#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205124.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205124_Fobs loop_ _publ_author_name 'Yathirajan, Hemmige S.' 'Gaonkar, Santhosh L.' 'Bolte, Michael' _publ_section_title ; 2-(5-Ethylpyridin-2-yl)ethanol ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o492 _journal_page_last o493 _journal_volume 61 _journal_year 2005 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.6920 _cell_length_b 14.6920 _cell_length_c 8.0106 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8208 _[local]_cod_data_source_file nc6018Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat17 in P-42(1)c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 159.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 17940.60 17925.60 673.17 o 1 3 0 1020.76 989.88 10.39 o 2 3 0 7047.42 6930.13 165.71 o 3 3 0 25535.06 26691.41 1437.63 o 0 4 0 141.48 97.50 13.13 o 1 4 0 2381.89 2348.16 35.59 o 2 4 0 804.18 763.88 10.96 o 3 4 0 1444.26 1437.52 58.04 o 4 4 0 2412.27 2666.44 193.96 o 1 5 0 5674.93 5842.44 105.19 o 2 5 0 2981.59 2953.97 58.04 o 3 5 0 1744.30 1607.93 36.29 o 4 5 0 945.95 910.40 30.90 o 5 5 0 594.95 667.16 53.60 o 0 6 0 376.83 396.35 11.54 o 1 6 0 1071.31 1135.91 13.65 o 2 6 0 15.61 13.44 8.61 o 3 6 0 2.94 1.50 4.29 o 4 6 0 84.82 79.56 5.45 o 5 6 0 45.73 50.63 4.48 o 6 6 0 1375.82 1356.80 124.94 o 1 7 0 256.66 271.46 6.02 o 2 7 0 253.93 228.07 8.42 o 3 7 0 578.83 571.00 41.62 o 4 7 0 2805.83 2798.12 101.99 o 5 7 0 1199.06 1164.53 44.11 o 6 7 0 1188.49 1213.37 51.08 o 7 7 0 424.35 427.76 48.93 o 0 8 0 17.14 16.67 8.90 o 1 8 0 1413.91 1428.46 26.92 o 2 8 0 2041.95 2133.24 87.07 o 3 8 0 2.99 2.73 5.35 o 4 8 0 8.07 5.05 5.09 o 5 8 0 263.61 239.89 9.42 o 6 8 0 82.84 80.36 3.65 o 7 8 0 95.71 91.93 3.44 o 8 8 0 140.64 141.50 12.34 o 1 9 0 56.08 54.10 5.71 o 2 9 0 105.87 95.05 6.13 o 3 9 0 104.13 93.77 5.50 o 4 9 0 15.36 17.55 5.30 o 5 9 0 46.94 36.53 5.14 o 6 9 0 0.16 -0.76 3.34 o 7 9 0 17.36 18.44 3.76 o 8 9 0 276.68 267.05 18.41 o 9 9 0 833.74 786.94 93.00 o 0 10 0 1459.68 1583.60 17.23 o 1 10 0 709.69 758.05 14.92 o 2 10 0 20.47 14.60 5.68 o 3 10 0 399.33 445.59 6.49 o 4 10 0 80.21 74.97 4.47 o 5 10 0 48.02 43.74 4.50 o 6 10 0 36.04 39.10 4.08 o 7 10 0 26.46 33.35 3.73 o 8 10 0 64.29 67.56 4.19 o 9 10 0 26.45 16.44 3.66 o 10 10 0 369.24 326.98 48.54 o 1 11 0 150.68 149.83 6.08 o 2 11 0 42.74 47.39 4.57 o 3 11 0 242.10 233.74 13.57 o 4 11 0 7.38 5.81 4.80 o 5 11 0 49.75 50.09 4.69 o 6 11 0 14.92 11.54 4.42 o 7 11 0 117.34 101.21 5.02 o 8 11 0 8.93 9.70 4.76 o 9 11 0 1.89 1.96 3.13 o 10 11 0 30.21 25.44 3.58 o 11 11 0 226.98 213.59 16.67 o 0 12 0 9.04 4.95 5.42 o 1 12 0 0.24 3.80 5.45 o 2 12 0 35.18 39.68 3.95 o 3 12 0 145.33 140.49 7.56 o 4 12 0 131.22 129.86 6.36 o 5 12 0 80.03 72.23 4.40 o 6 12 0 14.00 7.54 3.75 o 7 12 0 99.43 86.77 6.54 o 8 12 0 55.08 46.45 4.17 o 9 12 0 7.91 7.94 3.97 o 10 12 0 138.94 121.32 3.83 o 11 12 0 6.71 7.22 3.54 o 12 12 0 15.83 11.27 4.53 o 1 13 0 15.25 19.27 3.93 o 2 13 0 0.61 3.28 5.15 o 3 13 0 9.92 9.73 4.37 o 4 13 0 3.05 5.26 3.56 o 5 13 0 80.79 88.30 6.07 o 6 13 0 0.38 2.56 4.16 o 