#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180970 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/50/2205011.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205011_Fobs loop_ _publ_author_name 'Gao, Shan' 'Huo, Li-Hua' 'Liu, Ji-Wei' 'Ng, Seik Weng' _publ_section_title ; Twinned poly[[diaquacalcium(II)]-\m~4~-benzene-1,3-dioxyacetato] ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m407 _journal_page_last m409 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.647 _cell_angle_gamma 90.000 _cell_length_a 15.7947 _cell_length_b 7.9167 _cell_length_c 9.8291 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file bt6591Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 128.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 453.71 539.70 8.60 o 4 0 0 5862.36 6053.64 123.96 o 5 0 0 176.78 146.88 5.93 o 6 0 0 450.08 470.56 10.39 o 7 0 0 1457.39 1251.72 20.88 o 8 0 0 6095.83 5866.11 158.79 o 9 0 0 1515.62 1506.25 25.42 o 10 0 0 660.75 610.42 12.26 o 11 0 0 953.24 979.75 20.39 o 12 0 0 39.61 42.43 4.77 o 13 0 0 1018.52 1013.47 22.49 o 14 0 0 109.29 91.80 5.75 o 15 0 0 737.03 700.06 16.19 o 16 0 0 1459.70 1406.46 31.55 o 17 0 0 596.83 571.28 14.60 o 18 0 0 170.62 145.78 8.72 o 2 1 0 150.55 138.75 2.41 o 3 1 0 1542.36 1645.52 19.35 o 4 1 0 417.25 311.95 5.35 o 5 1 0 71.95 73.83 3.07 o 6 1 0 5649.60 5645.97 83.93 o 7 1 0 71.50 69.77 2.71 o 8 1 0 170.09 153.00 3.48 o 9 1 0 0.07 -0.79 1.48 o 10 1 0 1131.67 1097.89 16.12 o 11 1 0 528.51 514.63 8.42 o 12 1 0 78.09 80.72 4.19 o 13 1 0 153.89 142.82 4.72 o 14 1 0 696.41 682.22 11.15 o 15 1 0 72.49 78.09 3.38 o 16 1 0 83.41 76.79 3.69 o 17 1 0 2.42 1.31 1.57 o 18 1 0 246.74 244.19 8.05 o 0 2 0 9595.38 9532.52 222.50 o 1 2 0 103.44 95.66 3.55 o 2 2 0 4605.40 4475.18 62.22 o 3 2 0 17.37 26.93 2.86 o 4 2 0 3272.21 3067.28 38.64 o 5 2 0 597.80 562.01 8.00 o 6 2 0 3924.16 3881.87 53.29 o 7 2 0 3521.17 3456.72 48.07 o 8 2 0 1863.80 1959.50 25.56 o 9 2 0 592.51 588.36 9.20 o 10 2 0 281.24 256.57 7.52 o 11 2 0 141.02 123.77 4.06 o 12 2 0 352.08 336.10 5.57 o 13 2 0 350.28 346.06 7.23 o 14 2 0 320.32 322.61 6.40 o 15 2 0 100.85 106.35 4.19 o 16 2 0 138.81 120.40 7.48 o 17 2 0 78.42 82.22 5.85 o 18 2 0 4.07 -1.51 2.91 o 1 3 0 25.42 15.67 2.17 o 2 3 0 1331.52 1219.93 16.87 o 3 3 0 8.30 7.46 2.05 o 4 3 0 2877.38 2900.91 