#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205023.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205023_Fobs loop_ _publ_author_name 'Wang, Yue' 'Okabe, Nobuo' _publ_section_title ; Diaquabis(\m-4-hydroxybenzenecarboxylato-\k^2^O,O')disilver(I)(Ag---Ag) tetrahydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m382 _journal_page_last m384 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 115.532 _cell_angle_beta 107.508 _cell_angle_gamma 95.602 _cell_length_a 6.6350 _cell_length_b 9.2391 _cell_length_c 9.3592 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file cf6400Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wy145' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4515.06 4428.48 9.84 o 2 0 0 4870.15 4869.22 14.52 o 3 0 0 1102.84 1103.77 6.18 o 4 0 0 1697.66 1742.60 10.05 o 5 0 0 105.88 104.23 2.31 o 6 0 0 23.96 30.00 1.84 o 7 0 0 99.70 105.74 3.18 o -8 1 0 30.28 31.69 5.43 o -7 1 0 85.86 90.69 3.14 o -6 1 0 103.67 105.68 2.29 o -5 1 0 408.59 413.58 4.03 o -4 1 0 3309.60 3514.66 15.26 o -3 1 0 2284.57 2342.13 16.53 o -2 1 0 262.86 251.86 2.65 o -1 1 0 1372.17 1417.99 4.06 o 1 1 0 11.01 8.88 1.49 o 2 1 0 387.78 426.40 3.60 o 3 1 0 181.20 170.44 2.55 o 4 1 0 3.07 2.94 0.88 o 5 1 0 3.50 5.85 1.15 o 6 1 0 83.59 76.68 2.67 o 7 1 0 110.26 117.34 3.79 o -8 2 0 0.16 0.65 2.49 o -7 2 0 5.60 4.45 0.99 o -6 2 0 24.61 21.60 1.52 o -5 2 0 50.32 54.88 1.49 o -4 2 0 212.34 243.57 2.53 o -3 2 0 282.91 269.84 3.47 o -2 2 0 131.67 126.67 1.06 o -1 2 0 316.66 306.22 3.60 o 0 2 0 50.48 55.32 2.64 o 1 2 0 719.04 777.28 6.24 o 2 2 0 1110.40 1080.90 9.17 o 3 2 0 456.75 420.76 5.23 o 4 2 0 539.96 513.98 6.40 o 5 2 0 484.02 474.30 6.52 o 6 2 0 173.53 164.96 4.15 o 7 2 0 12.06 12.71 2.15 o -8 3 0 44.51 44.68 10.22 o -7 3 0 49.26 46.27 6.04 o -6 3 0 132.61 132.64 1.61 o -5 3 0 322.04 301.85 6.48 o -4 3 0 228.60 223.00 1.43 o -3 3 0 974.38 1028.24 10.14 o -2 3 0 951.59 843.27 4.07 o -1 3 0 6544.92 6837.28 111.65 o 0 3 0 11742.96 12100.94 105.11 o 1 3 0 6457.25 6679.96 34.99 o 2 3 0 5008.79 5471.09 51.21 o 3 3 0 373.74 341.53 5.59 o 4 3 0 868.44 866.37 9.49 o 5 3 0 210.22 222.51 5.04 o 6 3 0 101.67 113.24 4.27 o 7 3 0 0.24 0.50 1.28 o -8 4 0 98.14 91.40 8.90 o -7 4 0 90.00 83.35 