#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205016.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205016_Fobs loop_ _publ_author_name 'Ma, Zhi-Jie' 'Tao, Jun' 'Huang, Rong-Bin' 'Zheng, Lan-Sun' _publ_section_title ; Hexaaquamanganese(II) 5,5'-(1,4-phenylene)ditetrazolate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m361 _journal_page_last m363 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.149 _cell_angle_gamma 90.000 _cell_length_a 5.0587 _cell_length_b 13.4343 _cell_length_c 11.4989 _exptl_crystal_F_000 386.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file bv6009Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 246.33 221.79 4.69 o 6 0 0 72.98 76.63 3.29 o 1 1 0 1726.87 1800.12 17.20 o 2 1 0 772.97 810.55 8.09 o 3 1 0 855.52 816.74 8.39 o 4 1 0 226.91 219.50 4.55 o 5 1 0 424.52 414.25 6.43 o 6 1 0 0.42 1.62 0.61 o 0 2 0 5610.09 4680.11 84.51 o 1 2 0 56.25 60.10 1.02 o 2 2 0 96.18 82.61 1.19 o 3 2 0 137.54 141.19 1.96 o 4 2 0 707.85 670.58 9.11 o 5 2 0 0.11 0.89 0.49 o 6 2 0 173.84 173.69 3.75 o 1 3 0 3407.84 3412.57 32.40 o 2 3 0 737.31 836.60 8.38 o 3 3 0 254.52 229.88 2.82 o 4 3 0 0.08 0.59 0.50 o 5 3 0 180.75 176.05 3.08 o 6 3 0 28.92 25.87 1.39 o 1 4 0 814.79 849.01 8.50 o 2 4 0 1560.70 1547.17 16.06 o 4 4 0 257.39 244.23 3.64 o 5 4 0 38.64 36.33 1.28 o 6 4 0 76.56 78.77 2.40 o 1 5 0 950.29 1006.26 9.91 o 2 5 0 2.32 5.66 0.51 o 3 5 0 221.41 183.16 3.40 o 4 5 0 22.95 24.03 0.97 o 5 5 0 95.21 96.27 2.17 o 6 5 0 10.84 16.02 1.53 o 1 6 0 94.17 104.04 1.43 o 2 6 0 732.18 720.41 8.14 o 3 6 0 148.79 147.25 2.42 o 4 6 0 617.68 597.17 7.46 o 5 6 0 60.70 59.20 1.67 o 6 6 0 46.54 48.92 1.90 o 1 7 0 1579.29 1565.21 15.32 o 2 7 0 938.45 928.32 14.63 o 3 7 0 391.86 373.95 5.73 o 4 7 0 117.09 107.73 2.19 o 5 7 0 47.67 48.68 1.68 o 0 8 0 1028.39 980.58 16.48 o 1 8 0 47.82 56.29 1.04 o 2 8 0 1503.19 1487.24 19.18 o 3 8 0 6.37 5.08 0.56 o 4 8 0 2.02 2.35 0.48 o 5 8 0 5.36 7.95 0.75 o 1 9 0 101.46 78.14 3.07 o 2 9 0 86.49 81.88 1.65 o 3 9 0 600.00 586.65 7.32 o 4 9 0 2.36 2.22 0.50 o 5 9 0 148.32 148.30 3.49 o 0 10 0 478.15 479.41 9.24 o 1 10 0 18.49 20.71 1.47 o 2 10 0 1145.44 1115.58 14.09 o 3 10 0 149.73 144.23 2.92 o 4 10 0 83.88 80.58 