#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205114.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205114_Fobs loop_ _publ_author_name 'Mahboob, Sumera' 'Parvez, Masood' 'Mazhar, Muhammad' 'Ali, Saqib' _publ_section_title ; \b-Methyl-\g,\g-bis(8-quinolinoxy)germa-\g-lactone ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m358 _journal_page_last m360 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6950 _cell_length_b 17.2660 _cell_length_c 23.5430 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file lh6346Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X YELLOW PRISM PBCA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 296.89 _shelx_f_squared_multiplier 1.00 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1428.90 1306.85 55.22 o 6 0 0 8706.12 7921.23 235.65 o 8 0 0 4387.00 5212.64 169.03 o 10 0 0 2541.90 2777.03 177.06 o 12 0 0 1966.59 2256.73 203.25 o 2 1 0 3825.71 4565.04 172.14 o 4 1 0 12073.63 11905.56 222.17 o 6 1 0 8074.91 9143.31 214.14 o 8 1 0 741.88 923.95 46.40 o 10 1 0 184.20 241.10 57.03 o 12 1 0 16.22 -69.74 59.63 o 4 2 0 19885.59 20616.19 365.54 o 6 2 0 22063.90 22453.71 396.64 o 8 2 0 681.88 698.41 40.44 o 10 2 0 94.63 198.84 57.55 o 12 2 0 22.96 -93.33 62.22 o 2 3 0 71995.16 71863.19 1337.70 o 4 3 0 32312.31 32194.58 548.04 o 6 3 0 417.45 457.31 32.66 o 8 3 0 1924.82 2142.14 66.11 o 10 3 0 5372.55 5428.07 202.47 o 12 3 0 257.92 297.87 86.07 o 0 4 0 20368.70 20093.29 692.96 o 2 4 0 25873.94 26281.98 511.75 o 4 4 0 2199.14 2247.13 57.81 o 6 4 0 957.89 747.66 36.29 o 8 4 0 249.64 233.32 35.78 o 10 4 0 10.52 20.48 53.92 o 12 4 0 282.66 301.50 75.96 o 2 5 0 1785.78 1462.14 46.66 o 4 5 0 17588.67 17242.89 361.13 o 6 5 0 538.32 599.89 39.92 o 8 5 0 2871.24 3096.94 90.74 o 10 5 0 1872.46 1794.49 107.85 o 12 5 0 184.14 218.02 61.70 o 0 6 0 11714.29 10905.39 287.24 o 2 6 0 13643.26 14451.08 306.17 o 4 6 0 10380.42 10307.58 227.36 o 6 6 0 12621.71 12857.25 300.21 o 8 6 0 3715.41 3708.24 117.70 o 10 6 0 784.06 750.25 78.03 o 12 6 0 1205.27 1292.08 109.92 o 2 7 0 4920.39 5632.61 137.66 o 4 7 0 287.43 181.99 20.74 o 6 7 0 3864.78 3585.36 109.66 o 8 7 0 31.33 18.41 36.55 o 10 7 0 2.86 -56.77 43.81 o 0 8 0 11798.02 10328.32 289.84 o 2 8 0 17626.71 17660.02 365.28 o 4 8 0 5255.07 5001.61 115.10 o 6 8 0 11156.95 11728.50 242.65 o 8 8 0 320.74 310.32 44.85 o 10 8 0 572.54 612.34 73.11 o 2 9 0 7200.95 7500.99 176.29 o 4 9 0 9136.29 9437.81 187.95 o 6 9 0 543.41 548.56 31.11 o 8 9 0 6421.38 6628.37 190.80 o 10 9 0 2527.81 2707.81 164.36 o 0 10 0 11635.65 11883.52 321.98 o 2 10 0 102.55 150.62 38.63 o 4 10 0 264.10 250.69 33.96 o 6 10 0 599.59 653.30 49.52 o 8 10 0 33.59 33.70 28.26 o 10 10 0 69.06 67.14 56.77 o 2 11 0 3050.87 2760.96 85.55 o 4 11 0 6924.32 6719.89 158.66 o 6 11 0 33.00 -15.30 30.85 o 8 11 0 3820.45 3966.96 109.14 o 10 11 0 1649.11 1540.95 115.88 o 0 12 0 5408.11 4965.83 165.14 o 2 12 0 7052.09 7299.56 173.95 o 4 12 0 310.62 337.80 39.41 o 6 12 0 3674.45 3877.53 114.07 o 8 12 0 477.42 450.83 51.85 o 10 12 0 614.39 625.04 91.77 o 2 13 0 989.60 1006.13 54.96 o 4 13 0 20.18 20.48 40.96 o 6 13 0 13.58 -7.78 52.11 o 8 13 0 62.34 -62.22 54.70 o 10 13 0 62.06 116.40 67.14 