7.26 o -6 4 0 80.68 71.27 5.59 o -5 4 0 709.06 729.28 15.69 o -4 4 0 2092.25 2401.16 11.89 o -3 4 0 2094.12 2220.76 23.92 o -2 4 0 735.30 668.61 10.84 o -1 4 0 3118.08 3385.65 18.50 o 0 4 0 1770.53 1754.08 12.83 o 1 4 0 740.17 707.15 8.08 o 2 4 0 88.90 81.87 2.84 o 3 4 0 0.15 1.11 1.22 o 4 4 0 4.36 5.42 1.59 o 5 4 0 0.16 1.23 1.36 o 6 4 0 1.04 1.12 1.61 o -8 5 0 32.06 39.64 6.90 o -7 5 0 64.19 61.23 6.79 o -6 5 0 227.45 214.84 9.36 o -5 5 0 138.22 154.25 9.14 o -4 5 0 0.05 0.66 0.34 o -3 5 0 12.51 10.64 0.72 o -2 5 0 892.34 1000.61 9.88 o -1 5 0 1.30 0.79 0.58 o 0 5 0 31.54 39.64 1.74 o 1 5 0 182.61 192.66 4.88 o 2 5 0 217.01 217.46 5.46 o 3 5 0 125.78 129.20 4.47 o 4 5 0 117.91 111.32 4.73 o 5 5 0 188.25 173.25 5.34 o 6 5 0 6.23 6.57 2.52 o -7 6 0 44.63 47.56 6.59 o -6 6 0 574.85 566.85 17.04 o -5 6 0 61.64 58.96 7.24 o -4 6 0 107.92 109.50 1.40 o -3 6 0 538.61 541.89 8.45 o -2 6 0 518.73 532.88 10.21 o -1 6 0 984.26 940.82 9.60 o 0 6 0 713.06 701.80 9.20 o 1 6 0 2785.91 2747.44 38.26 o 2 6 0 568.13 566.76 13.65 o 3 6 0 238.13 241.68 6.62 o 4 6 0 168.14 172.63 6.24 o 5 6 0 180.81 181.02 6.49 o -6 7 0 320.49 321.92 16.34 o -5 7 0 133.79 154.10 8.61 o -4 7 0 493.29 490.58 4.48 o -3 7 0 927.31 903.00 15.60 o -2 7 0 938.69 932.43 9.85 o -1 7 0 451.16 419.80 6.78 o 0 7 0 424.52 392.97 6.91 o 1 7 0 1056.76 1009.14 15.08 o 2 7 0 36.73 38.31 3.26 o 3 7 0 1.41 2.26 2.00 o 4 7 0 8.57 8.72 3.47 o -6 8 0 16.94 19.69 5.33 o -5 8 0 18.28 25.26 4.94 o -4 8 0 11.61 9.62 0.89 o -3 8 0 72.57 62.16 2.31 o -2 8 0 103.83 109.69 3.11 o -1 8 0 54.73 63.27 3.15 o 0 8 0 73.49 78.96 3.90 o 1 8 0 29.51 24.05 2.86 o 2 8 0 104.31 101.20 5.10 o 3 8 0 48.37 47.46 4.51 o -6 9 0 71.82 75.35 11.49 o -5 9 0 152.72 140.55 9.92 o -4 9 0 158.21 153.37 3.29 o -3 9 0 48.28 58.33 2.73 o -2 9 0 195.45 193.49 4.80 o -1 9 0 253.93 248.21 6.03 o 0 9 0 133.33 132.99 4.98 o 1 9 0 224.37 224.72 7.00 o 2 9 0 71.57 73.46 5.09 o -3 10 0 139.25 146.57 5.10 o -2 10 0 225.46 220.50 6.38 o -1 10 0 85.52 79.43 4.57 o 0 10 0 166.39 161.44 6.03 o 1 -11 1 3.49 2.96 1.77 o 2 -11 1 1.99 1.71 2.02 o 3 -11 1 13.47 9.75 1.79 o -1 -10 1 122.18 112.96 5.44 o 0 -10 1 135.07 131.52 5.10 o 1 -10 1 445.64 441.53 11.26 o 2 -10 1 276.85 267.29 5.85 o 3 -10 