2.22 o 5 10 0 9.44 12.51 1.33 o 1 11 0 454.34 444.20 7.36 o 2 11 0 43.86 38.38 1.59 o 3 11 0 462.58 450.77 7.83 o 4 11 0 33.20 34.22 1.72 o 0 12 0 226.12 221.55 5.27 o 1 12 0 267.70 245.06 4.78 o 2 12 0 216.74 213.34 4.46 o 3 12 0 38.23 37.32 1.72 o 4 12 0 136.54 131.73 3.82 o 1 13 0 86.81 84.98 2.53 o 2 13 0 236.43 217.89 4.67 o 3 13 0 155.73 148.29 3.82 o 4 13 0 9.99 12.94 1.32 o 0 14 0 0.78 2.37 0.78 o 1 14 0 186.84 174.31 6.52 o 2 14 0 223.55 214.48 4.74 o 3 14 0 8.09 7.76 1.08 o 1 15 0 72.85 79.69 2.60 o 2 15 0 8.43 11.69 1.22 o 3 15 0 26.28 28.38 1.79 o 0 16 0 109.80 111.96 5.80 o 1 16 0 13.21 16.87 1.38 o 2 16 0 0.46 1.44 0.79 o -5 0 1 8.74 7.23 1.11 o -3 0 1 319.32 329.01 5.34 o -1 0 1 5375.41 5792.48 107.67 o 1 0 1 510.65 514.49 12.29 o 3 0 1 2323.46 2274.02 31.20 o 5 0 1 152.44 147.93 4.57 o -6 1 1 107.00 105.97 3.56 o -5 1 1 3.60 3.02 0.61 o -4 1 1 985.10 988.69 11.63 o -3 1 1 22.57 21.51 0.65 o -1 1 1 1904.85 2077.11 19.82 o 0 1 1 1137.42 1108.15 11.89 o 1 1 1 1047.52 1088.03 11.45 o 2 1 1 988.18 1012.32 10.02 o 3 1 1 93.98 105.14 1.59 o 4 1 1 174.92 172.42 2.77 o 5 1 1 176.12 164.26 3.36 o 6 1 1 157.52 150.18 3.46 o -6 2 1 24.52 23.61 1.39 o -5 2 1 265.71 255.42 3.95 o -4 2 1 319.08 308.95 4.27 o -3 2 1 1864.59 1984.37 19.38 o -2 2 1 960.01 1014.85 10.03 o 0 2 1 2840.98 2789.80 49.95 o 1 2 1 441.20 440.19 5.42 o 2 2 1 493.60 551.46 5.68 o 3 2 1 1231.51 1244.11 12.45 o 4 2 1 2.72 2.76 0.46 o 5 2 1 10.81 10.54 0.98 o 6 2 1 0.96 1.78 0.60 o -6 3 1 10.79 14.11 1.15 o -5 3 1 38.82 36.22 1.26 o -4 3 1 388.19 379.16 5.03 o -3 3 1 183.03 169.54 2.27 o -2 3 1 2098.83 2135.04 20.57 o -1 3 1 48.05 43.23 0.69 o 0 3 1 1020.08 1053.97 10.23 o 1 3 1 51.04 49.35 0.87 o 2 3 1 3736.46 3974.08 45.97 o 3 3 1 274.53 285.26 4.22 o 4 3 1 554.82 522.17 6.58 o 5 3 1 44.49 43.61 1.59 o 6 3 1 18.56 20.61 1.38 o -6 4 1 0.10 1.24 0.53 o -5 4 1 124.81 129.83 2.56 o -4 4 1 302.05 298.50 4.21 o -3 4 1 1101.37 1115.98 17.55 o -2 4 1 382.15 370.83 4.03 o -1 4 1 3520.32 3479.87 33.09 o 0 4 1 1250.51 1247.10 12.08 o 1 4 1 1213.75 1245.55 12.11 o 2 4 1 714.53 785.03 8.79 o 3 4 1 672.00 670.52 12.30 o 4 4 1 37.49 36.64 1.15 o 5 4 1 650.16 636.02 8.10 o 6 4 1 34.74 34.08 1.58 o -6 5 1 22.89 26.86 