o 0 14 0 994.70 986.95 70.26 o 2 14 0 2107.76 2137.47 89.44 o 4 14 0 681.60 703.59 56.77 o 6 14 0 7701.18 8464.86 253.02 o 8 14 0 1162.52 1055.13 79.33 o 2 15 0 3395.12 3833.45 132.47 o 4 15 0 5306.62 5198.12 168.77 o 6 15 0 90.71 105.77 51.33 o 8 15 0 1332.33 1489.62 102.14 o 0 16 0 295.96 250.69 54.70 o 2 16 0 21.92 85.81 47.18 o 4 16 0 5.60 69.74 64.55 o 6 16 0 125.39 82.96 67.66 o 8 16 0 125.03 46.66 67.40 o 2 17 0 4143.62 4161.66 184.06 o 4 17 0 5891.86 5950.19 243.43 o 6 17 0 14.29 69.74 57.03 o 8 17 0 1071.34 1122.53 112.51 o 0 18 0 1179.50 1259.41 133.77 o 2 18 0 792.89 851.10 92.03 o 4 18 0 573.33 597.30 87.11 o 6 18 0 1443.97 1601.61 122.36 o 2 19 0 467.71 701.00 148.29 o 4 19 0 857.50 1118.90 166.95 o 6 19 0 49.22 41.22 97.99 o 0 20 0 7675.95 8287.80 556.34 o 2 20 0 204.64 292.69 155.03 o 4 20 0 279.28 179.40 103.70 o 2 21 0 359.94 412.72 111.73 o 4 21 0 104.61 481.68 165.40 o 2 22 0 169.95 95.66 106.55 o 2 1 1 9029.10 9576.77 239.59 o 3 1 1 292.35 286.57 14.66 o 4 1 1 17296.73 16905.84 364.11 o 5 1 1 10166.17 10276.14 142.25 o 6 1 1 0.82 5.27 23.46 o 7 1 1 3508.03 3235.64 115.88 o 8 1 1 1848.75 1872.12 45.09 o 9 1 1 31.40 18.91 20.61 o 10 1 1 926.90 987.78 53.18 o 11 1 1 1263.62 1340.61 79.85 o 12 1 1 144.97 80.42 67.66 o 1 2 1 3854.83 3954.00 108.88 o 3 2 1 8832.07 8503.49 118.97 o 4 2 1 215.01 230.40 15.87 o 5 2 1 3870.58 4271.23 103.18 o 6 2 1 4848.07 4666.13 121.72 o 7 2 1 250.20 258.63 28.52 o 8 2 1 1333.18 1406.10 36.35 o 9 2 1 1243.37 1273.04 70.77 o 10 2 1 106.75 196.19 39.29 o 11 2 1 2612.38 2638.56 94.33 o 12 2 1 2332.20 2243.70 208.95 o 1 3 1 14509.46 14138.70 484.27 o 2 3 1 47171.70 47235.89 625.99 o 3 3 1 8391.05 8924.36 216.47 o 4 3 1 1.50 -9.07 16.85 o 5 3 1 128.78 67.36 29.81 o 6 3 1 2642.41 2999.01 224.64 o 7 3 1 3003.06 3253.62 63.90 o 8 3 1 181.13 216.06 25.84 o 9 3 1 59.36 53.37 29.81 o 10 3 1 48.73 36.28 62.09 o 11 3 1 30.10 -24.78 43.42 o 12 3 1 9.08 10.42 56.90 o 0 4 1 2291.48 2825.51 86.59 o 1 4 1 2446.93 2919.50 47.65 o 2 4 1 945.66 971.36 24.32 o 3 4 1 37928.62 36722.04 503.42 o 4 4 1 2449.10 2615.99 44.18 o 5 4 1 531.83 503.76 21.76 o 6 4 1 15113.63 15402.92 214.47 o 7 4 1 1801.93 1795.48 56.13 o 8 4 1 3796.08 3988.13 74.89 o 9 4 1 1379.71 1467.57 45.52 o 10 4 1 235.63 261.30 44.20 o 11 4 1 417.47 448.72 48.72 o 12 4 1 729.15 971.26 68.37 o 1 5 1 8024.43 7769.76 138.83 o 2 5 1 13722.77 14202.49 290.74 o 3 5 1 763.59 756.43 42.91 o 4 5 1 6607.16 6691.40 108.87 o 5 5 1 1693.65 1556.60 40.31 o 6 5 1 208.13 185.63 22.74 o 7 5 1 3538.31 3428.89 65.59 o 8 5 1 612.63 545.01 52.24 o 9 5 1 736.56 752.05 42.13 o 10 5 1 772.12 824.89 52.37 o 11 5 1 804.75 751.83 56.05 o 12 5 1 57.98 103.79 44.51 o 0 6 1 815.84 927.06 34.22 o 1 6 1 297.77 242.99 25.92 o 2 6 1 19592.72 20208.90 296.78 o 3 6 1 8232.35 8295.28 101.51 o 4 6 1 23.83 9.59 15.15 o 5 6 1 86.68 44.39 20.68 o 6 6 1 1069.34 1190.42 38.47 o 7 6 1 180.17 252.75 37.98 o 8 6 1 589.20 472.91 30.29 o 9 6 1 439.43 473.73 51.46 o 10 6 1 105.81 96.15 57.16 o 11 6 1 95.98 51.05 75.18 o 12 6 1 107.99 54.18 51.33 o 1 7 1 12266.40 11108.83 150.36 o 2 7 1 16869.03 17113.21 258.94 o 3 7 1 531.87 612.46 60.53 o 4 7 1 3698.47 3258.02 53.43 o 5 7 1 7760.38 