1 260.58 256.43 5.55 o 4 -10 1 149.75 147.82 9.57 o 5 -10 1 105.27 115.34 9.85 o -3 -9 1 73.67 70.00 6.00 o -2 -9 1 257.96 258.50 8.04 o -1 -9 1 308.16 317.35 9.62 o 0 -9 1 265.71 264.20 6.44 o 1 -9 1 424.35 441.91 7.73 o 2 -9 1 277.87 282.54 5.84 o 3 -9 1 174.57 176.48 3.53 o 4 -9 1 36.27 33.07 3.28 o 5 -9 1 11.22 8.43 4.47 o 6 -9 1 33.30 30.52 9.36 o -4 -8 1 17.19 15.74 3.63 o -3 -8 1 0.68 0.83 1.78 o -2 -8 1 38.14 45.90 4.05 o -1 -8 1 3.06 3.63 1.68 o 0 -8 1 1.85 3.76 1.43 o 1 -8 1 1.32 0.65 0.89 o 2 -8 1 25.97 26.44 1.54 o 3 -8 1 19.62 29.46 1.79 o 4 -8 1 175.51 169.63 2.01 o 5 -8 1 72.08 89.81 9.77 o 6 -8 1 40.95 44.31 6.88 o -5 -7 1 11.56 13.42 2.81 o -4 -7 1 93.35 99.19 6.07 o -3 -7 1 17.68 20.44 2.92 o -2 -7 1 162.75 154.93 5.57 o -1 -7 1 12.93 16.34 5.12 o 0 -7 1 1410.88 1331.23 14.65 o 1 -7 1 725.44 697.20 8.54 o 2 -7 1 929.72 913.97 9.23 o 3 -7 1 641.05 642.80 5.37 o 4 -7 1 722.20 678.23 17.84 o 5 -7 1 194.62 199.42 9.71 o 6 -7 1 187.23 183.09 10.55 o 7 -7 1 22.93 24.12 6.06 o -5 -6 1 96.24 112.72 4.63 o -4 -6 1 419.38 411.95 10.02 o -3 -6 1 671.96 655.83 14.93 o -2 -6 1 834.24 824.06 11.44 o -1 -6 1 970.76 939.21 11.18 o 0 -6 1 2388.74 2345.55 19.10 o 1 -6 1 1877.70 1852.24 14.28 o 2 -6 1 1147.20 1169.91 8.82 o 3 -6 1 885.90 896.61 5.42 o 4 -6 1 190.35 192.17 7.94 o 5 -6 1 172.64 168.12 8.18 o 6 -6 1 36.84 33.11 7.65 o 7 -6 1 6.73 4.69 4.14 o -6 -5 1 90.92 86.02 4.14 o -5 -5 1 30.87 29.12 2.90 o -4 -5 1 254.94 242.23 6.32 o -3 -5 1 65.55 74.18 3.55 o -2 -5 1 84.95 88.59 3.49 o -1 -5 1 17.70 14.97 1.46 o 0 -5 1 135.55 143.97 11.71 o 1 -5 1 3.78 4.65 0.66 o 2 -5 1 280.38 289.37 2.86 o 3 -5 1 39.84 51.07 1.13 o 4 -5 1 137.71 158.98 6.55 o 5 -5 1 158.63 161.22 7.49 o 6 -5 1 110.08 117.50 10.16 o 7 -5 1 13.47 16.22 5.16 o -6 -4 1 17.38 22.39 2.41 o -5 -4 1 180.82 188.08 4.60 o -4 -4 1 208.66 223.54 5.97 o -3 -4 1 287.17 289.56 5.48 o -2 -4 1 284.88 257.24 4.44 o -1 -4 1 241.62 197.19 3.34 o 0 -4 1 3307.74 3377.52 19.41 o 1 -4 1 802.20 757.17 5.33 o 2 -4 1 2441.23 2616.53 26.44 o 3 -4 1 829.83 797.30 13.14 o 4 -4 1 1215.70 1174.73 19.38 o 5 -4 1 336.67 340.77 10.59 o 6 -4 1 274.91 275.44 10.65 o 7 -4 1 18.73 22.81 5.32 o -7 -3 1 21.74 26.80 2.54 o -6 -3 1 101.43 108.63 3.58 o -5 -3 1 