1.56 o -5 5 1 15.46 18.10 1.00 o -4 5 1 515.73 503.86 7.02 o -3 5 1 1.17 3.05 0.41 o -2 5 1 4131.81 4285.73 40.84 o -1 5 1 0.24 0.35 0.16 o 0 5 1 79.14 80.91 1.28 o 1 5 1 931.09 997.70 9.83 o 2 5 1 1561.99 1544.54 16.65 o 3 5 1 46.65 39.25 1.20 o 4 5 1 312.59 289.81 4.20 o 5 5 1 40.39 35.93 1.28 o 6 5 1 49.64 52.50 1.97 o -6 6 1 1.83 3.30 0.63 o -5 6 1 507.80 498.10 6.72 o -4 6 1 213.84 202.93 3.26 o -3 6 1 114.55 114.55 3.47 o -2 6 1 15.75 14.99 0.51 o -1 6 1 922.57 977.93 9.72 o 0 6 1 477.69 538.73 5.56 o 1 6 1 1032.80 971.04 12.39 o 2 6 1 469.72 496.00 5.93 o 4 6 1 88.70 79.76 2.00 o 5 6 1 323.26 312.80 4.74 o -5 7 1 5.59 5.62 0.67 o -4 7 1 80.77 81.30 1.84 o -3 7 1 0.39 0.32 0.37 o -2 7 1 1314.26 1364.06 20.29 o -1 7 1 662.43 751.23 7.67 o 0 7 1 2246.99 2307.96 22.27 o 1 7 1 1.28 1.68 0.31 o 2 7 1 505.08 446.57 8.62 o 3 7 1 13.48 13.23 0.74 o 4 7 1 248.24 239.95 3.73 o 5 7 1 104.79 101.32 2.31 o -5 8 1 23.82 26.27 1.29 o -4 8 1 165.60 155.52 4.64 o -3 8 1 181.06 172.68 2.81 o -2 8 1 170.62 174.83 4.26 o -1 8 1 502.22 515.87 5.56 o 0 8 1 295.36 317.77 3.61 o 1 8 1 2447.56 2613.64 25.26 o 2 8 1 0.00 0.13 0.27 o 3 8 1 14.84 15.26 0.88 o 4 8 1 39.16 36.72 1.24 o 5 8 1 209.68 209.77 4.10 o -5 9 1 6.21 9.22 0.91 o -4 9 1 110.41 105.52 2.55 o -3 9 1 45.23 43.99 1.77 o -2 9 1 75.28 67.24 1.93 o -1 9 1 31.48 33.69 1.15 o 0 9 1 813.42 823.84 9.30 o 1 9 1 53.71 57.45 1.59 o 2 9 1 14.22 13.69 0.78 o 3 9 1 34.84 36.02 1.33 o 4 9 1 124.05 111.87 2.64 o 5 9 1 0.01 1.50 0.48 o -5 10 1 67.70 71.95 2.25 o -4 10 1 21.66 24.40 1.24 o -3 10 1 187.45 171.96 3.38 o -1 10 1 70.98 67.45 1.60 o 0 10 1 4.98 7.75 0.79 o 1 10 1 892.07 890.82 17.21 o 2 10 1 166.31 149.65 3.63 o 3 10 1 19.96 19.88 1.08 o 4 10 1 2.02 3.13 0.73 o 5 10 1 67.76 71.73 2.64 o -4 11 1 1.29 2.98 0.95 o -3 11 1 23.50 22.30 1.14 o -2 11 1 25.11 28.78 1.15 o -1 11 1 54.72 49.07 1.45 o 0 11 1 679.69 632.97 9.78 o 1 11 1 56.11 46.12 1.70 o 2 11 1 265.22 238.94 4.75 o 3 11 1 1.95 1.67 0.66 o 4 11 1 149.24 157.79 3.97 o -4 12 1 86.10 85.99 2.82 o -3 12 1 162.67 159.09 3.84 o -2 12 1 3.00 3.83 0.76 o -1 12 1 819.62 761.80 11.67 o 0 12 1 17.72 19.17 0.94 o 1 12 1 15.13 15.09 1.13 o 2 12 1 124.76 121.67 3.14 o 3 12 1 2.20 3.21 0.77 