7 13 0 99.25 96.48 6.93 o 8 13 0 16.74 15.05 4.20 o 9 13 0 39.41 32.98 3.79 o 10 13 0 10.82 8.40 3.31 o 11 13 0 12.05 16.78 3.75 o 12 13 0 28.54 45.31 5.60 o 0 14 0 5.47 4.90 4.21 o 1 14 0 23.78 18.13 3.21 o 2 14 0 12.32 13.07 5.06 o 3 14 0 15.10 14.80 4.34 o 4 14 0 7.54 8.13 4.90 o 5 14 0 4.94 3.64 3.78 o 6 14 0 11.77 8.62 4.83 o 7 14 0 1.65 4.43 3.88 o 8 14 0 154.51 136.95 11.53 o 9 14 0 44.49 39.57 3.70 o 10 14 0 5.38 2.06 4.08 o 11 14 0 1.41 3.47 6.04 o 1 15 0 3.20 8.06 3.08 o 2 15 0 0.09 1.35 3.54 o 3 15 0 2.34 5.32 4.30 o 4 15 0 10.84 11.08 3.49 o 5 15 0 9.51 7.85 4.88 o 6 15 0 1.72 0.67 4.23 o 7 15 0 54.59 62.70 4.86 o 8 15 0 31.30 23.74 7.53 o 9 15 0 3.59 0.02 3.76 o 0 16 0 1.52 0.05 4.01 o 1 16 0 6.70 6.26 3.66 o 2 16 0 30.70 32.74 3.64 o 3 16 0 122.41 126.30 4.55 o 4 16 0 31.43 29.39 4.89 o 5 16 0 13.03 16.44 3.46 o 6 16 0 41.54 38.81 4.35 o 7 16 0 2.75 6.12 4.23 o 8 16 0 17.56 34.19 5.85 o 1 17 0 1.38 2.33 3.18 o 2 17 0 2.27 -0.26 3.22 o 3 17 0 36.47 31.52 3.41 o 4 17 0 0.93 4.96 4.21 o 5 17 0 12.30 7.62 4.16 o 0 2 1 3199.02 2972.24 37.80 o 1 2 1 48.97 38.66 8.61 o 0 3 1 4151.88 3998.07 35.22 o 1 3 1 7960.47 7946.26 135.31 o 2 3 1 8526.94 8520.36 108.00 o 0 4 1 3.89 0.55 7.81 o 1 4 1 486.80 486.41 6.14 o 2 4 1 236.41 209.90 4.54 o 3 4 1 2002.58 1950.15 24.83 o 0 5 1 1443.19 1473.29 19.65 o 1 5 1 57.49 53.41 5.40 o 2 5 1 852.28 782.67 11.08 o 3 5 1 2777.33 2855.39 49.93 o 4 5 1 1010.03 1005.70 21.27 o 0 6 1 2439.12 2522.58 37.02 o 1 6 1 390.52 396.10 9.24 o 2 6 1 1057.82 1086.32 23.01 o 3 6 1 82.69 78.89 3.70 o 4 6 1 2509.07 2605.62 53.31 o 5 6 1 508.23 533.77 9.51 o 0 7 1 201.94 174.72 6.25 o 1 7 1 537.49 584.29 12.52 o 2 7 1 447.73 434.15 7.54 o 3 7 1 14.89 11.24 3.26 o 4 7 1 1559.85 1579.38 23.03 o 5 7 1 457.70 443.76 12.14 o 6 7 1 655.94 639.89 15.82 o 0 8 1 36.36 33.93 5.64 o 1 8 1 4.51 1.42 4.33 o 2 8 1 163.15 164.29 3.82 o 3 8 1 0.33 1.41 3.66 o 4 8 1 1036.14 1041.05 23.62 o 5 8 1 666.13 649.56 19.25 o 6 8 1 287.33 293.98 5.21 o 7 8 1 35.26 36.63 2.32 o 0 9 1 20.40 23.60 5.25 o 1 9 1 50.11 48.45 4.12 o 2 9 1 277.12 282.39 6.77 o 3 9 1 89.71 84.22 3.58 o 4 9 1 12.50 9.94 3.27 o 5 9 1 176.29 166.74 3.42 o 6 9 1 216.99 204.99 7.32 o 7 9 1 287.42 272.21 6.86 o 8 9 1 194.46 196.13 4.89 o 0 10 1 58.95 64.93 5.76 o 1 10 1 474.81 520.55 7.15 o 2 10 1 27.32 21.11 3.32 o 3 10 1 189.98 183.78 5.57 o 4 10 1 130.30 123.24 6.00 o 5 10 1 20.19 19.32 3.36 o 6 10 1 209.64 213.03 6.92 o 7 10 1 548.94 533.61 9.64 o 8 10 1 269.92 249.00 11.27 o 9 10 1 51.36 49.16 2.34 o 0 11 1 0.00 0.67 5.38 o 1 11 1 105.65 98.23 2.89 o 2 11 1 33.58 35.84 3.02 o 3 11 1 137.46 145.42 4.54 o 4 11 1 112.06 118.46 3.67 o 5 11 1 90.67 89.43 3.13 o 6 11 1 14.65 10.90 3.07 o 7 11 1 34.31 33.09 3.20 o 8 11 1 15.70 9.91 2.35 o 9 11 1 7.49 10.42 2.19 o 10 11 1 16.28 12.81 2.90 o 0 12 1 36.67 32.48 4.15 o 1 12 1 38.32 42.46 2.96 o 2 12 1 3.69 5.02 2.81 o 3 12 1 48.11 52.57 3.73 o 4 12 1 118.59 107.79 3.31 o 5 12 1 23.44 24.55 3.63 o 6 12 1 56.71 59.82 4.16 o 7 12 1 107.03 107.50 3.43 o 8 12 1 156.56 148.71 5.03 o 9 12 1 3.05 2.74 2.55 o 10 12 1 24.84 24.00 2.43 o 11 12 1 104.85 101.61 4.44 