 165.28 20.58 181.64 o 8 0 -6 1.29 15.85 7.79 o 2 2 2 11.80 18.47 13.36 o 4 1 -9 139.19 23.06 124.72 o 3 2 -1 37.47 16.82 27.38 o 6 1 4 64.51 18.15 53.29 o 3 2 0 17.79 20.94 15.60 o 3 0 9 144.35 18.52 155.62 o 3 2 -2 52.76 11.88 60.04 o 1 2 -4 1106.76 31.93 1165.14 o 1 1 9 10.66 32.89 28.72 o 0 2 4 55.49 11.03 64.74 o 7 1 -6 797.74 25.32 812.57 o 7 1 2 1.10 19.04 2.42 o 3 2 1 12.97 12.29 3.67 o 6 0 6 98.08 18.00 82.29 o 8 0 2 453.03 24.10 439.78 o 2 2 -4 454.43 23.66 463.26 o 3 2 -3 416.77 25.15 419.57 o 4 1 7 108.58 12.06 107.55 o 2 2 3 0.80 19.80 13.34 o 3 1 8 215.88 24.38 192.95 o 1 2 4 8638.60 214.14 8316.04 o 3 0 -11 299.09 20.80 314.48 o 1 0 -11 1512.99 41.09 1440.26 o 5 1 6 88.90 24.04 112.25 o 6 1 -8 157.20 10.44 202.67 o 3 2 2 71.23 20.00 74.56 o 2 0 10 185.88 16.41 170.10 o 5 1 -9 456.67 27.22 449.15 o 2 1 -10 165.05 41.88 159.18 o 8 1 -2 3.03 19.30 0.40 o 8 1 -3 2.50 21.54 7.12 o 3 2 -4 1107.82 37.61 1152.08 o 1 1 -10 60.72 19.92 49.11 o 1 2 -5 22.45 11.96 23.63 o 4 2 -1 1.33 15.74 7.66 o 9 0 -3 49.87 16.62 47.47 o 8 1 -1 61.40 20.58 63.65 o 4 2 -2 623.39 22.18 618.80 o 3 1 -10 24.69 22.91 22.80 o 0 2 5 6669.05 172.89 6917.44 o 4 2 0 27.80 23.18 30.22 o 7 0 -9 2153.22 56.42 1939.03 o 7 1 -7 57.00 12.30 61.65 o 2 1 9 365.19 19.08 346.45 o 2 2 -5 1018.74 35.02 1060.26 o 8 1 -4 343.19 19.48 338.99 o 7 0 5 131.95 20.27 123.01 o 7 1 3 1332.35 41.19 1264.24 o 6 0 -10 10.43 17.37 18.67 o 9 0 -1 4.82 20.40 3.02 o 6 1 5 209.09 23.58 229.89 o 2 2 4 6.90 22.15 4.39 o 4 2 -3 24.12 25.15 28.34 o 0 1 10 1315.89 40.37 1194.39 o 8 1 0 85.22 20.63 63.65 o 3 2 3 123.56 21.99 109.69 o 4 2 1 62.69 23.21 50.90 o 1 2 5 579.09 30.31 600.21 o 9 0 -5 8.84 16.39 11.34 o 4 1 -10 281.30 25.42 290.12 o 8 1 -5 138.89 17.05 150.90 o 3 2 -5 1917.55 55.01 1903.79 o 8 0 -8 53.02 16.25 52.87 o 4 2 -4 157.96 24.21 168.58 o 5 0 -11 4.70 16.12 5.43 o 1 0 11 3082.94 78.25 2948.15 o 8 1 1 4.51 19.42 1.99 o 4 2 2 12.59 20.78 0.00 o 1 2 -6 123.79 20.19 123.57 o 6 1 -9 173.78 26.05 178.29 o 1 1 10 558.84 27.94 542.43 o 4 1 8 282.17 16.25 296.20 o 2 2 -6 317.63 23.24 304.46 o 0 2 6 2170.82 62.50 2461.73 o 5 1 7 200.44 18.86 220.16 o 7 1 -8 146.96 12.66 142.01 o 8 1 -6 30.57 23.99 37.40 o 7 1 4 2070.54 57.08 1930.20 o 9 0 1 250.43 21.80 215.13 o 2 2 5 542.19 24.75 502.32 o 3 2 4 119.24 23.72 111.80 o 5 2 -1 77.07 24.82 59.41 o 5 2 -2 413.81 50.32 428.25 o 5 1 -10 184.36 25.73 152.18 o 8 0 4 462.62 25.34 437.02 o 3 1 9 95.57 24.31 117.06 o 4 2 -5 24.16 53.06 8.05 o 5 2 0 782.46 32.12 742.31 o 5 2 -3 199.64 29.20 195.84 