38.49 o 5 3 0 1432.63 1186.63 15.50 o 6 3 0 2514.88 2335.02 31.91 o 7 3 0 332.74 299.72 6.32 o 8 3 0 1939.33 1931.87 31.31 o 9 3 0 1066.28 971.00 14.34 o 10 3 0 1030.62 981.28 15.16 o 11 3 0 20.72 30.66 4.93 o 12 3 0 1018.96 994.87 12.67 o 13 3 0 365.90 361.32 7.86 o 14 3 0 0.02 -0.56 1.45 o 15 3 0 124.20 119.28 5.12 o 16 3 0 172.46 155.89 10.83 o 17 3 0 16.61 14.67 5.12 o 0 4 0 777.37 695.69 14.28 o 1 4 0 1681.26 1547.06 19.67 o 2 4 0 613.14 633.29 9.78 o 3 4 0 111.11 85.06 4.23 o 4 4 0 4.54 0.61 1.35 o 5 4 0 650.25 609.11 9.35 o 6 4 0 881.41 828.60 12.27 o 7 4 0 437.77 440.96 6.87 o 8 4 0 8.44 11.95 2.38 o 9 4 0 45.07 39.99 2.07 o 10 4 0 1476.93 1422.90 18.33 o 11 4 0 620.21 567.91 7.98 o 12 4 0 38.81 36.14 3.05 o 13 4 0 30.30 25.74 1.44 o 14 4 0 335.41 340.06 6.32 o 15 4 0 466.53 449.78 17.00 o 16 4 0 25.42 27.82 3.68 o 17 4 0 2.31 -1.45 3.54 o 1 5 0 1109.87 983.58 15.87 o 2 5 0 1807.09 1703.26 22.94 o 3 5 0 2202.10 2218.43 31.60 o 4 5 0 36.75 27.53 2.56 o 5 5 0 142.58 145.65 5.05 o 6 5 0 765.46 739.41 12.32 o 7 5 0 70.69 63.21 3.57 o 8 5 0 0.31 2.11 2.29 o 9 5 0 441.47 399.82 9.19 o 10 5 0 103.50 107.68 4.92 o 11 5 0 304.99 277.98 6.33 o 12 5 0 5.77 5.07 1.86 o 13 5 0 475.82 431.86 17.19 o 14 5 0 73.85 74.97 7.98 o 15 5 0 121.18 133.87 11.44 o 0 6 0 37.66 51.11 6.27 o 1 6 0 0.00 -0.55 1.80 o 2 6 0 11.88 4.18 2.52 o 3 6 0 1436.37 1344.19 18.90 o 4 6 0 127.59 129.62 5.22 o 5 6 0 93.90 113.84 5.38 o 6 6 0 369.45 357.09 6.62 o 7 6 0 2.52 4.27 1.80 o 8 6 0 1.13 1.72 1.83 o 9 6 0 256.16 230.18 6.52 o 10 6 0 30.19 32.86 3.07 o 11 6 0 148.78 148.35 4.74 o 12 6 0 105.88 97.42 3.38 o 13 6 0 165.98 138.94 12.87 o 14 6 0 53.90 44.01 10.06 o 1 7 0 175.16 206.95 7.59 o 2 7 0 1360.04 1381.79 21.45 o 3 7 0 19.75 19.78 3.04 o 4 7 0 0.76 1.98 2.75 o 5 7 0 1459.33 1384.39 22.32 o 6 7 0 721.73 712.02 12.75 o 7 7 0 75.92 71.54 4.60 o 8 7 0 243.19 237.12 7.40 o 9 7 0 180.72 193.60 5.19 o 10 7 0 143.70 149.68 5.97 o 11 7 0 6.80 5.37 3.00 o 12 7 0 357.74 370.51 20.63 o 0 8 0 126.15 127.21 7.58 o 1 8 0 24.99 25.27 3.71 o 2 8 0 5.01 8.52 3.83 o 3 8 0 351.99 337.80 9.53 o 4 8 0 39.86 42.03 3.91 o 5 8 0 156.99 172.25 7.29 o 6 8 0 0.08 1.75 2.73 o 7 8 0 98.47 110.59 5.71 o 8 8 0 19.02 28.51 4.39 o 9 8 0 73.32 68.35 6.70 o 1 9 0 139.85 157.03 7.32 o 2 9 0 164.90 176.53 8.10 o 3 9 0 6.33 4.10 2.76 o 4 9 0 2.84 