o 0 13 1 0.15 1.31 2.99 o 1 13 1 106.73 117.85 2.67 o 2 13 1 37.41 36.05 2.65 o 3 13 1 10.62 11.58 3.15 o 4 13 1 5.58 4.24 3.27 o 5 13 1 100.56 99.66 3.82 o 6 13 1 23.84 26.47 3.19 o 7 13 1 22.66 19.52 2.99 o 8 13 1 64.58 60.49 3.32 o 9 13 1 12.48 8.69 2.73 o 10 13 1 95.99 89.87 4.86 o 11 13 1 0.27 1.95 2.45 o 12 13 1 123.16 115.81 3.84 o 0 14 1 9.61 8.52 3.61 o 1 14 1 5.61 3.85 2.63 o 2 14 1 5.75 6.29 2.53 o 3 14 1 38.02 34.02 2.70 o 4 14 1 42.79 42.19 3.22 o 5 14 1 28.42 26.45 3.19 o 6 14 1 125.25 125.56 3.41 o 7 14 1 58.22 55.46 3.19 o 8 14 1 30.78 30.72 2.99 o 9 14 1 26.35 23.92 2.65 o 10 14 1 9.94 6.92 2.76 o 11 14 1 18.08 14.10 3.43 o 0 15 1 22.75 23.23 4.09 o 1 15 1 7.12 12.03 2.38 o 2 15 1 20.59 20.70 2.77 o 3 15 1 140.14 145.89 3.67 o 4 15 1 131.30 134.13 3.01 o 5 15 1 14.78 13.56 2.86 o 6 15 1 104.89 99.97 3.41 o 7 15 1 21.89 22.90 3.14 o 8 15 1 44.07 46.47 3.05 o 9 15 1 32.51 37.28 3.17 o 0 16 1 4.36 5.42 2.92 o 1 16 1 8.51 9.18 2.65 o 2 16 1 30.05 28.55 2.76 o 3 16 1 12.90 11.72 2.51 o 4 16 1 5.06 4.46 3.14 o 5 16 1 34.50 30.15 2.66 o 6 16 1 4.94 5.89 2.76 o 7 16 1 22.03 25.87 3.19 o 0 17 1 100.58 102.01 4.34 o 1 17 1 23.57 25.33 2.52 o 2 17 1 4.35 6.42 2.28 o 3 17 1 42.83 39.05 2.45 o 4 17 1 33.33 34.74 2.63 o 5 17 1 15.70 15.53 2.92 o 0 2 2 19.54 17.66 10.41 o 1 2 2 99.63 75.56 9.25 o 2 2 2 2815.18 2781.19 23.57 o 0 3 2 1029.76 957.40 21.14 o 1 3 2 1435.67 1364.16 14.49 o 2 3 2 708.65 686.14 6.27 o 3 3 2 280.97 278.05 6.88 o 0 4 2 3067.42 2917.73 51.71 o 1 4 2 209.31 192.96 4.53 o 2 4 2 302.02 297.72 5.12 o 3 4 2 411.53 409.21 5.23 o 4 4 2 663.60 651.48 10.80 o 0 5 2 146.17 146.12 6.89 o 1 5 2 51.87 57.71 3.78 o 2 5 2 262.07 242.40 3.95 o 3 5 2 399.06 417.00 7.26 o 4 5 2 208.45 214.52 3.76 o 5 5 2 326.41 330.53 9.78 o 0 6 2 10.46 42.82 8.26 o 1 6 2 110.24 107.44 4.56 o 2 6 2 123.74 126.62 3.52 o 3 6 2 630.44 654.35 19.72 o 4 6 2 138.10 133.95 3.98 o 5 6 2 151.63 160.47 3.22 o 6 6 2 29.23 30.49 3.47 o 0 7 2 57.43 58.96 5.67 o 1 7 2 110.35 95.03 4.11 o 2 7 2 67.62 63.52 4.08 o 3 7 2 243.21 252.27 3.66 o 4 7 2 76.33 72.22 2.85 o 5 7 2 223.47 210.86 5.10 o 6 7 2 18.65 19.79 2.90 o 7 7 2 146.24 147.49 5.39 o 0 8 2 20.22 20.83 4.49 o 1 8 2 150.52 141.39 3.68 o 2 8 2 301.26 298.02 5.53 o 3 8 2 385.31 377.67 7.16 o 4 8 2 111.68 110.21 3.92 o 5 8 2 166.87 165.02 3.84 o 6 8 2 30.99 31.66 2.85 o 7 8 2 286.74 295.54 5.27 o 8 8 2 212.93 209.55 4.07 o 0 9 2 97.71 115.26 5.67 o 1 9 2 57.41 59.80 3.20 o 2 9 2 79.02 70.27 3.60 o 3 9 2 67.38 59.60 3.29 o 4 9 2 11.07 10.39 2.74 o 5 9 2 104.23 97.09 2.83 o 6 9 2 512.31 511.00 13.59 o 7 9 2 11.41 12.68 2.86 o 8 9 2 214.79 208.53 6.61 o 9 9 2 91.94 90.58 5.02 o 0 10 2 0.12 0.02 4.43 o 1 10 2 146.58 150.81 3.69 o 2 10 2 127.66 129.12 3.07 o 3 10 2 360.94 371.78 5.42 o 4 10 2 37.68 36.82 3.25 o 5 10 2 390.93 400.98 4.83 o 6 10 2 31.72 31.67 2.97 o 7 10 2 102.76 97.40 3.73 o 8 10 2 28.78 28.63 2.65 o 9 10 2 20.55 22.63 2.70 o 10 10 2 27.21 28.84 3.66 o 0 11 2 540.51 545.84 6.84 o 1 11 2 42.36 41.80 2.97 o 2 11 2 0.69 -0.64 2.79 o 3 11 2 121.48 117.22 3.03 o 4 11 2 420.03 402.07 9.79 o 5 11 2 148.59 143.62 3.38 o 6 11 2 