o 3 2 -6 -4.89 25.56 1.57 o 2 0 -12 718.06 23.43 716.31 o 6 1 6 607.81 51.81 563.04 o 4 2 3 381.69 25.54 374.73 o 1 2 6 1138.51 39.52 1053.05 o 8 1 2 72.63 20.02 65.64 o 2 1 -11 144.50 45.59 149.97 o 5 2 1 8.80 46.46 5.06 o 9 0 -7 423.79 22.19 452.93 o 5 2 -4 162.70 27.01 176.27 o 3 1 -11 9.18 25.49 1.31 o 1 1 -11 5.16 20.94 4.25 o 8 1 -7 378.62 18.22 373.31 o 4 0 -12 141.65 15.86 138.57 o 2 1 10 63.41 17.97 60.71 o 1 2 -7 54.69 20.71 48.61 o 2 2 -7 931.43 34.49 981.81 o 4 2 -6 1152.96 40.23 1143.69 o 3 2 5 17.29 21.17 16.83 o 0 0 12 1359.16 40.46 1211.34 o 9 1 -3 273.64 22.55 277.28 o 9 1 -2 40.39 21.37 37.64 o 4 1 -11 667.24 31.99 673.70 o 5 2 2 49.38 23.15 29.53 o 0 1 11 285.24 23.28 301.48 o 0 2 7 4098.61 102.11 3867.52 o 2 2 6 300.00 27.10 263.61 o 7 1 -9 383.13 29.69 355.12 o 7 1 5 589.18 29.84 605.82 o 6 1 -10 548.72 30.96 485.16 o 5 2 -5 1190.16 41.40 1169.89 o 5 0 9 0.99 17.14 2.55 o 9 1 -4 323.21 21.47 363.50 o 4 2 4 7.43 46.27 19.18 o 9 1 -1 175.56 23.53 158.76 o 8 1 3 18.39 24.16 8.03 o 3 2 -7 18.47 23.67 15.61 o 6 0 8 155.38 18.77 167.39 o 4 0 10 0.95 16.46 3.59 o 10 0 -2 134.14 42.95 162.50 o 10 0 -4 111.12 21.67 121.33 o 6 2 -2 3364.62 85.49 3179.17 o 9 1 -5 72.14 18.06 67.51 o 6 2 -1 16.73 20.30 21.10 o 5 1 8 418.67 22.15 404.70 o 9 1 0 51.31 40.71 44.10 o 1 2 7 5.73 26.06 11.82 o 4 1 9 141.65 16.43 152.06 o 6 2 -3 43.43 21.12 85.29 o 9 0 3 87.87 23.86 72.28 o 8 1 -8 101.76 14.70 123.27 o 6 2 0 208.59 26.34 195.77 o 5 1 -11 108.17 26.54 88.32 o 5 2 3 260.78 24.77 236.34 o 1 1 11 417.00 23.70 337.57 o 7 0 -11 90.45 21.65 61.06 o 6 1 7 841.05 28.87 813.59 o 7 0 7 25.52 21.06 29.24 o 5 2 -6 38.46 25.92 38.40 o 3 0 11 67.13 18.21 90.43 o 8 0 -10 852.73 28.10 799.03 o 4 2 -7 20.33 25.76 20.11 o 6 2 -4 878.52 35.82 854.87 o 3 1 10 130.31 17.84 122.64 o 9 1 -6 9.14 17.79 17.18 o 10 0 0 25.30 22.30 13.00 o 3 2 6 21.31 26.78 22.21 o 9 1 1 1.37 19.87 1.14 o 6 2 1 143.55 24.43 129.34 o 1 2 -8 258.62 23.57 279.17 o 2 2 -8 12.55 22.68 7.96 o 4 2 5 125.31 26.94 117.41 o 10 0 -6 382.30 24.03 373.26 o 8 1 4 24.61 25.30 25.21 o 6 0 -12 49.46 23.35 42.16 o 2 2 7 0.46 25.60 4.10 o 0 2 8 270.98 27.73 263.03 o 6 2 -5 276.22 28.26 263.04 o 7 1 -10 315.62 24.27 289.97 o 3 2 -8 591.16 30.33 592.97 o 2 1 -12 -4.44 49.95 4.17 o 3 0 -13 165.28 22.17 180.81 o 7 1 6 358.44 53.86 319.56 o 9 0 -9 1.40 21.66 0.27 o 3 1 -12 69.37 27.50 87.55 o 1 1 -12 41.38 22.63 48.64 o 5 2 4 4.97 25.87 1.13 o 1 0 -13 0.27 21.20 0.19 o 6 2 2 8.12 24.39 5.56 o 6 1 -11 1923.73 75.60 1809.49 o 9 1 -7 82.19 17.17 