o 4 12 1 169.07 175.75 4.37 o -4 13 1 61.11 65.45 2.52 o -3 13 1 83.12 78.94 2.61 o -2 13 1 193.40 184.10 4.16 o -1 13 1 7.79 11.86 1.24 o 0 13 1 90.82 82.18 2.03 o 1 13 1 32.26 29.55 1.48 o 2 13 1 255.83 233.48 5.67 o 3 13 1 0.60 1.55 0.68 o 4 13 1 109.82 120.49 4.87 o -3 14 1 69.83 76.19 2.67 o -2 14 1 65.49 63.87 2.31 o -1 14 1 232.71 224.65 4.76 o 0 14 1 71.73 71.43 2.28 o 1 14 1 328.85 307.81 5.97 o 2 14 1 2.95 4.13 0.85 o 3 14 1 157.42 159.06 4.10 o -3 15 1 6.61 7.47 1.11 o -2 15 1 254.87 256.56 5.47 o -1 15 1 3.35 3.87 1.05 o 0 15 1 178.26 177.54 5.21 o 1 15 1 0.35 0.46 0.62 o 2 15 1 105.25 118.77 3.40 o 3 15 1 0.15 0.93 0.75 o -2 16 1 5.83 11.10 1.23 o -1 16 1 192.81 191.27 4.68 o 0 16 1 3.08 3.63 1.11 o 1 16 1 73.48 75.61 2.64 o 2 16 1 42.78 45.94 2.11 o 0 17 1 124.92 112.89 4.27 o -6 0 2 298.19 303.95 7.71 o -4 0 2 163.04 151.35 3.20 o -2 0 2 924.72 903.22 12.69 o 0 0 2 3819.21 3511.80 81.19 o 2 0 2 2409.94 2504.94 33.99 o 4 0 2 950.34 976.70 17.96 o 6 0 2 351.92 327.43 8.24 o -6 1 2 105.91 104.96 2.78 o -5 1 2 342.66 326.81 4.74 o -4 1 2 10.54 8.84 1.08 o -3 1 2 172.44 186.76 2.44 o -2 1 2 20.70 24.25 0.58 o -1 1 2 8965.11 9273.88 91.80 o 0 1 2 3442.94 3635.32 41.73 o 1 1 2 1821.73 1867.12 17.88 o 2 1 2 51.02 54.83 1.33 o 3 1 2 1473.99 1420.59 14.08 o 4 1 2 80.68 77.25 1.66 o 5 1 2 88.09 87.57 2.29 o 6 1 2 9.51 11.78 1.10 o -6 2 2 182.73 180.01 3.84 o -5 2 2 3.69 3.88 0.61 o -4 2 2 606.69 590.61 7.08 o -3 2 2 46.27 49.80 1.28 o -2 2 2 793.75 823.17 8.24 o -1 2 2 4340.08 4555.07 47.63 o 0 2 2 5753.63 5312.06 86.77 o 1 2 2 2249.92 2212.60 21.23 o 3 2 2 647.67 648.20 15.50 o 4 2 2 231.66 219.55 3.33 o 5 2 2 58.60 54.36 1.80 o 6 2 2 122.86 121.97 3.07 o -6 3 2 128.87 134.02 3.73 o -5 3 2 161.35 158.35 2.88 o -4 3 2 469.36 451.51 6.77 o -3 3 2 8.40 5.14 0.60 o -2 3 2 1235.50 1305.15 12.81 o -1 3 2 5409.37 5479.69 56.31 o 0 3 2 63.59 73.72 1.08 o 1 3 2 57.18 66.14 1.08 o 2 3 2 7.56 8.07 0.50 o 3 3 2 1006.23 827.87 20.54 o 4 3 2 0.04 0.20 0.35 o 5 3 2 346.69 327.36 5.48 o 6 3 2 1.00 1.91 0.66 o -6 4 2 0.77 2.42 0.66 o -5 4 2 0.26 0.47 0.41 o -4 4 2 182.61 166.33 2.76 o -3 4 2 18.19 23.40 0.83 o -2 4 2 3002.61 3178.39 30.41 o -1 4 2 58.86 57.17 1.33 o 0 4 2 141.88 148.40 