102.15 100.59 3.35 o 7 11 2 90.55 82.11 2.87 o 8 11 2 1.78 1.45 2.58 o 9 11 2 30.77 31.86 2.73 o 10 11 2 107.41 112.63 4.84 o 11 11 2 11.91 7.03 3.40 o 0 12 2 10.93 5.54 4.10 o 1 12 2 460.87 457.83 7.99 o 2 12 2 243.01 243.78 4.10 o 3 12 2 21.72 22.61 3.17 o 4 12 2 255.05 257.30 3.33 o 5 12 2 6.92 5.15 3.15 o 6 12 2 146.96 152.27 4.48 o 7 12 2 117.33 113.82 3.48 o 8 12 2 47.73 44.73 2.62 o 9 12 2 162.88 156.11 3.42 o 10 12 2 62.90 62.07 3.40 o 11 12 2 39.62 43.47 2.67 o 12 12 2 10.25 16.48 4.82 o 0 13 2 24.58 25.61 3.91 o 1 13 2 248.16 253.41 3.12 o 2 13 2 193.01 198.87 4.19 o 3 13 2 57.48 52.70 2.59 o 4 13 2 6.61 8.16 3.37 o 5 13 2 155.79 162.33 3.46 o 6 13 2 36.97 28.55 3.12 o 7 13 2 4.69 6.49 2.81 o 8 13 2 112.39 114.59 6.09 o 9 13 2 11.50 10.53 2.64 o 10 13 2 35.98 37.80 2.46 o 11 13 2 0.26 0.62 2.74 o 0 14 2 334.09 346.62 5.37 o 1 14 2 270.00 269.48 3.57 o 2 14 2 42.44 39.62 2.87 o 3 14 2 48.33 45.15 3.00 o 4 14 2 71.51 74.86 3.40 o 5 14 2 99.64 102.26 3.20 o 6 14 2 5.07 5.67 2.56 o 7 14 2 34.61 31.15 2.94 o 8 14 2 3.95 2.54 2.74 o 9 14 2 37.48 37.41 2.94 o 10 14 2 14.82 13.04 3.41 o 0 15 2 74.96 72.02 3.18 o 1 15 2 82.21 87.19 3.06 o 2 15 2 44.29 42.62 2.46 o 3 15 2 134.71 140.27 4.35 o 4 15 2 69.06 71.04 2.83 o 5 15 2 5.32 4.53 3.10 o 6 15 2 0.69 1.48 2.99 o 7 15 2 26.20 26.83 2.58 o 8 15 2 2.51 6.15 3.09 o 9 15 2 5.90 6.71 4.72 o 0 16 2 305.49 304.61 7.84 o 1 16 2 42.56 43.75 2.53 o 2 16 2 8.07 6.78 3.11 o 3 16 2 64.08 62.88 3.01 o 4 16 2 28.84 25.05 2.67 o 5 16 2 92.81 96.16 2.91 o 6 16 2 13.04 9.07 2.83 o 7 16 2 3.70 3.57 4.23 o 0 17 2 50.68 51.71 4.20 o 1 17 2 10.23 10.36 2.72 o 2 17 2 26.00 25.73 2.72 o 3 17 2 3.74 2.15 2.49 o 4 17 2 43.66 49.96 6.01 o 0 2 3 0.17 -0.85 10.23 o 1 2 3 164.97 157.52 8.10 o 0 3 3 146.39 137.96 9.36 o 1 3 3 651.84 746.52 12.41 o 2 3 3 747.59 804.00 17.06 o 0 4 3 1385.72 1450.40 78.33 o 1 4 3 1507.65 1618.38 49.52 o 2 4 3 201.79 222.15 4.58 o 3 4 3 596.10 609.65 12.02 o 0 5 3 1162.12 1154.27 53.28 o 1 5 3 111.15 122.85 3.92 o 2 5 3 779.07 829.93 15.00 o 3 5 3 2702.35 2866.25 44.13 o 4 5 3 274.19 277.30 6.78 o 0 6 3 34.65 27.20 5.37 o 1 6 3 50.73 63.99 3.65 o 2 6 3 346.06 380.97 7.28 o 3 6 3 142.92 145.43 3.52 o 4 6 3 301.55 337.87 6.43 o 5 6 3 497.51 469.27 9.26 o 0 7 3 78.90 84.70 4.86 o 1 7 3 940.56 982.96 7.38 o 2 7 3 221.82 229.08 3.43 o 3 7 3 487.29 496.91 9.36 o 4 7 3 443.20 452.76 7.23 o 5 7 3 582.92 622.20 10.05 o 6 7 3 17.93 12.65 2.89 o 0 8 3 230.02 222.81 6.66 o 1 8 3 164.18 165.30 3.56 o 2 8 3 647.10 653.21 7.18 o 3 8 3 89.52 104.21 2.88 o 4 8 3 153.75 161.08 3.87 o 5 8 3 11.64 8.19 2.95 o 6 8 3 1054.60 1062.11 12.81 o 7 8 3 231.80 231.26 6.06 o 0 9 3 232.92 212.83 5.62 o 1 9 3 409.03 392.45 5.90 o 2 9 3 329.04 325.36 4.38 o 3 9 3 30.91 29.91 3.16 o 4 9 3 283.56 289.56 5.51 o 5 9 3 366.75 362.95 3.54 o 6 9 3 1088.33 1102.25 14.28 o 7 9 3 46.10 46.92 2.99 o 8 9 3 19.66 19.49 2.75 o 0 10 3 20.72 18.83 5.11 o 1 10 3 68.52 69.42 3.65 o 2 10 3 5.41 4.58 2.75 o 3 10 3 5.10 3.10 2.64 o 4 10 3 158.44 152.64 3.04 o 5 10 3 402.59 398.75 5.97 o 6 10 3 98.92 94.89 2.77 o 7 10 3 208.82 211.36 5.04 o 8 10 3 42.20 39.79 