7399.56 192.49 o 6 7 1 32.46 43.10 23.66 o 7 7 1 7245.76 7677.50 169.42 o 8 7 1 2855.74 3021.97 109.14 o 9 7 1 169.03 104.82 37.33 o 10 7 1 1084.27 1138.52 64.33 o 11 7 1 775.22 802.21 67.17 o 0 8 1 10958.79 10651.59 210.25 o 1 8 1 2373.66 2196.69 40.51 o 2 8 1 3539.37 4058.84 74.53 o 3 8 1 7277.58 7269.09 116.59 o 4 8 1 239.30 153.19 20.07 o 5 8 1 655.18 639.24 18.97 o 6 8 1 944.44 845.07 40.31 o 7 8 1 500.67 517.90 32.02 o 8 8 1 384.78 359.86 34.38 o 9 8 1 1280.52 1192.03 58.36 o 10 8 1 505.75 407.06 56.00 o 11 8 1 32.61 55.79 49.86 o 1 9 1 6479.07 6628.37 149.33 o 2 9 1 1162.79 1369.53 37.85 o 3 9 1 1749.71 2008.46 59.37 o 4 9 1 319.99 377.51 25.79 o 5 9 1 3880.09 3918.67 69.82 o 6 9 1 633.08 622.84 36.68 o 7 9 1 208.72 195.68 21.12 o 8 9 1 681.65 716.85 149.07 o 9 9 1 48.05 31.54 30.39 o 10 9 1 130.58 96.53 45.11 o 11 9 1 176.21 170.11 104.73 o 0 10 1 6517.52 6333.35 137.66 o 1 10 1 4193.04 4350.93 71.22 o 2 10 1 4997.59 4956.86 79.21 o 3 10 1 4698.73 4541.82 120.16 o 4 10 1 2534.02 2543.84 64.16 o 5 10 1 3509.80 3512.88 66.08 o 6 10 1 2601.51 2587.27 54.90 o 7 10 1 700.71 658.82 23.10 o 8 10 1 135.51 111.50 19.67 o 9 10 1 4764.41 4991.28 189.90 o 10 10 1 515.56 610.35 82.18 o 11 10 1 56.41 113.89 143.75 o 1 11 1 827.27 866.11 57.03 o 2 11 1 1139.96 1140.34 54.44 o 3 11 1 283.81 230.01 28.06 o 4 11 1 470.28 441.64 29.50 o 5 11 1 204.12 287.94 28.64 o 6 11 1 41.77 1.70 24.88 o 7 11 1 799.81 753.11 37.58 o 8 11 1 642.91 622.64 23.14 o 9 11 1 52.14 73.86 39.83 o 10 11 1 207.75 89.11 49.65 o 0 12 1 321.05 354.91 42.26 o 1 12 1 753.31 773.69 29.86 o 2 12 1 468.30 492.97 20.00 o 3 12 1 2084.53 2139.00 58.21 o 4 12 1 508.02 512.39 34.73 o 5 12 1 674.87 758.68 33.73 o 6 12 1 1028.77 979.44 37.11 o 7 12 1 392.88 404.04 38.20 o 8 12 1 382.28 373.73 42.13 o 9 12 1 550.15 561.96 42.69 o 10 12 1 59.12 47.33 89.70 o 1 13 1 3282.04 3486.55 129.36 o 2 13 1 3970.42 3970.55 86.85 o 3 13 1 526.75 469.37 35.83 o 4 13 1 1917.76 2161.70 66.11 o 5 13 1 715.95 770.03 35.82 o 6 13 1 17.81 57.30 28.29 o 7 13 1 3647.37 3768.15 99.39 o 8 13 1 2011.83 2028.63 66.44 o 9 13 1 20.08 -5.77 47.66 o 10 13 1 436.82 383.07 58.39 o 0 14 1 742.82 698.41 53.92 o 1 14 1 52.74 85.93 40.44 o 2 14 1 704.24 744.59 25.32 o 3 14 1 581.94 528.64 41.25 o 4 14 1 4.50 -41.49 30.30 o 5 14 1 666.91 573.75 65.98 o 6 14 1 181.38 174.70 60.92 o 7 14 1 279.65 207.90 38.60 o 8 14 1 363.42 342.26 38.49 o 9 14 1 170.95 205.99 63.51 o 1 15 1 325.55 304.42 30.66 o 2 15 1 2946.22 3057.54 145.31 o 3 15 1 5.08 -20.39 31.15 o 4 15 1 239.12 303.97 51.59 o 5 15 1 2143.86 2252.12 71.76 o 6 15 1 40.34 33.38 37.39 o 7 15 1 1063.71 1079.62 80.50 o 8 15 1 701.46 645.30 54.51 o 9 15 1 18.74 82.39 66.71 o 0 16 1 460.41 560.49 53.15 o 1 16 1 1475.23 1612.00 49.21 o 2 16 1 1763.72 1683.16 60.49 o 3 16 1 4762.73 4933.41 121.46 o 4 16 1 456.95 555.05 51.53 o 5 16 1 781.49 704.66 44.86 o 6 16 1 2048.18 2035.18 74.70 o 7 16 1 219.01 176.41 40.20 o 8 16 1 207.85 180.88 51.29 o 1 17 1 187.11 215.29 50.55 o 2 17 1 818.09 918.68 250.95 o 3 17 1 18.50 22.32 73.50 o 4 17 1 75.32 97.06 49.39 o 5 17 1 162.91 182.37 45.37 o 6 17 1 103.73 121.25 43.62 o 7 17 1 253.80 158.91 51.01 o 8 17 1 56.88 167.93 