322.14 333.16 5.76 o -4 -3 1 1285.54 1294.97 11.53 o -3 -3 1 2107.27 2097.92 19.23 o -2 -3 1 1371.80 1302.97 11.14 o -1 -3 1 3962.03 4064.31 22.60 o 0 -3 1 6416.58 6734.53 27.49 o 1 -3 1 4125.77 4357.39 14.96 o 2 -3 1 3280.06 3367.95 30.36 o 3 -3 1 1957.34 1948.64 16.35 o 4 -3 1 419.10 407.28 7.21 o 5 -3 1 566.89 547.45 4.09 o 6 -3 1 68.24 69.99 1.37 o 7 -3 1 58.13 63.82 4.75 o -7 -2 1 207.04 200.80 4.79 o -6 -2 1 64.69 62.77 2.61 o -5 -2 1 652.58 642.45 7.33 o -4 -2 1 1038.26 1064.85 9.23 o -3 -2 1 1111.84 1240.03 8.90 o -2 -2 1 2.55 0.68 0.58 o -1 -2 1 458.49 458.64 3.98 o 0 -2 1 3.63 7.32 0.49 o 1 -2 1 866.22 890.46 8.67 o 2 -2 1 617.21 659.87 6.32 o 3 -2 1 62.26 68.23 8.52 o 4 -2 1 61.13 70.47 1.74 o 5 -2 1 143.83 132.18 3.71 o 6 -2 1 60.70 58.09 1.96 o 7 -2 1 25.29 21.98 1.70 o -7 -1 1 25.72 24.40 2.01 o -6 -1 1 150.79 162.84 3.46 o -5 -1 1 164.85 162.01 3.43 o -4 -1 1 347.56 354.68 4.32 o -3 -1 1 1626.89 1665.45 11.14 o -2 -1 1 814.81 735.92 5.76 o -1 -1 1 2516.98 2591.22 11.12 o 1 -1 1 2007.71 2175.77 8.58 o 2 -1 1 1877.88 2089.29 23.96 o 3 -1 1 830.86 802.42 4.60 o 4 -1 1 912.79 888.28 6.21 o 5 -1 1 435.45 438.64 4.43 o 6 -1 1 80.64 81.70 2.32 o 7 -1 1 62.10 65.05 2.28 o -8 0 1 28.09 32.41 2.74 o -7 0 1 26.98 26.21 5.67 o -6 0 1 519.14 539.34 6.28 o -5 0 1 395.62 398.96 4.22 o -4 0 1 3033.71 3068.63 18.87 o -3 0 1 2531.59 2444.20 10.10 o -2 0 1 3985.17 4144.29 16.55 o 1 0 1 3848.18 3932.87 14.92 o 2 0 1 2178.06 2081.60 9.86 o 3 0 1 713.97 717.34 5.49 o 4 0 1 661.98 657.78 11.36 o 5 0 1 290.28 283.83 4.35 o 6 0 1 59.14 69.87 2.38 o 7 0 1 143.75 156.80 4.23 o -8 1 1 31.06 30.25 2.30 o -7 1 1 219.77 226.92 5.64 o -6 1 1 219.40 226.56 4.02 o -5 1 1 1380.33 1379.82 16.61 o -4 1 1 1600.65 1622.71 12.34 o -3 1 1 3742.12 4006.54 17.45 o -2 1 1 174.29 156.51 3.17 o -1 1 1 1191.44 1212.52 5.48 o 0 1 1 30.26 32.20 2.04 o 1 1 1 2562.49 2679.50 20.71 o 2 1 1 79.66 87.37 1.70 o 3 1 1 688.61 708.71 6.33 o 4 1 1 0.35 0.87 0.91 o 5 1 1 23.95 18.02 1.68 o 6 1 1 26.11 21.44 2.11 o 7 1 1 1.40 4.32 1.78 o -8 2 1 44.89 49.25 6.53 o -7 2 1 38.76 37.61 1.64 o -6 2 1 2.82 3.58 0.66 o -5 2 1 42.10 39.65 1.06 o -4 2 1 200.00 198.03 2.06 o -3 2 1 722.87 769.64 9.37 o -2 2 1 681.14 679.46 4.03 o -1 2 1 4745.67 