3.20 o 9 10 3 46.64 43.80 2.93 o 0 11 3 174.01 169.92 5.56 o 1 11 3 62.16 63.64 3.27 o 2 11 3 3.85 5.04 2.87 o 3 11 3 312.79 318.25 6.17 o 4 11 3 512.58 513.16 4.92 o 5 11 3 14.77 14.17 2.75 o 6 11 3 288.06 292.94 4.89 o 7 11 3 153.41 146.36 2.86 o 8 11 3 0.31 0.95 2.70 o 9 11 3 33.44 32.62 2.89 o 10 11 3 14.19 13.43 3.12 o 0 12 3 44.51 45.54 5.12 o 1 12 3 10.52 6.74 3.50 o 2 12 3 444.70 465.87 9.08 o 3 12 3 546.30 560.62 8.46 o 4 12 3 139.97 138.55 2.90 o 5 12 3 15.50 12.40 2.64 o 6 12 3 12.87 11.29 2.70 o 7 12 3 57.87 59.64 2.60 o 8 12 3 21.75 16.42 2.46 o 9 12 3 27.04 28.17 3.03 o 10 12 3 1.64 3.18 2.73 o 11 12 3 11.10 13.03 2.81 o 0 13 3 234.62 242.05 8.58 o 1 13 3 159.62 159.34 3.09 o 2 13 3 213.71 213.46 4.21 o 3 13 3 110.63 108.30 3.04 o 4 13 3 254.63 263.25 4.25 o 5 13 3 141.71 146.97 2.77 o 6 13 3 14.73 14.60 2.90 o 7 13 3 24.08 20.68 2.91 o 8 13 3 64.52 67.70 2.93 o 9 13 3 56.18 58.40 2.62 o 10 13 3 46.00 49.36 2.76 o 0 14 3 120.20 120.66 5.16 o 1 14 3 35.68 34.26 2.57 o 2 14 3 21.29 20.74 2.67 o 3 14 3 23.55 20.27 2.51 o 4 14 3 38.71 37.57 2.90 o 5 14 3 172.27 175.95 3.26 o 6 14 3 8.76 6.13 3.16 o 7 14 3 37.03 36.24 2.90 o 8 14 3 41.09 41.02 3.39 o 9 14 3 15.68 18.24 2.70 o 0 15 3 402.93 404.08 9.15 o 1 15 3 78.12 81.14 2.56 o 2 15 3 189.25 194.12 2.96 o 3 15 3 44.43 47.35 2.64 o 4 15 3 22.49 25.17 2.42 o 5 15 3 19.20 17.73 2.59 o 6 15 3 82.20 89.24 3.66 o 7 15 3 41.33 44.48 2.71 o 8 15 3 23.24 25.55 3.38 o 0 16 3 20.32 22.33 3.38 o 1 16 3 68.87 73.46 2.68 o 2 16 3 19.56 22.78 2.70 o 3 16 3 50.79 53.86 2.80 o 4 16 3 104.41 114.45 2.93 o 5 16 3 11.93 11.06 2.49 o 0 17 3 9.66 9.42 3.63 o 1 17 3 6.06 8.13 3.18 o 0 2 4 21.65 16.64 8.98 o 1 2 4 471.26 518.83 21.54 o 2 2 4 945.87 1000.29 16.74 o 0 3 4 390.94 415.09 17.03 o 1 3 4 455.65 484.36 13.11 o 2 3 4 256.40 270.15 6.28 o 3 3 4 95.31 107.63 6.72 o 0 4 4 392.62 440.63 10.08 o 1 4 4 290.52 309.28 7.41 o 2 4 4 193.42 223.82 5.63 o 3 4 4 119.04 125.61 4.80 o 4 4 4 617.40 684.30 14.28 o 0 5 4 195.15 191.07 12.76 o 1 5 4 253.23 255.04 7.58 o 2 5 4 50.39 54.86 5.39 o 3 5 4 15.12 11.98 4.18 o 4 5 4 54.83 57.79 3.74 o 5 5 4 7.92 4.98 4.20 o 0 6 4 2497.24 2583.67 38.13 o 1 6 4 386.05 390.61 11.23 o 2 6 4 36.30 46.47 4.18 o 3 6 4 9.55 14.32 3.22 o 4 6 4 9.83 8.27 3.63 o 5 6 4 12.23 14.29 3.09 o 6 6 4 90.79 87.84 5.39 o 0 7 4 531.01 570.06 11.60 o 1 7 4 95.82 106.16 3.99 o 2 7 4 38.03 37.78 3.33 o 3 7 4 80.96 77.50 3.37 o 4 7 4 100.13 101.92 3.55 o 5 7 4 112.27 111.03 3.28 o 6 7 4 293.51 258.45 5.05 o 7 7 4 59.95 55.28 4.07 o 0 8 4 2.40 1.55 6.16 o 1 8 4 10.94 15.17 3.51 o 2 8 4 91.11 100.40 3.90 o 3 8 4 428.52 456.11 7.26 o 4 8 4 75.41 70.77 3.24 o 5 8 4 334.03 335.21 7.35 o 6 8 4 6.89 5.58 3.17 o 7 8 4 166.60 169.61 4.09 o 8 8 4 842.66 853.38 32.30 o 0 9 4 2.92 6.09 5.15 o 1 9 4 1.56 1.27 3.78 o 2 9 4 405.53 427.92 4.94 o 3 9 4 735.61 741.60 12.83 o 4 9 4 306.09 292.73 4.28 o 5 9 4 97.66 99.94 3.07 o 6 9 4 108.21 111.73 3.71 o 7 9 4 183.54 178.14 5.87 o 8 9 4 336.43 328.07 8.14 o 9 9 4 58.09 53.48 3.96 o 0 10 4 1.11 4.41 5.10 o 1 10 4 48.02 49.51 3.98 o 2 10 4 20.98 20.31 2.62 o 3 10 4 947.39 960.60 10.71 o 4 