61.31 o 0 18 1 2584.68 2686.55 110.96 o 1 18 1 402.97 352.83 48.90 o 2 18 1 66.48 -5.47 42.67 o 3 18 1 2301.22 2357.45 96.57 o 4 18 1 800.45 708.85 83.48 o 5 18 1 222.15 365.20 51.78 o 6 18 1 627.60 733.88 80.11 o 7 18 1 632.46 582.81 71.40 o 1 19 1 3114.62 3471.23 200.79 o 2 19 1 2069.00 2193.90 178.23 o 3 19 1 44.93 100.64 71.42 o 4 19 1 2167.86 2464.73 167.96 o 5 19 1 643.49 675.20 78.03 o 6 19 1 1.59 -26.20 54.14 o 0 20 1 237.72 488.42 94.62 o 1 20 1 272.58 197.98 102.40 o 2 20 1 81.32 43.01 77.77 o 3 20 1 4.27 39.98 71.31 o 4 20 1 0.04 -80.04 53.36 o 5 20 1 14.75 43.77 50.30 o 1 21 1 824.15 932.48 108.18 o 2 21 1 889.64 873.55 97.64 o 3 21 1 1.39 -120.79 117.70 o 4 21 1 764.31 911.80 97.07 o 0 22 1 1936.45 1696.76 188.73 o 1 22 1 1201.62 1065.66 113.03 o 2 22 1 393.28 401.29 103.06 o 2 0 2 37.35 204.80 52.37 o 3 0 2 23794.79 22089.21 438.90 o 4 0 2 2018.46 2062.81 50.81 o 5 0 2 23372.07 24881.28 433.72 o 6 0 2 1.37 25.92 23.33 o 7 0 2 1469.81 1481.58 51.07 o 8 0 2 7.62 36.04 28.26 o 9 0 2 5367.42 5716.87 161.77 o 10 0 2 85.04 64.81 44.33 o 11 0 2 2228.93 2295.61 126.77 o 12 0 2 179.76 90.74 80.37 o 1 1 2 11100.59 10699.94 284.65 o 2 1 2 2172.95 2419.27 105.25 o 3 1 2 11889.67 11804.45 159.16 o 4 1 2 4.96 -6.14 14.72 o 5 1 2 3290.19 3213.60 55.00 o 6 1 2 1055.49 1122.67 44.33 o 7 1 2 682.76 535.92 24.87 o 8 1 2 2.71 3.80 29.68 o 9 1 2 145.63 99.75 36.29 o 10 1 2 78.65 84.74 33.62 o 11 1 2 451.65 412.05 52.34 o 12 1 2 12.36 14.62 50.42 o 1 2 2 17414.35 17288.16 294.63 o 2 2 2 2467.80 2763.80 49.22 o 3 2 2 1594.55 1227.64 23.80 o 4 2 2 225.34 203.78 21.78 o 5 2 2 2207.84 1983.75 39.23 o 6 2 2 94.99 82.96 19.26 o 7 2 2 493.00 516.16 65.59 o 8 2 2 38.90 75.62 21.72 o 9 2 2 3361.65 3487.72 70.05 o 10 2 2 360.38 358.58 41.57 o 11 2 2 6.22 7.11 40.55 o 12 2 2 6.57 31.10 45.92 o 2 3 2 31439.51 30847.67 366.72 o 3 3 2 7443.72 7459.96 119.12 o 4 3 2 1513.00 1607.69 31.80 o 5 3 2 24447.26 24554.74 390.94 o 6 3 2 115.37 133.52 31.37 o 7 3 2 7866.26 7911.67 118.38 o 8 3 2 27.65 42.63 23.20 o 9 3 2 139.96 129.70 22.89 o 10 3 2 1.18 -2.87 22.38 o 11 3 2 2535.49 2837.60 105.48 o 12 3 2 134.06 109.22 53.15 o 0 4 2 8725.90 8748.48 190.54 o 1 4 2 29690.03 30085.16 355.76 o 2 4 2 1896.35 1911.47 37.35 o 3 4 2 512.11 323.69 19.44 o 4 4 2 5486.95 6180.50 95.69 o 5 4 2 626.09 601.94 20.29 o 6 4 2 85.74 150.20 21.04 o 7 4 2 851.13 997.38 54.44 o 8 4 2 410.36 463.43 42.78 o 9 4 2 354.88 378.12 29.48 o 10 4 2 265.26 334.31 40.56 o 11 4 2 229.27 211.93 44.86 o 12 4 2 0.64 -3.28 50.57 o 1 5 2 624.82 584.89 35.52 o 2 5 2 1168.46 1143.87 61.44 o 3 5 2 5.11 -22.13 14.76 o 4 5 2 3291.90 3779.34 100.46 o 5 5 2 11312.24 11195.30 162.62 o 6 5 2 389.80 422.41 30.07 o 7 5 2 17054.39 17687.33 239.40 o 8 5 2 190.27 175.27 25.65 o 9 5 2 1033.87 984.32 51.07 o 10 5 2 355.47 304.76 78.03 o 11 5 2 1525.10 1661.72 85.02 o 12 5 2 11.25 2.01 67.27 o 0 6 2 11114.04 10980.06 202.73 o 1 6 2 541.53 594.39 17.24 o 2 6 2 6327.17 6467.45 96.36 o 3 6 2 42239.67 41908.83 508.47 o 4 6 2 66.49 110.63 31.11 o 5 6 2 3901.52 3917.94 78.80 o 6 6 2 142.59 89.82 46.40 o 7 6 2 5049.25 5124.40 94.42 o 8 6 2 432.10 406.99 32.62 o 9 6 2 1977.59 2100.01 74.19 o 10 6 2 22.27 -7.41 