1.32 2.11 o 5 9 0 1.13 3.49 2.78 o -18 1 1 9.36 5.93 4.65 o -17 1 1 404.36 328.52 10.64 o -16 1 1 70.33 68.06 3.27 o -15 1 1 181.64 171.88 5.80 o -14 1 1 79.62 110.64 6.39 o -13 1 1 1357.57 1227.96 18.81 o -12 1 1 124.47 126.90 4.20 o -11 1 1 168.46 212.63 4.46 o -10 1 1 692.63 554.46 8.39 o -9 1 1 2711.85 2302.13 28.59 o -8 1 1 1127.18 1226.22 14.50 o -7 1 1 655.03 575.22 6.92 o -6 1 1 1504.93 1710.49 21.56 o -5 1 1 1690.00 1752.31 26.35 o -4 1 1 2034.06 2359.19 39.38 o -3 1 1 432.40 389.05 8.92 o -2 1 1 8747.90 8618.17 148.15 o -1 1 1 2490.61 2225.56 26.93 o 0 1 1 4975.53 4897.66 78.95 o 1 1 1 1344.95 1455.59 19.31 o 2 1 1 8194.18 8094.46 152.25 o 3 1 1 311.21 319.07 6.00 o 4 1 1 5772.30 4994.77 72.12 o 5 1 1 2374.02 2236.50 30.04 o 6 1 1 3573.86 3131.20 40.60 o 7 1 1 223.66 286.60 6.72 o 8 1 1 2057.87 1838.14 28.65 o 9 1 1 1715.48 1704.67 29.40 o 10 1 1 278.49 300.63 7.66 o 11 1 1 473.29 386.89 13.75 o 12 1 1 120.43 121.80 4.11 o 13 1 1 624.28 736.01 11.24 o 14 1 1 217.69 209.29 4.81 o 15 1 1 198.87 203.29 6.57 o 16 1 1 92.19 94.75 4.89 o 17 1 1 166.66 191.97 5.43 o 18 1 1 11.20 17.00 2.58 o -18 2 1 35.98 44.90 5.15 o -17 2 1 44.99 40.54 5.72 o -16 2 1 58.13 41.13 6.27 o -15 2 1 186.06 160.57 4.09 o -14 2 1 84.45 106.25 4.51 o -13 2 1 85.29 87.40 5.74 o -12 2 1 457.09 429.64 6.30 o -11 2 1 117.47 110.64 2.39 o -10 2 1 313.25 286.13 3.91 o -9 2 1 888.04 771.57 11.15 o -8 2 1 355.78 379.84 11.85 o -7 2 1 472.14 525.64 10.87 o -6 2 1 2340.50 2260.09 39.69 o -5 2 1 17.41 19.97 1.43 o -4 2 1 534.51 675.38 8.30 o -3 2 1 1006.30 915.23 11.79 o -2 2 1 469.97 444.63 7.46 o -1 2 1 3130.33 2625.14 34.45 o 0 2 1 703.63 645.28 9.64 o 1 2 1 1320.81 1459.36 17.64 o 2 2 1 169.74 216.01 4.25 o 3 2 1 570.67 624.96 7.94 o 4 2 1 1530.47 1363.48 17.85 o 5 2 1 50.39 40.22 2.13 o 6 2 1 1810.27 1884.20 23.31 o 7 2 1 1142.56 964.28 12.75 o 8 2 1 664.65 587.39 9.02 o 9 2 1 377.52 426.36 7.46 o 10 2 1 220.00 226.59 6.66 o 11 2 1 72.94 82.76 4.76 o 12 2 1 465.90 441.85 9.74 o 13 2 1 156.23 139.44 6.46 o 14 2 1 206.45 180.62 5.38 o 15 2 1 127.62 137.90 4.24 o 16 2 1 21.94 24.16 2.84 o 17 2 1 47.99 48.78 3.52 o 18 2 1 96.53 92.51 5.63 o -17 3 1 16.72 20.55 4.51 o -16 3 1 186.64 193.83 13.15 o -15 3 1 222.65 287.49 11.63 o -14 3 1 549.92 508.99 14.92 o -13 3 1 123.88 138.36 7.36 o -12 3 1 544.77 716.36 