73.78 o 8 0 6 17.14 23.03 22.27 o 8 1 -9 11.72 28.18 21.08 o 2 1 11 56.43 19.65 52.15 o 2 0 12 878.03 33.55 859.13 o 5 2 -7 27.19 27.66 25.45 o 9 1 2 56.70 20.54 63.32 o 4 1 -12 797.93 35.12 791.27 o 1 2 8 131.30 19.68 112.89 o 4 2 -8 87.23 26.88 66.60 o 6 2 -6 165.81 27.19 141.77 o 0 1 12 231.24 24.45 224.25 o 7 2 -2 216.22 21.94 240.21 o 7 2 -3 1011.26 32.06 869.88 o 7 2 -1 3.68 22.34 4.94 o 5 1 9 87.69 54.56 113.09 o 5 0 -13 21.50 25.15 0.18 o 4 2 6 218.53 29.12 207.85 o 3 2 7 6.94 43.69 1.77 o 6 2 3 0.76 24.69 0.12 o 10 0 2 27.76 49.23 21.32 o 6 1 8 24.61 28.37 18.80 o 4 1 10 395.61 21.24 415.26 o 8 1 5 27.19 19.80 16.60 o 10 1 -3 6.64 21.89 12.88 o 5 1 -12 747.87 34.92 720.99 o 7 2 -4 -16.38 23.06 0.06 o 7 2 0 27.19 26.63 25.76 o 10 1 -2 362.42 26.81 389.00 o 2 2 -9 49.53 48.48 37.08 o 9 1 -8 82.26 26.76 69.86 o 10 1 -4 84.01 23.51 69.59 o 1 2 -9 40.96 24.36 26.99 o 10 0 -8 19.61 19.43 25.54 o 5 2 5 69.97 27.99 90.33 o 9 1 3 3.83 19.80 3.58 o 2 2 8 17.52 27.38 7.96 o 10 1 -1 273.07 26.73 285.27 o 3 2 -9 34.17 25.64 16.97 o 5 2 -8 326.17 30.47 310.90 o 1 1 12 906.63 35.37 895.43 o 10 1 -5 137.37 20.70 154.61 o 0 2 9 157.01 52.22 122.63 o 6 2 -7 16.80 50.37 21.55 o 7 1 -11 118.10 23.12 111.78 o 9 0 5 65.54 24.37 72.60 o 7 2 -5 541.02 31.77 453.01 o 7 2 1 17.14 24.99 1.91 o 7 1 7 483.48 33.20 468.26 o 1 0 13 53.63 29.53 43.65 o 3 1 11 12.82 19.57 2.17 o 8 1 -10 55.26 29.80 44.46 o 11 0 -3 22.04 18.47 1.07 o 10 1 0 878.83 36.30 884.24 o 4 2 -9 77.22 27.74 93.25 o 10 1 -6 8.95 24.54 0.17 o 6 2 4 17.03 23.56 18.99 o 11 0 -5 9.56 23.18 23.12 o 6 1 -12 942.43 65.71 961.78 o 11 0 -1 334.32 26.38 319.18 o 1 2 9 111.81 20.66 105.77 o 2 1 -13 38.23 28.27 29.20 o 7 2 -6 2.54 25.03 7.72 o 3 1 -13 165.36 29.72 164.04 o 7 2 2 79.72 25.97 69.75 o 9 1 -9 266.13 29.24 264.24 o 2 0 -14 177.34 23.58 161.27 o 4 2 7 391.93 46.13 386.11 o 1 1 -13 16.12 27.00 6.39 o 10 1 1 615.31 31.83 622.90 o 9 1 4 178.82 28.25 197.69 o 8 1 6 222.51 27.89 228.88 o 3 2 8 99.52 57.21 94.23 o 2 1 12 148.90 27.37 163.29 o 4 1 -13 382.41 31.12 374.11 o 5 2 6 121.36 24.05 101.32 o 4 0 -14 34.93 25.62 38.15 o 6 2 -8 11.95 28.56 3.29 o 8 0 -12 14.90 17.53 19.50 o 10 1 -7 10.32 26.78 0.02 o 5 2 -9 92.69 29.68 100.00 o 9 0 -11 271.78 21.45 260.54 o 6 0 10 134.60 24.46 161.77 o 2 2 -10 95.61 27.49 98.10 o 8 2 -2 201.62 30.39 191.89 o 8 2 -3 41.42 23.12 35.56 o 5 0 11 41.23 22.78 46.12 o 5 1 10 197.97 29.72 195.38 o 1 2 -10 616.26 32.29 646.10 o 6 1 9 438.65 32.51 456.27 o 8 2 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