39.39 o 11 6 2 951.20 932.99 96.05 o 12 6 2 33.23 -71.72 67.53 o 1 7 2 105.41 142.93 17.81 o 2 7 2 1599.93 1571.12 31.94 o 3 7 2 19829.20 21220.96 291.48 o 4 7 2 1406.24 1538.62 32.37 o 5 7 2 156.43 191.60 28.39 o 6 7 2 0.07 -15.30 21.58 o 7 7 2 710.15 741.49 38.67 o 8 7 2 22.10 34.55 25.32 o 9 7 2 511.47 662.88 48.98 o 10 7 2 20.48 -58.44 43.22 o 11 7 2 37.24 93.67 90.61 o 0 8 2 1229.39 1458.25 42.78 o 1 8 2 1270.31 1324.41 31.05 o 2 8 2 2500.54 2835.33 49.33 o 3 8 2 9641.17 9470.21 142.53 o 4 8 2 339.25 460.96 27.04 o 5 8 2 4521.08 4445.56 71.95 o 6 8 2 746.56 625.99 96.05 o 7 8 2 37.36 49.30 31.24 o 8 8 2 238.21 195.53 26.71 o 9 8 2 6135.98 6307.68 149.48 o 10 8 2 111.77 144.34 42.91 o 11 8 2 438.04 362.69 52.05 o 1 9 2 11840.31 11345.81 153.43 o 2 9 2 20.91 -10.55 28.39 o 3 9 2 24.43 6.92 24.78 o 4 9 2 5356.72 5327.78 100.33 o 5 9 2 7503.45 7088.77 119.50 o 6 9 2 22.34 46.55 15.31 o 7 9 2 2698.56 2739.70 60.31 o 8 9 2 43.14 39.36 32.42 o 9 9 2 81.98 53.04 30.46 o 10 9 2 46.25 53.88 47.13 o 11 9 2 847.91 843.26 63.72 o 0 10 2 559.35 753.11 42.00 o 1 10 2 285.76 367.40 25.48 o 2 10 2 1234.80 1318.25 30.99 o 3 10 2 910.69 1006.63 48.48 o 4 10 2 367.87 431.28 28.38 o 5 10 2 92.40 122.34 28.91 o 6 10 2 200.39 193.72 22.51 o 7 10 2 15.93 3.76 42.91 o 8 10 2 195.62 190.35 32.15 o 9 10 2 0.05 27.71 38.94 o 10 10 2 1.51 58.72 54.06 o 11 10 2 7.71 -65.86 52.11 o 1 11 2 14228.67 13983.65 187.35 o 2 11 2 18.63 23.99 17.45 o 3 11 2 128.58 128.13 54.57 o 4 11 2 469.26 432.50 34.74 o 5 11 2 5172.97 5123.55 92.39 o 6 11 2 174.59 153.72 23.65 o 7 11 2 2842.24 2982.64 119.64 o 8 11 2 160.88 100.99 35.26 o 9 11 2 38.31 -26.88 38.02 o 10 11 2 116.10 151.67 58.46 o 0 12 2 50.73 54.44 30.85 o 1 12 2 296.52 277.55 25.17 o 2 12 2 397.49 414.91 39.53 o 3 12 2 11375.56 10921.32 188.08 o 4 12 2 682.11 647.16 31.74 o 5 12 2 1171.26 1126.88 39.80 o 6 12 2 249.11 213.13 28.27 o 7 12 2 1446.07 1458.31 54.99 o 8 12 2 5.73 25.00 33.78 o 9 12 2 2765.71 2533.26 86.97 o 10 12 2 4.58 61.08 46.23 o 1 13 2 157.93 140.49 25.75 o 2 13 2 175.16 181.41 19.24 o 3 13 2 258.42 235.97 37.17 o 4 13 2 42.67 24.90 41.35 o 5 13 2 501.35 444.80 33.55 o 6 13 2 589.48 635.50 55.22 o 7 13 2 309.92 252.42 39.59 o 8 13 2 70.17 50.76 49.00 o 9 13 2 25.29 41.20 41.66 o 10 13 2 10.64 80.88 66.24 o 0 14 2 421.42 546.23 50.03 o 1 14 2 4464.88 4534.33 82.40 o 2 14 2 291.92 239.62 20.98 o 3 14 2 10456.76 10958.25 199.67 o 4 14 2 92.63 80.15 27.50 o 5 14 2 1560.53 1447.89 49.16 o 6 14 2 71.56 40.07 32.27 o 7 14 2 913.48 915.64 45.91 o 8 14 2 128.56 149.78 39.02 o 9 14 2 2534.94 2767.45 121.09 o 1 15 2 1748.54 1682.50 93.59 o 2 15 2 0.89 -19.01 36.29 o 3 15 2 295.15 251.53 39.41 o 4 15 2 461.12 508.58 65.59 o 5 15 2 3309.71 3372.13 91.93 o 6 15 2 2.42 -29.69 47.96 o 7 15 2 1010.15 1079.08 54.56 o 8 15 2 137.54 150.44 45.89 o 9 15 2 1.05 87.25 93.59 o 0 16 2 115.27 108.88 41.48 o 1 16 2 331.61 311.42 62.87 o 2 16 2 1004.20 1128.49 60.66 o 3 16 2 9.51 144.05 40.61 o 4 16 2 74.82 75.05 41.78 o 5 16 2 206.98 235.08 38.89 o 6 16 2 1.47 -4.93 49.13 o 7 16 2 68.39 122.88 41.80 o 8 16 2 0.32 -59.68 50.40 o 1 17 2 4038.90 4085.22 85.56 o 2 17 2 33.82 54.66 36.05 o 3 17 2 10.27 54.84 62.35 o 