13.89 o -11 3 1 142.05 184.48 6.55 o -10 3 1 90.10 126.98 6.77 o -9 3 1 211.34 190.84 7.11 o -8 3 1 962.21 805.81 16.84 o -7 3 1 173.65 214.91 4.14 o -6 3 1 3332.26 3070.89 40.68 o -5 3 1 1281.48 1176.12 14.67 o -4 3 1 1234.17 1215.11 16.94 o -3 3 1 1598.63 1308.61 16.65 o -2 3 1 537.14 479.49 7.96 o -1 3 1 1119.58 1076.46 14.21 o 0 3 1 0.10 0.23 1.85 o 1 3 1 423.40 550.56 8.17 o 2 3 1 573.91 546.07 7.82 o 3 3 1 616.57 678.32 8.36 o 4 3 1 1006.87 1022.93 12.28 o 5 3 1 635.07 664.79 10.76 o 6 3 1 1149.69 1498.91 22.10 o 7 3 1 265.49 267.02 8.34 o 8 3 1 331.81 396.35 5.84 o 9 3 1 106.73 115.15 3.31 o 10 3 1 260.86 247.76 4.62 o 11 3 1 412.34 381.89 8.77 o 12 3 1 1580.02 1431.86 24.20 o 13 3 1 168.90 177.07 6.72 o 14 3 1 370.04 395.35 9.98 o 15 3 1 643.75 581.39 15.54 o 16 3 1 158.35 156.57 5.52 o 17 3 1 28.39 33.24 4.04 o -16 4 1 322.92 296.37 11.18 o -15 4 1 180.16 164.40 8.70 o -14 4 1 185.08 197.38 9.75 o -13 4 1 174.10 184.51 10.03 o -12 4 1 27.75 29.62 3.81 o -11 4 1 515.06 452.13 12.76 o -10 4 1 579.04 488.87 15.64 o -9 4 1 119.99 135.85 4.92 o -8 4 1 2090.82 1892.99 25.06 o -7 4 1 2135.35 1988.87 26.49 o -6 4 1 257.89 261.77 5.81 o -5 4 1 599.51 522.81 8.94 o -4 4 1 1485.57 1416.87 17.80 o -3 4 1 436.20 446.22 7.32 o -2 4 1 298.26 253.29 5.46 o -1 4 1 1754.40 1505.56 20.09 o 0 4 1 5521.35 5406.25 80.52 o 1 4 1 1144.75 1121.88 16.67 o 2 4 1 188.87 179.24 4.96 o 3 4 1 563.79 510.86 7.64 o 4 4 1 916.11 1007.97 13.33 o 5 4 1 310.61 330.34 5.82 o 6 4 1 421.86 353.18 8.50 o 7 4 1 1478.04 1520.36 20.95 o 8 4 1 1309.04 1339.02 17.26 o 9 4 1 250.72 213.43 4.58 o 10 4 1 285.13 310.18 7.50 o 11 4 1 360.21 362.99 6.07 o 12 4 1 14.93 17.99 1.88 o 13 4 1 280.99 258.20 7.12 o 14 4 1 239.31 240.93 7.34 o 15 4 1 114.17 111.96 9.59 o 16 4 1 112.05 156.75 11.75 o -15 5 1 35.20 40.50 6.25 o -14 5 1 20.31 17.37 4.95 o -13 5 1 0.83 0.19 2.78 o -12 5 1 396.37 345.60 15.64 o -11 5 1 25.84 13.66 5.77 o -10 5 1 1217.07 1083.12 15.28 o -9 5 1 19.07 23.09 1.78 o -8 5 1 110.43 131.01 4.97 o -7 5 1 319.01 277.76 6.91 o -6 5 1 125.06 112.33 3.55 o -5 5 1 80.67 114.69 4.10 o -4 5 1 1260.37 1150.11 16.93 o -3 5 1 27.02 28.04 3.43 o -2 5 1 697.93 561.96 11.01 o -1 5 1 1383.17 1301.77 17.91 o 0 5 1 159.92 154.45 4.53 o 1 5 1 940.86 1005.66 15.38 o 2 5 1 251.95 274.27 5.51 o 3 5 1 21.23 25.33 2.81 o 4 5 1 557.86 