1.93 o 1 4 2 557.21 567.57 6.28 o 2 4 2 152.80 106.92 1.76 o 3 4 2 523.84 520.03 6.84 o 4 4 2 602.08 563.16 7.05 o 5 4 2 17.20 20.86 1.24 o 6 4 2 60.24 61.29 2.12 o -6 5 2 20.18 21.84 1.22 o -5 5 2 209.64 213.75 3.83 o -4 5 2 9.01 9.44 0.91 o -3 5 2 500.69 488.21 6.79 o -2 5 2 0.74 1.40 0.35 o -1 5 2 1283.99 1274.36 13.52 o 0 5 2 1308.77 1458.25 15.43 o 2 5 2 408.27 477.73 5.72 o 3 5 2 1.35 2.36 0.85 o 4 5 2 0.23 -0.05 0.33 o 5 5 2 431.40 432.80 6.02 o -6 6 2 76.42 81.40 2.55 o -5 6 2 0.19 0.54 0.45 o -4 6 2 27.03 25.29 1.01 o -3 6 2 1.67 1.69 0.59 o -2 6 2 1093.92 1170.66 11.70 o -1 6 2 19.55 20.56 0.54 o 0 6 2 301.64 266.47 3.34 o 1 6 2 189.92 205.68 2.44 o 2 6 2 1715.82 1727.29 18.69 o 3 6 2 79.43 81.89 1.89 o 4 6 2 15.78 21.63 1.14 o 5 6 2 2.49 4.44 0.61 o -5 7 2 34.46 35.54 1.30 o -4 7 2 9.05 9.85 0.76 o -3 7 2 1039.91 1053.29 11.98 o -2 7 2 60.28 61.06 2.04 o -1 7 2 2.40 2.36 0.28 o 0 7 2 86.79 107.79 1.50 o 1 7 2 1432.63 1417.60 13.97 o 2 7 2 99.56 96.51 1.98 o 3 7 2 217.58 203.73 3.15 o 4 7 2 269.52 247.61 3.87 o 5 7 2 161.96 164.89 3.13 o -5 8 2 7.34 8.90 0.91 o -4 8 2 272.08 271.68 4.63 o -3 8 2 146.19 151.63 2.92 o -2 8 2 69.05 54.43 1.86 o -1 8 2 166.24 162.69 2.41 o 0 8 2 1192.44 1205.11 13.12 o 1 8 2 484.21 535.55 6.35 o 2 8 2 557.67 529.71 6.49 o 3 8 2 232.21 220.14 3.40 o 4 8 2 389.87 402.50 5.61 o 5 8 2 6.97 9.39 0.82 o -5 9 2 50.78 54.07 1.90 o -4 9 2 14.02 15.92 1.10 o -3 9 2 1694.37 1666.45 20.54 o -2 9 2 33.27 33.51 0.98 o -1 9 2 2.72 2.64 0.56 o 0 9 2 9.77 10.59 0.85 o 1 9 2 1574.51 1581.60 22.40 o 2 9 2 1.19 1.22 0.44 o 3 9 2 189.53 185.73 3.94 o 4 9 2 1.07 1.42 0.48 o 5 9 2 0.67 1.88 0.54 o -5 10 2 13.31 17.16 1.90 o -4 10 2 283.80 283.47 4.92 o -3 10 2 4.68 4.05 0.74 o -2 10 2 35.13 35.53 1.25 o -1 10 2 0.01 -0.02 0.30 o 0 10 2 1101.27 1083.00 14.53 o 1 10 2 619.38 619.26 12.03 o 2 10 2 649.21 636.19 12.26 o 3 10 2 93.86 95.44 2.34 o 4 10 2 155.25 155.25 3.34 o 5 10 2 1.36 2.90 0.71 o -4 11 2 1.18 2.76 0.60 o -3 11 2 224.41 232.84 4.20 o -2 11 2 34.54 34.11 1.27 o -1 11 2 36.12 32.57 1.50 o 0 11 2 181.49 166.10 3.41 o 1 11 2 1756.86 1719.47 27.34 o 2 11 2 299.10 275.41 4.77 o 3 11 2 511.56 522.91 7.71 o 4 11 2 11.13 12.69 1.22 o -4 12 2 275.83 