4 17 2 23.08 16.40 89.57 o 5 17 2 4157.83 4064.69 109.07 o 6 17 2 0.05 -38.45 35.36 o 7 17 2 1704.65 1627.76 86.48 o 8 17 2 35.33 67.89 48.16 o 0 18 2 52.56 204.80 53.92 o 1 18 2 238.94 277.81 40.31 o 2 18 2 175.71 251.61 55.25 o 3 18 2 2152.75 2413.65 116.14 o 4 18 2 79.10 131.35 45.76 o 5 18 2 535.39 618.29 59.29 o 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3 13 22.16 21.42 39.95 o 11 3 13 88.52 66.80 89.57 o 0 4 13 271.47 290.87 22.55 o 1 4 13 5857.60 5591.49 72.33 o 2 4 13 1.45 16.87 14.72 o 3 4 13 18548.64 18143.95 246.15 o 4 4 13 561.43 582.83 28.27 o 5 4 13 2947.74 2831.34 62.51 o 6 4 13 279.07 317.61 31.76 o 7 4 13 1839.68 1906.20 47.20 o 8 4 13 365.98 394.03 31.93 o 9 4 13 3707.99 3704.94 108.88 o 10 4 13 46.93 13.75 88.01 o 11 4 13 426.99 414.12 52.40 o 1 5 13 9156.33 9124.84 113.27 o 2 5 13 568.30 673.98 24.06 o 3 5 13 118.93 153.58 20.87 o 4 5 13 94.48 117.74 22.34 o 5 5 13 2171.50 2194.24 47.20 o 6 5 13 544.28 618.45 29.55 o 7 5 13 1792.09 1803.43 48.61 o 8 5 13 343.49 305.45 30.29 o 9 5 13 5.46 -3.65 50.29 o 10 5 13 3.83 78.00 52.24 o 11 5 13 542.30 606.91 62.74 o 0 6 13 1967.11 2261.65 48.48 o 1 6 13 85.71 83.30 23.07 o 2 6 13 316.00 346.07 18.23 o 3 6 13 2137.54 1997.19 39.43 o 4 6 13 272.18 260.62 41.61 o 5 6 13 6027.24 6171.03 119.51 o 6 6 13 82.74 113.40 10.37 o 7 6 13 712.57 680.68 33.16 o 8 6 13 116.98 123.48 44.33 o 9 6 13 235.03 215.61 39.02 o 10 6 13 3.44 29.44 77.90 o 1 7 13 7093.76 6991.46 87.90 o 2 7 13 106.19 189.82 25.92 o 3 7 13 0.73 32.13 33.57 o 4 7 13 75.26 86.70 25.92 o 5 7 13 6991.58 7155.49 95.24 o 6 7 13 620.45 569.30 32.15 o 7 7 13 1672.05 1778.73 59.76 o 8 7 13 222.85 241.23 21.13 o 9 7 13 91.15 75.44 30.98 o 10 7 13 91.71 19.61 51.04 o 0 8 13 533.07 546.23 30.85 o 1 8 13 1269.38 1265.02 29.43 o 2 8 13 6.96 20.48 17.87 o 3 8 13 5128.84 5169.36 77.09 o 4 8 13 540.89 565.35 48.22 o 5 8 13 132.58 131.69 20.57 o 6 8 13 232.28 218.81 18.44 o 7 8 13 808.08 826.89 28.24 o 8 8 13 439.65 512.48 78.81 o 9 8 13 242.35 242.22 31.01 o 10 8 13 9.32 64.37 48.90 o 1 9 13 999.36 947.30 26.58 o 2 9 13 30.35 21.42 24.63 o 3 9 13 1102.33 1188.40 101.62 o 4 9 13 146.15 122.10 22.31 o 5 9 13 3492.85 3657.38 69.42 o 6 9 13 25.92 40.53 23.55 o 7 9 13 731.00 626.03 32.15 o 8 9 13 0.16 -28.67 19.11 o 9 9 13 106.58 84.47 32.89 o 10 9 13 74.33 26.44 44.65 o 0 10 13 501.12 517.97 34.74 o 1 10 13 3562.32 3778.12 64.00 o 2 10 13 2955.36 3097.08 55.62 o 3 10 13 2953.01 3090.33 59.64 o 4 10 13 26.51 -21.84 28.39 o 5 10 13 2179.92 2123.51 106.94 o 6 10 13 306.98 370.53 24.76 o 7 10 13 1833.37 1907.70 63.06 o 8 10 13 395.22 387.83 32.25 o 9 10 13 1718.61 1527.36 78.14 o 1 11 13 1308.41 1371.17 64.03 o 2 11 13 160.50 129.33 23.59 o 3 11 13 53.79 42.76 22.30 o 4 11 13 90.33 100.86 24.17 o 5 11 13 2132.74 2113.98 49.39 o 6 11 13 899.94 910.04 37.20 o 7 11 13 600.61 599.83 34.94 o 8 11 13 94.21 92.86 33.12 o 9 11 13 6.26 9.34 34.98 o 0 12 13 867.66 927.06 46.40 o 1 12 13 1593.72 1525.14 36.48 o 2 12 13 76.23 74.54 22.30 o 3 12 13 866.00 840.67 44.46 o 4 12 13 28.35 -11.64 59.50 o 5 12 13 633.83 667.90 74.79 o 6 12 13 95.51 125.61 31.38 o 7 12 13 165.73 110.72 68.70 o 8 12 13 66.21 -11.29 43.94 o 9 12 13 973.14 