649.47 11.23 o 5 5 1 210.81 222.85 5.49 o 6 5 1 88.80 93.39 3.71 o 7 5 1 125.08 146.62 3.38 o 8 5 1 288.22 247.31 4.85 o 9 5 1 54.99 44.18 2.96 o 10 5 1 531.39 599.85 24.19 o 11 5 1 15.83 11.38 2.46 o 12 5 1 137.88 166.07 7.68 o 13 5 1 1.43 3.04 1.53 o 14 5 1 17.31 24.46 2.94 o 15 5 1 84.79 84.87 28.97 o -14 6 1 193.64 194.32 12.10 o -13 6 1 95.94 127.47 8.61 o -12 6 1 196.91 211.24 12.53 o -11 6 1 75.95 61.40 6.69 o -10 6 1 131.55 133.80 4.68 o -9 6 1 112.83 135.09 5.31 o -8 6 1 330.60 331.75 7.62 o -7 6 1 450.12 436.75 8.72 o -6 6 1 455.59 576.27 11.16 o -5 6 1 246.36 284.21 8.76 o -4 6 1 966.64 954.04 15.69 o -3 6 1 215.14 244.58 6.38 o -2 6 1 467.73 428.86 9.08 o -1 6 1 197.82 188.76 5.90 o 0 6 1 1223.13 1134.92 17.76 o 1 6 1 85.54 106.82 4.58 o 2 6 1 348.51 362.89 7.49 o 3 6 1 450.21 394.54 10.18 o 4 6 1 1141.34 1096.26 16.31 o 5 6 1 668.59 578.59 10.07 o 6 6 1 1318.75 1153.56 16.90 o 7 6 1 527.70 500.22 9.53 o 8 6 1 344.04 335.47 6.27 o 9 6 1 308.60 256.25 10.89 o 10 6 1 199.64 182.26 5.94 o 11 6 1 77.84 71.84 5.88 o 12 6 1 211.36 223.67 6.97 o 13 6 1 201.73 181.80 7.56 o 14 6 1 245.24 252.68 18.85 o -12 7 1 0.24 -6.60 6.68 o -11 7 1 21.88 22.66 7.93 o -10 7 1 96.32 80.55 11.08 o -9 7 1 37.46 42.69 4.30 o -8 7 1 60.34 65.19 3.76 o -7 7 1 24.26 20.16 4.44 o -6 7 1 56.05 58.19 4.13 o -5 7 1 33.54 37.46 3.79 o -4 7 1 134.52 119.80 6.99 o -3 7 1 124.30 109.19 4.98 o -2 7 1 625.73 597.95 13.58 o -1 7 1 98.39 117.09 5.52 o 0 7 1 0.00 -1.50 2.10 o 1 7 1 172.88 170.68 5.81 o 2 7 1 273.07 338.84 9.20 o 3 7 1 56.16 72.38 6.06 o 4 7 1 65.43 81.45 3.99 o 5 7 1 74.83 74.09 4.78 o 6 7 1 54.98 54.11 4.35 o 7 7 1 17.69 16.98 2.17 o 8 7 1 96.44 82.60 4.44 o 9 7 1 18.46 20.04 2.48 o 10 7 1 35.89 43.58 7.20 o 11 7 1 33.65 50.22 7.07 o 12 7 1 0.40 -0.47 5.32 o -9 8 1 21.98 18.58 2.83 o -8 8 1 365.07 395.31 11.68 o -7 8 1 106.95 99.65 5.66 o -6 8 1 25.54 30.60 3.71 o -5 8 1 0.22 2.41 2.26 o -4 8 1 236.17 235.18 7.02 o -3 8 1 315.82 300.26 9.86 o -2 8 1 253.37 270.58 7.40 o -1 8 1 245.58 230.62 6.86 o 0 8 1 521.75 540.04 12.94 o 1 8 1 97.94 128.60 6.75 o 2 8 1 424.10 404.44 9.38 o 3 8 1 197.42 220.31 7.48 o 4 8 1 170.88 178.68 5.77 o 5 8 1 0.21 1.72 2.03 o 6 8 1 49.05 46.24 4.99 o 7 8 1 88.05 88.69 5.05 o 8 8 1 333.24 368.40 12.59 o 9 8 1 59.72 63.98 5.23 o -5 9 1 47.73 60.39 5.03 o -4 9 1 12.94 