10 4 76.75 79.38 2.98 o 5 10 4 118.01 120.09 2.94 o 6 10 4 279.24 285.46 6.50 o 7 10 4 108.20 102.85 2.94 o 8 10 4 25.59 28.36 3.03 o 9 10 4 32.68 32.50 3.01 o 10 10 4 16.45 21.85 4.05 o 0 11 4 792.85 786.70 7.74 o 1 11 4 188.81 187.67 3.67 o 2 11 4 46.62 49.12 2.89 o 3 11 4 124.97 122.09 2.76 o 4 11 4 51.76 47.44 3.17 o 5 11 4 343.45 355.71 5.37 o 6 11 4 75.12 76.81 2.55 o 7 11 4 141.21 148.23 3.40 o 8 11 4 10.62 7.90 2.83 o 9 11 4 4.04 4.39 2.69 o 10 11 4 14.82 11.08 2.76 o 11 11 4 37.76 46.64 4.08 o 0 12 4 167.32 166.72 5.19 o 1 12 4 496.58 507.36 11.11 o 2 12 4 11.52 9.44 2.88 o 3 12 4 86.04 80.07 2.86 o 4 12 4 61.74 60.89 2.78 o 5 12 4 7.30 7.50 2.77 o 6 12 4 23.87 23.35 2.86 o 7 12 4 9.21 9.47 3.25 o 8 12 4 22.23 21.52 3.20 o 9 12 4 18.88 19.98 2.91 o 10 12 4 8.79 8.61 3.13 o 11 12 4 56.95 54.00 5.12 o 0 13 4 109.48 111.25 4.55 o 1 13 4 20.53 22.22 2.63 o 2 13 4 48.14 44.32 2.76 o 3 13 4 142.22 151.25 3.08 o 4 13 4 40.71 39.47 2.60 o 5 13 4 100.91 102.45 3.12 o 6 13 4 38.49 36.16 2.85 o 7 13 4 55.16 56.42 3.01 o 8 13 4 8.88 11.26 3.51 o 9 13 4 28.43 31.20 2.74 o 0 14 4 1.84 2.38 4.73 o 1 14 4 11.06 12.94 2.52 o 2 14 4 271.32 267.42 7.50 o 3 14 4 47.75 44.64 2.84 o 4 14 4 28.67 28.85 2.83 o 5 14 4 2.44 3.62 2.68 o 6 14 4 6.10 7.31 2.69 o 7 14 4 18.37 19.31 2.78 o 8 14 4 27.97 34.16 3.97 o 0 15 4 166.80 181.11 7.11 o 1 15 4 171.39 179.59 4.38 o 2 15 4 14.45 10.05 2.38 o 3 15 4 5.37 3.39 2.55 o 4 15 4 4.25 5.77 2.89 o 5 15 4 17.04 19.03 2.99 o 6 15 4 22.03 22.41 2.80 o 0 16 4 102.84 113.64 4.31 o 1 16 4 21.01 19.11 2.65 o 2 16 4 44.61 47.42 2.63 o 3 16 4 47.77 46.49 5.02 o 0 2 5 0.05 0.23 8.18 o 1 2 5 211.31 200.90 9.85 o 0 3 5 283.68 305.68 19.29 o 1 3 5 316.45 322.91 7.70 o 2 3 5 84.21 80.88 5.63 o 0 4 5 4.04 5.66 7.79 o 1 4 5 101.26 103.08 6.87 o 2 4 5 81.57 84.17 5.47 o 3 4 5 247.23 261.17 4.97 o 0 5 5 289.49 269.75 13.84 o 1 5 5 135.44 137.27 6.79 o 2 5 5 4.43 4.23 5.25 o 3 5 5 268.30 272.09 7.57 o 4 5 5 65.94 76.17 3.66 o 0 6 5 221.56 233.70 13.76 o 1 6 5 311.65 301.03 10.80 o 2 6 5 15.77 17.13 5.30 o 3 6 5 66.65 73.70 3.85 o 4 6 5 54.38 64.10 4.21 o 5 6 5 54.39 55.38 3.23 o 0 7 5 10.56 9.24 10.16 o 1 7 5 101.52 83.03 6.25 o 2 7 5 286.20 288.71 5.95 o 3 7 5 37.82 40.10 3.66 o 4 7 5 190.11 192.16 3.81 o 5 7 5 247.09 265.86 4.02 o 6 7 5 255.13 261.33 8.51 o 0 8 5 67.67 58.63 9.80 o 1 8 5 207.32 195.38 4.92 o 2 8 5 32.57 28.69 6.01 o 3 8 5 163.24 166.21 4.16 o 4 8 5 91.01 94.08 3.39 o 5 8 5 41.71 45.41 3.48 o 6 8 5 95.47 104.23 3.66 o 7 8 5 3.40 4.70 3.28 o 0 9 5 9.96 13.33 5.40 o 1 9 5 2.36 3.28 4.16 o 2 9 5 27.03 25.18 4.10 o 3 9 5 62.60 56.74 3.11 o 4 9 5 7.70 7.01 2.89 o 5 9 5 29.43 27.16 3.03 o 6 9 5 64.26 61.99 3.12 o 7 9 5 44.51 41.29 3.01 o 8 9 5 118.96 120.69 3.37 o 0 10 5 203.31 203.40 9.96 o 1 10 5 1.27 2.12 3.74 o 2 10 5 13.71 11.13 3.07 o 3 10 5 97.13 95.77 3.69 o 4 10 5 12.92 12.92 3.58 o 5 10 5 5.15 6.52 2.75 o 6 10 5 73.55 74.96 3.11 o 7 10 5 33.11 30.59 3.03 o 8 10 5 109.24 115.24 3.48 o 9 10 5 43.11 39.16 3.33 o 0 11 5 167.00 161.22 5.64 o 1 11 5 6.94 9.68 3.27 o 2 11 5 11.08 11.62 2.92 o 3 11 5 46.83 43.47 3.61 o 4 11 5 13.20 10.27 2.79 