879.47 70.26 o 1 13 13 2524.24 2521.32 53.89 o 2 13 13 125.85 102.27 22.18 o 3 13 13 297.91 327.33 32.20 o 4 13 13 403.60 411.56 37.98 o 5 13 13 4134.14 4283.53 95.82 o 6 13 13 4.43 -22.38 33.57 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41.52 o 2 18 13 28.51 -2.74 39.14 o 3 18 13 1505.16 1445.23 170.32 o 4 18 13 28.38 -125.25 129.75 o 5 18 13 7.18 -116.15 102.51 o 1 19 13 2552.18 2610.72 112.13 o 2 19 13 3.69 29.17 80.10 o 3 19 13 19.94 -31.81 80.06 o 0 20 13 9.37 -25.92 72.59 o 1 20 13 157.56 -98.18 207.53 o 0 0 14 3417.31 3369.15 88.66 o 1 0 14 6637.51 6904.73 101.62 o 2 0 14 2008.06 1962.22 40.70 o 3 0 14 21460.26 20791.96 440.46 o 4 0 14 5168.95 5161.31 138.96 o 5 0 14 1258.24 1370.11 67.92 o 6 0 14 2401.52 2489.79 96.44 o 7 0 14 757.16 750.25 66.89 o 8 0 14 1494.68 1332.78 100.33 o 9 0 14 941.39 810.14 124.70 o 10 0 14 2.77 31.37 91.25 o 11 0 14 792.22 753.11 173.18 o 1 1 14 6964.67 6900.29 86.64 o 2 1 14 1396.58 1311.91 23.05 o 3 1 14 968.87 1068.46 57.55 o 4 1 14 1365.36 1274.59 41.97 o 5 1 14 842.58 704.02 39.97 o 6 1 14 41.88 26.95 42.52 o 7 1 14 46.38 98.46 37.26 o 8 1 14 462.70 353.87 56.47 o 9 1 14 14.46 30.02 96.96 o 10 1 14 161.08 116.40 20.49 o 11 1 14 138.45 202.45 88.29 o 0 2 14 8354.94 7776.83 143.62 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5 14 1742.23 1620.72 44.98 o 3 5 14 21.21 54.88 14.13 o 4 5 14 379.99 367.92 52.89 o 5 5 14 47.84 128.25 46.66 o 6 5 14 170.62 203.77 31.24 o 7 5 14 5923.01 5527.69 106.59 o 8 5 14 554.62 566.92 49.39 o 9 5 14 7.54 28.25 26.83 o 10 5 14 714.68 598.10 57.17 o 0 6 14 4293.63 4005.33 70.77 o 1 6 14 328.97 349.80 32.02 o 2 6 14 4680.25 4809.72 72.89 o 3 6 14 10073.28 10038.62 142.11 o 4 6 14 876.24 866.29 33.31 o 5 6 14 225.64 215.96 23.93 o 6 6 14 2871.52 2578.67 56.64 o 7 6 14 1158.85 1180.93 41.87 o 8 6 14 234.15 203.67 32.45 o 9 6 14 1005.72 1002.47 52.27 o 10 6 14 45.84 15.48 57.03 o 1 7 14 433.53 480.18 21.40 o 2 7 14 6.45 16.24 28.52 o 3 7 14 6.15 10.61 19.92 o 4 7 14 1401.37 1546.28 36.89 o 5 7 14 541.04 535.46 22.04 o 6 7 14 210.67 199.09 9.67 o 7 7 14 29.87 45.43 26.70 o 8 7 14 108.97 97.20 31.59 o 9 7 14 1.33 47.53 34.13 o 10 7 14 5.61 -52.71 47.35 o 0 8 14 2117.62 1917.37 49.00 o 1 8 14 1353.47 1469.60 32.79 o 2 8 14 591.53 575.08 24.02 o 3 8 14 3342.12 3504.45 60.53 o 4 8 14 553.42 581.90 47.83 o 5 8 14 4602.78 4533.17 75.76 o 6 8 14 694.18 671.28 58.07 o 7 8 14 721.24 639.70 28.78 o 8 8 14 39.74 27.56 12.96 o 9 8 14 1290.38 1384.54 93.07 o 10 8 14 41.02 73.68 55.26 o 1 9 14 2871.12 2860.29 49.56 o 2 9 14 793.39 723.60 25.72 o 3 9 14 394.95 364.69 32.41 o 4 9 14 848.04 899.68 33.47 o 5 9 14 2269.77 2400.80 49.82 o 6 9 14 239.78 280.96 42.65 o 7 9 14 901.11 871.36 75.18 o 8 9 14 1070.42 958.00 33.53 o 9 9 14 115.03 113.62 24.42 o 0 10 14 656.58 663.67 36.81 o 1 10 14 30.91 70.44 21.77 o 2 10 14 116.99 109.15 21.90 o 3 10 14 42.62 38.69 18.18 o 4 10 14 654.11 681.15 29.02 o 5 10 14 26.87 73.32 17.69 o 6 10 14 38.79 33.71 23.43 o 7 10 14 176.28 211.88 68.83 o 8 10 14 9.98 17.37 25.69 o 9 10 14 67.58 87.25 68.44 o 1 11 14 3712.40 3963.97 93.07 o 2 11 14 1507.78 1419.58 104.35 o 3 11 14 59.46 4.69 21.91 o 4 11 14 1985.80 2006.47 61.18 o 5 