4967.26 42.75 o 0 2 1 690.88 701.77 5.33 o 1 2 1 3823.21 4208.70 23.34 o 2 2 1 706.73 745.90 7.89 o 3 2 1 444.14 432.29 7.00 o 4 2 1 396.35 378.76 5.54 o 5 2 1 304.34 312.64 5.53 o 6 2 1 46.92 44.81 2.76 o -8 3 1 10.78 12.63 6.45 o -7 3 1 117.38 119.11 1.98 o -6 3 1 269.16 271.54 2.85 o -5 3 1 968.08 942.76 8.74 o -4 3 1 2112.37 2213.94 17.06 o -3 3 1 2837.57 2947.68 13.60 o -2 3 1 3923.99 4023.53 18.02 o -1 3 1 3372.17 3404.50 17.75 o 0 3 1 3184.31 3166.69 40.68 o 1 3 1 2315.20 2233.95 38.45 o 2 3 1 777.71 735.99 8.51 o 3 3 1 86.51 88.49 3.16 o 4 3 1 224.40 237.07 6.09 o 5 3 1 49.14 55.23 3.44 o 6 3 1 79.91 99.96 4.14 o -8 4 1 31.61 28.87 5.67 o -7 4 1 122.43 126.82 7.81 o -6 4 1 200.01 213.55 4.18 o -5 4 1 1055.79 1113.06 6.21 o -4 4 1 1303.61 1326.97 9.60 o -3 4 1 2242.00 2350.58 12.95 o -2 4 1 722.69 699.96 5.73 o -1 4 1 334.82 287.09 3.59 o 0 4 1 122.26 119.82 14.29 o 1 4 1 371.41 374.72 5.63 o 2 4 1 136.45 145.10 3.95 o 3 4 1 146.17 162.67 4.70 o 4 4 1 6.56 8.48 1.91 o 5 4 1 0.00 1.49 1.65 o 6 4 1 3.44 6.42 2.25 o -8 5 1 27.17 25.77 5.79 o -7 5 1 41.72 41.03 5.65 o -6 5 1 13.75 16.38 3.84 o -5 5 1 8.88 11.25 0.64 o -4 5 1 7.12 6.26 0.60 o -3 5 1 16.83 16.94 0.99 o -2 5 1 204.32 230.35 3.26 o -1 5 1 589.93 619.63 6.95 o 0 5 1 260.80 277.73 4.85 o 1 5 1 1064.35 1082.26 12.63 o 2 5 1 45.14 39.77 3.27 o 3 5 1 245.98 229.53 6.75 o 4 5 1 78.84 68.84 3.70 o 5 5 1 133.44 126.97 5.08 o -7 6 1 80.49 78.24 7.35 o -6 6 1 91.52 90.47 6.92 o -5 6 1 626.19 617.08 6.44 o -4 6 1 541.86 537.55 5.33 o -3 6 1 1521.69 1479.12 18.55 o -2 6 1 1353.94 1393.19 12.95 o -1 6 1 1260.88 1227.35 12.76 o 0 6 1 1154.71 1105.30 12.96 o 1 6 1 1239.98 1216.85 15.33 o 2 6 1 82.71 87.10 4.13 o 3 6 1 67.89 73.53 4.34 o 4 6 1 32.25 37.66 3.98 o -6 7 1 204.25 226.88 14.42 o -5 7 1 282.15 292.96 5.42 o -4 7 1 595.56 594.46 6.93 o -3 7 1 851.35 819.41 9.41 o -2 7 1 411.11 425.67 9.79 o -1 7 1 50.56 48.96 2.86 o 0 7 1 126.17 119.38 4.47 o 1 7 1 91.77 93.16 4.80 o 2 7 1 11.73 12.84 3.12 o 3 7 1 3.39 5.37 2.56 o 4 7 1 14.77 17.83 3.71 o -6 8 1 38.63 48.42 6.92 o -5 8 1 0.69 1.14 1.12 o -4 8 1 4.65 4.01 1.00 o -3 8 1 27.58 21.62 3.02 o -2 8 1 41.06 43.51 2.49 o -1 8 1 32.46 36.69 2.63 o 0 8 1 88.36 101.30 4.34 o 1 8 1 18.58 20.58 