283.56 5.07 o -3 12 2 0.00 0.30 0.46 o -2 12 2 905.47 877.25 16.33 o -1 12 2 5.32 5.65 0.62 o 0 12 2 1.05 1.17 0.51 o 1 12 2 52.10 50.99 2.66 o 2 12 2 107.44 103.73 2.89 o 3 12 2 41.26 41.36 1.83 o 4 12 2 41.73 35.21 2.04 o -4 13 2 34.18 32.86 1.76 o -3 13 2 24.60 28.44 1.55 o -2 13 2 35.83 37.76 1.68 o -1 13 2 183.09 175.55 5.26 o 0 13 2 85.83 68.44 2.20 o 1 13 2 268.40 261.81 5.22 o 2 13 2 4.90 4.70 0.83 o 3 13 2 87.66 89.42 2.87 o 4 13 2 3.95 4.00 1.21 o -3 14 2 6.79 10.08 1.10 o -2 14 2 22.41 25.42 1.49 o -1 14 2 45.57 45.77 1.89 o 0 14 2 105.54 106.44 2.93 o 1 14 2 9.75 9.83 1.08 o 2 14 2 235.36 228.63 6.67 o 3 14 2 0.62 0.42 0.71 o -3 15 2 5.12 3.95 0.86 o -2 15 2 34.52 34.14 2.10 o -1 15 2 198.89 194.18 4.93 o 0 15 2 8.11 9.02 1.03 o 1 15 2 1.06 1.78 0.68 o 2 15 2 3.28 4.91 0.92 o -2 16 2 29.71 31.69 1.79 o -1 16 2 3.75 5.62 1.21 o 0 16 2 51.00 55.36 3.44 o 1 16 2 9.88 15.98 1.44 o 2 16 2 43.53 42.19 2.07 o 0 17 2 8.41 8.26 2.06 o -5 0 3 374.12 355.54 10.71 o -3 0 3 1243.00 1285.27 18.16 o 1 0 3 3717.29 3778.19 50.75 o 3 0 3 2430.79 1935.59 48.85 o 5 0 3 130.48 119.53 3.95 o -6 1 3 51.31 55.72 1.97 o -5 1 3 71.12 68.35 1.74 o -4 1 3 529.80 523.55 6.49 o -3 1 3 76.20 75.88 1.33 o -2 1 3 1415.23 1405.20 13.73 o -1 1 3 3543.38 3676.04 34.95 o 0 1 3 1292.33 1325.29 12.77 o 1 1 3 1704.75 1705.35 16.39 o 2 1 3 1858.73 1958.75 18.95 o 4 1 3 55.32 53.27 1.61 o 5 1 3 10.18 11.65 0.97 o 6 1 3 78.84 80.25 2.46 o -6 2 3 19.06 23.44 1.31 o -5 2 3 320.93 318.63 4.65 o -4 2 3 389.05 369.34 5.12 o -3 2 3 478.71 493.34 5.39 o -2 2 3 112.73 112.83 1.55 o -1 2 3 1852.25 1914.89 20.13 o 0 2 3 154.27 172.20 2.40 o 1 2 3 2277.79 2270.36 23.60 o 2 2 3 33.02 32.96 1.04 o 3 2 3 244.94 234.85 3.83 o 4 2 3 17.82 14.64 0.81 o 5 2 3 16.76 19.14 1.18 o 6 2 3 0.03 0.09 0.53 o -6 3 3 78.86 85.11 3.31 o -5 3 3 2.17 2.50 0.64 o -4 3 3 244.56 245.90 4.32 o -3 3 3 14.07 18.38 0.72 o -2 3 3 839.84 828.78 8.35 o -1 3 3 1084.08 1153.80 11.26 o 0 3 3 97.53 100.13 1.24 o 1 3 3 3700.41 3867.26 52.16 o 2 3 3 3655.18 3738.95 39.24 o 3 3 3 469.45 459.11 6.32 o 4 3 3 217.20 200.47 3.18 o 5 3 3 60.60 55.95 1.85 o 6 3 3 238.61 237.05 5.58 o -6 4 3 2.57 4.59 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