11 14 1632.11 1608.99 42.05 o 6 11 14 17.45 13.04 38.89 o 7 11 14 2457.64 2295.46 78.35 o 8 11 14 1091.48 1120.24 84.64 o 9 11 14 13.92 -9.78 36.04 o 0 12 14 1551.30 1548.99 52.11 o 1 12 14 14.82 3.42 32.28 o 2 12 14 486.17 419.45 25.76 o 3 12 14 151.20 127.07 25.15 o 4 12 14 1625.29 1693.07 84.77 o 5 12 14 1133.13 1166.48 45.91 o 6 12 14 1596.93 1596.53 52.92 o 7 12 14 498.65 458.67 77.64 o 8 12 14 405.43 383.37 45.80 o 1 13 14 352.58 344.65 30.05 o 2 13 14 439.48 461.85 33.11 o 3 13 14 25.30 2.69 62.35 o 4 13 14 555.28 535.83 46.92 o 5 13 14 0.51 -44.17 29.45 o 6 13 14 61.88 -9.39 39.76 o 7 13 14 1.06 -57.47 38.32 o 8 13 14 96.06 129.48 72.46 o 0 14 14 4551.81 4752.74 126.25 o 1 14 14 13.36 17.64 23.02 o 2 14 14 1665.53 1629.87 54.28 o 3 14 14 3250.79 3610.33 134.81 o 4 14 14 162.04 202.83 57.29 o 5 14 14 1073.54 1021.46 111.48 o 6 14 14 928.07 1020.20 92.03 o 7 14 14 174.49 144.06 39.29 o 1 15 14 515.55 502.97 36.04 o 2 15 14 336.83 322.42 31.63 o 3 15 14 13.48 39.69 29.54 o 4 15 14 833.11 866.40 58.16 o 5 15 14 621.42 721.17 284.13 o 6 15 14 49.07 -18.83 46.61 o 7 15 14 556.28 418.97 55.00 o 0 16 14 172.69 222.43 39.41 o 1 16 14 241.29 146.12 34.70 o 2 16 14 343.44 319.14 33.24 o 3 16 14 80.13 82.02 34.69 o 4 16 14 336.43 397.18 133.25 o 5 16 14 130.80 23.33 122.23 o 6 16 14 166.75 180.06 94.24 o 1 17 14 2052.94 1904.69 102.79 o 2 17 14 952.81 906.52 53.01 o 3 17 14 33.76 26.96 138.83 o 4 17 14 242.72 286.70 100.98 o 5 17 14 1166.45 1259.62 120.89 o 0 18 14 1109.26 1139.64 106.55 o 1 18 14 2.50 -24.87 46.61 o 2 18 14 128.53 87.18 78.03 o 3 18 14 735.02 736.51 112.91 o 4 18 14 4.87 -66.12 81.03 o 1 19 14 242.87 156.36 64.81 o 2 19 14 40.92 56.06 83.09 o 3 19 14 25.81 -93.07 86.16 o 1 1 15 662.19 713.13 19.25 o 2 1 15 20181.37 19512.54 196.00 o 3 1 15 1072.51 1086.33 30.91 o 4 1 15 8637.20 8274.13 144.08 o 5 1 15 1106.75 1097.91 69.09 o 6 1 15 14.01 43.18 30.22 o 7 1 15 111.05 61.12 33.86 o 8 1 15 1948.33 1830.49 246.80 o 9 1 15 0.10 73.72 74.56 o 10 1 15 1968.95 1946.96 199.49 o 0 2 15 11223.83 10651.59 189.25 o 1 2 15 73.90 141.75 14.18 o 2 2 15 1371.14 1396.85 24.59 o 3 2 15 2.15 29.67 14.39 o 4 2 15 2503.39 2614.52 44.92 o 5 2 15 563.40 654.75 40.38 o 6 2 15 2630.58 2579.17 71.27 o 7 2 15 39.75 48.43 32.77 o 8 2 15 1816.73 1830.67 97.18 o 9 2 15 268.81 151.20 87.92 o 10 2 15 122.35 240.18 73.89 o 1 3 15 196.65 180.89 34.74 o 2 3 15 654.75 620.57 19.49 o 3 3 15 5.68 10.59 14.31 o 4 3 15 1902.75 1799.82 43.42 o 5 3 15 505.27 476.74 20.80 o 6 3 15 228.81 242.86 30.72 o 7 3 15 102.47 83.04 18.77 o 8 3 15 1.03 -18.32 37.46 o 9 3 15 471.89 417.31 257.82 o 10 3 15 5.53 -81.78 67.84 o 0 4 15 11262.06 10735.85 168.77 o 1 4 15 121.57 182.83 15.55 o 2 4 15 5573.71 5722.40 84.51 o 3 4 15 53.60 54.87 16.27 o 4 4 15 1226.51 1215.79 30.68 o 5 4 15 0.28 -4.22 20.67 o 6 4 15 5349.10 5397.08 106.05 o 7 4 15 147.79 211.11 64.81 o 8 4 15 1971.53 2008.30 60.29 o 9 4 15 266.83 226.16 34.43 o 10 4 15 369.60 304.53 39.31 o 1 5 15 652.20 629.62 56.77 o 2 5 15 6676.29 6672.94 125.09 o 3 5 15 13.71 9.81 12.49 o 4 5 15 2873.26 2964.01 71.81 o 5 5 15 71.74 52.64 22.21 o 6 5 15 49.55 72.59 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