14.96 4.31 o -3 9 1 58.50 69.10 7.32 o -2 9 1 83.78 116.29 7.58 o -1 9 1 95.34 115.51 6.49 o 0 9 1 4.33 3.00 3.41 o 1 9 1 177.77 155.16 6.39 o 2 9 1 189.57 186.34 7.09 o 3 9 1 26.08 27.81 3.68 o 4 9 1 17.23 20.57 3.74 o 5 9 1 118.29 103.88 7.10 o -18 0 2 28.88 23.24 9.46 o -17 0 2 170.28 191.04 14.40 o -16 0 2 245.59 219.93 12.53 o -15 0 2 547.58 493.29 10.82 o -14 0 2 593.75 545.90 12.24 o -13 0 2 127.64 138.93 12.43 o -12 0 2 2557.38 2176.88 53.28 o -11 0 2 1550.67 1319.25 34.88 o -10 0 2 54.48 62.58 8.09 o -9 0 2 1602.04 1457.72 23.40 o -8 0 2 246.19 172.62 5.96 o -7 0 2 4827.98 4967.15 97.41 o -6 0 2 9125.14 10280.56 292.98 o -5 0 2 392.62 382.66 7.15 o -4 0 2 2626.71 3321.72 71.17 o -3 0 2 2987.99 3729.73 79.39 o -2 0 2 11425.22 10408.28 295.26 o -1 0 2 1440.09 1204.21 25.96 o 0 0 2 1115.40 1086.69 25.17 o 1 0 2 659.06 695.64 16.57 o 2 0 2 5620.18 6348.45 182.29 o 3 0 2 8308.87 7628.60 217.60 o 4 0 2 7521.65 6906.03 149.32 o 5 0 2 202.12 256.10 7.81 o 6 0 2 11959.72 12043.87 391.30 o 7 0 2 5745.71 5626.58 116.47 o 8 0 2 109.17 107.63 5.14 o 9 0 2 728.12 850.15 15.91 o 10 0 2 84.84 65.11 4.86 o 11 0 2 671.96 798.48 28.98 o 12 0 2 1098.95 1311.82 28.89 o 13 0 2 280.86 245.35 6.96 o 14 0 2 302.59 352.23 12.65 o 15 0 2 235.69 278.70 11.23 o 16 0 2 256.26 275.59 11.84 o 17 0 2 410.40 404.86 12.86 o 18 0 2 31.95 31.49 4.40 o -18 1 2 49.45 33.35 4.50 o -17 1 2 115.84 99.92 8.76 o -16 1 2 31.60 34.90 3.62 o -15 1 2 565.41 530.36 11.26 o -14 1 2 649.07 573.65 9.22 o -13 1 2 121.24 111.87 3.09 o -12 1 2 425.48 360.54 6.23 o -11 1 2 339.34 302.21 4.82 o -10 1 2 809.74 687.81 8.63 o -9 1 2 10.32 7.51 1.18 o -8 1 2 29.95 29.15 2.66 o -7 1 2 1664.72 1621.26 22.88 o -6 1 2 251.30 328.74 5.17 o -5 1 2 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o -6 0 10 135.65 124.76 17.28 o -5 0 10 326.73 451.01 21.05 o -4 0 10 110.00 130.32 12.89 o -3 0 10 77.25 37.06 7.61 o -2 0 10 326.26 476.78 23.66 o -1 0 10 57.08 80.39 9.89 o 0 0 10 5.68 2.45 5.53 o 1 0 10 22.75 10.09 6.79 o 2 0 10 176.41 118.47 16.97 o 3 0 10 182.79 277.51 17.97 o 4 0 10 83.21 41.82 21.61 o 5 0 10 192.56 171.55 16.52 o 6 0 10 167.86 227.19 18.72 o 7 0 10 175.56 -1.83 7.74 o 8 0 10 26.38 9.13 11.71 o 9 0 10 1.51 6.69 5.17 o -9 1 10 12.18 5.87 4.20 o -8 1 10 45.13 52.53 7.92 o -7 1 10 40.34 35.07 5.13 o -6 1 10 38.90 75.44 