o 5 11 5 22.67 24.13 3.44 o 6 11 5 68.29 69.83 3.04 o 7 11 5 194.06 196.78 3.30 o 8 11 5 68.52 76.18 3.26 o 9 11 5 0.31 2.75 3.07 o 10 11 5 7.23 8.90 3.14 o 0 12 5 305.47 325.78 6.40 o 1 12 5 6.06 5.79 3.49 o 2 12 5 59.50 66.18 3.59 o 3 12 5 18.41 19.94 2.91 o 4 12 5 23.20 19.85 2.98 o 5 12 5 4.46 5.03 3.18 o 6 12 5 4.14 5.29 3.12 o 7 12 5 54.61 57.77 2.65 o 8 12 5 46.66 48.10 2.87 o 9 12 5 11.83 12.78 2.86 o 0 13 5 25.49 22.79 4.92 o 1 13 5 50.79 50.46 2.71 o 2 13 5 4.03 5.18 2.93 o 3 13 5 38.53 39.55 3.31 o 4 13 5 53.06 60.25 2.97 o 5 13 5 77.55 76.71 3.23 o 6 13 5 35.43 36.29 3.06 o 7 13 5 3.57 4.11 2.72 o 8 13 5 7.13 8.15 3.22 o 0 14 5 15.55 17.39 4.30 o 1 14 5 12.56 13.64 2.91 o 2 14 5 17.63 20.34 2.73 o 3 14 5 27.39 28.76 2.89 o 4 14 5 154.32 160.10 3.25 o 5 14 5 15.54 16.02 3.15 o 6 14 5 40.78 42.43 3.98 o 0 15 5 3.67 4.59 4.22 o 1 15 5 9.31 11.25 2.73 o 2 15 5 70.38 67.35 3.07 o 3 15 5 113.20 118.58 3.52 o 0 2 6 174.64 156.87 7.58 o 1 2 6 207.58 199.83 8.06 o 2 2 6 552.97 519.13 14.51 o 0 3 6 1.37 1.28 7.71 o 1 3 6 154.01 151.27 6.66 o 2 3 6 270.61 269.53 6.32 o 3 3 6 371.25 390.95 12.94 o 0 4 6 17.84 22.97 8.15 o 1 4 6 77.39 72.53 6.54 o 2 4 6 159.31 159.62 6.40 o 3 4 6 753.22 790.65 10.70 o 4 4 6 494.68 502.51 8.49 o 0 5 6 30.44 27.62 11.53 o 1 5 6 49.77 42.70 4.70 o 2 5 6 140.13 153.28 5.67 o 3 5 6 198.21 195.13 4.15 o 4 5 6 41.96 41.37 3.87 o 5 5 6 52.47 49.17 4.96 o 0 6 6 15.99 11.60 11.67 o 1 6 6 152.47 140.91 5.98 o 2 6 6 30.07 31.82 4.71 o 3 6 6 86.64 86.27 4.64 o 4 6 6 72.83 73.86 3.88 o 5 6 6 176.71 178.33 4.77 o 6 6 6 300.98 293.92 5.98 o 1 7 6 49.86 46.82 6.58 o 2 7 6 110.02 104.96 4.78 o 3 7 6 11.77 6.85 3.75 o 4 7 6 238.34 242.33 4.63 o 5 7 6 84.14 88.33 3.72 o 6 7 6 84.16 84.23 3.75 o 7 7 6 86.47 81.08 5.87 o 1 8 6 43.88 41.84 7.09 o 2 8 6 109.21 90.73 5.50 o 3 8 6 72.18 71.12 3.75 o 4 8 6 19.84 17.41 3.72 o 5 8 6 84.46 90.12 4.18 o 6 8 6 46.65 49.06 3.33 o 7 8 6 1.32 2.55 3.56 o 8 8 6 146.41 144.83 8.34 o 0 9 6 6.80 6.02 8.58 o 1 9 6 1.00 11.06 8.65 o 2 9 6 141.36 137.49 5.77 o 3 9 6 87.83 72.51 4.45 o 4 9 6 1.97 5.97 4.09 o 5 9 6 73.44 71.04 4.11 o 6 9 6 62.30 58.90 3.60 o 7 9 6 6.53 9.35 3.22 o 8 9 6 73.17 70.76 3.36 o 9 9 6 95.46 111.78 5.84 o 0 10 6 190.26 146.32 9.44 o 1 10 6 126.87 110.72 6.66 o 2 10 6 2.55 5.39 4.77 o 3 10 6 14.05 12.03 3.40 o 4 10 6 16.75 22.33 4.68 o 5 10 6 1.61 1.98 3.50 o 6 10 6 25.75 22.80 3.31 o 7 10 6 1.35 0.84 4.02 o 8 10 6 0.99 2.91 3.01 o 9 10 6 66.96 73.95 3.72 o 0 11 6 3.71 5.43 8.48 o 1 11 6 27.79 23.32 6.09 o 2 11 6 30.66 36.64 5.42 o 3 11 6 29.89 28.82 3.57 o 4 11 6 2.92 1.53 4.23 o 5 11 6 6.09 5.19 3.88 o 6 11 6 17.25 17.14 3.67 o 7 11 6 9.76 13.79 3.36 o 8 11 6 27.71 29.74 4.05 o 0 12 6 1.36 1.12 4.95 o 1 12 6 8.81 6.84 4.02 o 2 12 6 15.20 11.88 2.98 o 3 12 6 37.08 37.36 3.56 o 4 12 6 1.25 2.55 3.33 o 5 12 6 69.20 74.32 3.95 o 6 12 6 4.77 8.77 3.57 o 7 12 6 62.46 64.96 3.41 o 0 13 6 2.56 4.46 4.99 o 1 13 6 6.01 6.64 3.14 o 2 13 6 18.82 16.98 2.72 o 3 13 6 15.58 14.28 3.15 o 4 13 6 31.10 31.16 3.38 o 5 13 6 9.44 10.60 3.70 o 0 14 6 3.56 4.00 4.70 o 1 14 6 15.79 14.05 4.29 o 0 2 7 98.57 101.55 