2.99 o 2 8 1 36.90 39.15 4.07 o 3 8 1 48.64 48.88 4.89 o -5 9 1 164.68 160.69 10.36 o -4 9 1 125.72 136.80 3.65 o -3 9 1 272.08 274.41 5.87 o -2 9 1 249.47 254.21 8.10 o -1 9 1 348.21 342.02 7.93 o 0 9 1 352.66 360.06 13.20 o 1 9 1 140.38 132.86 6.23 o -4 10 1 283.54 280.69 9.20 o -3 10 1 132.88 124.96 4.93 o -2 10 1 146.69 140.61 7.64 o -1 10 1 29.48 26.00 3.18 o 0 -11 2 50.72 44.75 3.60 o 1 -11 2 31.23 27.41 2.71 o 2 -11 2 20.31 20.21 2.43 o 3 -11 2 36.17 38.48 3.29 o -2 -10 2 211.52 214.06 7.62 o -1 -10 2 204.10 204.90 6.63 o 0 -10 2 281.53 275.78 7.53 o 1 -10 2 273.59 277.02 6.22 o 2 -10 2 159.61 156.93 4.44 o 3 -10 2 199.17 200.75 3.70 o 4 -10 2 6.86 12.98 6.57 o 5 -10 2 80.44 77.12 8.43 o -3 -9 2 187.62 187.67 7.25 o -2 -9 2 321.40 326.70 8.45 o -1 -9 2 339.32 335.81 8.35 o 0 -9 2 37.13 37.23 2.96 o 1 -9 2 167.75 173.00 6.31 o 2 -9 2 310.36 307.91 9.68 o 3 -9 2 182.18 170.45 2.83 o 4 -9 2 10.49 10.83 4.08 o 5 -9 2 55.74 47.80 6.63 o 6 -9 2 20.34 14.71 5.79 o -4 -8 2 6.39 7.15 2.82 o -3 -8 2 18.61 20.67 3.11 o -2 -8 2 83.17 92.84 4.73 o -1 -8 2 68.27 76.53 3.39 o 0 -8 2 442.87 402.51 8.85 o 1 -8 2 4.28 1.65 1.04 o 2 -8 2 34.79 35.28 1.71 o 3 -8 2 63.21 64.97 1.51 o 4 -8 2 244.38 260.18 10.43 o 5 -8 2 29.82 36.56 5.69 o 6 -8 2 12.30 14.20 5.37 o -5 -7 2 3.76 5.76 2.17 o -4 -7 2 403.91 373.52 10.14 o -3 -7 2 262.43 263.92 9.71 o -2 -7 2 435.19 419.45 7.92 o -1 -7 2 725.11 693.29 9.75 o 0 -7 2 3587.54 3491.12 27.40 o 1 -7 2 930.36 915.02 19.46 o 2 -7 2 738.19 729.53 6.71 o 3 -7 2 442.03 451.44 6.21 o 4 -7 2 201.56 213.15 9.02 o 5 -7 2 60.86 62.49 8.86 o 6 -7 2 0.26 -1.59 3.24 o 7 -7 2 183.26 181.67 12.47 o -6 -6 2 25.22 29.83 3.04 o -5 -6 2 170.86 189.16 5.57 o -4 -6 2 774.69 758.95 13.48 o -3 -6 2 1165.70 1187.92 20.28 o -2 -6 2 699.76 712.42 9.96 o -1 -6 2 1469.06 1457.11 14.49 o 0 -6 2 812.40 797.94 8.42 o 1 -6 2 460.52 458.86 5.20 o 2 -6 2 115.94 101.54 1.87 o 3 -6 2 785.94 784.10 15.83 o 4 -6 2 151.08 143.11 7.08 o 5 -6 2 36.73 34.87 5.10 o 6 -6 2 2.21 5.83 3.94 o 7 -6 2 156.12 148.88 11.20 o -6 -5 2 33.09 34.70 3.06 o -5 -5 2 49.53 49.17 2.85 o -4 -5 2 266.20 266.00 5.05 o -3 -5 2 54.58 66.43 3.15 o -2 -5 2 722.42 811.11 12.67 o 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