6.28 o -5 1 10 181.97 293.62 10.76 o -4 1 10 34.84 0.26 3.52 o -3 1 10 124.58 203.55 9.09 o -2 1 10 38.99 39.52 6.30 o -1 1 10 130.22 212.06 11.43 o 0 1 10 271.10 313.05 14.99 o 1 1 10 47.96 5.71 4.98 o 2 1 10 13.94 1.76 4.89 o 3 1 10 52.56 9.75 5.27 o 4 1 10 100.15 179.90 12.28 o 5 1 10 113.70 77.90 24.08 o 6 1 10 13.23 -2.00 4.72 o 7 1 10 39.59 8.28 6.79 o 8 1 10 40.32 37.26 23.34 o 9 1 10 22.40 34.54 9.49 o -9 2 10 213.04 296.08 10.63 o -8 2 10 220.91 403.65 14.92 o -7 2 10 52.93 6.03 3.45 o -6 2 10 142.59 146.58 7.34 o -5 2 10 59.34 99.01 6.97 o -4 2 10 152.71 270.24 11.13 o -3 2 10 209.32 292.93 13.47 o -2 2 10 172.60 190.15 10.51 o -1 2 10 350.52 669.78 20.04 o 0 2 10 148.86 196.48 12.48 o 1 2 10 122.11 1.01 4.84 o 2 2 10 224.41 291.46 15.57 o 3 2 10 154.80 156.97 16.12 o 4 2 10 53.88 3.84 6.18 o 5 2 10 29.75 9.41 7.31 o 6 2 10 177.94 281.80 18.69 o 7 2 10 144.87 268.78 16.44 o 8 2 10 75.90 4.76 6.64 o -7 3 10 111.41 127.88 8.38 o -6 3 10 22.47 16.10 4.41 o -5 3 10 15.02 13.82 4.77 o -4 3 10 37.35 69.21 10.49 o -3 3 10 32.17 32.90 13.85 o -2 3 10 34.92 61.66 13.22 o -1 3 10 125.78 97.73 9.73 o 0 3 10 5.88 6.45 5.95 o 1 3 10 213.27 359.31 22.25 o 2 3 10 20.81 8.08 6.02 o 3 3 10 27.94 17.84 7.04 o 4 3 10 14.43 6.18 6.99 o 5 3 10 12.43 7.60 7.13 o 6 3 10 21.40 17.11 7.57 o 7 3 10 123.15 146.54 18.22 o -5 4 10 137.01 220.83 24.42 o -4 4 10 6.08 5.89 5.01 o -3 4 10 57.76 52.44 11.36 o -2 4 10 22.56 3.48 3.66 o -1 4 10 50.72 39.21 13.46 o 0 4 10 7.40 6.97 4.85 o 1 4 10 56.33 43.52 12.31 o 2 4 10 56.00 94.98 7.26 o 3 4 10 81.58 136.39 7.60 o 4 4 10 3.85 -2.66 4.42 o 5 4 10 60.97 20.80 9.36 o -6 1 11 44.21 73.78 7.00 o -5 1 11 9.65 0.54 3.50 o -4 1 11 184.21 282.18 14.39 o -3 1 11 178.79 295.37 14.31 o -2 1 11 0.78 -3.18 5.09 o -1 1 11 113.60 72.80 7.67 o 0 1 11 175.72 239.02 12.97 o 1 1 11 238.64 447.66 17.41 o 2 1 11 1.62 -3.40 5.34 o 3 1 11 117.33 110.14 26.98 o 4 1 11 147.72 172.07 13.25 o 5 1 11 27.14 17.08 6.89 o -5 2 11 47.59 49.46 10.15 o -4 2 11 51.58 83.91 9.86 o -3 2 11 34.16 -1.17 3.79 o -2 2 11 1.41 -1.76 4.99 o -1 2 11 90.21 213.97 11.19 o 0 2 11 5.98 3.42 5.96 o 1 2 11 31.92 4.38 7.32 o 2 2 11 1.10 4.10 5.73 o 3 2 11 98.18 225.96 16.64 o 4 2 11 55.74 35.94 13.65 o -2 3 11 3.77 8.26 5.57 o -1 3 11 2.55 0.46 5.21 o 0 3 11 140.49 210.97 13.86 o 1 3 11 7.38 14.44 8.84 o