7.35 o 1 2 7 637.68 611.21 14.78 o 0 3 7 114.92 106.80 8.09 o 1 3 7 734.97 725.76 23.24 o 2 3 7 137.34 142.18 5.55 o 0 4 7 305.19 290.31 15.44 o 1 4 7 239.88 217.13 6.67 o 2 4 7 125.53 125.41 5.66 o 3 4 7 241.09 239.09 5.18 o 0 5 7 202.79 201.60 16.76 o 1 5 7 10.01 11.68 5.32 o 2 5 7 91.64 80.02 5.39 o 3 5 7 108.79 123.94 4.39 o 4 5 7 559.29 567.18 7.57 o 1 6 7 2.08 6.37 6.72 o 2 6 7 118.98 112.87 5.54 o 3 6 7 373.64 373.89 8.67 o 4 6 7 315.65 327.15 8.26 o 5 6 7 2.41 1.48 3.93 o 1 7 7 15.09 17.79 5.51 o 2 7 7 75.33 68.13 4.95 o 3 7 7 126.10 131.79 4.43 o 4 7 7 61.52 49.25 3.65 o 5 7 7 36.98 32.41 4.05 o 6 7 7 15.17 11.44 3.98 o 0 8 7 60.41 56.58 8.97 o 1 8 7 19.44 23.39 6.90 o 2 8 7 0.42 -1.79 5.15 o 3 8 7 9.32 8.12 3.74 o 4 8 7 62.22 67.05 4.15 o 5 8 7 116.87 125.86 3.93 o 6 8 7 160.15 164.71 5.69 o 7 8 7 51.38 49.96 3.36 o 0 9 7 134.44 105.06 7.24 o 1 9 7 68.42 53.87 8.65 o 2 9 7 17.85 15.62 4.32 o 3 9 7 1.81 2.46 4.96 o 4 9 7 2.75 2.80 4.01 o 5 9 7 31.72 32.59 3.97 o 6 9 7 2.20 2.62 3.92 o 7 9 7 9.22 12.79 3.49 o 8 9 7 44.06 51.15 4.10 o 0 10 7 10.13 9.12 6.19 o 1 10 7 4.74 5.29 4.95 o 2 10 7 10.94 11.90 4.69 o 3 10 7 31.34 32.91 4.29 o 4 10 7 6.09 5.59 4.06 o 5 10 7 21.98 26.22 3.99 o 6 10 7 29.18 27.51 3.22 o 7 10 7 12.96 16.42 3.66 o 0 11 7 58.36 52.31 8.92 o 1 11 7 16.12 10.16 6.12 o 2 11 7 15.11 19.65 4.65 o 3 11 7 26.51 24.43 3.78 o 4 11 7 13.11 13.66 4.80 o 5 11 7 17.59 17.58 4.81 o 0 12 7 3.67 3.61 8.75 o 1 12 7 12.02 12.11 3.66 o 2 12 7 11.47 13.20 3.64 o 3 12 7 5.17 4.09 5.48 o 0 1 8 359.56 310.62 15.03 o 1 1 8 5.20 4.47 6.54 o 0 2 8 18.27 20.72 8.51 o 1 2 8 77.94 75.90 5.71 o 2 2 8 141.76 151.33 9.19 o 0 3 8 70.34 70.99 14.02 o 1 3 8 5.42 6.42 5.60 o 2 3 8 69.95 64.65 4.51 o 3 3 8 40.84 33.44 6.68 o 1 4 8 2.42 1.31 5.77 o 2 4 8 17.38 18.71 4.33 o 3 4 8 0.10 0.40 4.31 o 4 4 8 8.50 8.28 5.77 o 1 5 8 18.00 18.15 6.82 o 2 5 8 106.26 110.25 4.90 o 3 5 8 68.37 66.78 4.45 o 4 5 8 1.44 3.33 3.97 o 5 5 8 106.69 109.44 6.70 o 0 6 8 32.46 29.47 6.00 o 1 6 8 19.87 16.13 7.13 o 2 6 8 22.43 22.09 4.04 o 3 6 8 29.07 31.27 3.60 o 4 6 8 8.51 7.11 3.95 o 5 6 8 12.05 12.87 3.56 o 6 6 8 36.20 30.03 4.68 o 0 7 8 27.99 19.69 8.12 o 1 7 8 31.46 35.39 8.53 o 2 7 8 46.65 50.32 5.41 o 3 7 8 102.57 108.13 4.99 o 4 7 8 1.10 1.44 4.07 o 5 7 8 12.35 13.36 4.03 o 6 7 8 1.32 2.98 3.98 o 7 7 8 129.52 118.91 6.31 o 0 8 8 1.43 3.46 5.39 o 1 8 8 27.61 21.42 8.31 o 2 8 8 25.73 23.49 5.21 o 3 8 8 44.37 43.78 4.57 o 4 8 8 9.05 8.18 4.28 o 5 8 8 13.23 14.67 4.02 o 6 8 8 31.89 33.69 4.75 o 0 9 8 7.95 2.88 7.68 o 1 9 8 37.96 33.60 5.71 o 2 9 8 0.22 0.13 5.60 o 3 9 8 66.43 70.89 5.42 o 4 9 8 7.90 7.54 4.87 o 0 10 8 10.03 10.26 5.58 o 1 10 8 52.31 47.19 4.39 o 0 1 9 11.87 7.69 4.72 o 0 2 9 0.46 1.01 5.89 o 1 2 9 11.98 13.06 4.61 o 0 3 9 65.14 43.10 7.90 o 1 3 9 10.93 10.71 5.68 o 2 3 9 1.84 5.20 4.89 o 0 4 9 26.48 22.98 8.82 o 1 4 9 14.88 20.25 5.41 o 2 4 9 14.43 15.92 4.79 o 3 4 9 5.84 7.49 4.51 o 0 5 9 8.02 6.02 7.38 o 1 5 9 12.63 14.99 7.31 o 2 5 9 6.09 7.48 5.16 o 3 5 9 70.26 77.79 4.86 o 4 5 9 29.52 27.04 4.35 o 0 6 9 3.79 -0.83 7.56 o 1 6 9 1.57 3.34 5.88 o 2 6 9 70.78 77.17 11.97 o